CN107603796A - A kind of astral oil rattan craft transparent soap and preparation method thereof - Google Patents

A kind of astral oil rattan craft transparent soap and preparation method thereof Download PDF

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Publication number
CN107603796A
CN107603796A CN201711030586.6A CN201711030586A CN107603796A CN 107603796 A CN107603796 A CN 107603796A CN 201711030586 A CN201711030586 A CN 201711030586A CN 107603796 A CN107603796 A CN 107603796A
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oil
astral
rattan
craft
transparent soap
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CN201711030586.6A
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李创华
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Abstract

The present invention relates to transparent soap preparing technical field, and in particular to a kind of astral oil rattan craft transparent soap and preparation method thereof;The transparent soap includes the raw material of following weight fraction:The sweet amino proline 1 5% of natural oil 20 40%, alkali 20 25%, glycerine 5 20%, carboxybetaine 1 3%, methyl, honey 1 3%, astral oil rattan oil 0.5 3%, astral oil rattan leaf composite fermentation liquid 0.5 3%, essential oil 0.01 0.5%, surplus are water;Astral oil rattan craft transparent soap provided by the invention contains astral oil rattan oil component, and moistening effect is good, while skin is moderately cleaned, can repair skin damage, make skin keep moistening smooth flexible.

Description

A kind of astral oil rattan craft transparent soap and preparation method thereof
Technical field
The present invention relates to transparent soap preparing technical field, and in particular to a kind of astral oil rattan craft transparent soap and its preparation side Method.
Background technology
In recent years, gradually stepping up with people's living standard, pure natural, nonirritant transparent soap is increasingly by city The welcome of field.Transparent soap is using vegetable oil and alkali as raw material, is obtained through cold process soap, and it can be effectively maintained in vegetable oil largely Nutriment, effective cleaning, Glycerin can be played a part of.
Containing abundant unrighted acid and tocopherol in astral oil rattan oil, there is excellent affinity and infiltration to skin Power, be easily absorbed by the skin, to supplement the lipid nutrient needed for skin, repair Dry and due to contact surfactant and The skin fat sour water of damage is put down, and is maintained and is strengthened Skin Cell film and the normal configuration and function of interstitial;Simultaneously can also be Skin surface forms ventilative water-retaining film, weakens the moisture loss of deep skin, makes skin keep moistening smooth flexible, has pole High its cosmetic values.In the prior art, it yet there are no the report applied about astral oil rattan oil in manual transparent soap.
The content of the invention
The first object of the present invention is to provide a kind of moistening effect good astral oil rattan craft transparent soap, in moderately cleaning flesh While skin, skin damage can be repaired, make skin keep moistening smooth flexible.
To achieve the above object, the technical solution adopted by the present invention is:A kind of astral oil rattan craft transparent soap, including following weight Measure the raw material of fraction:
The second object of the present invention is to provide a kind of method simplicity, the system of the astral oil rattan craft transparent soap of good product quality Preparation Method.
To achieve the above object, the technical solution adopted by the present invention is:A kind of preparation method of astral oil rattan craft transparent soap, Comprise the following steps:
(1) astral oil rattan oil is produced:
A. astral oil rattan fruit is taken, shells and dries to moisture content below 2%, the first crude oil is obtained using physical squeezing method;With The CO2 supercritical extractions processing astral oil rattan fruitcake dregs of rice obtain the second crude oil;Merge the first crude oil and the second crude oil, obtain astral oil rattan original Oil;
B. by astral oil rattan heating crude oil to 45-50 DEG C, with citric acid degumming;
C. continue to be heated to oil temperature as 90 DEG C, add boiling water and washed;Room temperature is cooled to, carries out water-oil separating;
D. winterization is carried out to astral oil rattan oil, then carries out initial filter with slipstream membrane separation technique, then with NF membrane to initial filter Liquid carries out secondary filter, produces astral oil rattan oil;
(2) astral oil rattan leaf composite fermentation liquid is produced:
A. astral oil rattan leaf is cleaned, dried in the shade, crushed, extracted with flooding, obtain crude extract;
B. 20-30wt% alkaline earth is added into crude extract, stirs, centrifuge slagging-off, then with micro-filtrate membrane filtration, is obtained clear Clear liquid;
C. 0.002-0.005vt% mixed fermentation strain is accessed into clarified solution, adds honey and 20wt% astral oil Rattan oil, is well mixed, and is placed in China fir tank constant temperature static fermentation 2-6 months;
D. tunning is taken out, is filtered with slipstream membrane separation technique, collects filtrate;
E. high-temperature sterilization is carried out to filtrate at 100 DEG C, is subsequently cooled to room temperature, produces the composite fermentation of astral oil rattan leaf Liquid;
(3) transparent soap is prepared:
A. natural oil and astral oil rattan oil are stirred and heated to 60 DEG C by formula, divide 2-5 addition alkali, stir 10-30 Minute completes saponification, obtains soap base;
B. glycerine, carboxybetaine and methyl sweet amino proline are added when soap base is cooled to 35 DEG C, is stirred to glue Shape;
C. continue to stir, the composite fermentation liquid of astral oil rattan leaf is added when temperature is down to normal temperature, treats that bubble is wholly absent Pour into mould;
D. it is put at 2-10 DEG C and freezes 24 hours, Transparent handmade soap is produced after taking-up.
Omega-3:Skin equilibrium moisturizing can be made and kept fit.It can strengthen around the soft and slender of each cell peripheral Cell membrane, cell is obtained sufficient nourishing, while effectively intracellular waste can be excluded.It can secrete skin corium Go out the collagen and elastomer of more strength, help smoothes away wrinkles and microgroove, and sturdy gradually in the skin of relaxation.Astral oil rattan oil contains Unrighted acid, there is excellent affinity and penetration to skin, be easily absorbed by the skin, to supplement needed for skin Lipid nutrient, the skin fat sour water repaired Dry and damaged due to contact surfactant are put down, maintain and strengthen skin The normal configuration and function of skin cell membrane and interstitial;Ventilative water-retaining film can also be formed in skin surface simultaneously, it is deep to weaken skin The moisture loss of layer, skin is set to keep moistening smooth flexible.
Vitamin E:Free radical can be removed, there is anti-oxidation efficacy, helps to pin moisture, skin is kept elasticity, also With photo-aging is delayed, sun-proof, suppression sunburn, even skin, the effect such as wrinkle of skin, moisturizing and anti-inflammatory is reduced.
Beneficial effect is caused by above-mentioned technical proposal:The astral oil rattan oil added in the present invention, can remove freedom Base, skin lines are eliminated, moisturizing water lock effect is good, and keeping skin, moistening is smooth flexible, and skincare effect is notable.This Outside, for the astral oil rattan leaf added in the present invention after composite fermentation, unrighted acid is decomposed into micromolecule polypeptide, permeability More preferably, make transparent soap that there is stronger function of moistening, repair and releive.
Embodiment
A kind of astral oil rattan craft transparent soap, include the raw material of following weight fraction:
Preferably, the natural oil is selected from coconut oil, castor oil, linseed oil, olive oil, camellia oil, green tea seed At least one of oil, hemp-seed oil.
Preferably, the alkali purity is not less than 98%.
A kind of preparation method of astral oil rattan craft transparent soap, comprises the following steps:
(1) astral oil rattan oil is produced:
A. astral oil rattan fruit is taken, shells and dries to moisture content below 2%, the first crude oil is obtained using physical squeezing method;With The CO2 supercritical extractions processing astral oil rattan fruitcake dregs of rice obtain the second crude oil;Merge the first crude oil and the second crude oil, obtain astral oil rattan original Oil;
B. by astral oil rattan heating crude oil to 45-50 DEG C, with citric acid degumming;
C. continue to be heated to oil temperature as 90 DEG C, add boiling water and washed;Room temperature is cooled to, carries out water-oil separating;
D. winterization is carried out to astral oil rattan oil, then carries out initial filter with slipstream membrane separation technique, then with NF membrane to initial filter Liquid carries out secondary filter, produces astral oil rattan oil;
(2) astral oil rattan leaf composite fermentation liquid is produced:
A. astral oil rattan leaf is cleaned, dried in the shade, crushed, extracted with flooding, obtain crude extract;
B. 20-30wt% alkaline earth is added into crude extract, stirs, centrifuge slagging-off, then with micro-filtrate membrane filtration, is obtained clear Clear liquid;
C. 0.002-0.005vt% mixed fermentation strain is accessed into clarified solution, adds honey and 20wt% astral oil Rattan oil, is well mixed, and is placed in China fir tank constant temperature static fermentation 2-6 months;
D. tunning is taken out, is filtered with slipstream membrane separation technique, collects filtrate;
E. high-temperature sterilization is carried out to filtrate at 100 DEG C, is subsequently cooled to room temperature, produces the composite fermentation of astral oil rattan leaf Liquid;
(3) transparent soap is prepared:
A. natural oil and astral oil rattan oil are stirred and heated to 60 DEG C by formula, divide 2-5 addition alkali, stir 10-30 Minute completes saponification, obtains soap base;
B. glycerine, carboxybetaine and methyl sweet amino proline are added when soap base is cooled to 35 DEG C, is stirred to glue Shape;
C. continue to stir, the composite fermentation liquid of astral oil rattan leaf is added when temperature is down to normal temperature, treats that bubble is wholly absent Pour into mould;
D. it is put at 2-10 DEG C and freezes 24 hours, Transparent handmade soap is produced after taking-up.
Preferably, contain Bulgarian Lactobacillus bacterium solution 1.5-2.0%, red yeast in the mixed fermentation strain Bacterium bacterium solution 1.5-2.0%, long shoot trichoderma bacterium solution 0.01-0.05%, pure mellow wine grain 30-35%, Mucor bacterium solution 0.1-1%, surplus are Pure water.
Preferably, contain 400,000,000/ml of Bulgarian Lactobacillus, red ferment in the Bulgarian Lactobacillus bacterium solution Contain red 200,000,000/ml of saccharomycete in female bacterium bacterium solution, contain 0.2 hundred million/ml of long shoot trichoderma in long shoot trichoderma bacterium solution, in Mucor bacterium solution Contain 0.5 hundred million/ml of Mucor.
Preferably, the slipstream film is one kind in flat film, tubular membrane, rolled film, hollow fiber form film, institute It is organic film or inorganic ceramic membrane to state membrane material, and slipstream membrane aperture is 100-300um.
Preferably, when extracting astral oil rattan leaf with flooding in the step (2), the dosage of water is astral oil rattan cormus Long-pending 1-5 times.
Preferably, the ferment at constant temperature temperature in the step (2) is 40-50 DEG C, most preferred fermentation temperature is 43 DEG C.
To further illustrate technical scheme disclosed by the invention, illustrate below by way of 3 embodiments:
Embodiment 1:
A kind of astral oil rattan craft transparent soap, include the raw material of following weight fraction:
Embodiment 2:
A kind of astral oil rattan craft transparent soap, include the raw material of following weight fraction:
Embodiment 3:
A kind of astral oil rattan craft transparent soap, include the raw material of following weight fraction:
Following table by acquisition transparent soap feature nutritional ingredient:
100 volunteers are chosen, are divided into 4 groups by 21-25 year, 26-30 year, 31-35 year, the age bracket of 36-40 year, often 25 people of group, daily respectively to use once sooner or later respectively using transparent soap produced by the present invention, observation sooner or later, contrast volunteer face flesh Skin situation, it is as a result as shown in the table:
21-25 year 26-30 year 31-35 year 36-40 year
Eye irritation Nothing Nothing Nothing Nothing
Average percentage of water loss 3.4% 3.8% 4.5% 5.2%
Degree is moistened in hydration 24.5% 22.6% 20.8% 20.2%
Performance is nourished in skin care It is excellent It is excellent It is excellent Well
Absorbent properties Absorb quickly Absorb quickly Absorb quickly It is very fast to absorb
Cleaning effect It is excellent It is excellent It is excellent It is excellent
It can be seen that from result of the test, transparent soap provided by the invention can not only clean skin, moreover it is possible to which effective moisturizing, skin care are grown It is good to moisten effect, helps to make skin keep moistening smooth flexible.

Claims (9)

1. a kind of astral oil rattan craft transparent soap, it is characterised in that include the raw material of following weight fraction:
2. astral oil rattan craft transparent soap as claimed in claim 1, it is characterised in that the natural oil is selected from coconut oil, castor At least one of sesame oil, linseed oil, olive oil, camellia oil, green tea seed oil, hemp-seed oil.
3. astral oil rattan craft transparent soap as claimed in claim 1, it is characterised in that the alkali purity is not less than 98%.
A kind of 4. preparation method of astral oil rattan craft transparent soap as any one of claim 1-3, it is characterised in that bag Include following steps:
(1) astral oil rattan oil is produced:
A. astral oil rattan fruit is taken, shells and dries to moisture content below 2%, the first crude oil is obtained using physical squeezing method;Surpassed with CO2 The critical treatment by extraction astral oil rattan fruitcake dregs of rice obtain the second crude oil;Merge the first crude oil and the second crude oil, obtain astral oil rattan crude oil;
B. by astral oil rattan heating crude oil to 45-50 DEG C, with citric acid degumming;
C. continue to be heated to oil temperature as 90 DEG C, add boiling water and washed;Room temperature is cooled to, carries out water-oil separating;
D. winterization is carried out to astral oil rattan oil, then carries out initial filter with slipstream membrane separation technique, then primary filtrate is entered with NF membrane Row secondary filter, produce astral oil rattan oil;
(2) astral oil rattan leaf composite fermentation liquid is produced:
A. astral oil rattan leaf is cleaned, dried in the shade, crushed, extracted with flooding, obtain crude extract;
B. 20-30wt% alkaline earth is added into crude extract, stirs, centrifuge slagging-off, then with micro-filtrate membrane filtration, must be clarified Liquid;
C. 0.002-0.005vt% mixed fermentation strain is accessed into clarified solution, adds honey and 20wt% astral oil rattan oil, It is well mixed, it is placed in China fir tank constant temperature static fermentation 2-6 months;
D. tunning is taken out, is filtered with slipstream membrane separation technique, collects filtrate;
E. high-temperature sterilization is carried out to filtrate at 100 DEG C, is subsequently cooled to room temperature, produces the composite fermentation liquid of astral oil rattan leaf;
(3) transparent soap is prepared:
A. natural oil and astral oil rattan oil are stirred and heated to 60 DEG C by formula, divide 2-5 addition alkali, stir 10-30 minutes Saponification is completed, obtains soap base;
B. glycerine, carboxybetaine and methyl sweet amino proline are added when soap base is cooled to 35 DEG C, is stirred to glue;
C. continue to stir, the composite fermentation liquid of astral oil rattan leaf is added when temperature is down to normal temperature, treats that bubble is wholly absent and pours into Mould;
D. it is put at 2-10 DEG C and freezes 24 hours, Transparent handmade soap is produced after taking-up.
5. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, it is characterised in that the mixed fermentation strain In contain Bulgarian Lactobacillus bacterium solution 1.5-2.0%, red saccharomycete bacterium solution 1.5-2.0%, long shoot trichoderma bacterium solution 0.01- 0.05%, pure mellow wine grain 30-35%, Mucor bacterium solution 0.1-1%, surplus is pure water.
6. the preparation method of astral oil rattan craft transparent soap as claimed in claim 5, it is characterised in that the Bulgarian lactic acid Contain 400,000,000/ml of Bulgarian Lactobacillus in bacillus bacterium solution, red 200,000,000/ml of saccharomycete is contained in red saccharomycete bacterium solution, it is long Contain 0.2 hundred million/ml of long shoot trichoderma in branch trichoderma bacterium solution, contain 0.5 hundred million/ml of Mucor in Mucor bacterium solution.
7. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, it is characterised in that the slipstream film is flat One kind in plate membrane, tubular membrane, rolled film, hollow fiber form film, the membrane material are organic film or inorganic ceramic membrane, tangentially Stream membrane aperture is 100-300um.
8. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, it is characterised in that used in the step (2) When flooding extracts astral oil rattan leaf, the dosage of water is 1-5 times of astral oil rattan leaf volume.
9. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, it is characterised in that in the step (2) Ferment at constant temperature temperature is 40-50 DEG C.
CN201711030586.6A 2017-10-27 2017-10-27 A kind of astral oil rattan craft transparent soap and preparation method thereof Pending CN107603796A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108192776A (en) * 2017-12-28 2018-06-22 佛山市星徽生物科技有限公司 A kind of astral oil rattan craft transparent soap and preparation method thereof
CN108186439A (en) * 2018-02-09 2018-06-22 广州御延堂生物科技有限公司 A kind of sea salt nourishes hair cream and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108192776A (en) * 2017-12-28 2018-06-22 佛山市星徽生物科技有限公司 A kind of astral oil rattan craft transparent soap and preparation method thereof
CN108186439A (en) * 2018-02-09 2018-06-22 广州御延堂生物科技有限公司 A kind of sea salt nourishes hair cream and preparation method thereof

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Application publication date: 20180119