CN108142977B - Cigarette moisture-retaining aroma-increasing agent - Google Patents
Cigarette moisture-retaining aroma-increasing agent Download PDFInfo
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- CN108142977B CN108142977B CN201711438744.1A CN201711438744A CN108142977B CN 108142977 B CN108142977 B CN 108142977B CN 201711438744 A CN201711438744 A CN 201711438744A CN 108142977 B CN108142977 B CN 108142977B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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Abstract
The invention discloses a cigarette moisture-retaining aroma-increasing agent which is prepared from the following raw materials in parts by weight: 25-35 parts of discolor cinquefoil herb, 15-30 parts of aleppo avens, 12-20 parts of fritillaria Hubei, 9-15 parts of magnolia officinalis flowers and a proper amount of propylene glycol, wherein the preparation method comprises the following steps: (1) preparing the potentilla discolor by weight parts to obtain an extract A; (2) preparing the blue cloth in parts by weight into an oily substance B; (3) preparing the fritillaria Hupehensis in parts by weight into an extract C; (4) preparing the magnolia flower in parts by weight into a crystal D; (5) and mixing the extract A, the oily matter B, the extract C and the crystalline matter D with a proper amount of propylene glycol to obtain the moisture-retaining flavor enhancer. The product of the invention is sprayed on tobacco shreds, and plays a significant role in keeping moisture and increasing flavor for cigarettes.
Description
Technical Field
The invention relates to the technical field of cigarette additives, in particular to a cigarette moisture-retaining aroma-increasing agent.
Background
In the prior art, the core competitiveness of Chinese style cigarettes is to form the characteristic style of products, reflect individuation and differentiation and adapt to the smoking habits and consumption needs of vast consumers in China. The essence and spice for Chinese style cigarettes is the 'soul' of Chinese style cigarette products, and is the mysterious place formed by the style characteristics of Chinese style cigarettes. The scientific flavoring and casing in the cigarette is an important means for highlighting the personalized style of the cigarette product. Meanwhile, in order to improve the safety of smoking, the harm reduction and the tar reduction become an important component of Chinese style cigarettes. The tar of the cigarette is reduced, and simultaneously, the smoke concentration and the fragrance are improved, and only the flavoring and feeding technology is used. With the deepening of harm and tar reduction work of Chinese style cigarettes, the importance of tobacco flavoring and casing is increasingly shown.
The essence and spice for Chinese cigarettes with independent intellectual property rights and a new technology are built, the essence and spice are extracted from natural herbal plants, the health idea is led to consumers along with the elegant fragrance of the cigarettes, and the essence and spice is one of basic researches for developing Chinese cigarettes.
The research on increasing aroma and keeping moisture of cigarettes is an important foundation for constructing a Chinese-style cigarette core technology and forming a characteristic style of a cigarette product. The aroma enhancement and moisture retention technology is one of key technologies for continuously improving the smoking pleasure, the comfort level and the physical moisture retention performance of the cigarettes. In recent years, the tobacco industry in China participates in international competition to a greater extent, and faces severe market competition and challenges. At present, compared with the famous international cigarette brands, domestic cigarette products have certain defects in aspects of fragrance amount, sense organ comfort and the like. In addition, along with the comprehensive and deep development of the work of the Chinese government for fulfilling the tobacco control frame convention and the continuous enhancement of the social concern on smoking and health problems, cigarettes with high fragrance, low tar and low harm become the inevitable trend of industrial development. This trend will lead to more intensive research on the cigarette aroma enhancement and moisture retention technology. Thirdly, the cigarette quality fluctuation caused by the weak adaptability across regions of the cigarette products in different degrees is also a problem which needs to be solved urgently for increasing the aroma and keeping the moisture of the cigarettes.
The ideal humectant has two effects of moisture retention and moisture prevention, namely, the sensitivity of the moisture content of the cigarettes to the change of the environmental temperature and humidity is reduced, and the moisture content of the cigarettes is always kept in a relatively stable range. Because the moisture retention of the cigarette not only includes physical moisture retention, but also includes sensory moisture retention. Physical moisture retention, i.e., moisture retention, refers to the maintenance of moisture in tobacco leaves, and aims to improve the processing resistance of tobacco shreds and maintain the moisture in smoke. The sense moisturizing is to directly solve the problem of mouthfeel and improve dry feeling, irritation, aftertaste and the like.
The development of physical moisture-retaining agents has been carried out from both hydrophilic water-retaining substances and hydrophobic water-blocking substances. The research of the hydrophilic physical moisture retention monomer needs to pay attention to varieties with remarkable advantages in moisture retention in natural plants and aquatic organisms, carry out the work of extracting and purifying the effective components of the natural plants and develop a novel natural moisture retention agent; in addition, chemical modification of polysaccharides may be an important approach for development of hydrophilic moisturizing monomers. The hydrophobic physical moisture-retention monomer has a moisture-insulation effect, and a water-insulation film needs to be formed on the surface of the tobacco leaves, so that sugar ester or polyol ester substances can be chemically synthesized, and the influence of the esterification degree and the fatty acid chain length on the formation of the water-insulation film and the water-insulation effect can be examined. On the basis, the physical moisture-retaining monomers are reasonably compounded in a targeted manner, and a novel physical moisture-retaining agent which can improve the physical quality and meet the sensory quality requirement is developed.
The smoke has proper moisture, is soft and fine, and has small stimulation to human body; when the moisture content in the mainstream smoke is low, the dry sensation of the smoke is enhanced, the irritation is increased, and the comfort is reduced. The dry feeling of the cigarette is mainly determined by the moisture of the smoke and is also related to the feeling of the cigarette irritation. Not only reducing the irritation and increasing the feeling of promoting the secretion of body fluid in the smoke, but also being beneficial to reducing the dry feeling of the cigarette and reducing the irritation of the cigarette. Therefore, in the research and development of novel humectants, the research of sensory humectants directed to the taste is also one of important contents.
Disclosure of Invention
The invention aims to provide a cigarette moisture-retaining aroma-increasing agent prepared by taking potentilla discolor, aleppo avens, Hubei fritillary and officinal magnolia flower as raw materials, and the cigarette moisture-retaining aroma-increasing agent is used as a tobacco product additive in cigarettes and makes a contribution to improving the quality of Chinese cigarettes.
The invention discloses a cigarette moisture-retaining aroma-increasing agent which is prepared from the following raw materials in parts by weight: 25-35 parts of discolor cinquefoil herb, 15-30 parts of aleppo avens, 12-20 parts of Hubei fritillary bulb, 9-15 parts of magnolia officinalis flowers and a proper amount of propylene glycol.
The preparation method of the cigarette moisture-retaining flavor enhancer comprises the following steps:
(1) drying the whole plant of the potentilla discolor in parts by weight at 50-60 ℃ for 6-8 hours, crushing, adding 2-3 times of 70% ethanol, performing ultrasonic intermittent extraction for 1-2 hours, heating and refluxing at 75-95 ℃ for 3-5 hours, extracting at 85 ℃ for 2-3 hours with 50% ethanol, collecting reflux extracting solution, and performing reduced pressure concentration to obtain an extract A;
(2) drying the whole plant of the bluegrass in parts by weight, grinding, sequentially percolating with 95% ethanol and 75% diethyl ether in volume fraction, combining filtrates, concentrating to obtain an extract, adding a proper amount of water into the extract for dispersing, extracting with n-butanol and n-hexane for 2-3 times respectively, removing water with anhydrous sodium sulfate, and filtering to obtain an oily substance B with special smell;
(3) grinding the fritillaria Hupehensis in parts by weight, adding 50-70% ethanol, performing ultrasonic primary extraction for 10min, then transferring to water bath extraction equipment for extraction for 6h, cooling, filtering, collecting extract, extracting for 1-2 times according to the method, combining the extract, and concentrating to obtain an extract C.
(4) Grinding the magnolia officinalis flowers in parts by weight into powder, adding 2-3 times of water, performing ultrasonic intermittent extraction for 1-2 hours, then returning to a volatile oil extractor in a normal method until an oil layer is not increased any more, condensing and collecting the oil layer, and putting the volatile oil below 0 ℃ to separate out crystals to obtain a crystal D;
(5) and mixing the extract A, the oily matter B, the extract C and the crystalline matter D with a proper amount of propylene glycol to obtain the moisture-retaining flavor enhancer.
The cigarette moisture-retaining flavor enhancer is applied to cigarettes in the following manner: diluting the moisture-keeping flavor enhancer by 0.01-0.1 per mill, uniformly spraying onto tobacco shreds, naturally drying, balancing at 22 deg.C and humidity of 60% for more than 10 hr, and making into cigarette with cigarette maker.
Compared with the prior art, the invention has the advantages and positive effects that:
potentilla discolor is a plant of Potentilla of Rosaceae, has mild nature and sweet taste, contains flavone, terpenoids, steroids, tannin, organic acid, adenosine, dolichol, azelaic acid, SOD enzyme, and polysaccharide. Has antiinflammatory, analgesic, antioxidant, blood sugar lowering, antibacterial, and antiviral effects. In the process of smoking cigarettes, macromolecular and alcohol compounds are cracked to generate a large amount of micromolecular phenolic acid compounds and sugar or components with strong stir-fried fruit fragrance and the like, so that the cigarette fragrance is clear, soft, mellow, full and smooth, the taste is sweet and comfortable, and the cigarette has the characteristics of flat and long aftertaste.
The blue cloth mainly comprises fatty acid, fatty acid methyl ester, terpenes, oxygen-containing derivatives thereof and the like, wherein the high content of the volatile components comprises macromolecules such as palmitic acid, 11, 14, 17-eicosatrienoic acid methyl ester, linoleic acid, caryophyllene oxide, eugenol, trans-phytol and the like, and aroma-causing components such as β -caryophyllene, β -elemene, citronellol, germacrone and epigalloketone, the macromolecules such as fatty acid and the like are attached to the surface layer of the cut tobacco, and a protective film is generated on the surface of the cut tobacco, so that the cut tobacco has the moisture retention property and the moisture resistance, meanwhile, the moisture cannot be absorbed from the outside in a high-humidity environment, so that the double effects of moisture retention and moisture resistance are achieved, the aroma component can effectively increase the aroma of the cigarette, improve the quality and harmony of the cigarette, reduce the odor and the irritation, increase the sweet feeling, make the residual taste more clean and the integral quality of the cigarette.
The Bulbus Fritillariae Hupehensis is bulb of Bulbus Fritillariae Hupehensis of Liliaceae, and contains many alkaloids, fatty acids, and terpenoids. Research shows that the Hubei fritillary bulb has various pharmacological effects of clearing heat, moistening lung, relieving cough, eliminating phlegm, relieving asthma and the like, and relieving cough, eliminating phlegm, relieving asthma and the like.
The flos Magnoliae officinalis is dry flower bud of Magnoliaceae plant cortex Magnolia officinalis or Magnolia officinalis with bitter taste and mild nature. Has effects of eliminating dampness with aromatics, regulating qi-flowing, and relieving epigastric distention, and can be used for treating spleen and stomach dampness obstruction and qi stagnation, chest and gastric cavity stuffiness and distention, and anorexia. Magnolia officinalis flower
Mainly contains magnolol, Camphora, volatile oil, etc., and also contains oligosaccharide and polysaccharide moisture keeping components, and the volatile oil of flos Magnoliae officinalis mainly contains hemiterpene compounds, aliphatic compounds, and aromatic compounds.
The invention adopts pure natural raw materials, is prepared according to the compatibility theory of natural spices and by adopting a compounding technology, is not added with chemical additives, has special sweet and fragrant smell, fully exerts the efficacy of natural plant extracts, can play the roles of reducing the dry sensation of oral cavity and throat and relieving the irritation of smoke, and simultaneously has the advantages of moisture retention, strong water resistance and moisture resistance, so that the cigarette does not stick to lips when being smoked. The invention is used as a tobacco additive, has obvious effect and has good application prospect for developing Chinese style cigarette products with special style.
Detailed Description
The technical scheme of the invention is explained in detail by combining the following embodiments:
example 1
A cigarette moisture-retaining flavor enhancer is prepared from the following raw materials in parts by weight: 25 parts of discolor cinquefoil herb, 15 parts of aleppo avens, 12 parts of Hubei fritillary bulb, 9 parts of officinal magnolia flower and a proper amount of propylene glycol.
The preparation method of the cigarette moisture-retaining flavor enhancer comprises the following steps:
(1) drying the whole plant of the discolor cinquefoil herb in parts by weight at 60 ℃ for 6h, crushing, adding 3 times of 70% ethanol, performing ultrasonic intermittent extraction for 2h, heating and refluxing at 95 ℃ for 3, extracting at 85 ℃ for 23h by using 50% ethanol, collecting refluxed extracting solution, and performing reduced pressure concentration to obtain an extract A;
(2) drying the whole plant of the bluegrass in parts by weight, grinding, sequentially percolating with 95% ethanol and 75% diethyl ether in volume fraction, combining filtrates, concentrating to obtain an extract, adding a proper amount of water into the extract for dispersing, respectively extracting with n-butanol and n-hexane for 3 times, removing water with anhydrous sodium sulfate, and filtering to obtain an oily substance B with special smell;
(3) grinding the fritillaria Hupehensis in parts by weight, adding 70% ethanol, performing ultrasonic primary extraction for 10min, then transferring to water bath extraction equipment for extraction for 6h, cooling, filtering, collecting extract, extracting for 2 times according to the method, combining the extract, and concentrating to obtain an extract C.
(4) Grinding the magnolia officinalis flowers in parts by weight into powder, adding 2 times of water, performing ultrasonic intermittent extraction for 2 hours, then returning to a volatile oil extractor in a normal method until an oil layer is not increased any more, condensing and collecting the oil layer, and putting the volatile oil below 0 ℃ to separate out crystals to obtain a crystal D;
(5) and mixing the extract A, the oily matter B, the extract C and the crystalline matter D with a proper amount of propylene glycol to obtain the moisture-retaining flavor enhancer.
Example 2
A cigarette moisture-retaining flavor enhancer is prepared from the following raw materials in parts by weight: 35 percent of discolor cinquefoil herb, 30 percent of blue cloth, 20 percent of Hubei fritillary bulb, 15 percent of officinal magnolia flower and proper amount of propylene glycol.
The preparation method of the cigarette moisture-retaining flavor enhancer comprises the following steps:
(1) drying the whole plant of the discolor cinquefoil herb in parts by weight at 50 ℃ for 8h, crushing, adding 2 times of 70% ethanol, performing ultrasonic intermittent extraction for 2h, heating and refluxing at 75 ℃ for 5h, extracting at 85 ℃ for 2h by using 50% ethanol, collecting reflux extracting solution, and performing reduced pressure concentration to obtain an extract A;
(2) drying the whole plant of the bluegrass in parts by weight, grinding, sequentially percolating with 95% ethanol and 75% diethyl ether in volume fraction, combining filtrates, concentrating to obtain an extract, adding a proper amount of water into the extract for dispersing, respectively extracting with n-butanol and n-hexane for 2 times, removing water with anhydrous sodium sulfate, and filtering to obtain an oily substance B with special smell;
(3) grinding the fritillaria Hupehensis in parts by weight, adding 55% ethanol, performing ultrasonic primary extraction for 10min, then transferring to water bath extraction equipment for extraction for 6h, cooling, filtering, collecting extract, extracting for 1 time according to the method, combining the extract, and concentrating to obtain an extract C.
(4) Grinding the magnolia officinalis flowers in parts by weight into powder, adding 2 times of water, performing ultrasonic intermittent extraction for 1 hour, then transferring into a volatile oil extractor, performing normal reflux until an oil layer is not increased any more, condensing and collecting the oil layer, and placing the volatile oil below 0 ℃ to separate out crystals to obtain a crystal D;
(5) and mixing the extract A, the oily matter B, the extract C and the crystalline matter D with a proper amount of propylene glycol to obtain the moisture-retaining flavor enhancer.
Example 3
A cigarette moisture-retaining flavor enhancer is prepared from the following raw materials in parts by weight: 30 parts of discolor cinquefoil herb, 18 parts of aleppo avens, 15 parts of Hubei fritillary bulb, 12 parts of officinal magnolia flower and a proper amount of propylene glycol.
The preparation method of the cigarette moisture-retaining flavor enhancer comprises the following steps:
(1) drying the whole plant of the discolor cinquefoil herb in parts by weight at 55 ℃ for 7h, crushing, adding 2 times of 70% ethanol, performing ultrasonic intermittent extraction for 2h, heating and refluxing at 85 ℃ for 3h, extracting at 85 ℃ for 5h by using 50% ethanol, collecting refluxed extracting solution, and performing reduced pressure concentration to obtain an extract A;
(2) drying the whole plant of the bluegrass in parts by weight, grinding, sequentially percolating with 95% ethanol and 75% diethyl ether in volume fraction, combining filtrates, concentrating to obtain an extract, adding a proper amount of water into the extract for dispersing, respectively extracting with n-butanol and n-hexane for 2 times, removing water with anhydrous sodium sulfate, and filtering to obtain an oily substance B with special smell;
(3) grinding the fritillaria Hupehensis in parts by weight, adding 65% ethanol, performing ultrasonic primary extraction for 10min, then transferring to water bath extraction equipment for extraction for 6h, cooling, filtering, collecting extract, extracting for 2 times according to the method, combining the extract, and concentrating to obtain an extract C.
(4) Grinding the magnolia officinalis flowers in parts by weight into powder, adding 2 times of water, performing ultrasonic intermittent extraction for 1 hour, then transferring into a volatile oil extractor, performing normal reflux until an oil layer is not increased any more, condensing and collecting the oil layer, and placing the volatile oil below 0 ℃ to separate out crystals to obtain a crystal D;
(5) and mixing the extract A, the oily matter B, the extract C and the crystalline matter D with a proper amount of propylene glycol to obtain the moisture-retaining flavor enhancer.
Test examples
(I) evaluation of moisturizing Effect
1. The test purpose is as follows: comparing the physical humidity keeping effect of the tobacco shred containing the humidity keeping and flavor enhancing agent with the tobacco shred containing propylene glycol (contrast) and blank tobacco shred (blank) under the same condition.
2. Test sample
Moisture-retaining flavor enhancer: 1% moisture-retaining aroma-increasing agent and middle-grade blank cut tobacco
Comparison: 1% propylene glycol and medium-grade blank tobacco shred
Blank: middle-grade blank tobacco shred
3. Test method
3.1 equilibration process: after the three groups of samples in the examples 1-3 are respectively diluted according to 0.01-0.1 per mill, the diluted samples are uniformly sprayed on the cut tobacco, and simultaneously, the cut tobacco and the control samples and the blank group samples are placed at the temperature: (22 ± 1) ° c, humidity: and (60 +/-3)% of the water content in the constant temperature and humidity chamber is balanced for 48 hours, and the initial water content of each group of test samples is measured by an oven method, namely the water content of 0 hour.
3.2 test procedure: adjusting the environment of the constant temperature and humidity box to be temperature: (22 ± 1) ° c, humidity: (40 ± 3)%, the above test samples were placed in the test tube, the sample weight was measured once at a certain time interval, and the instant water content was calculated from the sample weight at that time, and the results are shown in table 1 below:
TABLE 1 moisture content (%). In time
The moisturizing effect evaluation results in table 1 all show that: the invention has obvious moisturizing effect on the cut tobacco.
(II) sensory evaluation
Reference is made to GB5606.4-2005 cigarette part 4: sensory technical requirements and YC/T497-:
TABLE 2 cigarette sensory evaluation
The sensory evaluation results in Table 2 all show that the cigarettes added with the moisture-retaining flavor enhancer of the invention examples 1-3 have pleasant fresh scent of the smoke and obvious sweet feeling, can play the roles of reducing the dry feeling of the oral cavity and the throat and relieving the smoke irritation in the smoking process of the cigarettes, and are suitable for high-quality cigarettes.
The above embodiments are merely preferred embodiments of the present invention, and any simple modification, modification and substitution changes made to the above embodiments according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (2)
1. The cigarette moisture-retaining flavor enhancer is characterized by being prepared from the following raw materials in parts by weight: 25-35 parts of potentilla discolor, 15-30 parts of aleppo avens, 12-20 parts of Hubei fritillary bulb, 9-15 parts of magnolia officinalis flowers and a proper amount of propylene glycol;
the preparation method comprises the following steps:
(1) drying the whole plant of the potentilla discolor in parts by weight at 50-60 ℃ for 6-8 hours, crushing, adding 2-3 times of 70% ethanol, performing ultrasonic intermittent extraction for 1-2 hours, heating and refluxing at 75-95 ℃ for 3-5 hours, extracting at 85 ℃ for 2-3 hours with 50% ethanol, collecting reflux extracting solution, and performing reduced pressure concentration to obtain an extract A;
(2) drying the whole plant of the bluegrass in parts by weight, grinding, sequentially percolating with 95% ethanol and 75% diethyl ether in volume fraction, combining filtrates, concentrating to obtain an extract, adding a proper amount of water into the extract for dispersing, extracting with n-butanol and n-hexane for 2-3 times respectively, removing water with anhydrous sodium sulfate, and filtering to obtain an oily substance B with special smell;
(3) grinding the fritillaria Hupehensis in parts by weight, adding 50-70% ethanol, performing ultrasonic primary extraction for 10min, then transferring to water bath extraction equipment for extraction for 6h, cooling, filtering, collecting extract, extracting the extract for 1-2 times according to the method, combining the extract, and concentrating to obtain an extract C;
(4) grinding the magnolia officinalis flowers in parts by weight into powder, adding 2-3 times of water, performing ultrasonic intermittent extraction for 1-2 hours, then returning to a volatile oil extractor in a normal method until an oil layer is not increased any more, condensing and collecting the oil layer, and putting the volatile oil below 0 ℃ to separate out crystals to obtain a crystal D;
(5) and mixing the extract A, the oily matter B, the extract C and the crystalline matter D with a proper amount of propylene glycol to obtain the moisture-retaining flavor enhancer.
2. The application of the cigarette moisture-retaining flavor enhancer of claim 1 in cigarettes, wherein the moisture-retaining flavor enhancer is diluted by 0.01-0.1 per thousand, uniformly sprayed on tobacco shreds, naturally dried, balanced at the temperature of 22 ℃ and the humidity of 60% for more than 10 hours, and the tobacco shreds are made into cigarettes by a cigarette making device.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102613694A (en) * | 2012-03-27 | 2012-08-01 | 广西中烟工业有限责任公司 | Application of natural tobacco additive with effects of increasing aroma and preserving moisture |
| CN105167176A (en) * | 2015-08-18 | 2015-12-23 | 浙江中烟工业有限责任公司 | Composite tobacco humectant and composite tobacco humectant preparation method and application of composite tobacco humectant |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102613694A (en) * | 2012-03-27 | 2012-08-01 | 广西中烟工业有限责任公司 | Application of natural tobacco additive with effects of increasing aroma and preserving moisture |
| CN105167176A (en) * | 2015-08-18 | 2015-12-23 | 浙江中烟工业有限责任公司 | Composite tobacco humectant and composite tobacco humectant preparation method and application of composite tobacco humectant |
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| Title |
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| 蓝布正等四种药用植物化学成分的研究;王莉宁;《中国优秀硕士学位论文全文数据库 医药卫生科技辑》;20090115(第01期);第15页 * |
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