CN108078863A - A kind of bactericidal composition and Baby Care composition based on plant extracts - Google Patents
A kind of bactericidal composition and Baby Care composition based on plant extracts Download PDFInfo
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- CN108078863A CN108078863A CN201810082063.4A CN201810082063A CN108078863A CN 108078863 A CN108078863 A CN 108078863A CN 201810082063 A CN201810082063 A CN 201810082063A CN 108078863 A CN108078863 A CN 108078863A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of bactericidal composition based on plant extracts, including following weight percent composition：1.0 3.0% grape Fructus Citri grandis extract, 3.0 10.0% the bark of official magnolia bark extract, 3.0 8.0% ginger-root extract, 3.0 8.0% pepper extract and 71 90% polyalcohol.The composition of the present invention has prominent performance in terms of durable antibiotic.Composition Fructus Citri grandis extract containing grape, the bark of official magnolia bark extract, ginger-root extract, pepper extract and polyalcohol, can effectively control in cosmetics be difficult to control most of bacteriums and mould, and property it is mild, it is non-stimulated, without thermal sensation, it is very safe.Said composition can effectively kill bacterium in cosmetics, mould, saccharomycete, and said composition ingredient does not exist《Cosmetics safety technical specification》In the mutatis mutandis preservative list of defined, meet the requirement of product " no anti-corrosion " concept.
Description
Technical field
The present invention relates to field of daily chemicals, particularly a kind of bactericidal composition based on plant extracts.
Background technology
Chinese patent application CN201510899803.X discloses a kind of plant origin cosmetics anticorrosive composite and its system
Preparation Method, it is special including the preservation blends that grapefruit seed extract, wild marjoram herb extract, the bark of official magnolia bark extract form
Sign is to carry out anti-corrosion synergy to the preservation blends using raspberry fruit extract and Flos Sophorae extract.The anti-corrosion is mixed
It closes object, raspberry fruit extract and Flos Sophorae extract to be coated by matrix material, forms sub-micrometer grain lotion.The matrix material
It is 5-10 by mass ratio：1-3:3-5：It is the mannose erythrose alcohol ester of 20-50, sodium bacillus subtilis lipopeptide, hydrogenated lyso lecithin, sweet
Oil composition.The invention anticorrosive composite irritation is low, favorable anti-corrosion effect.
The program must use raspberry fruit extract and Flos Sophorae extract to carry out anti-corrosion increasing to the preservation blends
Effect.
Chinese patent application CN201510522007.4 discloses a kind of organic natural plant preservative, raw material composition
For：Quickbeam berry extract, the bark of official magnolia bark extract, golden elder berry extract, trembling poplar bark extract, bright string
The radish root tunning filtrate of coccus fermenting and producing, honeysuckle flower extract, licorice, peony extract, typha orientalis carry
Take object, french lavender extract, grape fruit extract, Folium Artemisiae Argyi extract, moutan root bark extract, radix scutellariae root extract, big
Garlic extract, radix-polygoni multiflori extract, Gentrin Knotweed P.E, 1,2- pentanediols, 1,2- hexylene glycols.Organic natural plants of the invention are prevented
Rotten agent is used in skin care item form the protective system of skin care item, can effectively inhibit bacteria growth.
The program is combined using various plants extract, can be only achieved the antibacterial effect of comprehensive anticorrosive.
Chinese patent application CN201611073111.0 discloses a kind of antisepsis and sterilization composition, mainly contains shaddock pericarp and carries
0.1-1 parts of object, 0.1-1 parts of the bark of official magnolia bark extract, 0.1-1 parts of Artemisinin are taken, there is good antisepsis and sterilization effect,
And without finding being irritating to the skin property.
The embodiment of the program confirms that shaddock pericarp extract, the bark of official magnolia bark extract, Artemisinin are indispensable.
Chinese patent application CN201510801718.5 discloses a kind of natural plant preservative composition, and composition is by weight
Percentage calculation is measured, including：Bright string coccus/radish root tunning filtrate 1-10%, the bark of official magnolia bark extract 1-10%, radix scutellariae
Extract 1-10%, peony root extractive 1-10%, surplus are corn propylene glycol and water.The invention natural plant preservative combines
All raw materials of object are all natural, and the multiple efficacies ingredient being rich in is reconciled mutually, cooperateed with, and product is made to have significant anti-corrosion
Effect.
Above-mentioned file is can be found that by analysis：
1st, can not deny, the bark of official magnolia bark extract, quickbeam berry extract, grape Fructus Citri grandis extract have sterilization to imitate
Fruit.
2nd, above-mentioned file has apparent indispensable property in Composition Aspects.
The contribution of above-mentioned file is that there are extensive plants antimicrobial extracts in nature.It is in the prior art
Problem is：Based on existing discovery, how effectively to be combined, develop highly efficient, more rational composition.
As composition maximally efficient in above-mentioned documents, technical solution disclosed in CN201510899803.X also without
Method reaches excellent fungistatic effect in a short time.
Further as the prior art improves and improves, and technical staff also adopts except being considered as plant extracts
It is disclosed natural wide containing grapefruit seed extract with other components matching bacteriostasis methods, such as CN2015108753460
Anticorrosive composite is composed, containing grapefruit seed extract, a kind of hydroximic acid, a kind of aromatic alcohol and one or more polyalcohol,
The formula can keep efficient sterilizing efficiency in 7 day time.
By above-mentioned file it can be found that the fungicide based on plant composition is the trend of future development.It is necessary to open
It sends out the fungicide based on plant composition a greater variety of, makes that bactericidal effect is more preferable, formula is simpler.
The content of the invention
It is an object of the invention to provide a kind of bactericidal compositions based on plant extracts, and said composition is in durable antibiotic
Property aspect there is prominent performance.Composition Fructus Citri grandis extract containing grape, the bark of official magnolia bark extract, ginger-root extract, Chinese prickly ash carry
Object and polyalcohol are taken, can effectively control the most of bacteriums and mould being difficult to control in cosmetics, and property is mild, nothing
It stimulates, without thermal sensation, it is very safe.Said composition can effectively kill bacterium in cosmetics, mould, saccharomycete, and said composition
Ingredient does not exist《Cosmetics safety technical specification》In the mutatis mutandis preservative list of defined, meet wanting for product " no anti-corrosion " concept
It asks.
It is a further object of the present invention to provide one group of Fructus Citri grandis extract containing grape, the bark of official magnolia bark extract, ginger-root extract,
Application of the composition of pepper extract and polyalcohol in infant's preservative free product is prepared.Said composition is suitable for breast
In the products such as liquid, cream, shampoo and shower cream, additive amount is few, can reduce Cosmetic Manufacture cost, and will not be in cosmetics
The harmful substances such as release formaldehyde, do not stimulate mildly.
The present invention specific technical solution be：A kind of bactericidal composition based on plant extracts, including following weight
Percent composition：
The grape Fructus Citri grandis extract of 1.0-3.0%, the bark of official magnolia bark extract of 3.0-10.0%, the race of 3.0-8.0%
The polyalcohol of extract, the pepper extract of 3.0-8.0% and 71-90%.
Grape Fructus Citri grandis extract derives from grape fruit fruit, and natural origin, the extract is to Escherichia coli, Pseudomonas aeruginosa, gold
The viruses such as the fungies such as the bacteriums such as staphylococcus aureus, Candida albicans, bird flu are respectively provided with good inhibiting effect, may replace tight
Cruel chemical method inhibits bacteria, fungi, saccharomycete and virus, be a kind of whole day that can be used safely in food, cosmetics
Right preservative substance；The bark of official magnolia bark extract has broad spectrum antibacterial, and the magnolol contained is to Escherichia coli, Staphylococcus aureus
Bacterium, Salmonella, bacillus subtilis, saccharomyces cerevisiae and black-koji mould have efficient inhibitory action；Ginger-root extract contains
Some volatile oil has very strong antifungal activity, and race element and Diphenylheptane and flavone compound have stronger anti-corrosion
And antioxidation；Pepper extract contains volatile oil, alkaloid and amide substance, to Escherichia coli, Pseudomonas aeruginosa, gold
Staphylococcus aureus, Candida albicans etc. have good bacteriostasis；Polyalcohol can enhance anti-corrosion effect in the composition.
Said composition has cooperative synergism effect after combining, and can kill micro- life such as Most bacterial in cosmetics, mould, saccharomycete
Object, and not stimulating mildly, can effectively in reduction system surfactant irritation.
In the above-mentioned bactericidal composition based on plant extracts, including following weight percent composition：
The grape Fructus Citri grandis extract of 1.5-2.5%, the bark of official magnolia bark extract of 4-8%, ginger-root extract, the 5- of 5-7%
7% pepper extract and the polyalcohol of 75.5-84.5%.
In the above-mentioned bactericidal composition based on plant extracts, the polyalcohol includes glycerine, 1,2- the third two
Alcohol, 1,3-PD, 1,2- butanediols, 1,2- pentanediols, 1,5-PD, 3- [2- (ethylhexyl) oxygen] -1,2- propylene glycol
The combination of any one or more.
Meanwhile the invention also discloses a kind of Baby Care composition, contain 0.3-0.7wt%'s in the composition
Bactericidal composition as described above.
Compared with prior art, the beneficial effects of the present invention are：
The formula of the present invention has reached excellent anti-corrosion effect in the case of few dosage, and 5 is good with synergy.
Specifically, grape Fructus Citri grandis extract derives from grape fruit fruit, and natural origin, the extract is to Escherichia coli, green
The viruses such as the fungies such as the bacteriums such as purulence bacillus, staphylococcus aureus, Candida albicans, bird flu, which are respectively provided with, to be inhibited to make well
With；The bark of official magnolia bark extract has broad spectrum antibacterial, and the magnolol contained is to Escherichia coli, staphylococcus aureus, sramana
Family name bacillus, bacillus subtilis, saccharomyces cerevisiae and black-koji mould have efficient inhibitory action；The volatilization that ginger-root extract contains
Oil has a very strong antifungal activity, and race element and Diphenylheptane and flavone compound have stronger anti-corrosion and anti-oxidant
Effect；Pepper extract contains volatile oil, alkaloid and amide substance, to Escherichia coli, Pseudomonas aeruginosa, golden yellow grape
Coccus, Candida albicans etc. have good bacteriostasis；Polyalcohol can enhance anti-corrosion effect in the composition.Said composition
There is cooperative synergism effect with reference to rear, the microorganisms such as Most bacterial in cosmetics, mould, saccharomycete can be killed.
Specific embodiment
With reference to embodiment, technical scheme is described in further detail, but do not formed pair
Any restrictions of the present invention.
Embodiment 1
Said composition is applied in infant's cream product, and formula is as follows：
The preparation process of the cream product is as follows：
It is accurate to weigh A phase each components, it adds in oil phase pot, opens agitating and heating, be warming up to 85 DEG C, be completely dissolved, keep the temperature
10 minutes；
The accurate B phases each component that weighs is added in vacuum emulsification pot, opens homogenizer, is warming up to 90 DEG C or more, and homogeneous is to complete
Fully dissolved keeps the temperature 10 minutes；
A phases are pumped into vacuum emulsification pot, are pumped into while stirring, start homogenizer, fast homogeneous is after 6 minutes, heat preservation 10
Minute；
The C phase components that are dissipated with a small amount of moisture are added in, homogeneous is after 1 minute, insulated and stirred 15 minutes or more；
Emulsification pot chuck is passed through cooling water, is cooled to 45-50 DEG C, adds in D phases and E phase components, stirs；
Continue stirring to be cooled into cream and complete.
In the present embodiment, anticorrosive composite is carried by the grape Fructus Citri grandis extract of 2.0wt%, the Magnolia bark of 5.0wt%
The 1,2-PD of object, the ginger-root extract of 5.0wt%, the pepper extract of 5.0wt% and 83wt% is taken to form.
The preparation method of the anticorrosive composite is：Said components are uniformly mixed.
Comparative example 1
Comparative example 1 is formulated with embodiment 1, preparation process is similar, the difference is that the anticorrosive composite in comparative example 1 is not
Fructus Citri grandis extract containing grape, anticorrosive composite are by weight percentage：5% the bark of official magnolia bark extract, the extraction of 5% race
Object, 5% pepper extract and 85% 1,2-PD.
Comparative example 2
Comparative example 2 is formulated with embodiment 1, preparation process is similar, the difference is that the anticorrosive composite in comparative example 2 is not
Containing the bark of official magnolia bark extract, anticorrosive composite is by weight percentage：2% grape Fructus Citri grandis extract, the extraction of 5% race
Object, 5% pepper extract and 88% 1,2-PD.
Comparative example 3
Comparative example 3 is formulated with embodiment 1, preparation process is similar, the difference is that the anticorrosive composite in comparative example 3 is not
Containing ginger-root extract, anticorrosive composite is by weight percentage：2% grape Fructus Citri grandis extract, the extraction of 5% Magnolia bark
Object, 5% pepper extract and 88% 1,2-PD.
Comparative example 4
Comparative example 4 is formulated with embodiment 1, preparation process is similar, the difference is that the anticorrosive composite in comparative example 4 is not
Containing pepper extract, anticorrosive composite is by weight percentage：2% grape Fructus Citri grandis extract, the extraction of 5% Magnolia bark
Object, 5% ginger-root extract and 88% 1,2-PD.
Embodiment 2
Said composition is applied in infant's shampoo product, and formula is as follows：
The preparation process of the shampoo product is as follows：
The accurate A phases each component that weighs is added in vacuum emulsification pot, and homogeneous is warming up to 85-90 DEG C, heat preservation 25 to being uniformly dispersed
Minute；
B phase each components are added in, are stirred evenly；
Emulsification pot chuck is passed through cooling water, is cooled to 45-50 DEG C, adds in C phase each components, stirs；
Continue stirring to be cooled to room temperature and complete.
In the present embodiment, anticorrosive composite is carried by the grape Fructus Citri grandis extract of 3.0wt%, the Magnolia bark of 3.0wt%
1, the 2- butanediols of object, the ginger-root extract of 8.0wt%, the pepper extract of 3.0wt% and 83wt% is taken to form.
The preparation method of the anticorrosive composite is：Said components are uniformly mixed.
Comparative example 5
Comparative example 5 is formulated with embodiment 2, preparation process is similar, the difference is that the anticorrosive composite in comparative example 5 is not
Fructus Citri grandis extract containing grape, anticorrosive composite are by weight percentage：3% the bark of official magnolia bark extract, the extraction of 8% race
Object, 3% pepper extract and 86% 1,2- butanediols.
Comparative example 6
Comparative example 6 is formulated with embodiment 2, preparation process is similar, the difference is that the anticorrosive composite in comparative example 6 is not
Containing the bark of official magnolia bark extract, anticorrosive composite is by weight percentage：3% grape Fructus Citri grandis extract, the extraction of 8% race
Object, 3% pepper extract and 86% 1,2- butanediols.
Comparative example 7
Comparative example 7 is formulated with embodiment 2, preparation process is similar, the difference is that the anticorrosive composite in comparative example 7 is not
Containing ginger-root extract, anticorrosive composite is by weight percentage：3% grape Fructus Citri grandis extract, the extraction of 3% Magnolia bark
Object, 3% pepper extract and 91% 1,2- butanediols.
Comparative example 8
Comparative example 8 is formulated with embodiment 2, preparation process is similar, the difference is that the anticorrosive composite in comparative example 8 is not
Containing pepper extract, anticorrosive composite is by weight percentage：3% grape Fructus Citri grandis extract, the extraction of 3% Magnolia bark
Object, 8% ginger-root extract and 86% 1,2- butanediols.
Embodiment 3
Said composition is applied in infant's shampoo product, and formula is as follows：
The preparation process of the shampoo product is as follows：
The accurate A phases each component that weighs is added in vacuum emulsification pot, and homogeneous is warming up to 85-90 DEG C, heat preservation 25 to being uniformly dispersed
Minute；
B phase each components are added in, are stirred evenly；
Emulsification pot chuck is passed through cooling water, is cooled to 45-50 DEG C, adds in C phase each components, stirs；
Continue stirring to be cooled to room temperature and complete.
In the present embodiment, anticorrosive composite is carried by the grape Fructus Citri grandis extract of 1.0wt%, the Magnolia bark of 10.0wt%
The glycerine of object, the ginger-root extract of 3.0wt%, the pepper extract of 8.0wt% and 78wt% is taken to form.
The preparation method of the anticorrosive composite is：Said components are uniformly mixed.
Once add the experiment of bacterium preservation challenge and evaluation mark according to what cosmetics spices and essence association of the U.S. (CTFA) was recommended
Standard carries out the anti-corrosion single challenge experiment of 28 days by a definite date.Test strain is：Escherichia coli ATCC8739, Staphylococcus aureus
Bacterium ATCC6538, Pseudomonas aeruginosa ATCC9027, Candida albicans ATCC10231, Candida albicans NCPF3179, aspergillus niger
ATCC16404, Trichoderma viride GIM3.139, penicillium funiculosum GIM3.103.The evaluation criterion of CTFA is：Mixed cell, mixing are mould
The inoculum concentration of bacterium and mixed yeast is respectively 1 × 106CFU/g(CFU/m1)、l×104CFU/g (CFU/m1) and 1 ×
104CFU/g (CFU/m1), it is desirable that at the 7th day, bacterium reduced by 99.9%, and yeast and mold respectively reduces by 90%, and 28
It is continued to decline in it.As a result it is as follows：
Table one：The inhibitor effectiveness result of embodiment 1 and comparative example 1-4：
Table two：The inhibitor effectiveness result of embodiment 2 and comparative example 5-8：
From table one, two result of table, the present embodiment 1-3, from the 1st day to the 28th day, bacterium and fungi were respectively less than
10, as a result meet《Cosmetics safety technical specification》Specified in microbiological indicator limits in cosmetics regulation.Comparative example 1-
At the 8, the 7th day, bacterium does not reduce by 99.9%, does not as a result meet《Cosmetics safety technical specification》Specified in it is micro- in cosmetics
The regulation of Biological indicators limitation.
Above-described is only presently preferred embodiments of the present invention, all timess made in the range of the spirit and principles in the present invention
What modifications, equivalent substitutions and improvements etc., should all be included in the protection scope of the present invention.
Claims (4)
1. a kind of bactericidal composition based on plant extracts, which is characterized in that including following weight percent composition：
The race extraction of the grape Fructus Citri grandis extract of 1.0-3.0%, the bark of official magnolia bark extract of 3.0-10.0%, 3.0-8.0%
The polyalcohol of object, the pepper extract of 3.0-8.0% and 71-90%.
2. the bactericidal composition according to claim 1 based on plant extracts, which is characterized in that including following weight hundred
Divide and compare component：
The grape Fructus Citri grandis extract of 1.5-2.5%, the bark of official magnolia bark extract of 4-8%, the ginger-root extract of 5-7%, 5-7%
The polyalcohol of pepper extract and 75.5-84.5%.
3. the bactericidal composition according to claim 1 or 2 based on plant extracts, which is characterized in that described is polynary
Alcohol includes glycerine, 1,2-PD, 1,3-PD, 1,2- butanediols, 1,2- pentanediols, 1,5-PD, 3- [2- (second
Base hexyl) oxygen] -1,2-PD the combination of any one or more.
4. a kind of Baby Care composition, which is characterized in that contain 0.3-0.7wt% such as claim in the composition
Any bactericidal compositions of 1-3.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810082063.4A CN108078863B (en) | 2018-01-29 | 2018-01-29 | Bactericidal composition based on plant extracts and infant care composition |
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| CN201810082063.4A CN108078863B (en) | 2018-01-29 | 2018-01-29 | Bactericidal composition based on plant extracts and infant care composition |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110731932A (en) * | 2019-11-19 | 2020-01-31 | 山东义才和锐生物技术有限公司 | plant bacteriostatic cream and preparation method thereof |
| CN112587458A (en) * | 2020-12-29 | 2021-04-02 | 花安堂生物科技集团有限公司 | Preservative composition and preparation method and application thereof |
| CN112791020A (en) * | 2020-12-29 | 2021-05-14 | 陕西省石油化工研究设计院 | A kind of cosmetic preservative based on plant source and preparation method thereof |
| CN113413341A (en) * | 2021-06-24 | 2021-09-21 | 广州萃普生物科技有限公司 | Plant source compound bacteriostatic agent |
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| CN105232411A (en) * | 2015-11-18 | 2016-01-13 | 中山市艾丽意素生物科技有限公司 | Natural plant preservative combination and application thereof in cosmetics |
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| CN105707139A (en) * | 2014-12-23 | 2016-06-29 | 株式会社韩国人参公社 | Natural preservative composition |
| CN105055244A (en) * | 2015-08-24 | 2015-11-18 | 上海东晟源日化有限公司 | Organic natural plant preservative |
| CN105232411A (en) * | 2015-11-18 | 2016-01-13 | 中山市艾丽意素生物科技有限公司 | Natural plant preservative combination and application thereof in cosmetics |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110731932A (en) * | 2019-11-19 | 2020-01-31 | 山东义才和锐生物技术有限公司 | plant bacteriostatic cream and preparation method thereof |
| CN112587458A (en) * | 2020-12-29 | 2021-04-02 | 花安堂生物科技集团有限公司 | Preservative composition and preparation method and application thereof |
| CN112791020A (en) * | 2020-12-29 | 2021-05-14 | 陕西省石油化工研究设计院 | A kind of cosmetic preservative based on plant source and preparation method thereof |
| CN113413341A (en) * | 2021-06-24 | 2021-09-21 | 广州萃普生物科技有限公司 | Plant source compound bacteriostatic agent |
| CN113413341B (en) * | 2021-06-24 | 2022-06-07 | 广州萃普生物科技有限公司 | Plant source compound bacteriostatic agent |
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| Publication number | Publication date |
|---|---|
| CN108078863B (en) | 2020-07-14 |
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