CN108147665A - Microcrystal grain glaze and preparation method thereof - Google Patents
Microcrystal grain glaze and preparation method thereof Download PDFInfo
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- CN108147665A CN108147665A CN201711304438.9A CN201711304438A CN108147665A CN 108147665 A CN108147665 A CN 108147665A CN 201711304438 A CN201711304438 A CN 201711304438A CN 108147665 A CN108147665 A CN 108147665A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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Abstract
The invention discloses a kind of microcrystal grain glaze and preparation method thereof, microcrystal grain glaze answers glaze and crystal grain two major parts to form by high temperature single-layer back, the different crystal grain of different colour match, different color high temperature single-layer backs answer each component quality difference of glaze, and red granules each component is as follows：30~35 parts of potassium feldspar；8~15 parts of albite；25~35 parts of quartz；13~18 parts of lime stone；8~12 parts of zinc oxide；8~14 parts of spodumene；8~12 parts of Jiepai clay of glaze；5~8 parts of titanium oxide；16 parts of zirconium iron pink.White particle each component is as follows：30~35 parts of potassium feldspar；8~15 parts of albite；25~35 parts of quartz；13~18 parts of lime stone；8~12 parts of zinc oxide；8~14 parts of spodumene；8~12 parts of Jiepai clay of glaze；10~15 parts of titanium oxide；30 parts of zirconium silicate.The effect that microcrystal grain glaze series is arranged in pairs or groups by different colours and particle, it is in the effect of microcrystallization glaze that class, which can be generated, but the glaze is by artificially controlling control more preferable than microcrystallization glaze, since the granular size of addition differs, it is the glaze in visual effect more naturally, the microcrystal grain glaze receives the favor of European client.
Description
Technical field
The invention discloses a kind of microcrystal grain glaze and preparation method thereof.
Background technology
At present, the domestic ceramic industry of ceramics is all with color under glaze in high temp, and in-glaze decoration, overglaze color is mainstream, fading from memory gradually
Traditional ceramics it is bright and colourful, microcrystal grain glaze disclosed by the invention is the crystalline glaze crystallite series glaze using traditional ceramics as base
Plinth in the requirement that dosage is produced according to client, tests out microcrystal grain glaze, beauty of the glaze i.e. with traditional crystalline glaze, glaze energy
It is adapted to large batch of production.Our company is just researching and developing each quasi-tradition glaze of traditional ceramics energetically, which is current season
The product of outstanding R＆D intensity.
Invention content
The technical problems to be solved by the invention are overcome the deficiencies in the prior art, and the effect of the glaze colours improves, the crystallite
Particle glaze answers glaze and crystal grain two major parts to form by high temperature single-layer back, the different crystal grain of different colour match, different
Color high temperature single-layer back answer each component quality of glaze different, cream-coloured single-layer back answers glaze each component as follows：35 parts of potassium feldspar~
40 parts；14 parts~23 parts of calcite；8 parts~16 parts of dolomite；8 parts~14 parts of zinc oxide；25 parts~35 parts of quartz；Titanium oxide 6
Part~8 parts；13 parts~16 parts of zirconium silicate；8 parts~13 parts of sodium glass powder；3 parts~5 parts of rutile；4 parts~6 parts of red granules.It is red
Coloured particles each component and each component quality are as follows：30 parts~35 parts of potassium feldspar；8 parts~15 parts of albite；Quartz 25 parts~35
Part；13 parts~18 parts of lime stone；8 parts~12 parts of zinc oxide；8 parts~14 parts of spodumene；8 parts~12 parts of Jiepai clay of glaze；Oxidation
5 parts~8 parts of titanium；16 parts of zirconium iron pink.The single-layer back of blue answers glaze each component as follows：40 parts~50 parts of potassium feldspar；14 parts of calcite
~23 parts；8 parts~16 parts of dolomite；8 parts~14 parts of zinc oxide；25 parts~35 parts of quartz；3 parts~5 parts of titanium oxide；Soda-lime glass
8 parts~13 parts of powder；3 parts~5 parts of rutile；4 parts~6 parts of red granules；3 parts of cobalt oxide；2 parts of di-iron trioxide.White particle
Each component and each component quality are as follows：30 parts~35 parts of potassium feldspar；8 parts~15 parts of albite；25 parts~35 parts of quartz；Lime stone
13 parts~18 parts；8 parts~12 parts of zinc oxide；8 parts~14 parts of spodumene；8 parts~12 parts of Jiepai clay of glaze；Titanium oxide 10 parts~15
Part；30 parts of zirconium silicate.
In order to solve the above-mentioned technical problem, the technical scheme is that：A kind of microcrystal grain glaze, its each component and each
Component mass parts are as follows；
B) 1.5 ︰ 0.6 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours after the glaze after ball milling crosses 200 mesh sieve, are adjusted
It is for use that 51~53 Baume concentration are made；
C) it stocks up according to each component and each component mass parts；
D) 1.4 ︰ 0.7 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours, the glaze after ball milling are crossed 200 mesh sieve, are dried
It is dry, 50 mesh sieve is crossed, is then sintered in 1000 degrees Celsius of drawer kiln again, it is for use to cross 50 mesh sieve；
E) crystal grain is weighed by 1：25 ratio is added in high temperature individual layer glaze；
F) clean green body is taken, upper microcrystal grain glaze is dry；
G) dried microcrystal grain glaze green body is put into drawer kiln and is burnt into through 1290 DEG C of oxidizing atmosphere.
After employing above-mentioned technical proposal, granule crystal glaze colours prepared by the present invention had not only had the beauty of traditional glaze colours, but also
More Product Experiences and reverie space are brought to consumer.It adapts to produce in enormous quantities.
Specific embodiment
In order that the present invention can be more clearly and readily understood, below according to specific embodiment, the present invention is made into
One step is described in detail.
Embodiment one：
The microcrystal grain glaze component and each component quality are as follows,
Cream-coloured single-layer back answers glaze each component as follows：35 parts~40 parts of potassium feldspar；14 parts~23 parts of calcite；Dolomite 8
Part~16 parts；8 parts~14 parts of zinc oxide；25 parts~35 parts of quartz；6 parts~8 parts of titanium oxide；13 parts~16 parts of zirconium silicate；Sodium glass
8 parts~13 parts of glass powder；3 parts~5 parts of rutile；4 parts~6 parts of red granules.Red granules each component and each component quality are as follows：
30 parts~35 parts of potassium feldspar；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；8 parts of zinc oxide~
12 parts；8 parts~14 parts of spodumene；8 parts~12 parts of Jiepai clay of glaze；5 parts~8 parts of titanium oxide；16 parts of zirconium iron pink.The list of blue
Layer reaction glaze each component is as follows：40 parts~50 parts of potassium feldspar；14 parts~23 parts of calcite；8 parts~16 parts of dolomite；Zinc oxide 8
Part~14 parts；25 parts~35 parts of quartz；3 parts~5 parts of titanium oxide；8 parts~13 parts of sodium glass powder；3 parts~5 parts of rutile；It is red
4 parts~6 parts of particle；3 parts of cobalt oxide；2 parts of di-iron trioxide.White particle each component and each component quality are as follows：Potassium feldspar 30
Part~35 parts；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；8 parts~12 parts of zinc oxide；Lithium
8 parts~14 parts of pyroxene；8 parts~12 parts of Jiepai clay of glaze；10 parts~15 parts of titanium oxide；30 parts of zirconium silicate.
A kind of the step of microcrystal grain glaze decorative art production method, this method, is as follows：
A stocks up according to each component and each component mass parts；
B) 1.5 ︰ 0.6 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours after the glaze after ball milling crosses 200 mesh sieve, are adjusted
It is for use that 51~53 Baume concentration are made；
C) crystal grain is stocked up according to each component and each component mass parts；
D) 1.4 ︰ 0.7 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours, the glaze after ball milling are crossed 200 mesh sieve, are dried
It is dry, 50 mesh sieve is crossed, is then sintered in 1000 degrees Celsius of drawer kiln again, it is for use to cross 50 mesh sieve；
E) crystal grain is weighed by 1：25 ratio is added in high temperature individual layer glaze；
F) clean green body is taken, upper microcrystal grain glaze is dry；
G) dried microcrystal grain glaze green body is put into drawer kiln and is burnt into through 1290 DEG C of oxidizing atmosphere.
Embodiment two：
A kind of microcrystal grain glaze component and each component quality are as follows：
Cream-coloured single-layer back answers glaze each component as follows：35 parts~40 parts of potassium feldspar；14 parts~23 parts of calcite；Dolomite 8
Part~16 parts；8 parts~14 parts of zinc oxide；25 parts~35 parts of quartz；6 parts~8 parts of titanium oxide；13 parts~16 parts of zirconium silicate；Sodium glass
8 parts~13 parts of glass powder；8 parts~10 parts of rutile；4 parts~6 parts of red granules.Red granules each component and each component quality are such as
Under：30 parts~35 parts of potassium feldspar；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；Zinc oxide 8
Part~12 parts；8 parts~14 parts of spodumene；8 parts~12 parts of Jiepai clay of glaze；5 parts~8 parts of titanium oxide；16 parts of zirconium iron pink.Blue
Single-layer back answer glaze each component as follows：40 parts~50 parts of potassium feldspar；14 parts~23 parts of calcite；8 parts~16 parts of dolomite；Oxygen
Change 8 parts~14 parts of zinc；25 parts~35 parts of quartz；3 parts~5 parts of titanium oxide；8 parts~13 parts of sodium glass powder；Rutile 8 parts~10
Part；4 parts~6 parts of red granules；3 parts of cobalt oxide；2 parts of di-iron trioxide.White particle each component and each component quality are as follows：Potassium
30 parts~35 parts of feldspar；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；Zinc oxide 8 parts~12
Part；8 parts~14 parts of spodumene；8 parts~12 parts of Jiepai clay of glaze；10 parts~15 parts of titanium oxide；30 parts of zirconium silicate.
A kind of the step of microcrystal grain glaze of the present invention, this method, is as follows：
A) high temperature individual layer glaze is stocked up according to each component and each component mass parts；
B) 1.5 ︰ 0.6 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours after the glaze after ball milling crosses 200 mesh sieve, are adjusted
It is for use that 51~53 Baume concentration are made；
C) crystal grain is stocked up according to each component and each component mass parts；
D) 1.4 ︰ 0.7 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours, the glaze after ball milling are crossed 200 mesh sieve, are dried
It is dry, 50 mesh sieve is crossed, is then sintered in 1000 degrees Celsius of drawer kiln again, it is for use to cross 50 mesh sieve；
E) crystal grain is weighed by 1：25 ratio is added in high temperature individual layer glaze；
F) clean green body is taken, upper microcrystal grain glaze is dry；
G) dried microcrystal grain glaze green body is put into drawer kiln and is burnt into through 1290 DEG C of oxidizing atmosphere.
Embodiment three：
The microcrystal grain glaze component and each component quality are as follows：
Cream-coloured single-layer back answers glaze each component as follows：35 parts~40 parts of potassium feldspar；14 parts~23 parts of calcite；Dolomite 8
Part~16 parts；8 parts~14 parts of zinc oxide；25 parts~35 parts of quartz；6 parts~8 parts of titanium oxide；13 parts~16 parts of zirconium silicate；Sodium glass
8 parts~13 parts of glass powder；3 parts~5 parts of rutile；4 parts~6 parts of red granules.Red granules each component and each component quality are as follows：
30 parts~35 parts of potassium feldspar；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；8 parts of zinc oxide~
12 parts；8 parts~14 parts of spodumene；8 parts~12 parts of Jiepai clay of glaze；5 parts~8 parts of titanium oxide；16 parts of zirconium iron pink.The list of blue
Layer reaction glaze each component is as follows：40 parts~50 parts of potassium feldspar；14 parts~23 parts of calcite；8 parts~16 parts of dolomite；Zinc oxide 8
Part~14 parts；25 parts~35 parts of quartz；3 parts~5 parts of titanium oxide；8 parts~13 parts of sodium glass powder；3 parts~5 parts of rutile；It is red
4 parts~6 parts of particle；3 parts of cobalt oxide；2 parts of di-iron trioxide.White particle each component and each component quality are as follows：Potassium feldspar 30
Part~35 parts；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；8 parts~12 parts of zinc oxide；Lithium
8 parts~14 parts of pyroxene；8 parts~12 parts of Jiepai clay of glaze；10 parts~15 parts of titanium oxide；30 parts of zirconium silicate；
The step of microcrystal grain glaze decorative art production method, this method, is as follows：
A) high temperature individual layer glaze is stocked up according to each component and each component mass parts；
B) 1.5 ︰ 0.6 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours after the glaze after ball milling crosses 200 mesh sieve, are adjusted
It is for use that 51~53 Baume concentration are made；
C) crystal grain is stocked up according to each component and each component mass parts；
D) 1.4 ︰ 0.7 of You Liao ︰ Qiu ︰ water=1 ︰, wet ball grinding 13~14 hours, the glaze after ball milling are crossed 200 mesh sieve, are dried
It is dry, 50 mesh sieve is crossed, is then sintered in 1180 degrees Celsius of roller kilns again, it is for use to cross 50 mesh sieve；
E) crystal grain is weighed by 1：25 ratio is added in high temperature individual layer glaze；
F) clean green body is taken, upper microcrystal grain glaze is dry；
G) dried microcrystal grain glaze green body is put into drawer kiln and is burnt into through 1290 DEG C of oxidizing atmosphere.
More than 3 points to test one as ideal developmental achievement.Experiment one：Meet the exploitation original intention of company, meet visitor
The demand at family.Experiment two：Since the rutile of addition is excessive, the overall beautiful of the microcrystal grain glaze is affected.Experiment three：The crystalline substance
Body particle reaches hemispherical fusion temperature after being burnt into 1180 degrees Celsius of roller kilns make particle make failure.
Particular embodiments described above, pair present invention solves the technical problem that, technical solution and advantageous effect carry out
It is further described, it should be understood that the above is only a specific embodiment of the present invention, is not limited to this
Invention, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should be included in this hair
Within bright protection domain.
Claims (2)
1. a kind of microcrystal grain glaze, it is characterised in that the microcrystal grain glaze answers glaze and crystal grain two major parts group by high temperature single-layer back
Into the different crystal grain of different colour match, different color high temperature single-layer back answers each component quality of glaze different, cream-coloured
Single-layer back answer glaze each component as follows：35 parts~40 parts of potassium feldspar；14 parts~23 parts of calcite；8 parts~16 parts of dolomite；Oxidation
8 parts~14 parts of zinc；25 parts~35 parts of quartz；6 parts~8 parts of titanium oxide；13 parts~16 parts of zirconium silicate；8 parts~13 parts of sodium glass powder；
3 parts~5 parts of rutile；4 parts~6 parts of red granules.Red granules each component and each component quality are as follows：Potassium feldspar 30 parts~35
Part；8 parts~15 parts of albite；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；8 parts~12 parts of zinc oxide；8 parts of spodumene
~14 parts；8 parts~12 parts of Jiepai clay of glaze；5 parts~8 parts of titanium oxide；16 parts of zirconium iron pink.The single-layer back of blue answers glaze each component such as
Under：40 parts~50 parts of potassium feldspar；14 parts~23 parts of calcite；8 parts~16 parts of dolomite；8 parts~14 parts of zinc oxide；25 parts of quartz
~35 parts；3 parts~5 parts of titanium oxide；8 parts~13 parts of sodium glass powder；3 parts~5 parts of rutile；4 parts~6 parts of red granules；Oxidation
3 parts of cobalt；2 parts of di-iron trioxide.White particle each component and each component quality are as follows：30 parts~35 parts of potassium feldspar；8 parts of albite
~15 parts；25 parts~35 parts of quartz；13 parts~18 parts of lime stone；8 parts~12 parts of zinc oxide；8 parts~14 parts of spodumene；Glaze circle
8 parts~12 parts of board mud；10 parts~15 parts of titanium oxide；30 parts of zirconium silicate.
2. the step of microcrystal grain glaze decorative art production method according to claim 1, this method, is as follows：
A) it stocks up according to each component and each component mass parts；
B) by material：You Liao ︰ Qiu ︰ water=1 ︰, 1.5 ︰ 0.6, wet ball grinding 13~14 hours, after the glaze after ball milling crosses 200 mesh sieve,
It is for use to be modulated into 51~53 Baume concentration；
C) it stocks up according to each component and each component mass parts：
D) by material：You Liao ︰ Qiu ︰ water=1 ︰, 1.4 ︰ 0.7, wet ball grinding 13~14 hours, the glaze after ball milling are crossed 200 mesh sieve, are dried
It is dry, 50 mesh sieve is crossed, is then sintered in 1000 degrees Celsius of drawer kiln again, it is for use to cross 50 mesh sieve；
E) crystal grain is weighed by 1：25 ratio is added in high temperature individual layer glaze；
F) clean green body is taken, upper microcrystal grain glaze is dry；
G) dried microcrystal grain glaze green body is put into drawer kiln and is burnt into through 1290 DEG C of oxidizing atmosphere.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711304438.9A CN108147665A (en) | 2017-12-11 | 2017-12-11 | Microcrystal grain glaze and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108328924A (en) * | 2018-02-05 | 2018-07-27 | 湖南陶润会文化传播有限公司 | Granule crystal glaze and preparation method thereof |
| CN111453991A (en) * | 2020-03-14 | 2020-07-28 | 湖南陶润会文化传播有限公司 | Golden crystal glaze and preparation method thereof |
| CN112142326A (en) * | 2020-09-10 | 2020-12-29 | 醴陵陶润实业发展有限公司 | Iron-cobalt-nickel crystal system crystal glaze and preparation method thereof |
| CN113480168A (en) * | 2021-07-01 | 2021-10-08 | 醴陵陶润实业发展有限公司 | Practical decorative particles and preparation method thereof |
-
2017
- 2017-12-11 CN CN201711304438.9A patent/CN108147665A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108328924A (en) * | 2018-02-05 | 2018-07-27 | 湖南陶润会文化传播有限公司 | Granule crystal glaze and preparation method thereof |
| CN111453991A (en) * | 2020-03-14 | 2020-07-28 | 湖南陶润会文化传播有限公司 | Golden crystal glaze and preparation method thereof |
| CN112142326A (en) * | 2020-09-10 | 2020-12-29 | 醴陵陶润实业发展有限公司 | Iron-cobalt-nickel crystal system crystal glaze and preparation method thereof |
| CN113480168A (en) * | 2021-07-01 | 2021-10-08 | 醴陵陶润实业发展有限公司 | Practical decorative particles and preparation method thereof |
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