CN108142977A - A kind of cigarette moist-keeping flavouring agent - Google Patents

A kind of cigarette moist-keeping flavouring agent Download PDF

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Publication number
CN108142977A
CN108142977A CN201711438744.1A CN201711438744A CN108142977A CN 108142977 A CN108142977 A CN 108142977A CN 201711438744 A CN201711438744 A CN 201711438744A CN 108142977 A CN108142977 A CN 108142977A
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cigarette
extract
weight
parts
medicinal extract
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CN108142977B (en
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邵灯寅
李赓
胡巍耀
苏加坤
罗海涛
谭明杰
何力
徐达
艾亦旻
张晓旭
蔡继宝
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China Tobacco Jiangxi Industrial Co Ltd
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China Tobacco Jiangxi Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of cigarette moist-keeping flavouring agent, are made from the following raw materials in parts by weight:Potentilla discolor 25 ~ 35, aleppo avens 15 ~ 30, Hupeh Fritillary Bulb 12 ~ 20, Flos Magnoliae Officinalis 9 ~ 15 and appropriate propylene glycol, preparation method include the following steps:(1)The potentilla discolor of the parts by weight is prepared into medicinal extract extract A;(2)The aleppo avens of the parts by weight is prepared into grease B;(3)The Hupeh Fritillary Bulb of the parts by weight is prepared into medicinal extract extract C;(4)The Flos Magnoliae Officinalis of the parts by weight is prepared into crystal D;(5)By medicinal extract extract A, grease B, medicinal extract extract C and crystal D and appropriate mixed with propylene glycol, moist-keeping flavouring agent is obtained.By product spray application of the present invention on pipe tobacco, play the role of apparent moist-keeping flavouring to cigarette.

Description

A kind of cigarette moist-keeping flavouring agent
Technical field
The present invention relates to additive in cigarette technical field, particularly a kind of cigarette moist-keeping flavouring agent.
Background technology
In the prior art, " Chinese-style cigarette " core competitiveness is to form selling point style, embodies personalized and differentiation, Adapt to Chinese consumers in general sucks custom and consumer need.Chinese style essence spice for cigarette is the " spirit of Chinese-style cigarette product Soul " is the secret place that " Chinese-style cigarette " style characteristic is formed.Scientifically flavoring and casing, exactly prominent cigarette produce in cigarette The important means of the personalized style of product.Meanwhile for the safety for improving smoking, lowering harm and decreasing coking has become " Chinese-style cigarette " One important component.While coke tar in cigarette is reduced, also promote and improve flue gas concentration and fragrance, only by means of adding Fragrant feeding technique.With going deep into for Chinese-style cigarette lowering harm and decreasing coking work, tobacco flavoring charging shows its importance further.
The Chinese style essence spice for cigarette and new technology of independent intellectual property right are constructed, it is fragrant that essence is extracted from natural herbal plant Material allows the theory of health to move towards consumer together with the refined perfume (or spice) of cigarette, be one of basic research for developing " Chinese-style cigarette ".
The research of cigarette flavouring humectation is to construct Chinese-style cigarette core technology, form the important of cigarette product distinctive style Basis.Flavouring humectation technology be continue promoted cigarette the key technology for sucking pleasant feeling, comfort level and physics humid keeping performance it One.In recent years, China's tobacco business took part in international competition wider, faced severe market competition and challenge.At present with International cigarette famous brand name is compared, and there are certain deficiencies in perfume quantity, sense organ comfort level etc. for domestic cigarette product.Separately Outside, as Chinese Government fulfils《The Framework Convention on Tobacco Control》Comprehensive deep expansion of work and society are to smoking and health problem The continuous enhancing of concern, high fragrance, low tar, Less harmful cigarette become the inexorable trend of industry development.This trend will be to volume Cigarette flavouring humectation technology needs do deeper into research.Again, cigarette product to varying degrees there are trans-regional adaptability not Cigarette quality fluctuation is also cigarette flavouring humectation urgent problem caused by strong.
Ideal humectant should have both moisturizing and moisture-proof two kinds of effects, that is, reduce cigarette moisture content and ambient temperature and humidity is changed Sensitivity, remain cigarette moisture content in a metastable range.Because the humectation of cigarette not only includes physics Humectation further includes sense organ humectation.Physics humectation, that is, moisturizing refers to maintain the moisture of tobacco leaf, it is therefore intended that improves the resistance to of pipe tobacco and adds Work performance and the moisture for maintaining flue gas.Sense organ humectation be then directly against sensory issues, to dry sensation, irritation, pleasant impression etc. into Row improves.
The exploitation of physics humectant is carried out in terms of hydrophily water conservation substance and hydrophobicity confining substance two.Hydrophily physics The research of humectation monomer needs the kind for having significant advantage in extensive concern natural plants, aquatile in terms of humectation, carries out The extraction of active ingredient of natural plant, Purification develop new type natural humectant;In addition the chemical modification of polysaccharide is also likely to be The important channel of hydrophily humectation monomer exploitation.Hydrophobicity physics humectation monomer will play the role of damp proof insulation, then need in tobacco leaf table Face forms one layer of water-separating film, therefore can be with some sugar esters of chemical synthesis or polyalcohol Ester, and investigates esterification degree and fat Sour chain length is to the formation of water-separating film and the influence of water proof effect.On this basis, targetedly physics humectation monomer is carried out Rationally compounding, the novel physical humectant that physical quality meets sense organ quality requirement again can be improved by developing.
Flue gas moisture is suitable, the soft exquisiteness of flue gas, then small to the stimulation of human body;And when moisture is low in main flume, Gas drying sense enhancing, irritation increase are frequently resulted in, comfort reduces.Cigarette dry sensation removes and depends primarily on flue gas moisture Outside, it is also related with the impression in terms of cigarette irritation.Reduce irritation, increase flue gas promotes the production of body fluid to feel and also contributes to reduce cigarette Dry sensation reduces cigarette irritation.Therefore, when researching and developing novel humectant, directly against the sense organ humectant of mouthfeel Research is also one of important content.
Invention content
The mesh of the present invention is to provide a kind of cigarette prepared as raw material using potentilla discolor, aleppo avens, Hupeh Fritillary Bulb, Flos Magnoliae Officinalis Moist-keeping flavouring agent, and as additive of tobacco product among cigarette, the quality to improve Chinese-style cigarette to be made contributions.
The invention discloses a kind of cigarette moist-keeping flavouring agent, are made from the following raw materials in parts by weight:Potentilla discolor 25 ~ 35, indigo plant Cloth is positive 15 ~ 30, Hupeh Fritillary Bulb 12 ~ 20, Flos Magnoliae Officinalis 9 ~ 15 and appropriate propylene glycol.
The preparation method of above-mentioned cigarette moist-keeping flavouring agent, includes the following steps:
(1)By the potentilla discolor complete stool of the parts by weight, 50 ~ 60 DEG C of dry 6 ~ 8h are crushed, and add in 2 ~ 3 times of 70% EtOH Sonicate interval 1 ~ 2h is extracted, then 3 ~ 5h is heated to reflux, then 2 ~ 3h is extracted at 85 DEG C with 50% ethyl alcohol for 75 ~ 95 DEG C, collects reflux extracting liquid, subtract Pressure concentration, obtains medicinal extract extract A;
(2)It is 95% ethyl alcohol to use volume fraction after the aleppo avens herb of the parts by weight dry, pulverize successively, and 75% ether oozes It filters, merging filtrate is concentrated to give medicinal extract, and medicinal extract adds suitable quantity of water to disperse, respectively with n-butanol, n-hexane extraction 2 ~ 3 times, with anhydrous sulphur Sour sodium removes moisture, and filtering obtains the grease B with special odor;
(3)After the Hupeh Fritillary Bulb of the parts by weight is pulverized, add in 50 ~ 70% EtOH Sonicates and just extract 10min, be then transferred to water Extraction equipment extraction 6h is bathed, after cooling, filtering is collected extracting solution and is extracted 1-2 times again as stated above, merging extracting solution, concentration, Obtain medicinal extract extract C.
(4)The Flos Magnoliae Officinalis of the parts by weight is ground to powdered, 2 ~ 3 times of water ultrasound interval 1 ~ 2h of extraction of addition, then It is transferred to volatile oil extractor well-established law and is back to oil reservoir and be not further added by, oil reservoir is collected in condensation, volatile oil is placed in less than 0 DEG C is precipitated and tie Crystalline substance obtains crystal D;
(5)By medicinal extract extract A, grease B, medicinal extract extract C and crystal D and appropriate mixed with propylene glycol, humectation increasing is obtained Pastil.
Application mode of the above-mentioned cigarette moist-keeping flavouring agent in cigarette is as follows:The moist-keeping flavouring agent is taken, according to 0.01- It after 0.1 ‰ dilutions, is uniformly sprayed on pipe tobacco, naturally dry, in 60% time 22 DEG C of temperature, humidity balance more than 10h, uses tobacco curing Cigarette is made in pipe tobacco by device.
Compared with prior art, advantages of the present invention and generation good effect are:
Potentilla discolor is rose family potentilla plants, mild-natured, sweet in flavor, more containing flavones, terpene, steroidal, tannin and organic acid etc. Kind chemical composition, also containing ingredients such as adenosine, dolichol, azelaic acid, SOD enzymes and polysaccharide.With anti-inflammatory and antalgic, anti-oxidant, drop Blood glucose, antibacterial, it is antiviral the effects that.Macromolecular and alcohol compound cracking during the smoking process, generate small point a large amount of Sub- phenolic acid compound and sugar or polyalcohol, ester, aldehyde, ketone have the cause ingredient of dense stir-fry fruit flavor etc., make cigarette perfume alcohol soft clearly Beautiful, flue gas it is full it is smooth, mouthfeel is sweet comfortable, make it have the gentle long characteristic of pleasant impression.
Aleppo avens is rose family avens south throatroot, has the function of analgesia, decompression, menstruation regulating, dispelling wind and eliminating dampness. Aleppo avens contains volatile oil, in aleppo avens volatile ingredient, predominantly aliphatic acid and fatty acid methyl ester, terpenes and its oxygen-containing Derivative etc., wherein content it is higher have palmitic acid, 11,14,17-Eicosatrienoic acid methyl esters, linoleic acid, carypohyllene oxidation The macromoleculars and β-carypohyllene, beta-elemene, citronellol, germacrone and epicurzerenone etc. such as object, eugenol and trans- phytol Aroma component.The macromoleculars such as aliphatic acid are attached to pipe tobacco surface layer, generate protective film on pipe tobacco surface, have humectation, prevent cigarette Careless embrittlement, while in the larger environment of humidity, moisture will not be absorbed from outside, there are humectation and moisture-proof double effects;It causes Fragrant ingredient can be effectively increased the perfume quantity of cigarette, improve cigarette perfume makings and harmony, reduce miscellaneous gas and irritation, increase sweet Sense makes pleasant impression cleaner, comfortable, the whole interior quality for promoting cigarette.
Hupeh Fritillary Bulb is the bulb of Liliaceae Fritillaria Linn Hupeh Fritillary Bulb, contains many alkaloids, aliphatic acid, terpene Close object.Research shows that Hupeh Fritillary Bulb has clearing heat and moistening lung, cough-relieving apophlegmatic and antibechics, eliminating the phlegm and a variety of pharmacology such as relieving asthma such as relieving asthma Efficacy effect.
Dry flower of the Flos Magnoliae Officinalis for Magnoliacea plant Cortex Magnoliae Officinalis or Magnolia bilola, bitter, slightly warm in nature.With remove dampness by means of aromatics, The effect of regulating the flow of QI to ease the stomach, it is not fragrant for taste retention of damp leading to blockage of QI, chest gastral cavity ruffian turgor, Na Gu.Flos Magnoliae Officinalis
It is thick also containing oligosaccharide and polysaccharide moisturizing ingredient mainly containing aroma components such as magnolol, magnolol, camphor, volatile oil The chemical composition majority of plain flowers volatile oil is hemiterpene compound, aliphatic, aromatic compound ingredient.
The present invention uses pure natural raw material, is made according to natural perfume material compatibility theory and using compounded technology, not addition The effect of learning additive, having special sweet faint scent, give full play to natural plant extracts, can play and reduce oral cavity and throat Dry sensation mitigates the irritating effect of flue gas, meanwhile, humectation moisturizing, water resistant moisture resistance are stronger, and cigarette is made not glued in suction Lip.The present invention is used as tobacco additive agent, with obvious effects, and to developing there is " Chinese-style cigarette " product of distinctive style to have and well should Use prospect.
Specific embodiment
Technical scheme of the present invention is described in detail with reference to embodiment:
Embodiment 1
A kind of cigarette moist-keeping flavouring agent, is made from the following raw materials in parts by weight:Potentilla discolor 25, aleppo avens 15, Hupeh Fritillary Bulb 12, thickness Piao spends 9 and appropriate propylene glycol.
The preparation method of above-mentioned cigarette moist-keeping flavouring agent, includes the following steps:
(1)By the potentilla discolor complete stool of the parts by weight, 60 DEG C of dry 6h are crushed, and add in 3 times of 70% EtOH Sonicate interval extraction 2h, Then 3 are heated to reflux, then 23h is extracted at 85 DEG C with 50% ethyl alcohol for 95 DEG C, collect reflux extracting liquid, be concentrated under reduced pressure, obtain medicinal extract and carry Take object A;
(2)It is 95% ethyl alcohol to use volume fraction after the aleppo avens herb of the parts by weight dry, pulverize successively, and 75% ether oozes It filters, merging filtrate is concentrated to give medicinal extract, and medicinal extract adds suitable quantity of water to disperse, and respectively with n-butanol, n-hexane extraction 3 times, uses anhydrous slufuric acid Sodium removes moisture, and filtering obtains the grease B with special odor;
(3)After the Hupeh Fritillary Bulb of the parts by weight is pulverized, add in 70% EtOH Sonicate and just extract 10min, be then transferred to water-bath and carry Taking equipment extracts 6h, and after cooling, filtering is collected extracting solution and extracted again as stated above 2 times, merges extracting solution, and concentration is soaked Cream extract C.
(4)The Flos Magnoliae Officinalis of the parts by weight is ground to powdered, adds in 2 times of water ultrasound interval extraction 2h, be then transferred to Volatile oil extractor well-established law is back to oil reservoir and is not further added by, and oil reservoir is collected in condensation, and volatile oil is placed in less than 0 DEG C is precipitated crystallization, Obtain crystal D;
(5)By medicinal extract extract A, grease B, medicinal extract extract C and crystal D and appropriate mixed with propylene glycol, humectation increasing is obtained Pastil.
Embodiment 2
A kind of cigarette moist-keeping flavouring agent, is made from the following raw materials in parts by weight:Potentilla discolor 35, aleppo avens 30, Hupeh Fritillary Bulb 20, thickness Piao spends 15 and appropriate propylene glycol.
The preparation method of above-mentioned cigarette moist-keeping flavouring agent, includes the following steps:
(1)By the potentilla discolor complete stool of the parts by weight, 50 DEG C of dry 8h are crushed, and add in 2 times of 70% EtOH Sonicate interval extraction 2h, Then 5h is heated to reflux, then 2h is extracted at 85 DEG C with 50% ethyl alcohol for 75 DEG C, collects reflux extracting liquid, be concentrated under reduced pressure, obtain medicinal extract and carry Take object A;
(2)It is 95% ethyl alcohol to use volume fraction after the aleppo avens herb of the parts by weight dry, pulverize successively, and 75% ether oozes It filters, merging filtrate is concentrated to give medicinal extract, and medicinal extract adds suitable quantity of water to disperse, and respectively with n-butanol, n-hexane extraction 2 times, uses anhydrous slufuric acid Sodium removes moisture, and filtering obtains the grease B with special odor;
(3)After the Hupeh Fritillary Bulb of the parts by weight is pulverized, add in 55% EtOH Sonicate and just extract 10min, be then transferred to water-bath and carry Taking equipment extracts 6h, and after cooling, filtering is collected extracting solution and extracted again as stated above 1 time, merges extracting solution, and concentration is soaked Cream extract C.
(4)The Flos Magnoliae Officinalis of the parts by weight is ground to powdered, adds in 2 times of water ultrasound interval extraction 1h, be then transferred to Volatile oil extractor well-established law is back to oil reservoir and is not further added by, and oil reservoir is collected in condensation, and volatile oil is placed in less than 0 DEG C is precipitated crystallization, Obtain crystal D;
(5)By medicinal extract extract A, grease B, medicinal extract extract C and crystal D and appropriate mixed with propylene glycol, humectation increasing is obtained Pastil.
Embodiment 3
A kind of cigarette moist-keeping flavouring agent, is made from the following raw materials in parts by weight:Potentilla discolor 30, aleppo avens 18, Hupeh Fritillary Bulb 15, thickness Piao spends 12 and appropriate propylene glycol.
The preparation method of above-mentioned cigarette moist-keeping flavouring agent, includes the following steps:
(1)By the potentilla discolor complete stool of the parts by weight, 55 DEG C of dry 7h are crushed, and add in 2 times of 70% EtOH Sonicate interval extraction 2h, Then 3h is heated to reflux, then 5h is extracted at 85 DEG C with 50% ethyl alcohol for 85 DEG C, collects reflux extracting liquid, be concentrated under reduced pressure, obtain medicinal extract and carry Take object A;
(2)It is 95% ethyl alcohol to use volume fraction after the aleppo avens herb of the parts by weight dry, pulverize successively, and 75% ether oozes It filters, merging filtrate is concentrated to give medicinal extract, and medicinal extract adds suitable quantity of water to disperse, and respectively with n-butanol, n-hexane extraction 2 times, uses anhydrous slufuric acid Sodium removes moisture, and filtering obtains the grease B with special odor;
(3)After the Hupeh Fritillary Bulb of the parts by weight is pulverized, add in 65% EtOH Sonicate and just extract 10min, be then transferred to water-bath and carry Taking equipment extracts 6h, and after cooling, filtering is collected extracting solution and extracted again as stated above 2 times, merges extracting solution, and concentration is soaked Cream extract C.
(4)The Flos Magnoliae Officinalis of the parts by weight is ground to powdered, adds in 2 times of water ultrasound interval extraction 1h, be then transferred to Volatile oil extractor well-established law is back to oil reservoir and is not further added by, and oil reservoir is collected in condensation, and volatile oil is placed in less than 0 DEG C is precipitated crystallization, Obtain crystal D;
(5)By medicinal extract extract A, grease B, medicinal extract extract C and crystal D and appropriate mixed with propylene glycol, humectation increasing is obtained Pastil.
Test example
(One)Humectation effect is tested and assessed
1st, test purpose:It compares under equal conditions, pipe tobacco and the pipe tobacco containing propylene glycol of the agent containing moist-keeping flavouring(Control), blank cigarette Silk(Blank)Physics humectation effect.
2nd, test sample
Moist-keeping flavouring agent:1% moist-keeping flavouring agent+middle-grade blank pipe tobacco
Control:1% propylene glycol+middle-grade blank pipe tobacco
Blank:Middle-grade blank pipe tobacco
3rd, test method
3.1 equilibrium process:After three groups of samples of Example 1-3 are diluted according to 0.01-0.1 ‰ respectively, it is uniformly sprayed on pipe tobacco On, while it is placed in temperature with control sample and blank group sample:(22 ± 1) DEG C, humidity:It is put down in the climatic chamber of (60 ± 3) % Weighing apparatus 48 hours measures the initial water content of above-mentioned each group test sample, the as moisture content of 0h with Oven Method.
3.2 test process:Climatic chamber environment is adjusted to temperature:(22 ± 1) DEG C, humidity:(40 ± 3) %, will be upper It states each group test sample to be placed in one, separated in time weighs an example weight, and calculates according to example weight at this time Its instant moisture content, it is as a result as shown in table 1 below:
The instant moisture content of 1 different time of table(%)
The humectation effect evaluating result of table 1 shows:The present invention is with obvious effects for the humectation of pipe tobacco.
(Two)Sense organ suction is commented
With reference to GB5606.4-2005《The 4th part of cigarette:The requirement of sense organ technology》With YC/T 497-2014《Cigarette Chinese-style cigarette Style sensory evaluation method》The cigarette of moist-keeping flavouring agent to being added with 1-3 of the embodiment of the present invention carries out sensory evaluation, as a result such as Shown in the following table 2:
2 cigarette sensory evaluation of table
The Analyses Methods for Sensory Evaluation Results of table 2 shows the cigarette of the moist-keeping flavouring agent added with 1-3 of the embodiment of the present invention, flue gas it is clear Fragrance is pleasant, and sweet sense is apparent, can play reduce oral cavity and dry throat sense during the smoking process, mitigates flue gas stimulation Effect, be suitble to high-quality cigarette.
Above-described embodiment is only the more excellent embodiment of the present invention, and every technical spirit according to the present invention to implementing above Any simple modification, modification and the alternate variation that example is made, belong in the range of technical solution of the present invention.

Claims (3)

1. a kind of cigarette moist-keeping flavouring agent, which is characterized in that be made from the following raw materials in parts by weight:Potentilla discolor 25 ~ 35, aleppo avens 15 ~ 30, Hupeh Fritillary Bulb 12 ~ 20, Flos Magnoliae Officinalis 9 ~ 15 and appropriate propylene glycol.
2. a kind of preparation method of cigarette moist-keeping flavouring agent as described in claim 1, which is characterized in that include the following steps:
(1)By the potentilla discolor complete stool of the parts by weight, 50 ~ 60 DEG C of dry 6 ~ 8h are crushed, and add in 2 ~ 3 times of 70% EtOH Sonicate interval 1 ~ 2h is extracted, then 3 ~ 5h is heated to reflux, then 2 ~ 3h is extracted at 85 DEG C with 50% ethyl alcohol for 75 ~ 95 DEG C, collects reflux extracting liquid, subtract Pressure concentration, obtains medicinal extract extract A;
(2)It is 95% ethyl alcohol to use volume fraction after the aleppo avens herb of the parts by weight dry, pulverize successively, and 75% ether oozes It filters, merging filtrate is concentrated to give medicinal extract, and medicinal extract adds suitable quantity of water to disperse, respectively with n-butanol, n-hexane extraction 2 ~ 3 times, with anhydrous sulphur Sour sodium removes moisture, and filtering obtains the grease B with special odor;
(3)After the Hupeh Fritillary Bulb of the parts by weight is pulverized, add in 50 ~ 70% EtOH Sonicates and just extract 10min, be then transferred to water Extraction equipment extraction 6h is bathed, after cooling, filtering is collected extracting solution and is extracted 1-2 times again as stated above, merging extracting solution, concentration, Obtain medicinal extract extract C;
(4)The Flos Magnoliae Officinalis of the parts by weight is ground to powdered, adds in 2 ~ 3 times of water ultrasound interval 1 ~ 2h of extraction, be then transferred to Volatile oil extractor well-established law is back to oil reservoir and is not further added by, and oil reservoir is collected in condensation, and volatile oil is placed in less than 0 DEG C is precipitated crystallization, Obtain crystal D;
(5)By medicinal extract extract A, grease B, medicinal extract extract C and crystal D and appropriate mixed with propylene glycol, humectation increasing is obtained Pastil.
3. application of a kind of cigarette moist-keeping flavouring agent in cigarette as described in claim 1, which is characterized in that take the humectation Fumet after being diluted according to 0.01-0.1 ‰, is uniformly sprayed on pipe tobacco, naturally dry, is put down in 22 DEG C of temperature, humidity 60% time Weigh more than 10h, and pipe tobacco is made cigarette with Cigarette making device.
CN201711438744.1A 2017-12-27 2017-12-27 Cigarette moisture-retaining aroma-increasing agent Active CN108142977B (en)

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Publication number Priority date Publication date Assignee Title
CN110680010A (en) * 2019-10-31 2020-01-14 湖北中烟工业有限责任公司 Magnolia bark gel bead for cigarettes and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110680010A (en) * 2019-10-31 2020-01-14 湖北中烟工业有限责任公司 Magnolia bark gel bead for cigarettes and preparation method thereof

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