CN106724473A - Silk quilt containing anion and preparation method thereof - Google Patents
Silk quilt containing anion and preparation method thereof Download PDFInfo
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- CN106724473A CN106724473A CN201611245092.5A CN201611245092A CN106724473A CN 106724473 A CN106724473 A CN 106724473A CN 201611245092 A CN201611245092 A CN 201611245092A CN 106724473 A CN106724473 A CN 106724473A
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- anion
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- silk
- coupling agent
- silk quilt
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G9/00—Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/06—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
- D01F2/08—Composition of the spinning solution or the bath
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention relates to a kind of silk quilt containing anion and preparation method thereof, the silk quilt containing anion includes core filler, and the core filler is made up of the component of following percentage by weight：100% pure natural silk 45 50% and anion viscose fibre 50 55%；It is long-term in the silk quilt that this method is made to preserve the concentration with anion releasing at more than 5000 per cubic centimeter；Human body temperature and human body friction can be well utilized simultaneously, increases anion burst size in silk, mulberry silk is preserved anion for a long time, so that negative ion concentration remains at a concentration higher, have broad application prospects.
Description
Technical field
The invention belongs to bedding technical field, and in particular to a kind of silk quilt containing anion and preparation method thereof.
Background technology
In recent years, with the continuous improvement of people's living standard, operating pressure is increasing, to anion product acceptance
More and more higher, a series of anion product has wide market.Anion can not only facilitate human body to synthesize and storage dimension life
Element, strengthens the physiological activity with human activin, therefore it is otherwise known as " air vitamin ", it is believed that it is as the vitamin one of food
Sample, has highly important influence to the vital movement of human body and other biological.
Silk is most light most soft most thin natural fiber in nature, can easily be restored to the original state after cancelling external force, and the inner tube of a tyre is not
Molding, not stuffy, not purse up, homogeneous soft forever can be exempted to turn over and use；Silk quilt, with novel fine footpath between fields structure, makes steam freedom
Circulation；Plus silk distinctive ventilative, water vapour permeability in itself, it is perceived silk and more slides, feels well not warm, it is warm but not dry；Silkworm
Silk is mainly made up of animal protein, rich in amino acid necessary to 18 kinds of human bodies, can promote Skin Cell vigor, and anti-blood vessel is hard
Change, long-term use can anti-skin senescence, have special antipruritic effect to some skin diseases, to arthritis, scapulohumeral periarthritis, asthma has
Certain health-care effect；Have " skin of human body second ", the good reputation of " fiber queen ".
Also have many researchs currently for existing quilt fabric, all exist hydrofuge poor air permeability, texture it is not soft, protect
The shortcomings of warm effect difference, especially in damp and hot summer, bacterium is extremely easily produced, exerted an adverse impact for human body.
The content of the invention
For defect present in prior art, the invention provides silk quilt containing anion and preparation method thereof, should
Product prepared by method has the advantages that slim and graceful softness, hydrofuge good permeability, comfortably warming, and the effect with antibacterial.
To achieve these goals, the technical solution adopted by the present invention is as follows：
The invention provides a kind of silk quilt containing anion, including core filler, the core filler is by following weight
The component of percentage is made：100% pure natural silk 45-50% and anion viscose fibre 50-55%；
Contain 0.5-1.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is ceramic powders weight
0.5-1.5%；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 20-40%, silica 20-30%, titanium dioxide
40-50%；
Coupling agent is made up of following weight percent composition：It is isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 20-30%, hard
Glycerol 20-40%, glycerin monostearate 30-50%.
According to the above-mentioned silk quilt containing anion, the anion viscose fibre is made up of following step：
（1）, zirconium dioxide, silica and titanium dioxide mixed, it is sintered after be crushed to average grain diameter for 0.2-0.8 μm
Ceramic powders；
（2）, coupling agent mixed with the ceramic powders, obtain modified ceramic powder；
（3）, by the modified ceramic powder and viscose glue blending, extrusion, section are obtained anion rayon section；
（4）, by anion rayon section heating melting, extruding, spinneret shaping, you can the anion rayon is obtained fine
Dimension.
According to the preparation method of the above-mentioned silk quilt containing anion, comprise the following steps：
（1）, 100% pure natural silk and anion viscose fibre is well mixed, add dispersant, binding agent, softening agent to carry out
Stirring, dries treatment；
（2）, will be by step（1）The fiber for the treatment of is processed through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting
To spun yarn；
（3）, using on plain weave, two, once twill or cassimere twill are weaved；
（4）, add 3% detergent and 2% softening agent to carry out washing process to fabric, water temperature is controlled at 40-45 DEG C, washing
10-15min；
（5）, add anti UV finishing agent, mosquito repellent finishing agent dipping adjustment pH value to 5-7, be warmed up to 80 DEG C, then impregnate 50 points
Clock, is obtained blend fibre finished product；
（6）, the finished product of blend fibre is made core filler by scutching cotton, carding process, so as to obtain the silkworm containing anion
Silk quilt.
According to the preparation method of the above-mentioned silk quilt containing anion, the anti UV finishing agent is by following percentage by weight
Component be made：Zinc oxide 20-30%, titanium dioxide 20-40% and polyester master particle 20-50%.
According to the preparation method of the above-mentioned silk quilt containing anion, the mosquito repellent finishing agent is N- diethylbenzene acetyl
Amine.
According to the preparation method of the above-mentioned silk quilt containing anion, the anti UV finishing agent is by following percentage by weight
Component be made：Zinc oxide 30%, titanium dioxide 40% and polyester master particle 30%.
Compared with prior art, the advantage of the invention is that：
1. due to adding the anti UV finishing agent being mixed by zinc oxide, titanium dioxide and polyester master particle in the present invention, can
To improve the ability and ultraviolet resistance of product, while using 100% pure natural silk so that product has slim and graceful soft, hydrofuge saturating
Gas, it is comfortable warming the advantages of；Anion viscose fibre is added, cell permeability can be increased, increase oxygen absorbed, improve lung work(
Can, adjust blood pH, make blood smooth, with stable nerve, improve the health care of sleep, anti-inflammatory analgetic the effects such as；Add mosquito repellent
Finishing agent, can effectively reduce biting for mosquito, reduce the worry that mosquito gives people to bring in summer.
2. in the silk quilt that this method is made it is long-term preserve and anion releasing concentration 5000 per cubic centimeter with
On；Can be very good, using human body temperature and human body friction, to increase anion burst size in silk simultaneously, enable mulberry silk long
Phase preserves anion, so that negative ion concentration remains at a concentration higher, has broad application prospects.
Specific embodiment
Following examples are that detailed specific description is carried out to present invention, but present disclosure is not limited such as
This.
Embodiment 1
A kind of silk quilt containing anion, including core filler, the core filler by following percentage by weight component
It is made：100% pure natural silk 45-50% and anion viscose fibre 50-55%；
Contain 0.5-1.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is ceramic powders weight
0.5-1.5%；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 20-40%, silica 20-30%, titanium dioxide
40-50%；
Coupling agent is made up of following weight percent composition：It is isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 20-30%, hard
Glycerol 20-40%, glycerin monostearate 30-50%.
The anion viscose fibre is made up of following step：
（1）, zirconium dioxide, silica and titanium dioxide mixed, it is sintered after be crushed to average grain diameter for 0.2-0.8 μm
Ceramic powders；
（2）, coupling agent mixed with the ceramic powders, obtain modified ceramic powder；
（3）, by the modified ceramic powder and viscose glue blending, extrusion, section are obtained anion rayon section；
（4）, by anion rayon section heating melting, extruding, spinneret shaping, you can the anion rayon is obtained fine
Dimension.
The preparation method of the above-mentioned silk quilt containing anion, comprises the following steps：
（1）, 100% pure natural silk and anion viscose fibre is well mixed, add dispersant, binding agent, softening agent to carry out
Stirring, dries treatment；
（2）, will be by step（1）The fiber for the treatment of is processed through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting
To spun yarn；
（3）, using on plain weave, two, once twill or cassimere twill are weaved；
（4）, add 3% detergent and 2% softening agent to carry out washing process to fabric, water temperature is controlled at 40-45 DEG C, washing
10-15min；
（5）, add anti UV finishing agent, mosquito repellent finishing agent dipping adjustment pH value to 5-7, be warmed up to 80 DEG C, then impregnate 50 points
Clock, is obtained blend fibre finished product；The anti UV finishing agent is made up of the component of following percentage by weight：Zinc oxide 20-30%,
Titanium dioxide 20-40% and polyester master particle 20-50%；The mosquito repellent finishing agent is N- diethylbenzene acetamides；
（6）, the finished product of blend fibre is made core filler by scutching cotton, carding process, so as to obtain the silkworm containing anion
Silk quilt.
Embodiment 2
A kind of silk quilt containing anion, including core filler, the core filler by following percentage by weight component
It is made：100% pure natural silk 45% and anion viscose fibre 55%；
Contain 1.0wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.0% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 30%, silica 25%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 25%, glycerin monostearate 50%.
The anion viscose fibre is made up of following step：
（1）, zirconium dioxide, silica and titanium dioxide mixed, it is sintered after be crushed to average grain diameter for 0.2-0.8 μm
Ceramic powders；
（2）, coupling agent mixed with the ceramic powders, obtain modified ceramic powder；
（3）, by the modified ceramic powder and viscose glue blending, extrusion, section are obtained anion rayon section；
（4）, by anion rayon section heating melting, extruding, spinneret shaping, you can the anion rayon is obtained fine
Dimension.
The preparation method of the above-mentioned silk quilt containing anion, comprises the following steps：
（1）, 100% pure natural silk and anion viscose fibre is well mixed, add dispersant, binding agent, softening agent to carry out
Stirring, dries treatment；
（2）, will be by step（1）The fiber for the treatment of is processed through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting
To spun yarn；
（3）, using on plain weave, two, once twill or cassimere twill are weaved；
（4）, add 3% detergent and 2% softening agent to carry out washing process to fabric, water temperature is controlled at 45 DEG C, washing
15min；
（5）, add anti UV finishing agent, mosquito repellent finishing agent dipping adjustment pH value to 6, be warmed up to 80 DEG C, then impregnate 50 minutes,
Blend fibre finished product is obtained；The anti UV finishing agent is made up of the component of following percentage by weight：Zinc oxide 30%, titanium dioxide
Titanium 40% and polyester master particle 30%；The mosquito repellent finishing agent is N- diethylbenzene acetamides；
（6）, the finished product of blend fibre is made core filler by scutching cotton, carding process, so as to obtain the silkworm containing anion
Silk quilt.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5300/cubic centimetre.
Embodiment 3
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 46% and anion viscose fibre 54%；
Contain 0.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 20%, silica 30%, titanium dioxide 50%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 40%, glycerin monostearate 35%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5240/cubic centimetre.
Embodiment 4
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 47% and anion viscose fibre 53%；
Contain 0.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 30%, silica 30%, titanium dioxide 40%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 30%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5120/cubic centimetre.
Embodiment 5
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 47% and anion viscose fibre 53%；
Contain 1.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 20%, silica 30%, titanium dioxide 50%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 25%, glycerin monostearate 50%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5300/cubic centimetre.
Embodiment 6
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 45% and anion viscose fibre 55%；
Contain 0.8wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.9% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 28%, silica 22%, titanium dioxide 50%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 25%, glycerin monostearate 45%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5380/cubic centimetre.
Embodiment 7
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 46.5% and anion viscose fibre 53.5%；
Contain 1.2wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 30%, silica 25%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 28%, stearic acid
Glyceride 32%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5140/cubic centimetre.
Embodiment 8
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 48.5% and anion viscose fibre 51.5%；
Contain 0.6wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.4% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 35%, silica 25%, titanium dioxide 40%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 35%, glycerin monostearate 35%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5180/cubic centimetre.
Embodiment 9
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 49.5% and anion viscose fibre 50.5%；
Contain 0.8wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 35%, silica 24%, titanium dioxide 41%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 35%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5340/cubic centimetre.
Embodiment 10
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 47.5% and anion viscose fibre 52.5%；
Contain 0.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 35%, silica 20%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 30%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5190/cubic centimetre.
Embodiment 11
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 50% and anion viscose fibre 50%；
Contain 0.7wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.6% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 40%, silica 20%, titanium dioxide 40%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 30%, glycerin monostearate 45%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5350/cubic centimetre.
Embodiment 12
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 52.2% and anion viscose fibre 47.8%；
Contain 0.8wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.2% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 25%, silica 20%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 26%, stearic acid
Glyceride 38%, glycerin monostearate 36%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5470/cubic centimetre.
Embodiment 13
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 46.5% and anion viscose fibre 53.5%；
Contain 0.8wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.9% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 28%, silica 22%, titanium dioxide 50%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 25%, glycerin monostearate 45%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5350/cubic centimetre.
Embodiment 14
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 45.5% and anion viscose fibre 54.5%；
Contain 1.2wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 30%, silica 25%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 28%, stearic acid
Glyceride 32%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5240/cubic centimetre.
Embodiment 15
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 49.5% and anion viscose fibre 50.5%；
Contain 0.6wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.4% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 35%, silica 25%, titanium dioxide 40%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 35%, glycerin monostearate 35%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5270/cubic centimetre.
Embodiment 16
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 56.5% and anion viscose fibre 53.5%；
Contain 0.8wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 35%, silica 24%, titanium dioxide 41%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 35%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5120/cubic centimetre.
Embodiment 17
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 48.5% and anion viscose fibre 51.5%；
Contain 0.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.5% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 35%, silica 20%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 30%, stearic acid
Glyceride 30%, glycerin monostearate 40%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5190/cubic centimetre.
Embodiment 18
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 50.5% and anion viscose fibre 49.5%；
Contain 0.7wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 0.6% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 40%, silica 20%, titanium dioxide 40%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 25%, stearic acid
Glyceride 30%, glycerin monostearate 45%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5450/cubic centimetre.
Embodiment 19
The present embodiment part same as Example 2 is no longer repeated, and difference is：The core filler is by following weight hundred
The component of ratio is divided to be made：100% pure natural silk 54.2% and anion viscose fibre 45.8%；
Contain 0.8wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is the 1.2% of ceramic powders weight；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 25%, silica 20%, titanium dioxide 45%；
Coupling agent is made up of following weight percent composition：Isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 26%, stearic acid
Glyceride 38%, glycerin monostearate 36%.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention
5370/cubic centimetre.
Above-described is only the preferred embodiment of the present invention, it is noted that for a person skilled in the art,
Under the premise of general idea of the present invention is not departed from, some changes and improvements can also be made, these should also be considered as of the invention
Protection domain.
Claims (6)
1. the silk quilt containing anion, including core filler, it is characterised in that the core filler is by following weight percent
The component of ratio is made：100% pure natural silk 45-50% and anion viscose fibre 50-55%；
Contain 0.5-1.5wt% ceramic powders and coupling agent in anion viscose fibre, coupling agent is ceramic powders weight
0.5-1.5%；
Ceramic powders are made up of following weight percent composition：Zirconium dioxide 20-40%, silica 20-30%, titanium dioxide
40-50%；
Coupling agent is made up of following weight percent composition：It is isopropyl three (dioctyl phosphoric acid acyloxy) titanate esters 20-30%, hard
Glycerol 20-40%, glycerin monostearate 30-50%.
2. the silk quilt containing anion according to claim 1, it is characterised in that：The anion viscose fibre is by following
Step is made：
（1）, zirconium dioxide, silica and titanium dioxide mixed, it is sintered after be crushed to average grain diameter for 0.2-0.8 μm
Ceramic powders；
（2）, coupling agent mixed with the ceramic powders, obtain modified ceramic powder；
（3）, by the modified ceramic powder and viscose glue blending, extrusion, section are obtained anion rayon section；
（4）, by anion rayon section heating melting, extruding, spinneret shaping, you can the anion rayon is obtained fine
Dimension.
3. the preparation method of the silk quilt containing anion according to claim 1, it is characterised in that comprise the following steps：
（1）, 100% pure natural silk and anion viscose fibre is well mixed, add dispersant, binding agent, softening agent to carry out
Stirring, dries treatment；
（2）, will be by step（1）The fiber for the treatment of is processed through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting
To spun yarn；
（3）, using on plain weave, two, once twill or cassimere twill are weaved；
（4）, add 3% detergent and 2% softening agent to carry out washing process to fabric, water temperature is controlled at 40-45 DEG C, washing
10-15min；
（5）, add anti UV finishing agent, mosquito repellent finishing agent dipping adjustment pH value to 5-7, be warmed up to 80 DEG C, then impregnate 50 points
Clock, is obtained blend fibre finished product；
（6）, the finished product of blend fibre is made core filler by scutching cotton, carding process, so as to obtain the silkworm containing anion
Silk quilt.
4. the preparation method of the silk quilt containing anion according to claim 3, it is characterised in that：The anti UV finishing
Agent is made up of the component of following percentage by weight：Zinc oxide 20-30%, titanium dioxide 20-40% and polyester master particle 20-50%.
5. the preparation method of the silk quilt containing anion according to claim 3, it is characterised in that：The mosquito repellent finishing agent
It is N- diethylbenzene acetamides.
6. the preparation method of the silk quilt containing anion according to claim 4, it is characterised in that：The anti UV finishing
Agent is made up of the component of following percentage by weight：Zinc oxide 30%, titanium dioxide 40% and polyester master particle 30%.
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| WO2021206113A1 (en) * | 2020-04-10 | 2021-10-14 | 竹本油脂株式会社 | Viscose rayon non-woven fabric treatment agent, aqueous solution of viscose rayon non-woven fabric treatment agent, viscose rayon, and method for manufacturing viscose rayon for non-woven fabrics |
| CN114555879A (en) * | 2020-04-10 | 2022-05-27 | 竹本油脂株式会社 | Treating agent for viscose rayon, aqueous solution of treating agent for viscose rayon, and method for producing viscose rayon |
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