CN108166157B - Moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base cloth and preparation method thereof - Google Patents
Moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base cloth and preparation method thereof Download PDFInfo
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- CN108166157B CN108166157B CN201711419662.2A CN201711419662A CN108166157B CN 108166157 B CN108166157 B CN 108166157B CN 201711419662 A CN201711419662 A CN 201711419662A CN 108166157 B CN108166157 B CN 108166157B
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/492—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/425—Cellulose series
- D04H1/4258—Regenerated cellulose series
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
Abstract
The invention discloses a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric and a preparation method thereof, which relate to the technical field of non-woven fabrics and comprise the following fibers in percentage by weight: 40-60% of sodium alginate viscose fiber and 40-60% of chitosan viscose fiber; the preparation method comprises the steps of preparing the sodium alginate viscose fiber and the chitosan viscose fiber, then respectively opening and carding, then crossly lapping, carrying out spunlace reinforcement on the lapped fiber nets, and drying to obtain the sodium alginate viscose fiber and the chitosan viscose fiber. The invention respectively adds sodium alginate and chitosan into viscose stock solution to spin functional viscose, and utilizes epoxy chloropropane to make sodium alginate, chitosan and viscose tightly combined, the prepared sodium alginate viscose fiber and chitosan viscose fiber have good air permeability and water retention and moisture absorption, and are bactericidal and bacteriostatic, then the non-woven fabric made by cross lapping and spunlace reinforcement is used as the substrate material of the mask, which is comfortable, skin-friendly, anti-inflammatory and bacteriostatic, and can clean skin, effectively protect skin and weaken the damage of cosmetics to skin.
Description
Technical Field
The invention relates to the technical field of non-woven fabrics, in particular to a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric and a preparation method thereof.
Background
Today, skin care, particularly facial skin care, has become a daily necessity for many beauty conscious individuals. Compared with the disadvantages of time and financial resources of professional beauty institutions, personal self-care has become the choice of most people, especially for urban people who are in tension and busy all day long. Among a variety of skin care products, facial masks are popular among many users because of their convenience and better beauty effects. The film-attached mask is prepared by making non-woven fabric or other film cloth with certain thickness into mask base cloth according with the size of face, and directly applying on face in combination with appropriate nutrient solution. The existing mask base cloth has common hygroscopicity, the amount of the loaded essence is small, and the comfort and skin-friendly performance is still required to be further improved.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric and the preparation method thereof, and the prepared mask base fabric absorbs moisture and holds water, is comfortable and skin-friendly, has the antibacterial and anti-inflammatory effects, can effectively protect the facial skin, and weakens the damage of cosmetics to the skin.
The invention provides a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric which is composed of the following fibers in percentage by weight: 40-60% of sodium alginate viscose fiber and 40-60% of chitosan viscose fiber.
The invention also provides a preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric, which comprises the following steps:
s1, preparing sodium alginate viscose fibers: dissolving sodium alginate in water, adjusting the pH value to 8-9, adding epoxy chloropropane, and heating for reaction to obtain a material A; adding the material A into viscose, stirring to obtain a material B, and performing wet spinning on the material B to obtain sodium alginate viscose;
s2, preparation of chitosan viscose fibers: adding chitosan into water, adjusting the pH value to 5-6, stirring for dissolving, adding epoxy chloropropane, and heating for reaction to obtain a material C; adjusting the pH value of the material C to 8-9, adding the material C into viscose, stirring and reacting to obtain a material D, and performing wet spinning on the material D to obtain chitosan viscose;
s3, preparing base cloth: respectively opening and carding the sodium alginate viscose fiber and the chitosan viscose fiber, then cross lapping, carrying out spunlace reinforcement on the lapped fiber nets, and drying to obtain the sodium alginate viscose fiber and the chitosan viscose fiber.
Preferably, in the step S1, sodium alginate is dissolved in water to prepare a 3-5% sodium alginate aqueous solution, the pH is adjusted to 8-9 by using a NaOH solution, epichlorohydrin which accounts for 3-7% of the weight of the sodium alginate is added into the aqueous solution, the temperature is raised to 70-80 ℃, the reaction is carried out for 2-3 hours with stirring, and the temperature is lowered to obtain a material A; adding the material A into the viscose, stirring and reacting for 2-3h to obtain a material B, and spinning the material B by a wet method to obtain the sodium alginate viscose fiber.
Preferably, the material A is added to the viscose in a proportion of 4-6% by weight of sodium alginate to the viscose.
Preferably, in the step S2, adding chitosan into water, adjusting the pH value to 5-6 with acetic acid, stirring and dissolving to prepare a 3-5% chitosan aqueous solution, adding epichlorohydrin into the aqueous solution, heating to 70-80 ℃, and stirring and reacting for 2-3 hours to obtain a material C; and (3) adjusting the pH value of the material C to 8-9 by using a sodium hydroxide solution, then adding the material C into the viscose, stirring and reacting for 1-2 hours to obtain a material D, and performing wet spinning on the material D to obtain the chitosan viscose fiber.
Preferably, the material a is added to the viscose in a proportion of chitosan in the range of 3-5% by weight of the viscose.
Preferably, in S3, the paving density of the fiber net is 20-30g/m2。
Has the advantages that: the invention adds sodium alginate and chitosan into the viscose stoste respectively to spin functional viscose, and uses epichlorohydrin to make the sodium alginate and chitosan combine with viscose tightly; wherein, the epichlorohydrin molecule contains high-activity chloride ion which is easy to be substituted and epoxy structure which is easy to open ring and polymerize, and the structure is used for modifying sodium alginate and chitosan; the molecular chain of the sodium alginate is also provided with abundant hydroxyl groups, and the sodium alginate can generate crosslinking reaction with epoxy chloropropane under the alkaline condition and then is combined with viscose, so that the problem of unstable viscosity of the ammonium alginate can be solved, and the viscosity stability, heat resistance and spinnability of the ammonium alginate are improved; the chitosan molecular chain contains abundant amino and hydroxyl, and can generate crosslinking reaction with epoxy chloropropane under an acidic condition and then be combined with viscose, so that the problems of small molecular weight, weak binding force with viscose fiber and the like of the chitosan can be solved; sodium alginate and chitosan are firmly combined with viscose through covalent bonds through epichlorohydrin respectively, so that the performance is stable; sodium alginate and chitosan both contain a large number of hydrophilic groups such as hydroxyl, amino and the like, have good hydrophilicity, hygroscopicity and biocompatibility, and have antibacterial, anti-inflammatory and itching relieving effects, sodium alginate fibers are cellulose fibers with negative charges and can promote healing of skin inflammation caused by infection or anaphylactic reaction, chitosan fibers are only animal cellulose fibers with positive charges in all fibers, have good bacteriostatic action on gram-positive bacteria, can relieve pain, fade scars and chelate heavy metal ions, sodium alginate and chitosan are respectively mixed with viscose for wet spinning, a plurality of microporous structures are formed among molecules, the prepared sodium alginate viscose fibers and chitosan viscose fibers have good air permeability, water retention and hygroscopicity, and good bactericidal and bacteriostatic effects on gram-positive bacteria and gram-negative bacteria, and the non-woven fabric prepared by cross-lapping and spunlacing the sodium alginate viscose fibers and the chitosan viscose fibers for spunlace reinforcement is used for a mask substrate material, the mask is comfortable and skin-friendly, can load more essence liquid by virtue of high hygroscopicity and air permeability, promotes facial skin to absorb more nutrient components, forms a complex with heavy metal ions of the skin, and has the effects of diminishing inflammation and inhibiting bacteria, so that the skin is cleaned, the skin is effectively protected, the damage of cosmetics to the skin is weakened, and the mask is particularly suitable for sensitive skin and can be used as a medical mask substrate.
Detailed Description
The technical solution of the present invention will be described in detail below with reference to specific examples.
Example 1
The invention provides a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric which is composed of the following fibers in percentage by weight: 40% of sodium alginate viscose fiber and 60% of chitosan viscose fiber.
The invention also provides a preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric, which comprises the following steps:
s1, preparing sodium alginate viscose fibers: dissolving sodium alginate in water, adjusting the pH value to 8, adding epoxy chloropropane, and heating for reaction to obtain a material A; adding the material A into viscose, stirring to obtain a material B, and performing wet spinning on the material B to obtain sodium alginate viscose;
s2, preparation of chitosan viscose fibers: adding chitosan into water, adjusting the pH value to 5, stirring and dissolving, adding epoxy chloropropane, and heating for reaction to obtain a material C; adjusting the pH value of the material C to 8, then adding the material C into viscose, stirring and reacting to obtain a material D, and performing wet spinning on the material D to obtain chitosan viscose;
s3, preparing base cloth: respectively opening and carding the sodium alginate viscose fiber and the chitosan viscose fiber, then cross lapping, carrying out spunlace reinforcement on the lapped fiber nets, and drying to obtain the sodium alginate viscose fiber and the chitosan viscose fiber.
Example 2
The invention provides a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric which is composed of the following fibers in percentage by weight: 50% of sodium alginate viscose fiber and 50% of chitosan viscose fiber.
The invention also provides a preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric, which comprises the following steps:
s1, preparing sodium alginate viscose fibers: dissolving sodium alginate in water, preparing 3% sodium alginate aqueous solution, adjusting pH to 8 with NaOH solution, adding epichlorohydrin accounting for 3% of the weight of the sodium alginate, heating to 70 ℃, stirring for reaction for 2h, and cooling to obtain material A; adding the material A into the viscose according to the weight ratio of the sodium alginate to the viscose of 4 percent, stirring and reacting for 2 hours to obtain a material B, and spinning the material B by a wet method to obtain sodium alginate viscose;
s2, preparation of chitosan viscose fibers: adding chitosan into water, adjusting the pH value to 5 by using acetic acid, stirring and dissolving to prepare a 3% chitosan water solution, adding epoxy chloropropane into the chitosan water solution, heating to 70 ℃, and stirring for reacting for 2 hours to obtain a material C; adjusting the pH value of the material C to 8 by using a sodium hydroxide solution, adding the material A into the viscose according to the proportion that the weight of chitosan accounts for 3% of the viscose, stirring and reacting for 1h to obtain a material D, and spinning the material D by adopting a wet method to obtain chitosan viscose;
s3, preparing base cloth: respectively opening and carding the sodium alginate viscose fiber and the chitosan viscose fiber, and then cross-lapping with the lapping density of 20g/m2And carrying out spunlace reinforcement on the laid fiber net, and drying to obtain the fiber net.
Example 3
The invention provides a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric which is composed of the following fibers in percentage by weight: 55% of sodium alginate viscose fiber and 45% of chitosan viscose fiber.
The invention also provides a preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric, which comprises the following steps:
s1, preparing sodium alginate viscose fibers: dissolving sodium alginate in water, preparing 4% sodium alginate aqueous solution, adjusting pH to 8.5 with NaOH solution, adding epichlorohydrin accounting for 5% of sodium alginate weight, heating to 75 deg.C, stirring for reaction for 2.5h, and cooling to obtain material A; adding the material A into the viscose according to the weight ratio of the sodium alginate accounting for 5% of the viscose, stirring and reacting for 2.5 hours to obtain a material B, and performing wet spinning on the material B to obtain sodium alginate viscose;
s2, preparation of chitosan viscose fibers: adding chitosan into water, adjusting the pH value to 5.5 by using acetic acid, stirring and dissolving to prepare a 4% chitosan aqueous solution, adding epoxy chloropropane into the chitosan aqueous solution, heating to 75 ℃, and stirring for reacting for 2.5 hours to obtain a material C; adjusting the pH value of the material C to 8.5 by using a sodium hydroxide solution, then adding the material A into the viscose according to the proportion that the weight of chitosan accounts for 4% of the viscose, stirring and reacting for 1.5h to obtain a material D, and performing wet spinning on the material D to obtain chitosan viscose;
s3, preparing base cloth: respectively opening and carding the sodium alginate viscose fiber and the chitosan viscose fiber, and then cross-lapping, wherein the lapping density is 25g/m2And carrying out spunlace reinforcement on the laid fiber net, and drying to obtain the fiber net.
Example 4
The invention provides a moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric which is composed of the following fibers in percentage by weight: 60% of sodium alginate viscose fiber and 40% of chitosan viscose fiber.
The invention also provides a preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric, which comprises the following steps:
s1, preparing sodium alginate viscose fibers: dissolving sodium alginate in water, preparing 5% sodium alginate aqueous solution, adjusting pH to 9 with NaOH solution, adding epichlorohydrin accounting for 7% of the weight of sodium alginate, heating to 80 ℃, stirring for reaction for 3h, and cooling to obtain material A; adding the material A into the viscose according to the weight ratio of the sodium alginate to 6% of the viscose, stirring and reacting for 3 hours to obtain a material B, and spinning the material B by a wet method to obtain sodium alginate viscose;
s2, preparation of chitosan viscose fibers: adding chitosan into water, adjusting the pH value to 6 by using acetic acid, stirring and dissolving to prepare a 5% chitosan aqueous solution, adding epoxy chloropropane into the chitosan aqueous solution, heating to 80 ℃, and stirring for reacting for 3 hours to obtain a material C; adjusting the pH value of the material C to 9 by using a sodium hydroxide solution, adding the material A into the viscose according to the proportion that the weight of chitosan accounts for 5% of the weight of the viscose, stirring and reacting for 2 hours to obtain a material D, and spinning the material D by adopting a wet method to obtain chitosan viscose;
s3, preparing base cloth: respectively opening and carding the sodium alginate viscose fiber and the chitosan viscose fiber, and then cross-lapping with the lapping density of 30g/m2And carrying out spunlace reinforcement on the laid fiber net, and drying to obtain the fiber net.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (6)
1. The moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base cloth is characterized by comprising the following fibers in percentage by weight: 40-60% of sodium alginate viscose fiber and 40-60% of chitosan viscose fiber;
the preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric comprises the following steps:
s1, preparing sodium alginate viscose fibers: dissolving sodium alginate in water, adjusting the pH value to 8-9, adding epoxy chloropropane, and heating for reaction to obtain a material A; adding the material A into viscose, stirring to obtain a material B, and performing wet spinning on the material B to obtain sodium alginate viscose;
s2, preparation of chitosan viscose fibers: adding chitosan into water, adjusting the pH value to 5-6, stirring for dissolving, adding epoxy chloropropane, and heating for reaction to obtain a material C; adjusting the pH value of the material C to 8-9, adding the material C into viscose, stirring and reacting to obtain a material D, and performing wet spinning on the material D to obtain chitosan viscose;
s3, preparing base cloth: respectively opening and carding the sodium alginate viscose fiber and the chitosan viscose fiber, then cross lapping, carrying out spunlace reinforcement on the lapped fiber nets, and drying to obtain the sodium alginate viscose fiber and the chitosan viscose fiber.
2. The preparation method of the moisture-absorbing and bacteriostatic spunlace nonwoven fabric beauty mask base fabric according to claim 1, wherein in S1, sodium alginate is dissolved in water to prepare a 3-5% sodium alginate aqueous solution, the pH is adjusted to 8-9 by using a NaOH solution, epichlorohydrin accounting for 3-7% of the weight of sodium alginate is added into the aqueous solution, the temperature is raised to 70-80 ℃, the mixture is stirred and reacted for 2-3 hours, and the temperature is reduced to obtain a material A; adding the material A into the viscose, stirring and reacting for 2-3h to obtain a material B, and spinning the material B by a wet method to obtain the sodium alginate viscose fiber.
3. The preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric according to claim 2, wherein the material A is added into the viscose according to the proportion that the weight of sodium alginate accounts for 4-6% of the viscose.
4. The preparation method of the moisture-absorbing and bacteriostatic spunlace nonwoven fabric beauty mask base fabric according to claim 1, wherein in S2, chitosan is added into water, acetic acid is used for adjusting the pH value to 5-6, the mixture is stirred and dissolved to prepare a 3-5% chitosan aqueous solution, epichlorohydrin is added into the chitosan aqueous solution, the temperature is raised to 70-80 ℃, and the mixture is stirred and reacted for 2-3 hours to obtain a material C; and (3) adjusting the pH value of the material C to 8-9 by using a sodium hydroxide solution, then adding the material C into the viscose, stirring and reacting for 1-2 hours to obtain a material D, and performing wet spinning on the material D to obtain the chitosan viscose fiber.
5. The preparation method of the moisture-absorbing and bacteriostatic spunlace non-woven fabric beauty mask base fabric as claimed in claim 4, wherein the material C is added into the viscose according to the proportion that the weight of chitosan accounts for 3-5% of the viscose.
6. The method for preparing the moisture-absorbing and bacteriostatic spunlace nonwoven fabric beauty mask base cloth according to claim 1, wherein in the step S3, the paving density of the fiber web is 20-30g/m2。
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| CN102304783A (en) * | 2011-07-07 | 2012-01-04 | 狄友波 | Preparation method of antibacterial anti-flaming protein viscose fiber |
| KR20130125901A (en) * | 2012-05-10 | 2013-11-20 | 한국생산기술연구원 | Mask sheet of nonwoven containing kenaf |
| CN103938368A (en) * | 2014-05-07 | 2014-07-23 | 东华大学 | Spunlaced non-woven material with one-way water guide function and preparing method and application thereof |
| CN204875072U (en) * | 2014-11-20 | 2015-12-16 | 周新民 | Double -deck water thorn facial mask non -woven fabrics |
| CN105908280A (en) * | 2016-07-10 | 2016-08-31 | 胡稳成 | Antibacterial viscose and preparation method thereof |
| CN106521707A (en) * | 2016-11-25 | 2017-03-22 | 陕西品达石化有限公司 | Preparation method of epichlorohydrin crosslinked sodium alginate fiber |
| CN106884323A (en) * | 2017-02-26 | 2017-06-23 | 浙江峰赫纺织有限公司 | A kind of preparation method of chitosan anti-bacteria viscose rayon |
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