CN108176909A - A kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride - Google Patents
A kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride Download PDFInfo
- Publication number
- CN108176909A CN108176909A CN201810097810.1A CN201810097810A CN108176909A CN 108176909 A CN108176909 A CN 108176909A CN 201810097810 A CN201810097810 A CN 201810097810A CN 108176909 A CN108176909 A CN 108176909A
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- oil
- fixedly connected
- tank reactor
- stirred tank
- continuous stirred
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K7/00—Cutting, scarfing, or desurfacing by applying flames
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K7/00—Cutting, scarfing, or desurfacing by applying flames
- B23K7/10—Auxiliary devices, e.g. for guiding or supporting the torch
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K7/00—Cutting, scarfing, or desurfacing by applying flames
- B23K7/10—Auxiliary devices, e.g. for guiding or supporting the torch
- B23K7/105—Auxiliary devices, e.g. for guiding or supporting the torch specially adapted for particular geometric forms
- B23K7/107—Auxiliary devices, e.g. for guiding or supporting the torch specially adapted for particular geometric forms for cutting circles
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
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- Geometry (AREA)
- Crushing And Pulverization Processes (AREA)
Abstract
A kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride, fixed plate upper left-hand are fixedly connected with work piece holder;Rotating platform is rotationally connected to the top of locomotive by being fixedly connected on the shaft of its underpart;Support column is fixed on front side of rotary platform upper;Vertical slideway is equipped on front side of support column, hoist engine is fixedly installed at the top of support column;Mechanical arm is made of fixed arm and travelling arm, and travelling arm left end lower part is fixedly connected with cutting gun nozzle, and the right end of fixed arm is fixedly connected with reel;Sliding block is provided with two vertically extending and T-shaped cross section sliding slots two close to the side of slideway, and two T-shaped one slide rails of cross section are slidably equipped in two sliding slots two, and the top and bottom of two one slide rails are fixedly connected respectively with the top and bottom of slideway;Two oil filling devices correspond to the front side that two two ground of sliding slot are fixed at sliding block respectively.The device operating process is convenient, operating efficiency is high, suitable for the cutting operation of round piece.
Description
Technical field
The invention belongs to cutting equipment technical fields, and in particular to a kind of to be cut for handling the high-pressure steam pipe of carbon tetrachloride
Cut device.
Background technology
When traditional manual type cuts steam pipe, since the outer profile of pipe is periphery, therefore the cutting on its surface
Also it is arcwall face, in artificial cutting or cutting burner is motionless, the outer surface cutting of hand-turning pipe;Pipe
Motionless, cutting burner cuts its outer surface around pipe.Due to human factor, cutting speed is unstable, leads to cutting not
Uniformly, cutting efficiency is low, affects cut quality;And it works under the high temperature conditions and in the case that dust is big, to human body
Injury is very big.
Since traditional-handwork cutting mode many is asked there are cutting efficiency is low, labor intensity is big, cut quality is unstable etc.
Topic, is gradually substituted by automatic cutting device, and for the cutter device of higher-end because needing mating ancillary equipment, cost is higher, and
Such cutter device is fixed using tri-claw plate and pneumatic oil cylinder and is cut part, it is slow thus to generate ETCD estimated time of commencing discharging, it is impossible to protect
The problems such as card cutting quality.
Invention content
In view of the above existing problems in the prior art, the present invention provides a kind of for handling the high-pressure steam pipe of carbon tetrachloride
Cutter device, the plant automation degree is high, operating process is convenient, operating efficiency is high, and the cutting that can be suitably used for round pipe fitting is made
Industry can help to the raising of cut quality.
To achieve these goals, the present invention provides a kind of dress is cut for handling the high-pressure steam pipe of carbon tetrachloride
It puts, including fixed plate, the running track extended along the longitudinal direction that is fixed at fixed plate upper right, is slidably arranged in fortune
Locomotive, rotating platform, support column, mechanical arm and the two oil filling devices of row rail superior portion;
Position of the fixed plate top on the left of running track is fixedly connected with work piece holder;
The work piece holder includes two parallel fixed seats extending along the longitudinal direction, the front end of every fixed seat,
Rear end is respectively fitted with driven load carrier, active load carrier;The driven load carrier and active load carrier structure phase
Together, include the pedestal being fixedly connected in fixed seat, the V-shaped bracket for being hinged on pedestal upper end, be arranged on V-shaped bracket
Two idler wheels of two upper ends, wherein each idler wheel is rotatably connected to by the shaft at its center in V-shaped bracket, it is described
The left and right ends of shaft are pierced by the outside of V-shaped bracket;The side of V-shaped bracket in each active load carrier is solid
Surely synchronous motor is connected with, the synchronous motor is used to drive the rotation of an idler wheel in active load carrier;
The rotating platform is rotationally connected to the top of locomotive by being fixedly connected on the shaft of its underpart;The branch
Dagger is fixed on front side of rotary platform upper;It is provided with vertical slideway, support column along its length on front side of support column
Top be fixedly installed hoist engine;The mechanical arm is arranged on the front side of support column, and cunning is fixedly connected on rear side of mechanical arm
The dynamic sliding block being set in slideway;Roller is fixedly connected on the output shaft of the hoist engine, steel wire is arranged on the roller
Rope, the one end of steel wire rope far from roller is connect with the sliding block;
The mechanical arm is made of fixed arm and travelling arm, and the sliding block is fixedly connected on the rear side of fixed arm, the cunning
The left upper part of swing arm is fixedly connected with oxygen cylinder, left end lower part is fixedly connected with cutting gun nozzle, the right end of the fixed arm
Reel is fixedly connected with, is connected between the oxygen cylinder and cutting gun nozzle by pipeline;One end of the acetylene gas pipe with
Cutting gun nozzle connects, and other end winding is connect after crossing reel with acetylene cylinder;Middle part is provided with transverse direction on front side of the travelling arm
The sliding slot one of extension, a horizontal mounting arm of the fixed arm are horizontally slidingly assemblied in the sliding slot one;Before travelling arm
Upper lateral part is also associated with the rack extended along its length, and fixed arm is fixedly connected with horizontal drive motor above rack;
The gear of drive rack is equipped on the output shaft of horizontal drive motor;
The sliding block is provided with two vertically extending and T-shaped cross section sliding slots two close to the side of slideway, two
Two T-shaped one slide rails of cross section are slidably equipped in sliding slot two, the top and bottom of two one slide rails are upper with slideway respectively
End is fixedly connected with lower end;
Two oil filling devices correspond to the leading flank that two two ground of sliding slot are fixed at sliding block respectively;
The oil filling device includes superposed rotary electric machine, the turntable positioned at middle part, the branch positioned at lower part
Support plate, the equally distributed oil cylinder of multiple circular turntable rotation centers between turntable and support plate and it is fixedly connected on support
The oil syringe of disk lower part;The output shaft of the rotary electric machine is fixedly connected with the rotation center of turntable, rotary electric machine and support plate
It is fixedly connected in the front side of sliding block;The upper end of the oil cylinder is fixedly connected with turntable, the bottom plate of oil cylinder lower end and the support
Disk upper surface slide connects;The type of lubricating oil being equipped in each oil cylinder differs, and is respectively provided on the bottom plate of each oil cylinder
It is useful for the oil-through hole one of outflow of lubrication oil, multiple oil-through holes one circle concentric with surrounding turntable rotation center;Adjacent two
Partition board is provided between a oil cylinder;The upper end of partition board is fixedly connected with turntable, the lower face of partition board and the upper table of the support plate
Face is slidably matched;There are one oil-through holes two in the position setting of corresponding oil-through hole one for the support plate;
The oil syringe includes oiling housing, and the oiling housing has the rectangular oil inlet positioned at upper end, is located at
The compartment at middle part, positioned at lower part and tilt to the right extension fuel-displaced portion and connection oil inlet and compartment between oil inlet
Channel, the oil inlet of the oil syringe are fixedly connected with the outer of oil-through hole two;The oil inlet of oil syringe by oil-through hole two according to
It is secondary to be connected with one suitching type of oil-through hole of each oil cylinder bottom;The lower end in the fuel-displaced portion is fuel-displaced in sliding slot two with penetrating
Mouthful;Be provided with a pair of of hollow channel boards of symmetrical distribution in the oil inlet passage, a pair of of hollow channel boards extend through it is fixed
It is arranged on the left side wall of oiling housing on right side wall, spaced apart formed falls oily lead between a pair of of hollow channel boards inner end
Road;The middle part of the hollow channel boards has horizontal concrete chute, is slidably provided in the horizontal concrete chute of the hollow channel boards of side
For adjusting the slide damper for falling oily channel opening size;The left and right sides outside compartment is each provided with a vibration unit,
The vibration unit is by the oscillating plate being fixedly connected on oiling hull outside wall, the vibrating motor being fixedly connected on oscillating plate
And the vibrating head composition on oscillating plate is fixedly connected on, the vibrating head is extend into across oiling housing inside compartment;Separate
Room lower part left end is additionally provided with roller bearing, and the rear and front end of roller bearing is rotatably connected to the front side wall and rear wall of oiling housing
On;One end of roller bearing is pierced by oiling hull outside and is drivingly connected with decelerating motor;
The cutting gun nozzle includes nozzle housing, and the nozzle housing is internally provided with oxygen spray pipe and the spray of Duo Gen acetylene
Pipe is provided with acetylene connecting tube, under the nozzle housing has superposed positive frustum section and is located at outside nozzle housing
The inversed taper platform section in portion, the top of positive frustum section are closed by top plate, and the lower end of positive frustum section is welded with the upper end of inversed taper platform section,
The bottom end of frustum section has the flame export for being communicated to nozzle housing inner cavity;
The oxygen spray pipe is fixed on the axial line in positive frustum section;The upper end of oxygen spray pipe is pierced by positive frustum section
Top top plate after connect with one end of oxygen flow valve, the upper and lower ends of part of the oxygen spray pipe in positive frustum section are respectively
The connecting rod radially set by more is fixedly connected with connection ring, positioned at the internal diameter of the connection ring of positive frustum section big opening end side
More than the internal diameter of the connection ring positioned at the small openend side of positive frustum section;Multiple acetylene jet pipes are circumferentially set around oxygen spray pipe
It puts, the both ends of acetylene jet pipe are fixedly connected respectively with two connection rings;Superposed connection ring has hollow lumen, and it will
The inner cavity of more multiple acetylene jet pipes is interconnected;The surface of oxygen spray pipe and acetylene jet pipe is equipped with largely to be connected with its inner cavity
Logical through-hole;
One end of the acetylene connecting tube penetrates inside nozzle housing and is connect with superposed connection ring through-lumen,
The other end of acetylene connecting tube is connect with acetylene gas pipe;The other end of the oxygen flow valve is connect with oxygen cylinder;
The synchronous motor, decelerating motor, horizontal drive motor, rotary electric machine, vibrating motor, hoist engine are each by leading
Line is connected with controller.
In the technical scheme, by the way that rotary platform upper is made to be provided with support column, and mechanical arm is made to pass through sliding block and cunning
Road coordinates the adjusting that can realize setting lengthwise position, is realized by the change for enabling relative position between travelling arm and fixed arm
The setting laterally above adjusting of position, so as to neatly adjust the position of setting, to adapt to different processing operating modes.Pass through
Two fixed seat tops that formula part puts down tool are both provided with driving and driven load carrier and can realize the at the uniform velocity rolling of pipe to be cut
It is dynamic, i.e., after setting location determination, the cutting operation of automation, and then the device can be completed by way of rotating pipe
Can realize the automation cutting operation of pipe, operating process is convenient, and cutting efficiency is high, cut quality is good, to it is artificial according to
Rely degree small.By making that there are multiple oil cylinders for being mounted with variety classes lubricating oil in oil syringe, make rotary electric machine driving disc
Rotation, and then multiple oil cylinder rotations can be driven to provide the filling of different types of lubricating oil, while easy to operation, moreover it is possible to have
Effect selects the filling of variety classes lubricating oil according to the different operating mode of sliding rail, so as to which the cost of lubricating oil can not only be saved, and
The service life of sliding rail can effectively be extended.A pair of of hollow channel boards are provided in oil inlet passage by making oil syringe, cunning can be passed through
Dynamic baffle slides in and out the size for changing and falling oily channel, and then can be convenient for adjusting the adding amount of lubricating oil;It is set in oil syringe
Put vibration unit, can promote the outer row of lubricating oil, the rotation of roller bearing can have a guide effect, and then can by the rotation of roller bearing into
One step drives being discharged to oil outlet for lubricating oil, and to be added in sliding slot, sliding rail and sliding slot are effectively lubricated.Cutting gun
Multiple acetylene jet pipes are arranged on the outside of oxygen spray pipe in nozzle, the oxygen of supply can in this way sprayed with the acetylene gas supplied
Sufficient mixing is carried out in mouth shell, so as to can guarantee the stability of cutting flame, is conducive to significantly improve cut quality.
Further, in order to improve the uniformity of mixing, the acetylene cant of the jet angle is 30 DEG C~60 DEG C, and quantity is not
Less than 10.
Further, in order to avoid the generation of slippery conditions, the surface anti-skidding line of the idler wheel.
Further, in order to ensure bonding strength, each connection ring passes through circumferential four connecting rods being uniformly arranged on the inside of it
It is welded with oxygen spray pipe.
As a preferred embodiment, the quantity of the oil cylinder and partition board is 6, material is stainless steel.
In order to solve the easy gas leakage of existing acetylene connecting tube, it is easy to aging and caused by cutter device whole service life it is low
The problem of, the acetylene connecting tube is molded by high molecular material pressing mold, and acetylene connecting tube is matched in parts by weight by following components
Composition:
323.7~548.0 parts of ultra-pure water, 115.1~157.8 parts of 2- methyl dodecyls aldehyde, 2- methoxyl group -3- methyl pyrroles
118.4~227.9 parts of piperazine, 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] methylamino] second
114.1~131.6 parts of sulfuric acid, 117.0~174.5 parts of yeast rna, 4,4'- (1- methyl ethylidene) biphenols and chloromethane
120.5~181.6 parts of the polymer of hexadecyl ethylene oxide and α-hydrogen-based-ω-hydroxyl poly- (oxidation -1,2- second diyl), Ruthenium nanometers of millis
122.1~177.3 parts of particle, poly- 115.1~157.2 parts of decanedioic acid propylene glycol ester, formaldehyde and 4- (1,1- dimethyl propyl) benzene
117.8~157.1 parts of the polymer of phenol, xylenol and methylphenol, the polymer of same (vertical structure) -1,3-butadiene
117.5~140.2 parts, 106.6~142.6 parts of 5- methoxyl group -1H- indole -3-formaldehydes, 2- methyl -2- nitro-1,3-propylene glycols
105.9~148.7 parts, 114.4~159.5 parts of formic acid, 124.1~168.9 parts of mandarin oil, mass concentration for 114ppm~
147.8~201.2 parts of the alpha-brominated -2- chlorobenzene acetic acids of 381ppm.
In order to solve the easy gas leakage of existing acetylene connecting tube, it is easy to aging and caused by cutter device whole service life it is low
The problem of, the manufacturing process of the acetylene connecting tube is as follows:
1st step:In continuous stirred tank reactor, ultra-pure water and 2- methyl dodecyl aldehyde are added in, startup is continuously stirred
The blender in tank reactor is mixed, setting speed is 116rpm~162rpm, starts leading in continuous stirred tank reactor
Hot oil makes temperature rise to 131.7 DEG C~132.0 DEG C, adds in 2- methoxyl group -3- methylpyrazines and stirs evenly, and carries out anti-
It answers 108.1~119.8 minutes, adds in 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] first ammonia
Base] etherosulfuric acid, flow is passed through as 107.6m3/ min~148.6m3The xenon of/min 108.1~119.8 minutes;Later continuous
Yeast rna is added in stirred-tank reactor, the hotline heater being again started up in continuous stirred tank reactor,
Temperature is made to rise to 148.4 DEG C~181.9 DEG C, keeps the temperature 108.1~119.6 minutes, adds in 4,4'- (1- methyl ethylidene) biphenol
The polymer of (oxidation -1,2- second diyl) poly- with chloromethyloxirane and α-hydrogen-based-ω-hydroxyl, adjustment continuously stir autoclave
The pH value of solution is 4.0~8.5 in reactor, keeps the temperature 108.0~348.0 minutes;
2nd step:Ruthenium nanoparticles separately are taken, in power are ultrasonic wave under 6.48KW~11.92KW by Ruthenium nanoparticles
After processing 0.114~1.181 hour;Ruthenium nanoparticles are added in another continuous stirred tank reactor, add in matter
The poly- decanedioic acid propylene glycol ester dispersion Ruthenium nanoparticles of a concentration of 118ppm~348ppm are measured, startup continuously stirs autoclave reaction
Hotline heater in device makes solution temperature between 41 DEG C~85 DEG C, starts the stirring in continuous stirred tank reactor
Machine, and with 4 × 102Rpm~8 × 102The speed stirring of rpm, adjustment pH value is between 4.6~8.6, insulated and stirred 114~181
Minute;Stop reaction later and stand 6.48 × 10~11.92 × 10 minutes, remove impurity;By suspension add in formaldehyde and 4- (1,
1- dimethyl propyls) phenol, xylenol and methylphenol polymer, for adjustment pH value between 1.6~2.6, it is heavy to be formed
The ultrapure water elution of starch, by centrifuge in rotating speed 4.497 × 103Rpm~9.909 × 103Solid content is obtained under rpm,
2.734×102DEG C~3.868 × 102It is dry at a temperature of DEG C, 0.497 × 10 is crossed after grinding3~1.909 × 103Mesh sieves, spare;
3rd step:With Ruthenium nanometers of millimicros after being handled in the polymer of (vertical structure) -1,3- butadiene and claim 9 between separately taking
Grain is irradiated after mixing using β reflected radiations, and the energy of β reflected radiations irradiation is 105.9MeV~133.7MeV, dosage is
153.9kGy~193.7kGy, irradiation time are 117.9~142.7 minutes, obtain same (vertical structure) -1,3- fourths between character change
The polymer of diene and Ruthenium nanoparticles mixtures;With the polymer and Ruthenium nanometers of millimicros of (vertical structure) -1,3- butadiene by between
Grain mixture is placed in another continuous stirred tank reactor, starts the hotline heater in continuous stirred tank reactor,
116.4 DEG C~162.5 DEG C of set temperature, start continuous stirred tank reactor in blender, rotating speed for 108rpm~
503rpm, pH are adjusted between 4.1~8.9, are dehydrated 117.1~131.9 minutes, spare;
4th step:With the polymer of (vertical structure) -1,3- butadiene and Ruthenium nanometers between the character change that above-mentioned steps are obtained
Milimicron particle mixture is added in the 5- methoxyl group -1H- indole -3-formaldehydes that mass concentration is 118ppm~348ppm, and cocurrent adds to
In the continuous stirred tank reactor of 1st step, flow acceleration is 253mL/min~981mL/min;It is anti-that startup continuously stirs autoclave
Mechanical stirrer is answered, setting speed is 122rpm~162rpm;Stirring 4~8 minutes;Add 2- methyl -2- nitros -1,3- the third two
Alcohol starts the hotline heater in continuous stirred tank reactor, is warming up to 152.8 DEG C~189.2 DEG C, pH is adjusted to 4.8
Between~8.2, xenon ventilatory capacity is passed through as 107.189m3/ min~148.642m3/ min, heat preservation stand 142.7~172.0 points
Clock;Continuous stirred tank reactor blender is again started up, rotating speed is 117rpm~162rpm, adds in formic acid, and cause pH tune
It is whole between 4.8~8.2, heat preservation stands 141.1~181.8 minutes;
5th step:Start the blender in continuous stirred tank reactor, setting speed is 114rpm~181rpm, is started
Hotline heater in continuous stirred tank reactor sets temperature in continuous stirred tank reactor as 1.714 × 102
DEG C~2.515 × 102DEG C, mandarin oil is added in, is reacted 108.4~119.9 minutes;Alpha-brominated -2- chlorobenzene acetic acids are added in later, are opened
Hotline heater in dynamic continuous stirred tank reactor, sets the temperature in continuous stirred tank reactor as 192.1 DEG C
~248.6 DEG C, pH is adjusted between 4.0~8.0, and pressure is 1.14MPa~1.15MPa, and the reaction time is 0.4~0.9 hour;
It is depressurized to gauge pressure later as 0MPa, is cooled to 108.4 DEG C~119.9 DEG C and discharges into molding press to get to acetylene connecting tube.
The grain size of the Ruthenium nanoparticles is 122 μm~132 μm.
The present invention, which can realize, automatically cuts pipe, and cut quality can be effectively ensured, help to improve cutting
Efficiency, while its cutting process uniform, controllable, the destabilizing factor for being avoided that manual operation and bringing;It is automatically cut due to using
Scheme is cut, is not influenced by working environment, convenient for carrying out cutting work in the big environment of high temperature and dust.
Description of the drawings
Fig. 1 is the structure diagram in the present invention;
Fig. 2 is the structure diagram of work piece holder in the present invention;
Fig. 3 is the structure diagram of mechanical arm in the present invention;
Fig. 4 is the fit structure schematic diagram of the sliding slot two in the present invention and sliding rail;
Fig. 5 is the structure diagram of oil filling device in the present invention;
Fig. 6 is the structure diagram of oil syringe in the present invention;
Fig. 7 is the structure diagram of cutting gun nozzle in the present invention;
Fig. 8 is the structure diagram of rotating connecting part between rotating platform and locomotive in the present invention;
Fig. 9 is the fatigue strength time history plot of acetylene connecting tube in the present invention.
In figure:1st, running track, 2, fixed plate, 3, locomotive, 3-1, angle adjustment motor, 3-2, drive gear, 4, rotation
Turn platform, 4-1, shaft, 4-2, external toothing, 6, support column, 6-1, slideway, 7, hoist engine, 8, mechanical arm, 8-1, reel, 8-
2nd, horizontal drive motor, 8-3, acetylene gas pipe, 8-4, oxygen cylinder, 8-5, cutting gun nozzle, 8-5-1, nozzle housing, 8-5-2, second
Alkynes jet pipe, 8-5-3, oxygen flow valve, 8-5-4, acetylene connecting tube, 8-5-5, oxygen spray pipe, 8-5-6, flame export, 8-5-7,
Connection ring, 8-6, sliding block, 8-6-1, sliding slot two, 8-6-2, oil filling device, 8-6-2-1, oil cylinder, 8-6-2-2, oiling
Device, 8-6-2-2-0, oiling housing, 8-6-2-2-1, oil inlet, 8-6-2-2-2, hollow channel boards, 8-6-2-2-3, slide damper,
8-6-2-2-4, roller bearing, 8-6-2-2-5, compartment, 8-6-2-2-6, oil outlet, 8-6-2-2-7, vibrating motor, 8-6-2-2-
8th, oscillating plate, 8-6-2-2-9, vibrating head, 8-6-2-3, rotary electric machine, 8-6-2-4, turntable, 8-6-2-5, partition board, 8-6-2-6,
Support plate, 8-6-3, sliding rail, 8-7, fixed arm, 8-8, travelling arm, 8-9, acetylene cylinder, 9, controller, 10, workpiece, 11, workpiece clamp
Tool, 11-1, active load carrier, 11-2, fixed seat, 11-3, driven load carrier, 11-4, angular transducer, 11-5, synchronization
Motor, 11-6, pedestal, 11-7, V-shaped bracket, 11-8, idler wheel.
Specific embodiment
The invention will be further described below in conjunction with the accompanying drawings.
As shown in Figures 1 to 8, it is a kind of for handling the high-pressure steam pipe cutter device of carbon tetrachloride, including fixed plate 2,
It is fixed at the running track 1 extended along the longitudinal direction of 2 upper right of fixed plate, is slidably arranged in 1 top of running track
Locomotive 3, rotating platform 4, support column 6, mechanical arm 8 and two oil filling device 8-6-2;
2 top of fixed plate is fixedly connected with work piece holder 11 in the position in 1 left side of running track;
The work piece holder 11 includes the two parallel fixed seat 11-2 extended along the longitudinal direction, every fixed seat
Front end, the rear end of 11-2 is respectively fitted with driven load carrier 11-3, active load carrier 11-1;The driven load carrier
11-3 is identical with active load carrier 11-1 structures, includes the pedestal 11-6 being fixedly connected on fixed seat 11-2, is hinged
V-shaped bracket 11-7 in pedestal 11-6 upper ends, two idler wheel 11-8 for being arranged on two upper ends of V-shaped bracket 11-7, wherein often
A idler wheel 11-8 is rotatably connected to by the shaft at its center in V-shaped bracket 11-7, the left and right ends of the shaft
It is pierced by the outside of V-shaped bracket 11-7;The side of V-shaped bracket 11-7 in each active load carrier 11-1 is fixed
It is connected with synchronous motor 11-5, the synchronous motor 11-5 and is used to drive an idler wheel 11-8's in active load carrier 11-1
Rotation;Angular transducer 11-4 is provided on synchronous motor 11-5.The surface anti-skidding line of the idler wheel 11-8.
The rotating platform 4 is rotationally connected to the top of locomotive 3 by being fixedly connected on the shaft of its underpart, specifically
Ground, as shown in figure 8, the lower end of shaft 4-1 is rotationally plugged in the blind hole for being arranged on 3 top of locomotive, and in shaft 4-1
Fixing sleeve is equipped with external toothing 4-2 on the outside of portion, and 3 top of locomotive is fixedly connected with angled adjustment motor 3-1, angle adjustment motor 3-
The drive gear 3-2 of driving external toothing 4-2 is equipped on 1 output shaft, angle adjustment motor 3-1 can be carried out by controller 9
Control;Rotating platform 4 also can guarantee the fixation of relative position, the positioning in rotation process by positioning device and locomotive 3
Device can be the long bolt connected between locomotive 3 and rotating platform 4.The support column 6 is fixed on rotating platform 4
On front side of portion;6 front side of support column is provided with vertical slideway 6-1 along its length, and the top of support column 6 is fixedly installed elevator
Machine 7;The mechanical arm 8 is arranged on the front side of support column 6, and the rear side of mechanical arm 8, which is fixedly connected with, to be slideably positioned in slideway 6-1
Sliding block 8-6;Roller is fixedly connected on the output shaft of the hoist engine 7, steel wire rope is arranged on the roller, steel wire rope is remote
One end from roller is connect with the sliding block 8-6;
The mechanical arm 8 is made of fixed arm 8-7 and travelling arm 8-8, and the sliding block 8-6 is fixedly connected on fixed arm 8-7
Rear side, the left upper part of the travelling arm 8-8 is fixedly connected with oxygen cylinder 8-4, left end lower part is fixedly connected with cutting gun spray
The right end of mouth 8-5, the fixed arm 8-7 are fixedly connected with reel 8-1, between the oxygen cylinder 8-4 and cutting gun nozzle 8-5
It is connected by pipeline;One end of the acetylene gas pipe 8-3 is connect with cutting gun nozzle 8-5, after reel 8-1 is crossed in other end winding
It is connect with acetylene cylinder 8-9;Middle part is provided with the sliding slot one being laterally extended on front side of the travelling arm 8-8, and the one of the fixed arm 8-7
A horizontal mounting arm is horizontally slidingly assemblied in the sliding slot one;The forward upper of travelling arm 8-8 is also associated with side along its length
To the rack of extension, fixed arm 8-7 is fixedly connected with horizontal drive motor 8-2 above rack;Horizontal drive motor 8-2's is defeated
The gear of drive rack is equipped on shaft;
The sliding block 8-6 is provided with two vertically extending and T-shaped cross section sliding slots two close to the side of slideway 6-1
Two T-shaped one slide rail 8-6-3 of cross section are slidably equipped in 8-6-1, two two 8-6-1 of sliding slot, two one slide rail 8-6-3's
Top and bottom of the top and bottom respectively with slideway 6-1 are fixedly connected;
Before two oil filling device 8-6-2 are fixed at sliding block 8-6 with corresponding to two two 8-6-1 of sliding slot respectively
Side;
The oil filling device 8-6-2 includes superposed rotary electric machine 8-6-2-3, the turntable 8- positioned at middle part
6-2-4, multiple surround positioned at the support plate 8-6-2-6 of lower part, between turntable 8-6-2-4 and support plate 8-6-2-6 turn
The equally distributed oil cylinder 8-6-2-1 of the disk 8-6-2-4 rotation centers and oil syringe 8- for being fixedly connected on support plate 8-6-2-6 lower parts
6-2-2;The output shaft of the rotary electric machine 8-6-2-3 is fixedly connected with the rotation center of turntable 8-6-2-4, rotary electric machine 8-6-
2-3 and support plate 8-6-2-6 are fixedly connected in the front side of sliding block 8-6;The upper end of the oil cylinder 8-6-2-1 and turntable 8-6-2-
4 are fixedly connected, and the bottom plate of oil cylinder 8-6-2-1 lower ends is connect with the support plate 8-6-2-6 upper surface slides;Each oil cylinder 8-6-
The type for the lubricating oil being equipped in 2-1 differs, and is both provided on the bottom plate of each oil cylinder 8-6-2-1 for outflow of lubrication oil
Oil-through hole one, multiple oil-through holes one with around the concentric circle of turntable 8-6-2-4 rotation centers;Two adjacent oil cylinder 8-6-
Partition board 8-6-2-5 is provided between 2-1;The upper end of partition board 8-6-2-5 is fixedly connected with turntable 8-6-2-4, partition board 8-6-2-5's
Lower face and the upper surface slide of the support plate 8-6-2-6 coordinate;The support plate 8-6-2-6 is in the position of corresponding oil-through hole one
Oil-through hole two there are one installing;
The oil syringe 8-6-2-2 includes oiling housing 8-6-2-2-0, and the oiling housing 8-6-2-2-0, which has, to be located at
The rectangular oil inlet 8-6-2-2-1 of upper end, positioned at the compartment 8-6-2-2-5 at middle part, incline positioned at lower part and to the right
Oil inlet passage between the fuel-displaced portion tiltedly extended and connection oil inlet 8-6-2-2-1 and compartment 8-6-2-2-5, the oil syringe
The oil inlet 8-6-2-2-1 of 8-6-2-2 is fixedly connected with the outer of oil-through hole two;The oil inlet 8-6-2- of oil syringe 8-6-2-2
2-1 is connected by oil-through hole two with one suitching type of oil-through hole of each oil cylinder 8-6-2-1 bottoms successively;The lower end in the fuel-displaced portion
With the oil outlet 8-6-2-2-6 penetrated in two 8-6-1 of sliding slot;A pair of symmetrical distribution is provided in the oil inlet passage
Hollow channel boards 8-6-2-2-2, a pair of of hollow channel boards 8-6-2-2-2 are fixed at oiling housing 8-6-2-2-0 with extending through
Left side wall on and right side wall on, between a pair of of hollow channel boards 8-6-2-2-2 inner ends it is spaced apart formation fall oily channel;Institute
The middle part for stating hollow channel boards 8-6-2-2-2 has horizontal concrete chute, in the horizontal concrete chute of the hollow channel boards 8-6-2-2-2 of side
It is slidably provided with to adjust the slide damper 8-6-2-2-3 for falling oily channel opening size;Outside compartment 8-6-2-2-5
The left and right sides is each provided with a vibration unit, and the vibration unit is by being fixedly connected on oiling housing 8-6-2-2-0 lateral walls
On oscillating plate 8-6-2-2-8, the vibrating motor 8-6-2-2-7 that is fixedly connected on oscillating plate 8-6-2-2-8 and be fixedly connected
Vibrating head 8-6-2-2-9 compositions on oscillating plate 8-6-2-2-8, the vibrating head 8-6-2-2-9 pass through oiling housing 8-6-
2-2-0 is extend into inside compartment 8-6-2-2-5;Compartment 8-6-2-2-5 lower parts left end is additionally provided with roller bearing 8-6-2-2-4,
The rear and front end of roller bearing 8-6-2-2-4 is rotatably connected on the front side wall and rear wall of oiling housing 8-6-2-2-0;Roller bearing
One end of 8-6-2-2-4 is pierced by outside oiling housing 8-6-2-2-0 and is drivingly connected with decelerating motor;
The cutting gun nozzle 8-5 includes nozzle housing 8-5-1, the nozzle housing 8-5-1 and is internally provided with oxygen spray
Pipe 8-5-5 and Duo Gen acetylene jet pipe 8-5-2, is provided with acetylene connecting tube 8-5-4, the nozzle outside nozzle housing 8-5-1
Shell 8-5-1 has superposed positive frustum section and the inversed taper platform section positioned at lower part, and the top of positive frustum section is sealed by top plate
It closes, the lower end of positive frustum section is welded with the upper end of inversed taper platform section, and the bottom end of inversed taper platform section, which has, to be communicated in nozzle housing 8-5-1
The flame export 8-5-6 of chamber;
The oxygen spray pipe 8-5-5 is fixed on the axial line in positive frustum section;It wears the upper end of oxygen spray pipe 8-5-5
It is connect after going out the top plate at the top of positive frustum section with one end of oxygen flow valve 8-5-3, oxygen spray pipe 8-5-5 is in positive frustum section
Part upper and lower ends each by more radially setting connecting rod be fixedly connected with connection ring 8-5-7, positioned at positive frustum section
The internal diameter of the connection ring 8-5-7 of big opening end side is more than the interior of the connection ring 8-5-7 positioned at the small openend side of positive frustum section
Diameter;Multiple acetylene jet pipe 8-5-2 are circumferentially set around oxygen spray pipe 8-5-5, the both ends of acetylene jet pipe 8-5-2 respectively with two
Connection ring 8-5-7 is fixedly connected;Superposed connection ring 8-5-7 has a hollow lumen, and it is by more multiple acetylene jet pipes
The inner cavity of 8-5-2 is interconnected;The surface of oxygen spray pipe 8-5-5 and acetylene jet pipe 8-5-2 are equipped with largely to be connected with its inner cavity
Logical through-hole;
One end of the acetylene connecting tube 8-5-4 penetrates inside nozzle housing 8-5-1 and superposed connection ring 8-5-7
It connects to through-lumen, the other end of acetylene connecting tube 8-5-4 is connect with acetylene gas pipe 8-3;The oxygen flow valve 8-5-3's
The other end is connect with oxygen cylinder 8-4;
The synchronous motor 11-5, decelerating motor, horizontal drive motor 8-2, rotary electric machine 8-6-2-3, vibrating motor 8-
6-2-2-7, hoist engine 7 are connected each by conducting wire with controller 9.
The acetylene jet pipe 8-5-2 angles of inclination are 30 DEG C~60 DEG C, and quantity is no less than 10.
Each connection ring 8-5-7 is welded by circumferential four connecting rods being uniformly arranged on the inside of it with oxygen spray pipe 8-5-5.
The quantity of the oil cylinder 8-6-2-1 and partition board 8-6-2-5 is 6, and material is stainless steel.
The acetylene connecting tube 8-5-4 is molded by high molecular material pressing mold, and acetylene connecting tube 8-5-4 is by following components by weight
Measure number proportioning composition:
323.7~548.0 parts of ultra-pure water, 115.1~157.8 parts of 2- methyl dodecyls aldehyde, 2- methoxyl group -3- methyl pyrroles
118.4~227.9 parts of piperazine, 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] methylamino] second
114.1~131.6 parts of sulfuric acid, 117.0~174.5 parts of yeast rna, 4,4'- (1- methyl ethylidene) biphenols and chloromethane
120.5~181.6 parts of the polymer of hexadecyl ethylene oxide and α-hydrogen-based-ω-hydroxyl poly- (oxidation -1,2- second diyl), Ruthenium nanometers of millis
122.1~177.3 parts of particle, poly- 115.1~157.2 parts of decanedioic acid propylene glycol ester, formaldehyde and 4- (1,1- dimethyl propyl) benzene
117.8~157.1 parts of the polymer of phenol, xylenol and methylphenol, the polymer of same (vertical structure) -1,3-butadiene
117.5~140.2 parts, 106.6~142.6 parts of 5- methoxyl group -1H- indole -3-formaldehydes, 2- methyl -2- nitro-1,3-propylene glycols
105.9~148.7 parts, 114.4~159.5 parts of formic acid, 124.1~168.9 parts of mandarin oil, mass concentration for 114ppm~
147.8~201.2 parts of the alpha-brominated -2- chlorobenzene acetic acids of 381ppm.
The manufacturing process of the acetylene connecting tube 8-5-4 is as follows:
1st step:In continuous stirred tank reactor, ultra-pure water and 2- methyl dodecyl aldehyde are added in, startup is continuously stirred
The blender in tank reactor is mixed, setting speed is 116rpm~162rpm, starts leading in continuous stirred tank reactor
Hot oil makes temperature rise to 131.7 DEG C~132.0 DEG C, adds in 2- methoxyl group -3- methylpyrazines and stirs evenly, and carries out anti-
It answers 108.1~119.8 minutes, adds in 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] first ammonia
Base] etherosulfuric acid, flow is passed through as 107.6m3/ min~148.6m3The xenon of/min 108.1~119.8 minutes;Later continuous
Yeast rna is added in stirred-tank reactor, the hotline heater being again started up in continuous stirred tank reactor,
Temperature is made to rise to 148.4 DEG C~181.9 DEG C, keeps the temperature 108.1~119.6 minutes, adds in 4,4'- (1- methyl ethylidene) biphenol
The polymer of (oxidation -1,2- second diyl) poly- with chloromethyloxirane and α-hydrogen-based-ω-hydroxyl, adjustment continuously stir autoclave
The pH value of solution is 4.0~8.5 in reactor, keeps the temperature 108.0~348.0 minutes;
2nd step:Ruthenium nanoparticles separately are taken, in power are ultrasonic wave under 6.48KW~11.92KW by Ruthenium nanoparticles
After processing 0.114~1.181 hour;Ruthenium nanoparticles are added in another continuous stirred tank reactor, add in matter
The poly- decanedioic acid propylene glycol ester dispersion Ruthenium nanoparticles of a concentration of 118ppm~348ppm are measured, startup continuously stirs autoclave reaction
Hotline heater in device makes solution temperature between 41 DEG C~85 DEG C, starts the stirring in continuous stirred tank reactor
Machine, and with 4 × 102Rpm~8 × 102The speed stirring of rpm, adjustment pH value is between 4.6~8.6, insulated and stirred 114~181
Minute;Stop reaction later and stand 6.48 × 10~11.92 × 10 minutes, remove impurity;By suspension add in formaldehyde and 4- (1,
1- dimethyl propyls) phenol, xylenol and methylphenol polymer, for adjustment pH value between 1.6~2.6, it is heavy to be formed
The ultrapure water elution of starch, by centrifuge in rotating speed 4.497 × 103Rpm~9.909 × 103Solid content is obtained under rpm,
2.734×102DEG C~3.868 × 102It is dry at a temperature of DEG C, 0.497 × 10 is crossed after grinding3~1.909 × 103Mesh sieves, spare;
3rd step:With Ruthenium nanometers of millimicros after being handled in the polymer of (vertical structure) -1,3- butadiene and claim 9 between separately taking
Grain is irradiated after mixing using β reflected radiations, and the energy of β reflected radiations irradiation is 105.9MeV~133.7MeV, dosage is
153.9kGy~193.7kGy, irradiation time are 117.9~142.7 minutes, obtain same (vertical structure) -1,3- fourths between character change
The polymer of diene and Ruthenium nanoparticles mixtures;With the polymer and Ruthenium nanometers of millimicros of (vertical structure) -1,3- butadiene by between
Grain mixture is placed in another continuous stirred tank reactor, starts the hotline heater in continuous stirred tank reactor,
116.4 DEG C~162.5 DEG C of set temperature, start continuous stirred tank reactor in blender, rotating speed for 108rpm~
503rpm, pH are adjusted between 4.1~8.9, are dehydrated 117.1~131.9 minutes, spare;
4th step:With the polymer of (vertical structure) -1,3- butadiene and Ruthenium nanometers between the character change that above-mentioned steps are obtained
Milimicron particle mixture is added in the 5- methoxyl group -1H- indole -3-formaldehydes that mass concentration is 118ppm~348ppm, and cocurrent adds to
In the continuous stirred tank reactor of 1st step, flow acceleration is 253mL/min~981mL/min;It is anti-that startup continuously stirs autoclave
Mechanical stirrer is answered, setting speed is 122rpm~162rpm;Stirring 4~8 minutes;Add 2- methyl -2- nitros -1,3- the third two
Alcohol starts the hotline heater in continuous stirred tank reactor, is warming up to 152.8 DEG C~189.2 DEG C, pH is adjusted to 4.8
Between~8.2, xenon ventilatory capacity is passed through as 107.189m3/ min~148.642m3/ min, heat preservation stand 142.7~172.0 points
Clock;Continuous stirred tank reactor blender is again started up, rotating speed is 117rpm~162rpm, adds in formic acid, and cause pH tune
It is whole between 4.8~8.2, heat preservation stands 141.1~181.8 minutes;
5th step:Start the blender in continuous stirred tank reactor, setting speed is 114rpm~181rpm, is started
Hotline heater in continuous stirred tank reactor sets temperature in continuous stirred tank reactor as 1.714 × 102
DEG C~2.515 × 102DEG C, mandarin oil is added in, is reacted 108.4~119.9 minutes;Alpha-brominated -2- chlorobenzene acetic acids are added in later, are opened
Hotline heater in dynamic continuous stirred tank reactor, sets the temperature in continuous stirred tank reactor as 192.1 DEG C
~248.6 DEG C, pH is adjusted between 4.0~8.0, and pressure is 1.14MPa~1.15MPa, and the reaction time is 0.4~0.9 hour;
It is depressurized to gauge pressure later as 0MPa, is cooled to 108.4 DEG C~119.9 DEG C and discharges into molding press to get to acetylene connecting tube 8-5-
4。
The grain size of the Ruthenium nanoparticles is 122 μm~132 μm.
The course of work:Locomotive 3 is rollably arranged on by the runner of its lower end in running track 1, so as to realize branch
The movement of the position in the longitudinal direction of dagger 6, hoist engine 7 is moved in the longitudinal direction by rope belt movable slider 8-6, so as to reality
The adjusting of existing mechanical arm 8 position in the longitudinal direction.Mechanical arm 8 is made of fixed arm 8-7 and travelling arm 8-8, and then passes through 8-2 levels
The rotation of driving motor can drive travelling arm 8-8 relative to stretchings of the fixed arm 8-7 to left part or the retraction to right part, so as to
Easily change the position of jobs node.The mixed gas of oxygen and acetylene is passed through flame export 8-5-6 by cutting gun nozzle 8-5
Uniformly discharge, so as to be convenient for the stability of cutting flame, is conducive to the raising of cut quality.When the position of cutting gun nozzle 8-5
Put it is fixed after, by control the synchronous motor 11-5 in two active load carrier 11-1 at a same speed, same direction
Idler wheel 11-8 uniform rotations are driven, can make to be located at active load carrier 11-1 and the workpiece 10 on driven load carrier 11-3 tops
It equably rotates, so as to automatically carry out cutting operation.
The content that following embodiment further illustrates the present invention, but should not be construed as limiting the invention.Without departing substantially from
In the case of spirit and essence of the invention, to modification and replacement that the method for the present invention, step or condition are made, the present invention is belonged to
Range.Unless otherwise specified, the conventional means that technological means used in embodiment is well known to those skilled in the art.
Embodiment 1
Acetylene connecting tube 8-5-4 of the present invention is prepared, and count in parts by weight according to following steps:
1st step:In continuous stirred tank reactor, 323.7 parts of ultra-pure water and 2- methyl dodecyls aldehyde 115.1 are added in
Part, start the blender in continuous stirred tank reactor, setting speed 116rpm starts in continuous stirred tank reactor
Hotline heater, temperature is made to rise to 131.7 DEG C, 118.4 parts of 2- methoxyl group -3- methylpyrazines is added in and stirs evenly, carry out
Reaction 108.1 minutes adds in 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] methylamino] second
114.1 parts of sulfuric acid is passed through flow as 107.6m3The xenon of/min 108.1 minutes;Add in continuous stirred tank reactor later
Enter 117.0 parts of yeast rna, the hotline heater being again started up in continuous stirred tank reactor rises to temperature
148.4 DEG C, keep the temperature 108.1 minutes, add in 4,4'- (1- methyl ethylidene) biphenols and chloromethyloxirane and α-hydrogen-based-
120.5 parts of the polymer of ω-hydroxyl poly- (oxidation -1,2- second diyl) adjusts the pH value of solution in continuous stirred tank reactor
It is 4.0, keeps the temperature 108.0 minutes;
2nd step:122.1 parts of Ruthenium nanoparticles separately are taken, by Ruthenium nanoparticles at power is ultrasonic wave under 6.48KW
Reason is after 0.114 hour;Ruthenium nanoparticles are added in another continuous stirred tank reactor, adding in mass concentration is
115.1 parts of dispersion Ruthenium nanoparticles of poly- decanedioic acid propylene glycol ester of 118ppm, start leading in continuous stirred tank reactor
Hot oil makes solution temperature at 41 DEG C, starts the blender in continuous stirred tank reactor, and with 4 × 102Rpm's
Speed stirs, and adjustment pH value is 4.6, insulated and stirred 114 minutes;Stop reaction later and stand 6.48 × 10 minutes, remove impurity;
Suspension is added in 117.8 parts of the polymer of formaldehyde and 4- (1,1- dimethyl propyl) phenol, xylenol and methylphenol,
PH value is adjusted 1.6, the ultrapure water elution of sediment is formed, by centrifuge in rotating speed 4.497 × 103Solid is obtained under rpm
Object, 2.734 × 102It is dry at a temperature of DEG C, 0.497 × 10 is crossed after grinding3Mesh sieves, spare;
3rd step:With Ruthenium nanometers of millimicros after the processing of 117.5 and the 2nd step of polymer of (vertical structure) -1,3- butadiene between separately taking
Grain, after mixing using β reflected radiations irradiate, β reflected radiations irradiation energy be 105.9MeV, dosage 153.9kGy,
Irradiation time is 117.9 minutes, obtains the polymer and Ruthenium nanoparticles of same (vertical structure) -1,3-butadiene between character change
Mixture;By between another continuous stirred tank is placed in the polymer of (vertical structure) -1,3- butadiene and Ruthenium nanoparticles mixtures
In formula reactor, start the hotline heater in continuous stirred tank reactor, 116.4 DEG C of set temperature, startup is continuously stirred
The blender in tank reactor is mixed, rotating speed 108rpm, pH are adjusted to 4.1, are dehydrated 117.1 minutes, spare;
4th step:The character that 3rd step the is obtained polymer of same (vertical structure) -1,3- butadiene and Ruthenium nanometers of millis between changing
Particle mixture is added in 106.6 parts of the 5- methoxyl group -1H- indole -3-formaldehydes that mass concentration is 118ppm, and cocurrent adds to the 1st
In the continuous stirred tank reactor of step, flow acceleration 253mL/min;Start continuous stirred tank reactor blender, if
Rotating speed is determined for 122rpm;Stirring 4 minutes;105.9 parts of 2- methyl -2- nitro-1,3-propylene glycols are added, start continuous stirred tank
Hotline heater in formula reactor is warming up to 152.8 DEG C, and pH is adjusted to 4.8, is passed through xenon ventilatory capacity as 107.189m3/
Min, heat preservation stand 142.7 minutes;Continuous stirred tank reactor blender is again started up, rotating speed 117rpm adds in formic acid
114.4 parts, and pH is caused to be adjusted to 4.8, heat preservation stands 141.1 minutes;
5th step:Start the blender in continuous stirred tank reactor, setting speed 114rpm, startup continuously stirs
Hotline heater in tank reactor sets temperature in continuous stirred tank reactor as 1.714 × 102DEG C, it adds in
124.1 parts of mandarin oil reacts 108.4 minutes;Alpha-brominated -2- the chlorobenzene acetic acids 147.8 that mass concentration is 114ppm are added in later
Part, start the hotline heater in continuous stirred tank reactor, set temperature in continuous stirred tank reactor as
192.1 DEG C, pH is adjusted to 4.0, and pressure 1.14MPa, the reaction time is 0.4 hour;It is depressurized to gauge pressure later as 0MPa, cooling
It discharges to 108.4 DEG C into molding press to get to acetylene connecting tube 8-5-4;
The grain size of the Ruthenium nanoparticles is 122 μm.
Embodiment 2
Acetylene connecting tube 8-5-4 of the present invention is prepared, and count in parts by weight according to following steps:
1st step:In continuous stirred tank reactor, 548.0 parts of ultra-pure water and 2- methyl dodecyls aldehyde 157.8 are added in
Part, start the blender in continuous stirred tank reactor, setting speed 162rpm starts in continuous stirred tank reactor
Hotline heater, temperature is made to rise to 132.0 DEG C, 227.9 parts of 2- methoxyl group -3- methylpyrazines is added in and stirs evenly, carry out
Reaction 119.8 minutes adds in 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] methylamino] second
131.6 parts of sulfuric acid is passed through flow as 148.6m3The xenon of/min 119.8 minutes;Add in continuous stirred tank reactor later
Enter 174.5 parts of yeast rna, the hotline heater being again started up in continuous stirred tank reactor rises to temperature
181.9 DEG C, keep the temperature 119.6 minutes, add in 4,4'- (1- methyl ethylidene) biphenols and chloromethyloxirane and α-hydrogen-based-
181.6 parts of the polymer of ω-hydroxyl poly- (oxidation -1,2- second diyl) adjusts the pH value of solution in continuous stirred tank reactor
It is 8.5, keeps the temperature 348.0 minutes;
2nd step:177.3 parts of Ruthenium nanoparticles separately are taken, by Ruthenium nanoparticles at power is ultrasonic wave under 11.92KW
Reason is after 1.181 hours;Ruthenium nanoparticles are added in another continuous stirred tank reactor, adding in mass concentration is
157.2 parts of dispersion Ruthenium nanoparticles of poly- decanedioic acid propylene glycol ester of 348ppm, start leading in continuous stirred tank reactor
Hot oil makes solution temperature between 85 DEG C, starts the blender in continuous stirred tank reactor, and with 8 ×
102The speed stirring of rpm, adjustment pH value is 8.6, insulated and stirred 181 minutes;Stop reaction later and stand 11.92 × 10 minutes,
Remove impurity;Suspension is added in into polymerizeing for formaldehyde and 4- (1,1- dimethyl propyls) phenol, xylenol and methylphenol
157.1 parts of object, adjustment pH value form the ultrapure water elution of sediment, by centrifuge in rotating speed 9.909 × 10 2.63rpm
Under obtain solid content, 3.868 × 102It is dry at a temperature of DEG C, 1.909 × 10 are crossed after grinding3Mesh sieves, spare;
3rd step:With Ruthenium nanometers of millimicros after 140.2 parts of the polymer of (vertical structure) -1,3- butadiene and the processing of the 2nd step between separately taking
Grain, after mixing using β reflected radiations irradiate, β reflected radiations irradiation energy be 133.7MeV, dosage 193.7kGy,
Irradiation time is 142.7 minutes, obtains the polymer and Ruthenium nanoparticles of same (vertical structure) -1,3-butadiene between character change
Mixture;By between another continuous stirred tank is placed in the polymer of (vertical structure) -1,3- butadiene and Ruthenium nanoparticles mixtures
In formula reactor, start the hotline heater in continuous stirred tank reactor, 162.5 DEG C of set temperature, startup is continuously stirred
The blender in tank reactor is mixed, rotating speed 503rpm, pH are adjusted to 8.9, are dehydrated 131.9 minutes, spare;
4th step:The character that 3rd step the is obtained polymer of same (vertical structure) -1,3- butadiene and Ruthenium nanometers of millis between changing
Particle mixture is added in 142.6 parts of the 5- methoxyl group -1H- indole -3-formaldehydes that mass concentration is 348ppm, and cocurrent adds to the 1st
In the continuous stirred tank reactor of step, flow acceleration 981mL/min;Start continuous stirred tank reactor blender, if
Rotating speed is determined for 162rpm;Stirring 8 minutes;148.7 parts of 2- methyl -2- nitro-1,3-propylene glycols are added, start continuous stirred tank
Hotline heater in formula reactor is warming up to 189.2 DEG C, and pH is adjusted to 8.2, is passed through xenon ventilatory capacity as 148.642m3/
Min, heat preservation stand 172.0 minutes;Continuous stirred tank reactor blender is again started up, rotating speed 162rpm adds in formic acid
159.5 parts, and pH is caused to be adjusted to 8.2, heat preservation stands 181.8 minutes;
5th step:Start the blender in continuous stirred tank reactor, setting speed 181rpm, startup continuously stirs
Hotline heater in tank reactor sets temperature in continuous stirred tank reactor as 2.515 × 102DEG C, it adds in
168.9 parts of mandarin oil reacts 119.9 minutes;Alpha-brominated -2- the chlorobenzene acetic acids 201.2 that mass concentration is 381ppm are added in later
Part, start the hotline heater in continuous stirred tank reactor, set temperature in continuous stirred tank reactor as
248.6 DEG C, pH is adjusted to 8.0, and pressure 1.15MPa, the reaction time is 0.9 hour;It is depressurized to gauge pressure later as 0MPa, cooling
It discharges to 119.9 DEG C into molding press to get to acetylene connecting tube 8-5-4;
The grain size of the Ruthenium nanoparticles is 132 μm.
Embodiment 3
Acetylene connecting tube 8-5-4 of the present invention is prepared, and count in parts by weight according to following steps:
1st step:In continuous stirred tank reactor, 323.9 parts of ultra-pure water and 2- methyl dodecyls aldehyde 115.9 are added in
Part, start the blender in continuous stirred tank reactor, setting speed 116rpm starts in continuous stirred tank reactor
Hotline heater, temperature is made to rise to 131.9 DEG C, 118.9 parts of 2- methoxyl group -3- methylpyrazines is added in and stirs evenly, carry out
Reaction 108.9 minutes adds in 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] methylamino] second
114.9 parts of sulfuric acid is passed through flow as 107.9m3The xenon of/min 108.9 minutes;Add in continuous stirred tank reactor later
Enter 117.9 parts of yeast rna, the hotline heater being again started up in continuous stirred tank reactor rises to temperature
148.9 DEG C, keep the temperature 108.9 minutes, add in 4,4'- (1- methyl ethylidene) biphenols and chloromethyloxirane and α-hydrogen-based-
120.9 parts of the polymer of ω-hydroxyl poly- (oxidation -1,2- second diyl) adjusts the pH value of solution in continuous stirred tank reactor
It is 4.9, keeps the temperature 108.9 minutes;
2nd step:122.9 parts of Ruthenium nanoparticles separately are taken, by Ruthenium nanoparticles at power is ultrasonic wave under 6.489KW
Reason is after 0.1149 hour;Ruthenium nanoparticles are added in another continuous stirred tank reactor, adding in mass concentration is
115.9 parts of dispersion Ruthenium nanoparticles of poly- decanedioic acid propylene glycol ester of 118.9ppm, start in continuous stirred tank reactor
Hotline heater makes solution temperature at 41.9 DEG C, starts the blender in continuous stirred tank reactor, and with 4.9 ×
102The speed stirring of rpm, adjustment pH value is 4.9, insulated and stirred 114.9 minutes;Stop reaction later and stand 6.48 × 10 points
Clock removes impurity;Suspension is added in into the poly- of formaldehyde and 4- (1,1- dimethyl propyls) phenol, xylenol and methylphenol
Close 117.9 parts of object, adjustment pH value forms the ultrapure water elution of sediment 1.9, by centrifuge rotating speed 4.497 ×
103Solid content is obtained under rpm, 2.734 × 102It is dry at a temperature of DEG C, 0.497 × 10 is crossed after grinding3Mesh sieves, spare;
3rd step:With Ruthenium nanometers of millimicros after the processing of 117.9 and the 2nd step of polymer of (vertical structure) -1,3- butadiene between separately taking
Grain, after mixing using β reflected radiations irradiate, β reflected radiations irradiation energy be 105.9MeV, dosage 153.9kGy,
Irradiation time is 117.9 minutes, obtains the polymer and Ruthenium nanoparticles of same (vertical structure) -1,3-butadiene between character change
Mixture;By between another continuous stirred tank is placed in the polymer of (vertical structure) -1,3- butadiene and Ruthenium nanoparticles mixtures
In formula reactor, start the hotline heater in continuous stirred tank reactor, 116.9 DEG C of set temperature, startup is continuously stirred
The blender in tank reactor is mixed, rotating speed 108rpm, pH are adjusted to 4.9, are dehydrated 117.9 minutes, spare;
4th step:The character that 3rd step the is obtained polymer of same (vertical structure) -1,3- butadiene and Ruthenium nanometers of millis between changing
Particle mixture is added in 106.9 parts of the 5- methoxyl group -1H- indole -3-formaldehydes that mass concentration is 118.9ppm, and cocurrent adds to
In the continuous stirred tank reactor of 1st step, flow acceleration 253.9mL/min;Start continuous stirred tank reactor stirring
Machine, setting speed 122rpm;Stirring 4.9 minutes;105.9 parts of 2- methyl -2- nitro-1,3-propylene glycols are added, starts and connects
Hotline heater in continuous stirred-tank reactor, is warming up to 152.9 DEG C, pH is adjusted to 4.9, is passed through xenon ventilatory capacity and is
107.9m3/ min, heat preservation stand 142.9 minutes;It is again started up continuous stirred tank reactor blender, rotating speed 117rpm,
114.9 parts of formic acid is added in, and pH is caused to be adjusted to 4.9, heat preservation stands 141.9 minutes;
5th step:Start the blender in continuous stirred tank reactor, setting speed 114rpm, startup continuously stirs
Hotline heater in tank reactor sets temperature in continuous stirred tank reactor as 1.714 × 102DEG C, it adds in
124.9 parts of mandarin oil reacts 108.9 minutes;Alpha-brominated -2- the chlorobenzene acetic acids 147.8 that mass concentration is 114ppm are added in later
Part, start the hotline heater in continuous stirred tank reactor, set temperature in continuous stirred tank reactor as
192.9 DEG C, pH is adjusted to 4.9, and pressure 1.14MPa, the reaction time is 0.41 hour;It is depressurized to gauge pressure later as 0MPa, drop
Temperature discharges into molding press to get to acetylene connecting tube 8-5-4 to 108.9 DEG C;
The grain size of the Ruthenium nanoparticles is 122 μm.
Reference examples
Reference examples are tested for the property experiment using the acetylene connecting tube of certain commercially available brand.
Embodiment 4
The acetylene connecting tube that Examples 1 to 3 and reference examples are obtained is tested for the property experiment, to body after test
The parameters such as product quantitative ratio, 3 years serviceability rates (%), anticorrosion rate (%), surface smoothness are analyzed.Data analysis such as 1 institute of table
Show.
As seen from Table 1, acetylene connecting tube 8-5-4 of the present invention, volume quantitative ratio, are prevented 3 years serviceability rates (%)
Rate of corrosion (%), surface smoothness are above the product of prior art production.
In addition, as shown in figure 9, acetylene connecting tube 8-5-4 of the present invention is carried out with reference examples, during with using
Between variation test data statistics.Find out in figure, Examples 1 to 3 is substantially given birth to better than the prior art in fatigue strength technical indicator
The product of production.
Claims (10)
1. it is a kind of for handling the high-pressure steam pipe cutter device of carbon tetrachloride, including fixed plate (2), it is fixed at fixed plate
(2) running track (1) extended along the longitudinal direction of upper right and the locomotive for being slidably arranged in running track (1) top
(3);It is characterized in that, further include rotating platform (4), support column (6), mechanical arm (8) and two oil filling device (8-6-
2);
Position of fixed plate (2) top on the left of running track (1) is fixedly connected with work piece holder (11);
The work piece holder (11) includes the two parallel fixed seats (11-2) extended along the longitudinal direction, every fixed seat
Front end, the rear end of (11-2) are respectively fitted with driven load carrier (11-3), active load carrier (11-1);The driven carrying
Mechanism (11-3) is identical with active load carrier (11-1) structure, includes the pedestal being fixedly connected in fixed seat (11-2)
(11-6), the V-shaped bracket (11-7) for being hinged on pedestal (11-6) upper end, be arranged on two upper end of V-shaped bracket (11-7) two
A idler wheel (11-8), wherein each idler wheel (11-8) is rotatably connected to V-shaped bracket (11- by the shaft at its center
7) in, the left and right ends of the shaft are pierced by the outside of V-shaped bracket (11-7);In each active load carrier (11-1)
The side of V-shaped bracket (11-7) be fixedly connected with synchronous motor (11-5), the synchronous motor (11-5) is for driving
The rotation of an idler wheel (11-8) in active load carrier (11-1);
The rotating platform (4) is rotationally connected to the top of locomotive (3) by being fixedly connected on the shaft of its underpart;It is described
Support column (6) is fixed on front side of rotating platform (4) top;It is vertical to be provided with along its length on front side of support column (6)
Slideway (6-1) is fixedly installed hoist engine (7) at the top of support column (6);Before the mechanical arm (8) is arranged on support column (6)
Side is fixedly connected with the sliding block (8-6) being slideably positioned in slideway (6-1) on rear side of mechanical arm (8);The hoist engine (7)
Roller is fixedly connected on output shaft, steel wire rope, the one end of steel wire rope far from roller and the sliding block are arranged on the roller
(8-6) is connected;
The mechanical arm (8) is made of fixed arm (8-7) and travelling arm (8-8), and the sliding block (8-6) is fixedly connected on fixed arm
The rear side of (8-7), the left upper part of the travelling arm (8-8) is fixedly connected with oxygen cylinder (8-4), left end lower part is fixedly connected with
Cutting gun nozzle (8-5), the right end of the fixed arm (8-7) are fixedly connected with reel (8-1), the oxygen cylinder (8-4) and
It is connected between cutting gun nozzle (8-5) by pipeline;One end of the acetylene gas pipe (8-3) is connect with cutting gun nozzle (8-5),
Other end winding is crossed reel (8-1) and is connect afterwards with acetylene cylinder (8-9);Middle part is provided with transverse direction on front side of the travelling arm (8-8)
The sliding slot one of extension, a horizontal mounting arm of the fixed arm (8-7) are horizontally slidingly assemblied in the sliding slot one;Travelling arm
The forward upper of (8-8) is also associated with the rack extended along its length, and fixed arm (8-7) is fixedly connected with above rack
Horizontal drive motor (8-2);The gear of drive rack is equipped on the output shaft of horizontal drive motor (8-2);
The sliding block (8-6) is provided with two vertically extending and T-shaped cross section sliding slots two close to the side of slideway (6-1)
(8-6-1) is slidably equipped with T-shaped two one slide rails (8-6-3) in cross section, two one slide rails in two sliding slots two (8-6-1)
Top and bottom of the top and bottom of (8-6-3) respectively with slideway (6-1) are fixedly connected;
Two oil filling devices (8-6-2) are fixed at sliding block (8-6) with corresponding to two sliding slots two (8-6-1) respectively
Leading flank;
The oil filling device (8-6-2) includes superposed rotary electric machine (8-6-2-3), the turntable positioned at middle part
(8-6-2-4), positioned at the support plate (8-6-2-6) of lower part, between turntable (8-6-2-4) and support plate (8-6-2-6)
The equally distributed oil cylinder of multiple circular turntable (8-6-2-4) rotation centers (8-6-2-1) and it is fixedly connected on support plate (8-6-2-
6) oil syringe (8-6-2-2) of lower part;In the output shaft of the rotary electric machine (8-6-2-3) and the rotation of turntable (8-6-2-4)
The heart is fixedly connected, and rotary electric machine (8-6-2-3) and support plate (8-6-2-6) are fixedly connected in the front side of sliding block (8-6);It is described
The upper end of oil cylinder (8-6-2-1) is fixedly connected with turntable (8-6-2-4), the bottom plate and the support of oil cylinder (8-6-2-1) lower end
Disk (8-6-2-6) upper surface slide connects;The type of lubricating oil being equipped in each oil cylinder (8-6-2-1) differs, each
The oil-through hole one for outflow of lubrication oil is both provided on the bottom plate of oil cylinder (8-6-2-1), multiple oil-through holes one are with surrounding turntable
The concentric circle of (8-6-2-4) rotation center;Partition board (8-6-2-5) is provided between two adjacent oil cylinders (8-6-2-1);Every
The upper end of plate (8-6-2-5) is fixedly connected with turntable (8-6-2-4), the lower face of partition board (8-6-2-5) and the support plate (8-
Upper surface slide cooperation 6-2-6);There are one excessively oily in the position setting of corresponding oil-through hole one for the support plate (8-6-2-6)
Hole two;
The oil syringe (8-6-2-2) includes oiling housing (8-6-2-2-0), and the oiling housing (8-6-2-2-0) has position
Rectangular oil inlet (8-6-2-2-1) in upper end, positioned at the compartment (8-6-2-2-5) at middle part, positioned at lower part and to the right
Oil inlet passage between the fuel-displaced portion of inclined downward extension and connection oil inlet (8-6-2-2-1) and compartment (8-6-2-2-5),
The oil inlet (8-6-2-2-1) of the oil syringe (8-6-2-2) is fixedly connected with the outer of oil-through hole two;Oil syringe (8-6-2-
2) oil inlet (8-6-2-2-1) passes through oil-through hole two successively one suitching type of oil-through hole with each oil cylinder (8-6-2-1) bottom
Connection;The lower end in the fuel-displaced portion has the oil outlet (8-6-2-2-6) penetrated in sliding slot two (8-6-1);The oil inlet passage
In be provided with a pair of of hollow channel boards (8-6-2-2-2) of symmetrical distribution, a pair of of hollow channel boards (8-6-2-2-2) extend through
Ground is fixed on the left side wall of oiling housing (8-6-2-2-0) on right side wall, and a pair of of hollow channel boards (8-6-2-2-2) are inner
Spaced apart formed falls oily channel between end;The middle part of the hollow channel boards (8-6-2-2-2) has horizontal concrete chute, is located at
It is slidably provided with to adjust the cunning for falling oily channel opening size in the horizontal concrete chute of the hollow channel boards (8-6-2-2-2) of side
Dynamic baffle (8-6-2-2-3);The external left and right sides of compartment (8-6-2-2-5) is each provided with a vibration unit, described to shake
Moving cell by be fixedly connected on oiling housing (8-6-2-2-0) lateral wall oscillating plate (8-6-2-2-8), be fixedly connected on and shake
Vibrating motor (8-6-2-2-7) on movable plate (8-6-2-2-8) and the vibrating head being fixedly connected on oscillating plate (8-6-2-2-8)
(8-6-2-2-9) is formed, and the vibrating head (8-6-2-2-9) extend into compartment (8-6- across oiling housing (8-6-2-2-0)
It is 2-2-5) internal;Compartment (8-6-2-2-5) lower part left end is additionally provided with roller bearing (8-6-2-2-4), roller bearing (8-6-2-2-4)
Rear and front end is rotatably connected on the front side wall and rear wall of oiling housing (8-6-2-2-0);Roller bearing (8-6-2-2-4)
One end is pierced by oiling housing (8-6-2-2-0) outside and is drivingly connected with decelerating motor;
The cutting gun nozzle (8-5) includes nozzle housing (8-5-1), and the nozzle housing (8-5-1) is internally provided with oxygen
Jet pipe (8-5-5) and more acetylene jet pipes (8-5-2) are provided with acetylene connecting tube (8-5- outside nozzle housing (8-5-1)
4), the nozzle housing (8-5-1) has superposed positive frustum section and the inversed taper platform section positioned at lower part, the top of positive frustum section
Portion is closed by top plate, and the lower end of positive frustum section is welded with the upper end of inversed taper platform section, and the bottom end of inversed taper platform section, which has, is communicated to spray
The flame export (8-5-6) of mouth shell (8-5-1) inner cavity;
The oxygen spray pipe (8-5-5) is fixed on the axial line in positive frustum section;It wears the upper end of oxygen spray pipe (8-5-5)
It is connect after going out the top plate at the top of positive frustum section with one end of oxygen flow valve (8-5-3), oxygen spray pipe (8-5-5) is in positive frustum
The connecting rod that the upper and lower ends of part in section are radially set each by more is fixedly connected with connection ring (8-5-7), positioned at just
The internal diameter of the connection ring (8-5-7) of frustum section big opening end side is more than the connection ring positioned at the small openend side of positive frustum section
The internal diameter of (8-5-7);Multiple acetylene jet pipes (8-5-2) are circumferentially set around oxygen spray pipe (8-5-5), acetylene jet pipe (8-5-
2) both ends are fixedly connected respectively with two connection rings (8-5-7);Superposed connection ring (8-5-7) has hollow lumen,
And its inner cavity by more multiple acetylene jet pipes (8-5-2) is interconnected;Oxygen spray pipe (8-5-5) and acetylene jet pipe (8-5-2)
Surface be equipped with the through-hole being largely connected with its inner cavity;
One end of the acetylene connecting tube (8-5-4) penetrates nozzle housing (8-5-1) inside and superposed connection ring (8-5-
7) it connects to through-lumen, the other end of acetylene connecting tube (8-5-4) is connect with acetylene gas pipe (8-3);The oxygen flow valve
The other end of (8-5-3) is connect with oxygen cylinder (8-4);
The synchronous motor (11-5), decelerating motor, horizontal drive motor (8-2), rotary electric machine (8-6-2-3), vibrating motor
(8-6-2-2-7), hoist engine (7) are connected each by conducting wire with controller (9).
2. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 1, which is characterized in that
Acetylene jet pipe (8-5-2) angle of inclination is 30 DEG C~60 DEG C.
3. according to claim 1 or 2 a kind of for handling the high-pressure steam pipe cutter device of carbon tetrachloride, feature exists
In the surface anti-skidding line of the idler wheel (11-8).
4. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 3, which is characterized in that
The quantity of the acetylene jet pipe (8-5-2) is no less than 10.
5. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 4, which is characterized in that
Each connection ring (8-5-7) is welded by circumferential four connecting rods being uniformly arranged on the inside of it with oxygen spray pipe (8-5-5).
6. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 5, which is characterized in that
The quantity of the oil cylinder (8-6-2-1) and partition board (8-6-2-5) is 6.
7. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 6, which is characterized in that
The material of the oil cylinder (8-6-2-1) and partition board (8-6-2-5) is stainless steel.
8. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 7, which is characterized in that
The acetylene connecting tube (8-5-4) is molded by high molecular material pressing mold, acetylene connecting tube (8-5-4) by following components by weight
Number proportioning composition:
323.7~548.0 parts of ultra-pure water, 115.1~157.8 parts of 2- methyl dodecyls aldehyde, 2- methoxyl group -3- methylpyrazines
118.4~227.9 parts, 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] methylamino] second sulphur
114.1~131.6 parts of acid, 117.0~174.5 parts of yeast rna, 4,4'- (1- methyl ethylidene) biphenols and chloromethyl
120.5~181.6 parts of the polymer of ethylene oxide and α-hydrogen-based-ω-hydroxyl poly- (oxidation -1,2- second diyl), Ruthenium nanometers of millimicros
122.1~177.3 parts of grain, poly- 115.1~157.2 parts of decanedioic acid propylene glycol ester, formaldehyde and 4- (1,1- dimethyl propyl) phenol,
117.8~157.1 parts of the polymer of xylenol and methylphenol, the polymer 117.5 of same (vertical structure) -1,3-butadiene
~140.2 parts, 106.6~142.6 parts of 5- methoxyl group -1H- indole -3-formaldehydes, 2- methyl -2- nitro-1,3-propylene glycols 105.9
~148.7 parts, 114.4~159.5 parts of formic acid, 124.1~168.9 parts of mandarin oil, mass concentration is 114ppm~381ppm's
Alpha-brominated 147.8~201.2 parts of -2- chlorobenzene acetic acids.
9. a kind of high-pressure steam pipe cutter device for being used to handle carbon tetrachloride according to claim 8, which is characterized in that
The manufacturing process of the acetylene connecting tube (8-5-4) is as follows:
1st step:In continuous stirred tank reactor, ultra-pure water and 2- methyl dodecyl aldehyde are added in, starts continuous stirred tank
Blender in formula reactor, setting speed are 116rpm~162rpm, start the conduction oil in continuous stirred tank reactor
Heater makes temperature rise to 131.7 DEG C~132.0 DEG C, adds in 2- methoxyl group -3- methylpyrazines and stirs evenly, is reacted
108.1~119.8 minutes, add in 2- [(methyl ester amino)-[2- nitros -5- (n- sulfopropyls)-phenylimino] first ammonia
Base] etherosulfuric acid, flow is passed through as 107.6m3/ min~148.6m3The xenon of/min 108.1~119.8 minutes;Later continuous
Yeast rna is added in stirred-tank reactor, the hotline heater being again started up in continuous stirred tank reactor,
Temperature is made to rise to 148.4 DEG C~181.9 DEG C, keeps the temperature 108.1~119.6 minutes, adds in 4,4'- (1- methyl ethylidene) biphenol
The polymer of (oxidation -1,2- second diyl) poly- with chloromethyloxirane and α-hydrogen-based-ω-hydroxyl, adjustment continuously stir autoclave
The pH value of solution is 4.0~8.5 in reactor, keeps the temperature 108.0~348.0 minutes;
2nd step:Ruthenium nanoparticles separately are taken, in power are ultrasonication under 6.48KW~11.92KW by Ruthenium nanoparticles
After 0.114~1.181 hour;Ruthenium nanoparticles are added in another continuous stirred tank reactor, it is dense to add in quality
It spends and disperses Ruthenium nanoparticles for the poly- decanedioic acid propylene glycol ester of 118ppm~348ppm, start in continuous stirred tank reactor
Hotline heater, make solution temperature between 41 DEG C~85 DEG C, start continuous stirred tank reactor in blender, and
With 4 × 102Rpm~8 × 102The speed stirring of rpm, adjustment pH value is between 4.6~8.6, insulated and stirred 114~181 minutes;
Stop reaction later and stand 6.48 × 10~11.92 × 10 minutes, remove impurity;Suspension is added in into formaldehyde and 4- (1,1- bis-
Methyl-propyl) phenol, xylenol and methylphenol polymer, adjustment pH value between 1.6~2.6, formed sediment
With ultrapure water elution, by centrifuge in rotating speed 4.497 × 103Rpm~9.909 × 103Solid content is obtained under rpm, 2.734
×102DEG C~3.868 × 102It is dry at a temperature of DEG C, 0.497 × 10 is crossed after grinding3~1.909 × 103Mesh sieves, spare;
3rd step:With Ruthenium nanoparticles after being handled in the polymer of (vertical structure) -1,3-butadiene and claim 9 between separately taking, mix
It is irradiated after closing uniformly using β reflected radiations, the energy of β reflected radiations irradiation is 105.9MeV~133.7MeV, dosage is
153.9kGy~193.7kGy, irradiation time are 117.9~142.7 minutes, obtain same (vertical structure) -1,3- fourths between character change
The polymer of diene and Ruthenium nanoparticles mixtures;With the polymer and Ruthenium nanometers of millimicros of (vertical structure) -1,3- butadiene by between
Grain mixture is placed in another continuous stirred tank reactor, starts the hotline heater in continuous stirred tank reactor,
116.4 DEG C~162.5 DEG C of set temperature, start continuous stirred tank reactor in blender, rotating speed for 108rpm~
503rpm, pH are adjusted between 4.1~8.9, are dehydrated 117.1~131.9 minutes, spare;
4th step:The polymer and Ruthenium nanometers of millimicros of the character that above-mentioned steps are obtained same (vertical structure) -1,3- butadiene between changing
Grain mixture is added in the 5- methoxyl group -1H- indole -3-formaldehydes that mass concentration is 118ppm~348ppm, and cocurrent adds to the 1st
In the continuous stirred tank reactor of step, flow acceleration is 253mL/min~981mL/min;Startup continuously stirs autoclave reaction
Mechanical stirrer, setting speed are 122rpm~162rpm;Stirring 4~8 minutes;Add 2- methyl -2- nitros -1,3- the third two
Alcohol starts the hotline heater in continuous stirred tank reactor, is warming up to 152.8 DEG C~189.2 DEG C, pH is adjusted to 4.8
Between~8.2, xenon ventilatory capacity is passed through as 107.189m3/ min~148.642m3/ min, heat preservation stand 142.7~172.0 points
Clock;Continuous stirred tank reactor blender is again started up, rotating speed is 117rpm~162rpm, adds in formic acid, and cause pH tune
It is whole between 4.8~8.2, heat preservation stands 141.1~181.8 minutes;
5th step:Start the blender in continuous stirred tank reactor, setting speed is 114rpm~181rpm, is started continuous
Hotline heater in stirred-tank reactor sets temperature in continuous stirred tank reactor as 1.714 × 102DEG C~
2.515×102DEG C, mandarin oil is added in, is reacted 108.4~119.9 minutes;Alpha-brominated -2- chlorobenzene acetic acids are added in later, are started and are connected
Hotline heater in continuous stirred-tank reactor, set temperature in continuous stirred tank reactor as 192.1 DEG C~
248.6 DEG C, pH is adjusted between 4.0~8.0, and pressure is 1.14MPa~1.15MPa, and the reaction time is 0.4~0.9 hour;It
After be depressurized to gauge pressure as 0MPa, be cooled to 108.4 DEG C~119.9 DEG C and discharge into molding press to get to acetylene connecting tube (8-5-
4)。
10. according to claim 9 a kind of for handling the high-pressure steam pipe cutter device of carbon tetrachloride, feature exists
In the grain size of the Ruthenium nanoparticles is 122 μm~132 μm.
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CN110328613A (en) * | 2019-07-15 | 2019-10-15 | 徐州腾睿智能装备有限公司 | A kind of PEIC anaerobic reactor reaction pipeline apparatus for examination and repair |
CN110328585A (en) * | 2019-07-15 | 2019-10-15 | 徐州筱翔知识产权服务有限公司 | One kind is for pipeline examination and repair system in carbon tetrachloride processing unit |
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CN110340776A (en) * | 2019-07-15 | 2019-10-18 | 徐州筱翔知识产权服务有限公司 | It can control pipe-line maintenance platform under a kind of Tunnel Engineering environment |
CN110344489A (en) * | 2019-07-15 | 2019-10-18 | 徐州筱翔知识产权服务有限公司 | A kind of urban pipe network pipeline repairing apparatus |
CN110340777A (en) * | 2019-07-15 | 2019-10-18 | 徐州绿源智能科技有限公司 | A kind of wisdom piping lane maintenance system with polishing and detection function |
CN111331584A (en) * | 2020-03-27 | 2020-06-26 | 厦门理工学院 | Robot system for complex curved surface machining |
CN111468957A (en) * | 2020-05-07 | 2020-07-31 | 卢秀丽 | Integrated synchronous processing device after aluminum alloy extrusion |
CN111673153A (en) * | 2020-06-05 | 2020-09-18 | 华创天元实业发展有限责任公司 | On-site sealing and pipe breaking equipment and method for steel-plastic composite pipeline |
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