CN105648652A - High-elasticity silk complex fiber thermal cotton - Google Patents

High-elasticity silk complex fiber thermal cotton Download PDF

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Publication number
CN105648652A
CN105648652A CN201610011135.7A CN201610011135A CN105648652A CN 105648652 A CN105648652 A CN 105648652A CN 201610011135 A CN201610011135 A CN 201610011135A CN 105648652 A CN105648652 A CN 105648652A
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China
Prior art keywords
parts
composite fiber
high resiliency
fiber insulation
suspension
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CN201610011135.7A
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Inventor
洪义锋
孙亚军
姚文稳
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Fujian Jinjiang Hengfeng Polyester Wadding Weaving Co Ltd
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Fujian Jinjiang Hengfeng Polyester Wadding Weaving Co Ltd
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Priority to CN201610011135.7A priority Critical patent/CN105648652A/en
Publication of CN105648652A publication Critical patent/CN105648652A/en
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    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
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Abstract

The invention discloses high-elasticity silk complex fiber thermal cotton. The high-elasticity silk complex fiber thermal cotton is prepared from 10-30 parts of mulberry silk, 10-15 parts of polyethylene fiber, 12-20 parts of polytetrafluoroethylene fiber, 5-9 parts of artificial cotton, 10-14 parts of hollow polyester fiber, 2-5 parts of glue spraying emulsion, 3-12 parts of bamboo fiber, 2-3 parts of nano calcium carbonate, 10-25 parts of nanometer titania turbid liquid, 6-10 parts of graphene sol, 2-4 parts of nanometer bamboo charcoal powder and 2-5 parts of dispersing agent. By adopting bamboo fiber, hollow polyester fiber and other effective constituents, the strength, air permeability and thermal insulation and moisture absorption functions of silk are improved.

Description

A kind of high resiliency silk composite fiber insulation cotton
Technical field
The invention belongs to textile material technical field, be specifically related to a kind of high resiliency silk composite fiber insulation cotton.
Background technology
Silkworm silk is matured silkworm secreted silk liquid concretionary continuous fiber when cocooing, also referred to as natural silk, it is the lightest the thinnest the most soft natural fiber in nature, is mainly made up of animal proteinum, rich in aminoacid necessary to 18 kinds of human bodies, can promote Skin Cell vigor, anti-sclerosis of blood vessels, life-time service can anti-skin aging, some dermatosis there is special antipruritic effect, to arthritis, scapulohumeral periarthritis, asthma has certain health-care effect. Have the good reputation of " human body the second skin ", " fiber queen ". Elongated due to silkworm silk light weight, fabric sheen is good, comfortable and easy to wear, and feel is smooth plentiful, poor heat conductivity, and moisture absorption is breathed freely, and determines the health care that silkworm silk is good, is widely used in industry, beauty treatment and medicine and other fields. Prior art use natural silk there is many defects: one, use cost is too high; Two, make moist because of the humidity of environment, preserve the improper raw demodicid mite that easily goes mouldy; Three, intensity is poor, conglomeration, reduces warmth retention property, affects attractive in appearance; Four, frequent static electrification, brings inconvenience etc.
Summary of the invention
It is an object of the invention to provide a kind of high resiliency silk composite fiber insulation cotton, adopt the effective ingredient such as bamboo fibre, hollow terylene, add the intensity of silkworm silk, breathability and warming moisture-absorbing function.
A kind of high resiliency silk composite fiber insulation cotton, its formula is as follows: mulberry silk 10-30 part, polyethylene fibre 10-15 part, polytetrafluoroethylene fibre 12-20 part, synthetic cotton 5-9 part, hollow terylene 10-14 part, glue spraying emulsion 2-5 part, bamboo fibre 3-12 part, nano-calcium carbonate 2-3 part, nano titanium oxide suspension 10-25 part, graphene sol 6-10 part, nano bamboo powdered carbon 2-4 part, dispersant 2-5 part.
The titanium dioxide particle diameter that described nano titanium oxide suspension adopts is 10-20nm.
The preparation method of described nano titanium oxide suspension is as follows: be stirred vigorously by dehydrated alcohol, adds nano titanium oxide obtained solution A, by water, ethanol, acetic acid Homogeneous phase mixing, obtained solution B; When being stirred vigorously, solution A is added drop-wise in solution B, is added dropwise to complete stopping stirring.
The preparation method of described graphene sol is that graphite oxide grinds to form the fine powder that particle diameter is 1-40 micron, and it is configured to, with solvent, the suspension that concentration is 0.5-6mg/ml, after supersound process 10-120 minute, remove the unstable impurity in suspension, obtain graphene oxide colloidal sol.
Described dispersant adopts the one in ethylene-acrylic acid copolymer, ethylene-vinyl acetate copolymer, glycerol monostearate, glyceryl tristearate.
Described glue spraying emulsion adopts acrylonitrile and styrene dual MCU system copolymerization to form.
Compared with prior art, the method have the advantages that
1, the present invention adopts the effective ingredient such as bamboo fibre, hollow terylene, adds the intensity of silkworm silk, breathability and warming moisture-absorbing function.
The excellent serviceabilities such as 2, the present invention has free from extraneous odour, loft height, good springiness, antistatic, water-fastness, life-time service is indeformable.
3, the present invention has good antibacterial effect, and after washing, antibacterial effect is splendid, without alleviating problem.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further:
Embodiment 1
A kind of high resiliency silk composite fiber insulation cotton, its formula is as follows: 10 parts of mulberry silk, polyethylene fibre 10 parts, polytetrafluoroethylene fibre 12 parts, synthetic cotton 5 parts, hollow terylene 10 parts, glue spraying emulsion 2 parts, bamboo fibre 3 parts, nano-calcium carbonate 2 parts, nano titanium oxide suspension 10 parts, graphene sol 6 parts, nano bamboo powdered carbon 2 parts, dispersant 2 parts.
The titanium dioxide particle diameter that described nano titanium oxide suspension adopts is 10nm.
The preparation method of described nano titanium oxide suspension is as follows: be stirred vigorously by dehydrated alcohol, adds nano titanium oxide obtained solution A, by water, ethanol, acetic acid Homogeneous phase mixing, obtained solution B; When being stirred vigorously, solution A is added drop-wise in solution B, is added dropwise to complete stopping stirring.
The preparation method of described graphene sol is that graphite oxide grinds to form the fine powder that particle diameter is 1 micron, and is configured to, with solvent, the suspension that concentration is 0.5mg/ml, and supersound process, after 10 minutes, removes the unstable impurity in suspension, obtains graphene oxide colloidal sol.
Described dispersant adopts ethylene-acrylic acid copolymer.
Described glue spraying emulsion adopts acrylonitrile and styrene dual MCU system copolymerization to form.
Embodiment 2
A kind of high resiliency silk composite fiber insulation cotton, its formula is as follows: 30 parts of mulberry silk, polyethylene fibre 15 parts, polytetrafluoroethylene fibre 20 parts, synthetic cotton 9 parts, hollow terylene 14 parts, glue spraying emulsion 5 parts, bamboo fibre 12 parts, nano-calcium carbonate 3 parts, nano titanium oxide suspension 25 parts, graphene sol 10 parts, nano bamboo powdered carbon 4 parts, dispersant 5 parts.
The titanium dioxide particle diameter that described nano titanium oxide suspension adopts is 20nm.
The preparation method of described nano titanium oxide suspension is as follows: be stirred vigorously by dehydrated alcohol, adds nano titanium oxide obtained solution A, by water, ethanol, acetic acid Homogeneous phase mixing, obtained solution B; When being stirred vigorously, solution A is added drop-wise in solution B, is added dropwise to complete stopping stirring.
The preparation method of described graphene sol is that graphite oxide grinds to form the fine powder that particle diameter is 40 microns, and is configured to, with solvent, the suspension that concentration is 6mg/ml, and supersound process, after 120 minutes, removes the unstable impurity in suspension, obtains graphene oxide colloidal sol.
Described dispersant adopts ethylene-vinyl acetate copolymer.
Described glue spraying emulsion adopts acrylonitrile and styrene dual MCU system copolymerization to form.
Embodiment 3
A kind of high resiliency silk composite fiber insulation cotton, its formula is as follows: 20 parts of mulberry silk, polyethylene fibre 13 parts, polytetrafluoroethylene fibre 16 parts, synthetic cotton 7 parts, hollow terylene 12 parts, glue spraying emulsion 3 parts, bamboo fibre 7 parts, nano-calcium carbonate 3 parts, nano titanium oxide suspension 18 parts, graphene sol 8 parts, nano bamboo powdered carbon 3 parts, dispersant 3 parts.
The titanium dioxide particle diameter that described nano titanium oxide suspension adopts is 15nm.
The preparation method of described nano titanium oxide suspension is as follows: be stirred vigorously by dehydrated alcohol, adds nano titanium oxide obtained solution A, by water, ethanol, acetic acid Homogeneous phase mixing, obtained solution B; When being stirred vigorously, solution A is added drop-wise in solution B, is added dropwise to complete stopping stirring.
The preparation method of described graphene sol is that graphite oxide grinds to form the fine powder that particle diameter is 21 microns, and it is configured to, with solvent, the suspension that concentration is 3.3mg/ml, after supersound process 75 minutes, remove the unstable impurity in suspension, obtain graphene oxide colloidal sol.
Described dispersant adopts glycerol monostearate.
Described glue spraying emulsion adopts acrylonitrile and styrene dual MCU system copolymerization to form.
The embodiment catalytic effect of embodiment 1-3 is as follows:
The foregoing is only one embodiment of the invention, be not limiting as the present invention, all employings are equal to the technical scheme that the mode of replacement or equivalent transformation obtains, and all fall within protection scope of the present invention.

Claims (6)

1. a high resiliency silk composite fiber insulation cotton, its formula is as follows: mulberry silk 10-30 part, polyethylene fibre 10-15 part, polytetrafluoroethylene fibre 12-20 part, synthetic cotton 5-9 part, hollow terylene 10-14 part, glue spraying emulsion 2-5 part, bamboo fibre 3-12 part, nano-calcium carbonate 2-3 part, nano titanium oxide suspension 10-25 part, graphene sol 6-10 part, nano bamboo powdered carbon 2-4 part, dispersant 2-5 part.
2. a kind of high resiliency silk composite fiber insulation cotton according to claims 1, it is characterised in that the titanium dioxide particle diameter that described nano titanium oxide suspension adopts is 10-20nm.
3. a kind of high resiliency silk composite fiber insulation cotton according to claims 1, it is characterized in that, the preparation method of described nano titanium oxide suspension is as follows: be stirred vigorously by dehydrated alcohol, add nano titanium oxide obtained solution A, by water, ethanol, acetic acid Homogeneous phase mixing, obtained solution B; When being stirred vigorously, solution A is added drop-wise in solution B, is added dropwise to complete stopping stirring.
4. a kind of high resiliency silk composite fiber insulation cotton according to claims 1, it is characterized in that, the preparation method of described graphene sol is that graphite oxide grinds to form the fine powder that particle diameter is 1-40 micron, and it is configured to, with solvent, the suspension that concentration is 0.5-6mg/ml, after supersound process 10-120 minute, remove the unstable impurity in suspension, obtain graphene oxide colloidal sol.
5. a kind of high resiliency silk composite fiber insulation cotton according to claims 1, it is characterised in that described dispersant adopts the one in ethylene-acrylic acid copolymer, ethylene-vinyl acetate copolymer, glycerol monostearate, glyceryl tristearate.
6. a kind of high resiliency silk composite fiber insulation cotton according to claims 1, it is characterised in that described glue spraying emulsion adopts acrylonitrile and styrene dual MCU system copolymerization to form.
CN201610011135.7A 2016-01-10 2016-01-10 High-elasticity silk complex fiber thermal cotton Pending CN105648652A (en)

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CN106835680A (en) * 2016-12-13 2017-06-13 宁波芸生纺织品科技有限公司 A kind of calcium carbonate enhancing silk fabric and preparation method thereof
CN108035165A (en) * 2017-12-21 2018-05-15 芜湖品度电子科技有限公司 Mould-proof antibacterial braid and preparation method thereof
CN108505210A (en) * 2017-02-28 2018-09-07 夏小华 Washable silk and its manufacture craft
CN109749268A (en) * 2017-11-02 2019-05-14 丹阳博亚新材料技术服务有限公司 A kind of degradable plastics
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CN110341258A (en) * 2019-08-07 2019-10-18 广州广微新材料科技有限公司 A kind of ultra-thin macromolecule thermal fabric
CN110575034A (en) * 2019-07-30 2019-12-17 江苏缔凡蚕丝科技创意园有限公司 silk graphene quilt
CN113981675A (en) * 2021-11-16 2022-01-28 武汉纺织大学 Preparation method of photo-induced heating textile

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CN113981675A (en) * 2021-11-16 2022-01-28 武汉纺织大学 Preparation method of photo-induced heating textile
CN113981675B (en) * 2021-11-16 2023-07-07 武汉纺织大学 Preparation method of photo-induced heating textile

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Application publication date: 20160608