CN108101518A - 毛细管 - Google Patents
毛细管 Download PDFInfo
- Publication number
- CN108101518A CN108101518A CN201711036078.9A CN201711036078A CN108101518A CN 108101518 A CN108101518 A CN 108101518A CN 201711036078 A CN201711036078 A CN 201711036078A CN 108101518 A CN108101518 A CN 108101518A
- Authority
- CN
- China
- Prior art keywords
- capillary
- grinding
- micron
- fine grain
- zirconium oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5445—Particle size related information expressed by the size of the particles or aggregates thereof submicron sized, i.e. from 0,1 to 1 micron
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5454—Particle size related information expressed by the size of the particles or aggregates thereof nanometer sized, i.e. below 100 nm
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/602—Making the green bodies or pre-forms by moulding
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/602—Making the green bodies or pre-forms by moulding
- C04B2235/6021—Extrusion moulding
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/94—Products characterised by their shape
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Materials For Medical Uses (AREA)
Abstract
本发明公开了一种毛细管,用于电外科手术器械电极环等的绝缘,由细晶粒纳微粒径高纯氧化铝粉,纳微粒径氧化锆增韧细晶粒纳微粒径高纯氧化铝粉经混料练泥、陈腐、熟化、挤出、干燥、烧结等工序制成长的陶瓷管;经切断、里孔研磨、外圆同心磨、端面磨削工序制成毛细管。这样的毛细管,机械强度高,同心,壁厚均匀,电气绝缘强度高。
Description
技术领域
本发明涉及微创医疗技术领域汽化电切镜等电切环绝缘用毛细管。
背景技术
微创医疗技术对设备的小型化、微型化提出了更高要求。而电外科手术器械汽化电切镜等用的电切环对电极的绝缘强度和机械强度提出很高要求:机械强度足够高,安装时能够承受一定外力而不能折断、破裂;电气绝缘强度足够高,壁厚0.20mm的毛细管要能承受直流3000V、3秒电压而不击穿。尺寸要小巧,满足紧凑空间狭小条件。苛刻的技术要求对电切环用绝缘材料的选择提出了挑战:外径尺寸要小,以便插入很细的电极支撑体;内径要大,方便穿入电极和绝缘胶。机械强度足够高:能够承受一定外力而不损坏。电气绝缘强度足够高:承受直流高电压而不击穿。
发明内容
本发明要解决的技术问题是提供一种尺寸小巧、机械强度高、电气绝缘高的电切环电极等用毛细管。
为解决上述技术问题,本发明的技术方案是:使用细晶粒纳微粒径高纯陶瓷粉,对细晶粒纳微粒径高纯陶瓷粉增韧改性提高机械性能。细晶粒超细陶瓷份加入黏合剂增塑剂溶剂制成柔软的坯料,放进液压挤出机挤成坯体,干燥,烧结。对烧成后的毛细管切断,精密研磨里孔,以里孔定位在同心磨上磨削外圆,保证毛细管同心,壁厚一致。
该技术方案制成的毛细管,同心度好,机械强度高,电气绝缘强度高,方便电切环的制造,延长电切环使用寿命,降低医生手术强度,患者手术体验更佳。
附图说明
下面结合附图对本发明作进一步详细说明。
附图1是本发明毛细管的剖面图。
具体实施方式
下面结合实例说明:
实施例1
1kg细晶粒、200nm的99.9%氧化铝粉,与70g羧甲级纤维素,混合,球磨24h。倒在瓷盆里,加入50g桐油,再加入220g蒸馏水,拌和均匀,制成面团。用干净塑料布密封瓷盆,陈腐24h。放面团到挤出机,挤成管坯,干燥,装窑,烧结。烧成的陶瓷管,切断,研磨里孔。磨好里孔的毛细管,穿在精磨好的钢丝上,固定在同心磨夹具上,拉紧钢丝,开动同心磨,加工毛细管到图纸要求的尺寸。从钢丝上取下磨好外径的毛细管,装在夹具里,在数显平面磨床上,磨削到图纸要求的长度。
实施例2
100g粒径80nm的氧化锆粉与900g细晶粒、150nm的99.9%氧化铝粉,混合,球磨24h。倒在瓷盆里,加入230g液态羧甲级纤维素,拌和均匀,制成面团。用干净塑料布密封瓷盆,陈腐24h。放面团到挤出机,挤成管坯,干燥,装窑,烧结。烧成的陶瓷管,切断,研磨里孔。磨好里孔的毛细管,穿在精磨好的钢丝上,固定在同心磨夹具上,拉紧钢丝,开动同心磨,加工毛细管到图纸要求的尺寸。从钢丝上取下磨好外径的毛细管,装在夹具里,在数显平面磨床上,磨削到图纸要求的长度。
实施例3
100g粒径80nm的氧化锆粉与900g细晶粒、150nm的99.9%氧化铝粉,混合,球磨24h。与120g石蜡一起倒入真空和蜡机里抽真空,加热,搅拌,制成陶瓷蜡饼。加热蜡饼倒入热压铸机蜡桶,维持流动状态。压铸成型。经脱蜡,烧结,制成陶瓷毛坯。经里外孔加工,端面磨削,制成毛细管。
Claims (15)
1.一种毛细管,用陶瓷材料、黏合剂、增塑剂和水制成陶瓷坯料,陈腐24小时,放入液压挤出机,挤出成长度约2m管坯,平放在平板上,自然干燥,干燥好的管坯挂在立式烧成窑顶棚碳化硅横梁上,用吊车放顶棚到烧成窑的顶部,形成密封的窑体,按烧成曲线经升温、保温、降温等工序,完成毛细管毛坯烧成;切断毛细管毛坯到一定长度,研磨里孔到要求的尺寸,研磨好里孔的毛细管穿在精磨过的钢丝上,钢丝固定在磨床上,绷紧钢丝,开动磨床,磨削毛细管毛坯到要求的直径;磨好外径的毛细管,用夹具固定好,在磨床上磨削到一定尺寸,成为符合图纸要求的产品。
2.一种毛细管,用陶瓷蜡饼,热压铸成型,烧结,研磨里孔,磨削外圆,端磨长度到要求尺寸。
3.如权利要求1所述的毛细管,其特征在于:毛细管内径0.3~0.8mm,壁厚0.2~0.4mm。
4.如权利要求1所述的毛细管,其特征在于:所述陶瓷材料是细晶粒纳微米尺寸高纯氧化铝粉、纳微米尺寸氧化锆增韧细晶粒纳微米尺寸氧化铝粉。
5.如权利要求1所述的毛细管,其特征在于:所述黏合剂是糊精、聚乙烯醇、羧甲基纤维素、聚醋酸乙烯酯、聚苯乙烯等。
6.如权利要求1所述的毛细管,其特征在于:所述增塑剂是甘油、太酸二丁酯、草酸乙酯、己酸三甘醇酯等。
7.如权利要求1所述的毛细管,其特征在于:所述水是蒸馏水、去离子水等。
8.如权利要求1所述的毛细管,其特征在于:切断是在数显切断机上完成的。
9.如权利要求1所述的毛细管,其特征在于:里孔研磨是在扩孔机上完成的。
10.如权利要求1所述的毛细管,其特征在于:外径磨削是在同心磨上实现的。
11.如权利要求1所述的毛细管,其特征在于:长度磨削是在端面磨床、数显平面磨上完成。
12.如权利要求4所述的陶瓷材料,其特征在于:所述纳微米尺寸陶瓷粉是指粒径50nm~300nm。
13.如权利要求4所述的陶瓷材料,其特征在于:纳微米尺寸氧化锆增韧细晶粒纳微米尺寸氧化铝粉的氧化锆质量比是5%~10%,优选氧化锆质量比是10%。
14.如权利要求2所述的毛细管,其特征在于:所述陶瓷材料是细晶粒纳微米尺寸高纯氧化铝粉、纳微米尺寸氧化锆增韧细晶粒纳微米尺寸氧化铝粉。
15.如权利要求2所述的毛细管,其特征在于:所述蜡是石蜡。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2017201984806 | 2017-03-02 | ||
CN201720198480 | 2017-03-02 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN108101518A true CN108101518A (zh) | 2018-06-01 |
CN108101518B CN108101518B (zh) | 2020-12-29 |
Family
ID=62206286
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201711036078.9A Active CN108101518B (zh) | 2017-03-02 | 2017-10-28 | 毛细管 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN108101518B (zh) |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5333962B2 (zh) * | 1972-09-06 | 1978-09-18 | ||
JPH06314721A (ja) * | 1993-04-28 | 1994-11-08 | Kyocera Corp | ワイヤボンディング用キャピラリ |
CN101683663A (zh) * | 2008-09-28 | 2010-03-31 | 刘文军 | 一种毛细管加工工艺 |
CN201872021U (zh) * | 2010-08-05 | 2011-06-22 | 常熟市创新陶瓷有限公司 | 细长陶瓷管内孔磨削装置 |
CN102515768A (zh) * | 2011-12-26 | 2012-06-27 | 宁波伏尔肯机械密封件制造有限公司 | 一种碳化硅陶瓷管的制备方法 |
CN105801094A (zh) * | 2016-03-01 | 2016-07-27 | 深圳市商德先进陶瓷有限公司 | 毛细管陶瓷体及其制造方法与应用 |
-
2017
- 2017-10-28 CN CN201711036078.9A patent/CN108101518B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5333962B2 (zh) * | 1972-09-06 | 1978-09-18 | ||
JPH06314721A (ja) * | 1993-04-28 | 1994-11-08 | Kyocera Corp | ワイヤボンディング用キャピラリ |
CN101683663A (zh) * | 2008-09-28 | 2010-03-31 | 刘文军 | 一种毛细管加工工艺 |
CN201872021U (zh) * | 2010-08-05 | 2011-06-22 | 常熟市创新陶瓷有限公司 | 细长陶瓷管内孔磨削装置 |
CN102515768A (zh) * | 2011-12-26 | 2012-06-27 | 宁波伏尔肯机械密封件制造有限公司 | 一种碳化硅陶瓷管的制备方法 |
CN105801094A (zh) * | 2016-03-01 | 2016-07-27 | 深圳市商德先进陶瓷有限公司 | 毛细管陶瓷体及其制造方法与应用 |
Also Published As
Publication number | Publication date |
---|---|
CN108101518B (zh) | 2020-12-29 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP2604592B2 (ja) | 金属、セラミック粉末等の成形方法及びそのための組成物 | |
US9790129B2 (en) | Method of fabricating high light transmission zirconia blanks for milling into natural appearance dental appliances | |
TWI430975B (zh) | 陶瓷擠壓成形體用組成物及陶瓷擠壓成形體之製造方法 | |
CN110128115A (zh) | 一种闪烧制备氧化物共晶陶瓷的方法 | |
CN108203300B (zh) | 一种高韧性、高电阻率碳化硅陶瓷的制备方法 | |
US9822041B2 (en) | Ceramic honeycomb bodies including cold set plugs | |
CN108101518A (zh) | 毛细管 | |
JP6218617B2 (ja) | 歯科用ジルコニア質焼結体、クラウン用フレーム、ブリッジ用フレーム | |
JP5036110B2 (ja) | 軽量セラミック焼結体 | |
TW201602054A (zh) | 多孔質陶瓷的製造方法及多孔質陶瓷 | |
JP2019133951A (ja) | 点火プラグ用絶縁体のための合成物、および、点火プラグ用絶縁体を製造する方法 | |
CN110041056A (zh) | 一种氧化铝陶瓷发热管及其制备方法 | |
JP6266596B2 (ja) | 誘電体磁器焼成体及び複合セラミックス構造体 | |
CN113263611A (zh) | 一种管式陶瓷及其制备方法、模具和支撑体制备方法 | |
KR101379203B1 (ko) | 고체산화물형 연료전지 지지체의 제조방법 | |
CN105906340B (zh) | 采用固相氮气烧结法制备二氧化钛基巨介电陶瓷材料的方法 | |
JPH1171188A (ja) | 多孔質体の製造方法 | |
CN105753455B (zh) | 一种氧化铝陶瓷柱塞的制备方法 | |
JP5164385B2 (ja) | 押出成形装置 | |
CN108558396A (zh) | 火焰喷涂用高纯细晶氧化锆陶瓷条棒的制备方法 | |
CN103992104A (zh) | 一种采用溶胶凝胶法制备钛酸铜铋巨介电陶瓷材料的方法 | |
JP2004269290A (ja) | 透光性アルミナセラミックスの製造方法、透光性アルミナセラミックス、高圧放電灯用発光容器、造粒粉末および成形体 | |
JP3283346B2 (ja) | 押出成形用坏土組成物 | |
KR20120043285A (ko) | 머시너블 세라믹 복합체 및 그 제조방법 | |
JP2002210717A (ja) | セラミックス成形体の製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CP02 | Change in the address of a patent holder | ||
CP02 | Change in the address of a patent holder |
Address after: Room 2336, Building 8, Taida Service Outsourcing Park, No. 19 Xinhuan West Road, Binhai New Area Development Zone, Tianjin, 300450 Patentee after: TIANJIN DEVELOPMENT AREA TIANDI INFORMATION TECHNOLOGY Co.,Ltd. Address before: Box 103, Balitai post office, 215 Weijin Road, Heping District, Tianjin 300070 Patentee before: TIANJIN DEVELOPMENT AREA TIANDI INFORMATION TECHNOLOGY Co.,Ltd. |