KR102294276B1 - A repellet composition of a bird and preparation method thereof - Google Patents

A repellet composition of a bird and preparation method thereof Download PDF

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KR102294276B1
KR102294276B1 KR1020150032949A KR20150032949A KR102294276B1 KR 102294276 B1 KR102294276 B1 KR 102294276B1 KR 1020150032949 A KR1020150032949 A KR 1020150032949A KR 20150032949 A KR20150032949 A KR 20150032949A KR 102294276 B1 KR102294276 B1 KR 102294276B1
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김인순
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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    • AHUMAN NECESSITIES
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    • A01N25/24Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients to enhance the sticking of the active ingredients
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
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    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/06Coniferophyta [gymnosperms], e.g. cypress
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/22Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor

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Abstract

본 발명은 조류기피제 조성물 및 그 제조방법에 관한 것으로 천연 오일성분을 유효성분으로 함유하는 신규한 조류기피제 조성물을 제공하는 효과가 있고 아울러 점증성과 기피성이 뛰어난 조류기피제의 제조방법을 제공하는 효과가 있어 조류피해로 인한 농작물 및 주변 시설물의 피해를 현저히 저하시키는 뛰어난 효과가 있다.The present invention relates to an algae repellent composition and a method for manufacturing the same, which has the effect of providing a novel algae repellent composition containing a natural oil component as an active ingredient, and also has the effect of providing a method for manufacturing an algae repellent excellent in thickening and repelling properties It has an excellent effect of significantly reducing damage to crops and surrounding facilities due to bird damage.

Description

조류기피제 조성물 및 그 제조방법{A repellet composition of a bird and preparation method thereof}Bird repellent composition and its manufacturing method {A repellet composition of a bird and preparation method thereof}

본 발명은 조류기피제 조성물 및 그 제조방법에 관한 것이다. 더욱 상세하게는 천연 오일성분인 캡시컴, 타임(Thyme), 페퍼민트, 라벤더, 시더우드, 님(Neem), 시나몬, 멘톨, 메틸안드라닐레이트 및 자외선흡수제 시너메이트를 유효성분으로 함유하는 조류기피제 조성물 및 그 제조방법에 관한 것이다.
The present invention relates to a bird repellent composition and a method for preparing the same. More specifically, an algae repellent composition containing natural oil ingredients such as capsicum, thyme, peppermint, lavender, cedarwood, neem, cinnamon, menthol, methylandranilate, and UV absorber cinnamate as active ingredients. and to a manufacturing method thereof.

먹이가 풍부한 과거와 달리 최근 조류들은 녹지가 줄어들고 서식지가 파괴됨에 따라 인가로 이동하여 콩, 감자 및 인삼 등의 작물을 파먹거나 포도, 사과 및 배 등의 과실을 상하게 하는 등 다양한 농작물에 피해를 주고 있다. 뿐만 아니라 조류의 배설물은 전력설비 또는 건물의 부식 등 인근 시설물의 피해를 입히고 있다(까치 과연 길조인가, 한국전력공사 대구지사, p1-18, 1999). Unlike the past when food was plentiful, birds recently moved to in-house as green areas were reduced and habitats were destroyed, causing damage to various crops, such as eating soybeans, potatoes and ginseng, or damaging fruits such as grapes, apples and pears. have. In addition, bird droppings cause damage to nearby facilities such as corrosion of power facilities or buildings (Is a magpie really auspicious, Korea Electric Power Corporation Daegu Branch, p1-18, 1999).

또, 2004년 환경부에서 조사한 유해조수에 의한 작물 피해실태에 따르면 사과, 배, 포도, 호도, 벼, 채소류 및 기타 농작물의 피해액이 200억원에 이르는 것으로 집계되었다(2004년도 유해조수에 의한 피해실태 및 포획현황, 환경부).In addition, according to the crop damage caused by harmful tides surveyed by the Ministry of Environment in 2004, the damage to apples, pears, grapes, walnuts, rice, vegetables, and other crops was estimated at 20 billion won (the damage caused by harmful tides in 2004 and Capture status, Ministry of Environment).

이러한 농작물의 피해는 주로 참새, 비둘기, 까치 등이며(유재기 외., 벼 담수직파 재배답 및 전작물의 새 피해 경감연구, 농촌진흥청, 646-657. 1997) 이들의 피해를 막기 위해 방조망, 기피제 및 소음기 사용 등의 다양한 퇴치용 기술이 개발 및 이용되고 있다.The damage to these crops is mainly sparrows, pigeons, and magpies (Yoo Jae-gi et al., a study on the reduction of damage to birds in freshwater cultivation and previous crops, Rural Development Administration, 646-657. 1997). Various anti-removal technologies, such as the use of a silencer, are being developed and used.

한편, 본 발명에서 사용한 타임(Thyme)은 우리나라에서는 그 향이 100리까지 간다고 하여 백리향으로 불리며 그 자체로도 천연 방충방향제 역할을 한다. 타임은 다른 허브와 분명하게 구별되는 강한 향을 가지고 있으며(최수근 외., 셰프가 추천하는 54가지 향신료 수첩, 우듬지, 2011), 장기간 저장해도 손실되지 않는 특성이 있다. 방부 및 항균 효능으로 고대시절부터 시체 보관 및 항생제로 사용하였으며 최음제로도 사용하기도 하였다(김진 외., 조리용어사전, 광문각, 2007). 학명은 Thymus vulgaris이고 식물계 속씨식물문 쌍떡잎식물강 통화식물목에 속하며 원산지는 유럽 중남부 및 북아프리가 지역이지만 전세계에 분포하고 있다. 잔뿌리가 많은 뿌리에서 사각 모양의 줄기가 나와 위로 올라가며 곁가지를 많이 친다. 잎줄기는 매우 짧고 길이 5~9㎜, 너비 3㎜ 정도인 긴 타원형의 잎 가장자리는 안으로 굽고 잔털이 많으며 높이는 30㎝까지 자란다. 타임은 연분홍색 꽃은 상층부 잎의 잎겨드랑이에서 돌려나기처럼 나오며 5~10월에 수상꽃차례로 핀다. 꽃받침은 길이 3~5㎜의 약한 잎맥이 있, 뻣뻣한 머리와 같은 관이 있으며 위 잎이 아래 잎에 비해서 짧다. 꽃부리는 길이 4~6㎜로 보라색이나 담홍색이다. 씨의 크기는 1㎜ 정도로 납작한 알 모양이다. On the other hand, thyme used in the present invention is called thyme in Korea because its fragrance goes up to 100 li, and acts as a natural insect repellent by itself. Thyme has a strong scent that is distinctly different from other herbs (Choi Su-geun et al., Chef's Guide to 54 Spices Recommendation, Udumji, 2011), and has a characteristic that is not lost even after long-term storage. Because of its antiseptic and antibacterial effects, it has been used as an antibiotic and corpse storage since ancient times, and was also used as an aphrodisiac (Jin Kim et al., Dictionary of Cooking Terms, Gwangmungak, 2007). The scientific name is Thymus. vulgaris, and belongs to the angiosperm phylum Dicotyledonous plant, and the order of origin is central and southern Europe and northern Africa, but is distributed all over the world. A square-shaped stem emerges from the root with many fine roots, ascends upwards, and strikes a lot of side branches. The leaf stem is very short, and the edge of the long oval leaf with a length of 5-9 mm and a width of 3 mm is curved inward, has a lot of fine hairs, and grows up to 30 cm in height. Thyme is a pale pink flower that comes out like a stalk from the leaf axil of the upper leaf, and blooms in May-October as a dendritic inflorescence. The calyx has weak leaf veins of 3-5 mm in length, has a tube like a stiff head, and the upper leaf is shorter than the lower leaf. The corolla is 4-6 mm long and is purple or pink. The size of the seed is about 1 mm and is in the shape of a flat egg.

페퍼민트(Peppermint)는 식물계 속씨식물문 쌍떡잎식물강 통화식물목에 속하고 서늘한 기후를 좋아하는 허브로써 학명은 Mentha piperita이다(박원만 외., 텃밭백과(유기농 채소 기르기), 도서출판 들녘, 2012).. 원산지는 유럽이지만 현재 유럽, 미국, 일본 등에 분포하고 있다. 특유의 상쾌한 향으로 인헤 치약에 첨가되어 구취를 예방하고 달인 액이나 생잎을 부순 것은 습포제(濕布劑)로 피부 염증이나 타박상 치료에 사용하며 독소를 없애는 작용도 한다. 또, 피부의 가려움증에도 효과가 있는 것으로 알려져 있다(하순혜, 허브도감, 아카데미서적, 2006).Peppermint (Peppermint) belongs to the angiosperm phylum Dicotyledonous plants of the botanical family, and is a cool climate-loving herb whose scientific name is Mentha. piperita (Park Won-man et al., Garden Encyclopedia (organic vegetable growing), Book Publishing Field, 2012).. Origin is Europe, but it is currently distributed in Europe, the United States, and Japan. It is added to Inhe toothpaste with a unique refreshing scent to prevent bad breath. Decoctions or fresh leaves crushed are used as poultices to treat skin inflammation or bruises, and also remove toxins. In addition, it is known to be effective against itching of the skin (Sunhye Ha, Herbal Encyclopedia, Academy Books, 2006).

라벤더(Lavender)는 식물계 피자식물문 쌍떡잎식물강 통꽃식물목 꿀풀과에 속하고 원산지는 지중해 연안이며 습하지 않고 햇빛이 잘 드는 곳에서 자라며 학명은 Lavandula angustifolia이다. 방향성이 우수한 허브로 꽃과 잎은 허브 차로 이용하면 불안, 두통, 헛배부름, 메스꺼움, 현기증 및 구취를 없애는 효과가 있다(하순혜, 허브도감, 아카데미서적, 2006).Lavender (Lavender) is a plant-based dicotyledon angiosperms door tongkkot steel plant grows in the neck and in the Lamiaceae and is native to the Mediterranean coast is humid but sunny sunshine where the scientific name Lavandula angustifolia . As an herb with excellent aromaticity, flowers and leaves are effective in relieving anxiety, headache, flatulence, nausea, dizziness and bad breath when used as herbal tea (Sunhye Ha, Herbal Encyclopedia, Academy Books, 2006).

시더우드는 식물계 겉씨식물문 구과식물목으로 학명은 Cedrus atlantica이며 원산지는 모로코이다. 상쾌하고 은은한 향기를 지니고 있으며 심신을 안정시켜주는 효과가 있다. 살충·소독·수렴·이뇨·피부연화·강장·거담·살균·진정 등의 작용을 한고 탈모 및 비듬 예방에도 효과가 있다. 남성 화장품과 면도한 뒤 사용하는 애프터쉐이브 제품에 많이 사용되고 향수의 고착제로도 많이 사용된다.Cedarwood is a coniferous plant in the plant family gymnosperm, and its scientific name is Cedrus. atlantica and is native to Morocco. It has a refreshing and subtle scent and has a calming effect on the mind and body. Insecticide, disinfection, astringent, diuretic, skin softening, tonic, expectorant, sterilizing, soothing, etc., and is effective in preventing hair loss and dandruff. It is widely used in men's cosmetics and aftershave products used after shaving, and is also used as a fixing agent in perfumes.

님(Neem)은 식물계 멀구슬나무과에 속하며 학명은 Azadirachta indica이고 아열대 및 열대지방에서 많이 자라며 50% 이상이 인도에 서식하고 있다. 2~3월 흰 꽃이 피고 난 후 녹색 열매는 7~8월이 되면 노랗게 익어 새들이 즐겨 찾는다. 님은 건조에 강하며 내염성도 높다. 열매는 식용 가능하며 열매에서 추출하는 님오일은 특유의 향을 가지고 있다. 열매 및 씨는 쓴맛이 있고 치질약, 구충제로 사용되고 해독작용이 있다. 씨에서는 45%의 오일이 추출되는데 마늘, 유황과 비슷한 냄새가 나는 쓴맛의 오일로서 지방산이 풍부하며 비타민 E, 필수 아미노산 등이 들어 있다. 열매 및 씨의 주요성분인 아자디라크틴(azadirachtin)은 곤충의 성장 및 생식에 영향을 미쳐 생물농약으로 유용하게 사용되고 있다(민태영 외., 경전 속 불교식물, 이담북스, 2011). Neem belongs to the botanical family Azadirachta, and its scientific name is Azadirachta. indica , and grows in subtropical and tropical regions, with more than 50% inhabiting India. After the white flowers bloom in February-March, the green fruits ripen to yellow in July-August, and birds often visit them. Neem is resistant to drying and has high flame resistance. The fruit is edible and the neem oil extracted from the fruit has a unique flavor. The fruits and seeds have a bitter taste and are used as a hemorrhoid and anthelmintic and have detoxifying properties. 45% of the oil is extracted from the seeds. It is a bitter oil with a smell similar to garlic and sulfur. It is rich in fatty acids and contains vitamin E and essential amino acids. Azadirachtin, a major component of fruits and seeds, affects the growth and reproduction of insects and is therefore usefully used as a biological pesticide (Min Tae-young et al., Buddhist Plants in the Sutras, Edam Books, 2011).

시나몬(Cinnamon)은 식물계 피자식물문 쌍떡잎식물강 녹나무과이고 학명은 Cinnamomum verum이며 원산지는 동남아시아, 스리랑카 및 미얀마이다(하순혜, 허브도감, 아카데미서적, 2006). 시나몬은 6월에 개화하고 주로 줄기껍질을 향신료로 사용하며 독특한 청량감, 달콤한 맛 및 고상한 향을 지니고 있는 것이 특징이다(최수근 외., 셰프가 추천하는 54가지 향신료 수첩, 우듬지, 2011).Cinnamon is an angiosperm phylum Dicotyledonous camphoraceae, scientific name Cinnamomum verum, and its origin is Southeast Asia, Sri Lanka and Myanmar (Sunhye Ha, Herbal Encyclopedia, Academy Books, 2006). Cinnamon blooms in June, mainly uses stem bark as a spice, and is characterized by a unique refreshing feeling, sweet taste, and noble fragrance (Choi Sugeun et al., Chef's Guide to 54 Spices Recommended by Chef, Urumji, 2011).

박하는 경엽을 증류하여 냉각정제한 백색결정체로서 향기가 있고 시원한 맛이 있어서 건위제와 신경통, 결핵 등의 약재 및 구강의 향료에 쓰인다(농업용어사전, 농촌진흥청).Peppermint is a white crystal obtained by distilling and cooling the leaves, and has a fragrant and cool taste, so it is used as a medicine for stomach upset, neuralgia, tuberculosis, etc., and as a flavoring for the oral cavity (Agricultural Glossary, Rural Development Administration).

은행잎은 대부분 쭈글쭈글하거나 부서져있고 완전한 것은 부채 모양이며 길이 3~12cm 폭은 5~15cm이다(김창민 외., 한약재감별도감, 아카데미서적, 2014). 또, 특유한 냄새가 있고 맛은 약간 떫으며 어혈을 제거하고 피를 잘 돌게 하여 순환을 돕고 통증을 줄여주며 천증(喘症)을 다스리는 효능이 있다. 이런 효능을 이용해 기침과 천증, 심혈관계질환, 고지혈증, 치매, 대뇌 부전 등에서 긍정적인 효과가 있다고 보고된 바 있다. Most of the ginkgo leaves are wrinkled or broken, and the complete ones are fan-shaped, 3~12cm long and 5~15cm wide (Changmin Kim et al., Differential Encyclopedia of Herbal Medicines, Academy Books, 2014). In addition, it has a unique smell and a slightly astringent taste, and it has the effect of removing eohyeol and circulating blood, helping circulation, reducing pain, and controlling nephropathy. Using this effect, it has been reported that it has a positive effect on cough and asthma, cardiovascular disease, hyperlipidemia, dementia, and cerebral insufficiency.

어성초는 Houttuynia cordata Thunberg(삼백초과 Saururaceae)의 꽃필 때의 지상부를 의미하며 즙채, 중약, 십약이라고 한다. 줄기는 길이 20~35cm, 지름 0.2~0.3cm이고 세로 주름이 있으며 마디가 명료한 것이 특징이다. 잎은 길이 3~5cm, 너비 3~4cm이고 끝은 뾰족하다. 잎의 윗면은 어두운 황록색~황갈색이고 아랫면은 회록색~회갈색이다. 잎을 비벼서 부수면 생선비린내가 나고 맛은 약간 떫다(김창민 외., 한약재감별도감, 아카데미서적, 2014). 어성초는 해열, 배농작용이 뛰어나 폐농양으로 인한 기침, 피고름을 토할 때, 폐렴, 급만성기관지염, 장염, 요로감염증, 종기에 쓰며, 고열의 경우 사용하는 것이 특징이다.Eoseongcho is Houttuynia Cordata Thunberg (Saururaceae) refers to the above-ground part at the time of flowering, and is called succulent, Chinese medicine, and ten medicine. The stem is 20-35cm long, 0.2-0.3cm in diameter, has vertical wrinkles, and has clear nodes. The leaves are 3~5cm long and 3~4cm wide, and the tip is pointed. The upper side of the leaf is dark yellow-green to yellowish-brown, and the lower side is gray-green to gray-brown. If the leaves are rubbed and crushed, a fishy smell is produced and the taste is slightly astringent (Chang-Min Kim et al., Differential Encyclopedia of Herbal Medicines, Academy Books, 2014). Eoseongcho has excellent antipyretic and drainage properties, so it is used for coughing and vomiting blood pus due to lung abscess, pneumonia, acute and chronic bronchitis, enteritis, urinary tract infection, and boils.

녹차는 발효시키지 않은 찻잎(綠茶)을 사용하여 바로 증기로 찌거나 솥에서 덖어 발효가 되지 않도록 만든 불발효차이다. 적채한 차의 생잎을 재빨리 증열(증자) 또는 부초(釜炒) 등의 열처리를 하여 차 잎 중의 산화효소를 위시한 각종의 효소의 활성을 정지시켜 건조한 차이다. 차 잎 성분의 변화가 적으므로 회관에 녹색계통이 보존되어 있는 것이 특징이다. 녹차는 발효과정을 거치지 않기 때문에 차의 성분이 그대로 남아 있어 비타민 C가 레몬의 5∼8배나 함유되어 있고 노화 억제, 암 예방 및 식중독 방지 등 다양한 질병의 예방 및 억제 효과를 나타내는 카테킨 성분이 다량 함유되어 있다(홍익재, 녹차 [綠茶, green tea], 차생활문화대전, 2012).Green tea is a non-fermented tea made by steaming unfermented tea leaves or boiling in a pot to prevent fermentation. It is dried tea by quickly heat-treating fresh leaves of red-picked tea, such as steaming or steaming, to stop the activity of various enzymes including oxidase in the tea leaves. The characteristic feature is that the green system is preserved in the hall because there is little change in the composition of the tea leaves. Because green tea does not go through the fermentation process, the components of tea remain as it is, and contains 5 to 8 times more vitamin C than lemon. (Ikjae Hong, green tea [綠茶, green tea], Tea Life Culture Exhibition, 2012).

불가사리는 불가사리과의 극피동물에 속하는 해양 저서생물이다(Paine, R.T., A short term experimental investigation of resource partitioning in a New Zealand rocky intertidal habitat, Ecology, 52, 1096-1106, 1971). 또, 우리나라의 경우 약 200여종이 서식하며 외래종인 아무르불가사리(Asterias amurensis), 토속종인 별불가사리(Asterina pectinifera), 거미불가사리(Ophioplocus japonicus) 등이 많이 분포되어 있다(Kim, Y.S., Selective feeding on the several bivalve mollusks by starfish, Asterias amurensis Lutken, Bull. Fac. Fish. 19, 244-249, 1969). Starfish are marine benthic organisms belonging to the echinoderms of the family Starfish (Paine, RT, A short term experimental investigation of resource partitioning in a New Zealand rocky intertidal habitat, Ecology, 52, 1096-1106, 1971). In addition, about 200 species inhabit in Korea, and the exotic starfish ( Asterias amurensis ) and the native starfish ( Asterina) pectinifera ), spider starfish ( Ophioplocus ) japonicus ) and the like are widely distributed (Kim, YS, Selective feeding on the several bivalve mollusks by starfish, Asterias amurensis Lutken, Bull. Fac. Fish. 19, 244-249, 1969).

자외선은 파장이 약 397∼10nm인 전자기파이지만 보통은 파장이 약 400∼100nm의 전자기파를 지칭한다. 자외선은 크게 단파장 200~280 nm의 UV-C, 중파장 280~320 nm의 UV-B 및 장파장인 320~400 nm UV-A로 구분된다. 태양으로부터 지구에 도달하는 자외선 중 에너지가 가장 크고 강한 살균 작용을 갖는 UV-C는 대기권 상층부에 있는 오존층에서 흡수 및 산란되어 지상에는 도달하지 않으며 피부에 영향을 미치는 것으로 알려진 자외선은 UV-B 및 UV-A이다(A. Mahns, et al ., Contribution of UVB and UVA to UV-dependent stimulation of cyclooxygenase-2 expression in artificial epidermis, Photochem. Photobiol . Sci ., 3(3), 257, 2004; C. Huang, W. Ma and Z. Dong, Signal transduction through atypical PKCs, but not the EGF receptor, is necessary for UVC induced AP-1 activation in immortal murine cells, Oncogene , 14(16), 1997).Ultraviolet is an electromagnetic wave with a wavelength of about 397 to 10 nm, but usually refers to an electromagnetic wave with a wavelength of about 400 to 100 nm. Ultraviolet rays are largely divided into short-wavelength UV-C of 200-280 nm, medium-wavelength UV-B of 280-320 nm, and long-wavelength 320-400 nm UV-A. Among the ultraviolet rays reaching the earth from the sun, UV-C, which has the highest energy and has a strong bactericidal action, is absorbed and scattered in the ozone layer in the upper atmosphere and does not reach the ground. The ultraviolet rays known to affect the skin are UV-B and UV -A (A. Mahns, et al. al ., Contribution of UVB and UVA to UV-dependent stimulation of cyclooxygenase-2 expression in artificial epidermis, Photochem. Photobiol . Sci ., 3(3), 257, 2004; C. Huang, W. Ma and Z. Dong, Signal transduction through atypical PKCs, but not the EGF receptor, is necessary for UVC induced AP-1 activation in immortal murine cells, Oncogene , 14(16), 1997).

한편, 고압 송전선 주변에 코로나 방전이 일상적으로 일어나며 불규칙한 섬광이 발생하는데 이때 발생하는 코로나 및 섬광의 파장이 너무 짧아 인간은 감지할 수 없으나 최근 포유류 및 조류들이 이러한 자외선을 감지하여 회피하는 특성을 보인다는 연구결과가 발표된 바 있다(Nicholas Tyler et al ., Ultraviolet Vision and Avoidance of Power Lines in Birds and Mammals, Conservation Biology , Volume 28, Issue 3, pages 630-631, 2014). On the other hand, corona discharges routinely occur around high-voltage power lines and irregular flashes occur. The wavelength of the corona and flashes generated at this time is too short to be detected by humans. Research results have been published (Nicholas Tyler et al. al ., Ultraviolet Vision and Avoidance of Power Lines in Birds and Mammals, Conservation Biology , Volume 28, Issue 3, pages 630-631, 2014).

본 발명과 관련하여 본 발명자에 의한 야생동물 차단제 조성물 제조방법이 대한민국 등록특허 제10-1192980호에 공지되어 있으나 이는 3단계 제조방법으로 이루어진 3% 내지 15%의 피마자 추출물, 0.5% 내지 7%의 갈릭 추출물, 멘톨+캡사이신 및 메틸안드라닐레이트 중 선택된 하나; 0.1 내지 7.5% 추가성분; 및 나머지 함량의 유화제를 포함하는 야생동물 차단제 조성물에 관한 것이다. 그리고 액상형 동물 및 조류 퇴치용 조성물이 대한민국 등록특허 제10-1181454호에 공지된 바 있으나 이는 단지 계피정유, 박하정유 및 초피추출물이 함유된 액상형 동물 및 조류퇴치용 조성물의 제공에 관한 것이다.In relation to the present invention, a method for preparing a wild animal blocker composition by the present inventor is known in Korean Patent Registration No. 10-1192980, but it contains 3% to 15% castor extract, 0.5% to 7% one selected from garlic extract, menthol + capsaicin and methylandranilate; 0.1 to 7.5% additional ingredients; And it relates to a wild animal blocking composition comprising the remaining amount of an emulsifier. And, although a liquid composition for repelling animals and birds is known in Korean Patent Registration No. 10-1181454, it relates only to the provision of a composition for combating animals and birds containing cinnamon essential oil, peppermint essential oil and herbaceous extract.

또, 야생조류 퇴치용 조성물이 대한민국 등록특허 제10-1152343호에 공지되어 있으나 이는 크레오소트유와 목타르 5 내지 60 중량%, 알코올 2.5 내지 40 중량%, 해포석 5 내지 35 중량% 및 프탈산무수물 10 내지 40 중량%를 포함하는 야생조류 퇴치용 조성물에 관한 것이다. 그리고 조류 퇴치용 조성물이 대한민국 등록특허 제10-1008308호에 공지된 바 있으나 이는 점착 부여제, 바셀린, 미네랄오일, 실리콘 및 천연 신미(辛味) 성분을 포함하는 조류 퇴치용 조성물에 관한 것이다. In addition, a composition for combating wild algae is known in Korean Patent Registration No. 10-1152343, but it is creosote oil and wood tar 5 to 60% by weight, alcohol 2.5 to 40% by weight, haeposeok 5 to 35% by weight, and phthalic anhydride 10 to 40 It relates to a composition for combating wild algae comprising % by weight. And although the composition for combating algae is known in Korean Patent Registration No. 10-1008308, it relates to a composition for combating algae comprising a tackifier, petrolatum, mineral oil, silicone, and a natural sweetener.

또한, 겔상의 조류퇴치용 조성물이 대한민국 등록특허 제10-0798290호에 공지되어 있으나 이는 계피정유 및 박하정유로 이루어진 겔상의 조류퇴치용 조성물에 관한 것이다. 그리고, 천연물질로 이루어진 야생동물 기피제 조성물이 대한민국 등록특허 제10-1167069호에 공지되어 있으나 이는 계피정유, 박하정유, 캡사이신 추출물, 초피나무추출물 및 소나무 정유로 구성되는 것을 특징으로 하는 멧돼지 기피제 조성물에 관한 것이다.In addition, although a gel-like composition for repelling algae is known in Korean Patent Registration No. 10-0798290, it relates to a gel-like composition for repelling algae comprising cinnamon essential oil and peppermint essential oil. And, a wild animal repellent composition made of a natural material is known in Korean Patent Registration No. 10-1167069, which is a wild boar repellent composition, characterized in that it consists of cinnamon essential oil, peppermint essential oil, capsaicin extract, chrysanthemum extract and pine essential oil. it's about

따라서, 상기 특허문헌 어디에도 천연 오일성분인 캡시컴, 타임(Thyme), 페퍼민트, 라벤더, 시더우드, 님(Neem), 시나몬, 멘톨, 메틸안드라닐레이트 및 자외선흡수제 시너메이트를 유효성분으로 함유하는 조류기피제 조성물에 대한 발명은 공지된 바 없다.
Therefore, algae containing natural oil ingredients such as capsicum, Thyme, peppermint, lavender, cedarwood, Neem, cinnamon, menthol, methylandranilate and UV absorber cinnamate as active ingredients anywhere in the above patent literature The invention of the repellent composition is not known.

따라서, 본 발명의 목적은 천연 오일성분인 캡시컴, 타임(Thyme), 페퍼민트, 라벤더, 시더우드, 님(Neem), 시나몬, 멘톨, 메틸안드라닐레이트 및 자외선흡수제 시너메이트의 혼합물을 유효성분으로 함유하는 조류기피제 조성물을 제공하는 데 있다.Accordingly, it is an object of the present invention to use a mixture of natural oil ingredients such as capsicum, thyme, peppermint, lavender, cedarwood, Neem, cinnamon, menthol, methylandranilate and UV absorber cinnamate as an active ingredient. To provide a bird repellent composition containing.

본 발명의 다른 목적은 상기 조류기피제 조성물의 제조방법을 제공하는 데 있다.
Another object of the present invention is to provide a method for preparing the algae repellent composition.

본 발명의 상기 목적은 (a)캡시컴, 타임(Thyme), 페퍼민트, 라벤더, 시더우드, 님(Neem), 시나몬, 멘톨, 메틸안드라닐레이트, 시너메이트의 천연 오일성분 및 계면활성제를 혼합하는 단계와; (b)은행잎 추출물, 어성초 추출물, 불가사리 추출물 및 녹차 추출물의 천연 액상성분을 제오라이트 침출수와 함께 혼합하는 단계와; (c)상기 (a)단계에서 얻은 혼합물을 알코올과 혼합하는 단계와; (d)카보풀(CARBOPOL)을 증류수에 용해하는 단계와; (e)상기 (b) 내지 (d)단계에서 얻은 혼합물을 동일한 부피비로 배합하고 다시 혼합하는 단계와; (f)상기 (e)단계에서 얻은 혼합물에 페녹시에탄올 및 TEA를 첨가하여 점도를 증진시키는 단계와; (g)상기 (f)단계에서 얻은 증점성 혼합물과 정제수를 다시 혼합하여 제품화 하는 단계로 이루어지고 상기 (g)단계에서 얻은 본 발명 제품의 pH 및 점도를 평가하고 흡광도를 측정하여 조류기피제로서의 품질을 평가함으로써 달성하였다.The above object of the present invention is to mix natural oil components and surfactants of (a) capsicum, thyme, peppermint, lavender, cedarwood, neem, cinnamon, menthol, methylandranilate, cinnamate step; (b) mixing the natural liquid components of ginkgo leaf extract, eoseongcho extract, starfish extract and green tea extract with zeolite leachate; (c) mixing the mixture obtained in step (a) with alcohol; (d) dissolving CARBOPOL in distilled water; (e) mixing the mixture obtained in steps (b) to (d) in the same volume ratio and mixing again; (f) increasing the viscosity by adding phenoxyethanol and TEA to the mixture obtained in step (e); (g) consists of a step of mixing the thickening mixture obtained in step (f) and purified water again to commercialize, and evaluating the pH and viscosity of the product of the present invention obtained in step (g) and measuring the absorbance to measure the quality as an algae repellent was achieved by evaluating

상기와 같은 본 발명은 천연 오일성분을 유효성분으로 함유하는 신규한 조류기피제 조성물을 제공하는 효과가 있고 아울러 점증성과 기피성이 뛰어난 조류기피제의 제조방법을 제공하는 효과가 있어 조류피해로 인한 농작물 및 주변 시설물의 피해를 현저히 저하시키는 뛰어난 효과가 있다.
The present invention as described above has the effect of providing a novel bird repellent composition containing a natural oil component as an active ingredient, and also has the effect of providing a method for producing a bird repellent excellent in thickening properties and repellent properties, so that crops and It has an excellent effect of significantly reducing damage to surrounding facilities.

도 1는 본 발명 조류기피제 조성물의 제조공정을 나타낸 흐름도이다.
도 2은 본 발명 조류기피제 조성물의 필드테스트 결과를 나타낸 사진도이다.
도 3은 본 발명 조류기피제 조성물의 효능평가 결과를 나타낸 그래프이다.
도 4는 본 발명 조류기피제 조성물의 자외선 흡광도를 측정한 그래프이다.
도 5는 본 발명 조류기피제 조성물의 자외선 흡광도를 측정한 사진도이다.
도 6는 본 발명 조류기피제 조성물을 이용해 제조한 조류피해 방지용 조류기피제를 보인 도이다.
1 is a flow chart showing the manufacturing process of the algae repellent composition of the present invention.
2 is a photograph showing the field test results of the algae repellent composition of the present invention.
Figure 3 is a graph showing the efficacy evaluation results of the bird repellent composition of the present invention.
Figure 4 is a graph measuring the ultraviolet absorbance of the algae repellent composition of the present invention.
Figure 5 is a photograph of measuring the ultraviolet absorbance of the algae repellent composition of the present invention.
6 is a view showing a bird repellent for preventing damage to birds prepared using the bird repellent composition of the present invention.

본 발명의 구체적인 내용을 실시예를 들어 상세하게 설명한다. 하기 실시예는 본 발명을 예시하기 위한 것일 뿐 발명이 하기 실시예에 한정되는 것은 아니다.
The specific content of the present invention will be described in detail with reference to examples. The following examples are only for illustrating the present invention, but the present invention is not limited to the following examples.

본 발명 조류기피제 조성물의 수득은 하기의 공정을 통하여 달성된다(도 1).Obtaining the algae repellent composition of the present invention is achieved through the following process (Fig. 1).

제 1단계 : 천연 오일성분 및 계면활성제 혼합공정Step 1: Mixing process of natural oil component and surfactant

본 발명 주원료 중에서 캡시컴, 타임(Thyme), 페퍼민트, 라벤더, 시더우드, 님(Neem), 시나몬, 멘톨, 메틸안드라닐레이트 및 자외선흡수제 시너메이트의 천연 오일성분 10종을 먼저 계면활성제와 실온에서 30분간 믹서로 혼합한다.Among the main ingredients of the present invention, 10 kinds of natural oil components of capsicum, thyme, peppermint, lavender, cedarwood, neem, cinnamon, menthol, methylandranilate, and UV absorber cinnamate were first mixed with a surfactant at room temperature. Mix with a mixer for 30 minutes.

본 발명에 따른 캡시컴은 전체 조성물의 0.04 내지 1 부피%를 첨가하는 것이 바람직하고 타임(Thyme) 오일은 전체 조성물의 0.05 내지 0.44 부피%를 첨가하는 것이 바람직하며 페퍼민트 오일은 전체 조성물의 0.05 내지 0.46 부피%를 첨가하는 것이 바람직하다. Capsicum according to the present invention is preferably added in an amount of 0.04 to 1% by volume of the total composition, thyme oil is preferably added in an amount of 0.05 to 0.44% by volume of the total composition, and peppermint oil is 0.05 to 0.46% by volume of the total composition. It is preferable to add volume %.

그리고, 라벤더 오일은 전체 조성물의 0.2 내지 0.44 부피%를 첨가하는 것이 바람직하고 시더우드 오일은 전체 조성물의 0.02 부피%를 첨가하는 것이 바람직하며 님(Neem) 오일은 전체 조성물의 0.1 부피%를 첨가하는 것이 바람직하다. And, lavender oil is preferably added 0.2 to 0.44 volume % of the total composition, cedarwood oil is preferably added 0.02 volume % of the total composition, and neem oil is added 0.1 volume % of the total composition. it is preferable

또, 시나몬 오일은 전체 조성물의 0.03 내지 0.10 부피%를 첨가하는 것이 바람직하고 멘톨 오일은 전체 조성물의 0.1 부피%를 첨가하는 것이 바람직하며 메틸안드라닐레이트 오일은 전체 조성물의 0.5 내지 3 부피%를 첨가하는 것이 바람직하다.In addition, cinnamon oil is preferably added in an amount of 0.03 to 0.10% by volume of the total composition, menthol oil is preferably added in 0.1% by volume of the total composition, and methylandranilate oil is added in an amount of 0.5 to 3% by volume of the total composition. It is preferable to do

또한, 자외선흡수제로서 시너메이트 오일은 전체 조성물의 0.03 부피%를 첨가하는 것이 바람직하고 계면활성제(tween20)는 전체 조성물의 2.70 내지 12 부피%를 첨가하는 것이 바람직하다.In addition, cinnamate oil as a UV absorber is preferably added in an amount of 0.03% by volume of the total composition, and surfactant (tween20) is preferably added in an amount of 2.70 to 12% by volume of the total composition.

제 2단계 : 천연 액상성분 및 제오라이트 침출수 혼합공정Step 2: Mixing process of natural liquid ingredients and zeolite leachate

본 발명 주원료 중에서 은행잎 추출물, 어성초 추출물, 불가사리 추출물 및 녹차 추출물의 천연 액상성분 4종을 25 부피%의 제오라이트 침출수와 함께 혼합한다.Among the main raw materials of the present invention, 4 types of natural liquid components of ginkgo leaf extract, eoseongcho extract, starfish extract and green tea extract are mixed with 25% by volume of zeolite leachate.

본 발명에 따른 은행잎 추출물은 액상의 형태로 전체 조성물의 0.25 부피%를 첨가하는 것이 바람직하고 어성초 추출물은 액상의 형태로 전체 조성물의 0.1 부피%를 첨가하는 것이 바람직하며 불가사리 추출물은 액상의 형태로 전체 조성물의 1 내지 5 부피%를 첨가하는 것이 바람직하다.The ginkgo leaf extract according to the present invention is preferably added to 0.25% by volume of the total composition in the form of a liquid, and it is preferable to add 0.1% by volume of the total composition to the eosinthia extract in the form of a liquid, and the starfish extract is in the form of a liquid. It is preferred to add 1 to 5% by volume of the composition.

또, 녹차 추출물은 액상의 형태로 전체 조성물의 0.1 내지 0.12 부피%를 첨가하는 것이 바람직하고 산화방지제는 분말의 형태로 전체 조성물의 0.02 내지 0.2 부피%를 첨가하는 것이 바람직하다. In addition, the green tea extract is preferably added in an amount of 0.1 to 0.12% by volume of the total composition in the form of a liquid, and the antioxidant is preferably added in an amount of 0.02 to 0.2% by volume of the total composition in the form of a powder.

제 3단계 : 알코올 혼합공정Step 3: Alcohol mixing process

상기 1단계에서 얻은 혼합물을 알코올과 혼합한다.The mixture obtained in step 1 is mixed with alcohol.

본 발명에 따른 알코올은 전체 조성물의 2.25 내지 10 부피%를 첨가하는 것이 바람직하다.The alcohol according to the present invention is preferably added in an amount of 2.25 to 10% by volume of the total composition.

제 4단계 : 카보풀 용해공정Step 4: Carbopool dissolution process

본 발명에 다른 카보풀(CARBOPOL)(940)을 0.1 내지 0.2 부피%가 되도록 정제수에 잘 용해시킨다.Carbopool (CARBOPOL) (940) according to the present invention is well dissolved in purified water so as to be 0.1 to 0.2% by volume.

제 5단계 : 믹서 혼합공정Step 5: Mixer Mixing Process

상기 2 내지 4단계에서 얻은 혼합물을 동일한 부피비로 배합하고 호모믹서 및 아지믹서로 혼합한다.
The mixtures obtained in steps 2 to 4 are mixed in the same volume ratio and mixed with a homomixer and an azimixer.

제 6단계 : 점도 증진 공정Step 6: Viscosity Enhancement Process

상기 5단계에서 얻은 혼합물에 페녹시에탄올 및 TEA를 첨가하여 점도를 증가시켜 준다.Phenoxyethanol and TEA are added to the mixture obtained in step 5 to increase the viscosity.

본 발명에 따른 페녹시에탄올은 방부제로서 전체 조성물의 0.5 부피%를 첨가하는 것이 바람직하고 TEA는 전체 조성물의 0.1 내지 0.2 부피%를 첨가하는 것이 바람직하다. Phenoxyethanol according to the present invention is preferably added as a preservative in 0.5% by volume of the total composition, and TEA is preferably added in an amount of 0.1 to 0.2% by volume of the total composition.

제 7단계 : 혼합물 및 정제수 혼합 제품화 공정Step 7: Mixture and purified water mixture production process

상기 6단계에서 얻은 증점성 혼합물에 전체 조성물이 100%가 되도록 정제수를 첨가하고 다시 혼합한다.Purified water is added to the thickening mixture obtained in step 6 so that the total composition becomes 100%, and the mixture is mixed again.

제 8단계 : 본 발명 기피제 품질 평가Step 8: Quality evaluation of the repellent of the present invention

상기 7단계에서 얻은 혼합물의 pH 및 점도를 측정하여 품질을 평가한다.
The quality is evaluated by measuring the pH and viscosity of the mixture obtained in step 7 above.

실시예Example 1. 본 발명 1차 조류기피제 조성물 제조 1. Preparation of the present invention primary algae repellent composition

표 1의 조성비 및 상기 공정별 단계에 따라 본 발명 1차 조류 기피제 조성물을 얻었다.According to the composition ratio of Table 1 and the steps for each process, the present invention primary algae repellent composition was obtained.

제 1차 조류기피제 조성물 제조 조성비1st algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 0.40%0.40% 메틸안드라닐레이트Methylandranilate oiloil 0.50%0.50% 불가사리 추출물Starfish Extract 액상liquid 2.00%2.00% 녹차 추출물green tea extract 액상liquid 0.10%0.10% 핵심원료(計)Core raw materials 3.00%3.00% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 2.25%2.25% CARBOPOL(940)CARBOPOL(940) 분말powder -- 계면활성제(tween20)Surfactant (tween20) -- 2.70%2.70% 부원료(計)Sub-ingredient (計) 5.45%5.45% 첨가물additive 정제수Purified water 액상liquid 66.55%66.55% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실시예Example 2. 본 발명 2차 조류기피제 조성물 제조 2. Preparation of the present invention secondary algae repellent composition

표 2의 조성비 및 상기 실시예 1과 동일한 방법으로 본 발명 2차 조류 기피제 조성물을 얻었다.A composition ratio of Table 2 and a secondary algae repellent composition of the present invention were obtained in the same manner as in Example 1.

제 2차 조류기피제 조성물 제조 조성비Secondary algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 1.00%1.00% 메틸안드라닐레이트Methylandranilate oiloil 3.00%3.00% 불가사리 추출물Starfish Extract 액상liquid 5.00%5.00% 핵심원료(計)Core raw materials 9.00%9.00% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 10.00%10.00% 계면활성제(tween20)Surfactant (tween20) -- 12.00%12.00% 부원료(計)Sub-ingredient (計) 22.50%22.50% 첨가물additive 정제수Purified water 액상liquid 43.50%43.50% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실시예Example 3. 본 발명 3차 조류기피제 조성물 제조 3. Preparation of tertiary algae repellent composition of the present invention

표 3의 조성비 및 상기 실시예 1과 동일한 방법으로 본 발명 3차 조류 기피제 조성물을 얻었다.The composition ratio of Table 3 and the tertiary algae repellent composition of the present invention were obtained in the same manner as in Example 1.

제 3차 조류기피제 조성물 제조 조성비3rd algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 0.05%0.05% ThymeThyme oiloil 0.05%0.05% 페퍼민트peppermint oiloil 0.05%0.05% 시나몬cinnamon oiloil 0.08%0.08% 멘톨menthol oiloil 0.10%0.10% 메틸안드라닐레이트Methylandranilate oiloil 0.70%0.70% 자외선흡수제UV absorber oiloil 0.03%0.03% 불가사리 추출물Starfish Extract 액상liquid 1.05%1.05% 녹차 추출물green tea extract 액상liquid 0.12%0.12% 핵심원료(計)Core raw materials 2.23%2.23% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 2.65%2.65% TEATEA -- 0.10%0.10% CARBOPOL(940)CARBOPOL(940) 분말powder 0.10%0.10% 계면활성제(tween20)Surfactant (tween20) -- 3.18%3.18% 부원료(計)Sub-ingredient (計) 6.53%6.53% 첨가물additive 정제수Purified water 액상liquid 66.24%66.24% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실시예Example 4. 본 발명 4차 조류기피제 조성물 4. The quaternary bird repellent composition of the present invention 제조Produce

표 4의 조성비 및 상기 실시예 1과 동일한 방법으로 본 발명 4차 조류 기피제 조성물을 얻었다.The composition ratio of Table 4 and the quaternary algae repellent composition of the present invention were obtained in the same manner as in Example 1.

제 4차 조류기피제 조성물 제조 조성비4th algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 0.05%0.05% ThymeThyme oiloil 0.44%0.44% 페퍼민트peppermint oiloil 0.46%0.46% 라벤더lavender oiloil 0.44%0.44% 시나몬cinnamon oiloil 0.03%0.03% 멘톨menthol oiloil 0.10%0.10% 메틸안드라닐레이트Methylandranilate oiloil 0.60%0.60% 자외선흡수제UV absorber oiloil 0.03%0.03% 불가사리 추출물Starfish Extract 액상liquid 1.00%1.00% 녹차 추출물green tea extract 액상liquid 0.12%0.12% 핵심원료(計)Core raw materials 3.27%3.27% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 5.40%5.40% TEATEA -- 0.10%0.10% CARBOPOL(940)CARBOPOL(940) 분말powder 0.10%0.10% 계면활성제(tween20)Surfactant (tween20) -- 6.45%6.45% 부원료(計)Sub-ingredient (計) 12.55%12.55% 첨가물additive 정제수Purified water 액상liquid 59.18%59.18% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실시예Example 5. 본 발명 5차 조류기피제 조성물 5. 5th algae repellent composition of the present invention 제조Produce

표 5의 조성비 및 상기 실시예 1과 동일한 방법으로 본 발명 5차 조류 기피제 조성물을 얻었다.The composition ratio of Table 5 and the fifth algae repellent composition of the present invention were obtained in the same manner as in Example 1.

제 5차 조류기피제 조성물 제조 조성비Fifth algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 0.04%0.04% ThymeThyme oiloil 0.44%0.44% 페퍼민트peppermint oiloil 0.42%0.42% 라벤더lavender oiloil 0.20%0.20% 어성초추출물Eoseongcho Extract 액상liquid 0.10%0.10% 멘톨menthol oiloil 0.10%0.10% 메틸안드라닐레이트Methylandranilate oiloil 0.60%0.60% 자외선흡수제UV absorber oiloil 0.03%0.03% 불가사리 추출물Starfish Extract 액상liquid 1.00%1.00% 녹차 추출물green tea extract 액상liquid 0.12%0.12% 핵심원료(計)Core raw materials 3.05%3.05% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 4.60%4.60% TEATEA -- 0.10%0.10% CARBOPOL(940)CARBOPOL(940) 분말powder 0.10%0.10% 계면활성제(tween20)Surfactant (tween20) -- 5.49%5.49% 부원료(計)Sub-ingredient (計) 10.79%10.79% 첨가물additive 정제수Purified water 액상liquid 61.16%61.16% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실시예Example 6. 본 발명 6차 조류기피제 6. The 6th algae repellent of the present invention 조성물 제조composition preparation

표 6의 조성비 및 상기 실시예 1과 동일한 방법으로 본 발명 6차 조류 기피제 조성물을 얻었다.The composition ratio of Table 6 and the sixth algae repellent composition of the present invention were obtained in the same manner as in Example 1.

제 6차 조류기피제 조성물 제조 조성비6th algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 0.04%0.04% 페퍼민트peppermint oiloil 0.10%0.10% 라벤더lavender oiloil 0.20%0.20% 시더우드Cedarwood oiloil 0.20%0.20% 은행잎추출물Ginkgo Leaf Extract 액상liquid 0.25%0.25% NeemNeem oiloil 0.10%0.10% 어성초추출물Eoseongcho Extract 액상liquid 0.10%0.10% 멘톨menthol oiloil 0.10%0.10% 메틸안드라닐레이트Methylandranilate oiloil 0.60%0.60% 자외선흡수제UV absorber oiloil 0.03%0.03% 불가사리 추출물Starfish Extract 액상liquid 1.00%1.00% 녹차 추출물green tea extract 액상liquid 0.12%0.12% 핵심원료(計)Core raw materials 2.84%2.84% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 3.40%3.40% TEATEA -- 0.20%0.20% CARBOPOL(940)CARBOPOL(940) 분말powder 0.20%0.20% 계면활성제(tween20)Surfactant (tween20) -- 4.11%4.11% 부원료(計)Sub-ingredient (計) 8.41%8.41% 첨가물additive 정제수Purified water 액상liquid 63.75%63.75% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실시예Example 7. 본 발명 7차 조류기피제 7. The 7th algae repellent of the present invention 조성물 제조composition preparation

표 7의 조성비 및 상기 실시예 1과 동일한 방법으로 본 발명 7차 조류 기피제 조성물을 얻었다.The composition ratio of Table 7 and the 7th algae repellent composition of the present invention were obtained in the same manner as in Example 1.

제 7차 조류기피제 조성물 제조 조성비7th algae repellent composition manufacturing composition ratio 구분division 형상shape 조성(부피%)Composition (volume %) 주원료main raw material 캡시컴capsicum oiloil 0.05%0.05% 페퍼민트peppermint oiloil 0.10%0.10% 시나몬cinnamon oiloil 0.10%0.10% 멘톨menthol oiloil 0.10%0.10% 메틸안드라닐레이트Methylandranilate oiloil 0.70%0.70% 자외선흡수제UV absorber oiloil 0.03%0.03% 불가사리 추출물Starfish Extract 액상liquid 1.05%1.05% 녹차 추출물green tea extract 액상liquid 0.12%0.12% 핵심원료(計)Core raw materials 2.25%2.25% 부원료auxiliary material 페녹시에탄올Phenoxyethanol -- 0.50%0.50% 알코올Alcohol -- 4.32%4.32% TEATEA -- 0.20%0.20% CARBOPOL(940)CARBOPOL(940) 분말powder 0.20%0.20% 계면활성제(tween20)Surfactant (tween20) -- 3.14%3.14% 부원료(計)Sub-ingredient (計) 8.36%8.36% 첨가물additive 정제수Purified water 액상liquid 64.39%64.39% 제오라이트 침출수Zeolite Leachate 액상liquid 25.00%25.00% 총계sum 100%100%

실험예Experimental example 1. 본 발명 조류기피제 조성물의 1. Of the present invention bird repellent composition 필드테스트field test 평가 evaluation

본 발명에 따른 실시예 1 내지 실시예 7에서 얻은 본 발명 제 1차 내지 제 7차 조류기피제 조성물의 기피효과를 확인하기 위하여 경기도 성남시 야탑동 소재의 공원에서 서식하는 비둘기를 대상으로 본 발명 조류기피제 조성물의 적응 여부를 평가하였다. 평가 방법은 실험군으로 사료 옆에 실시예 1 내지 실시예 7 에서 얻은 본 발명 조류기피제를 각각 위치시키고 대조구는 사료만을 방치하여 7시간 동안 비둘기의 반응을 관찰평가하였다.In order to confirm the repelling effect of the first to seventh bird repellent compositions of the present invention obtained in Examples 1 to 7 according to the present invention, the present invention bird repellent composition for pigeons living in a park located in Yatap-dong, Seongnam-si, Gyeonggi-do was evaluated for adaptation. As an evaluation method, the bird repellents of the present invention obtained in Examples 1 to 7 were respectively placed next to the feed as an experimental group, and the control group was left alone with the feed to observe and evaluate the pigeon's response for 7 hours.

실험결과 본 발명 모든 제 1차 내지 제 7차 조류기피제 조성물에서 비둘기의 기피반응이 나타났으며, 특히 제 5차 조류기피제 조성물에서 머리를 흔들거나 극도의 흥분상태를 나타내는 등 강한 기피 효과를 나타냈다(도 2). 제 5차 조류기피제 조성물, 제 6차 조류기피제 조성물 및 제 4차 조류기피제 조성물 순으로 조류 기피 효과가 높게 나타났다.
As a result of the experiment, all of the first to seventh bird repellent compositions of the present invention showed a pigeon repellent reaction, and in particular, the fifth bird repellent composition showed a strong repellent effect such as shaking the head or showing an extremely excited state ( 2). The 5th algae repellent composition, the 6th algae repellent composition, and the 4th algae repellent composition showed a high algae repellent effect in that order.

실험예Experimental example 2. 실내 조류 기피 효능평가 2. Indoor bird repelling efficacy evaluation

경기도 성남시 야탑동 소재의 공원에서 정상적인 먹이활동을 하는 비둘기를 포획하여 사용하였다. 포획한 비둘기는 실험실 조건에서 일주일간 순화기간을 거쳐 이상 반응을 보이지 않는 개체 10마리를 공시조류로 사용하였다.Pigeons with normal feeding activities were captured and used in a park located in Yatap-dong, Seongnam-si, Gyeonggi-do. The captured pigeons were acclimatized for a week under laboratory conditions, and 10 animals that did not show any abnormal reaction were used as test birds.

실험은 본 발명 조류기피제 조성물을 첨가하지 않은 사료를 급여한 5마리의 대조군 및 사료 옆에 필드테스트 결과 가장 효과가 뛰어났던 본 발명 제 5차 조류기피제 조성물를 첨가한 5마리의 실험군을 이용하여 실험하였다. 5일간 비디오 카메라로 촬영하여 공시조류의 반응 및 이상 행동유무를 관찰하였다.The experiment was conducted using a control group of 5 animals fed a feed without the addition of the bird repellent composition of the present invention and a group of 5 animals to which the fifth bird repellent composition of the present invention was added, which was the most effective as a result of a field test next to the feed. . The reaction and abnormal behavior of the specimens were observed by filming with a video camera for 5 days.

실험결과 대조군의 경우 급여하는 모든 사료를 섭취하였으나, 본 발명 조류기피제 조성물을 첨가한 사료를 급여한 실험군의 경우 초기엔 사료에 다가가지 않았으나 일정시간 이후 허기짐으로 인해 사료를 섭취하는 것을 확인하였다. 그러나 실험군 중 가장 많은 사료를 섭취한 3일차의 경우에도 대조군에 비해 40% 수준으로 사료기피 효과를 나타냈다(도 3).
As a result of the experiment, the control group consumed all the feed, but in the case of the experimental group fed the feed containing the bird repellent composition of the present invention, it did not approach the feed at the beginning, but it was confirmed that the feed was consumed due to hunger after a certain period of time. However, even on the 3rd day, when the most feed was consumed among the experimental groups, the effect of avoiding feed was exhibited at a level of 40% compared to the control group (FIG. 3).

실험예Experimental example 3. 본 발명 조류기피제 조성물의 자외선 흡수 측정 3. Measurement of UV absorption of the algae repellent composition of the present invention

본 발명에 따른 실시예 1 내지 실시예 7에서 얻은 본 발명 제 1차 내지 제 7차 조류기피제 조성물의 자외선(UV) 흡광도를 측정하였다. 본 발명 조류기피제 조성물을 증류수로 102배 희석한 후 이를 석영 96 well plate에 200 ㎕ 분주하였다. ELISA Reader(SPECTRAMAX 190, Molecular Devices)를 이용하여 UV 파장 260 nm 내지 400 nm 범위에서 흡광도를 측정하였다. 측정 결과 파장의 흡수 가장 모든 시료가 310 내지 350 nm에서 가장 높은 흡광도를 보였으며 특히, 가장 강한 조류기피 효능을 보인 제 5차 조류기피제 조성물의 경우 320 내지 330 nms에서의 흡광도가 가장 높게 나타나 본 발명 조류기피제 조성물은 조류가 기피하는 UV-A 파장을 나타내는 것을 확인하였다(도 4).The ultraviolet (UV) absorbance of the first to seventh algae repellent compositions of the present invention obtained in Examples 1 to 7 according to the present invention was measured. After diluting the algae repellent composition of the present invention 10 to 2 times with distilled water, 200 μl was dispensed into a quartz 96 well plate. Absorbance was measured in the UV wavelength range of 260 nm to 400 nm using an ELISA Reader (SPECTRAMAX 190, Molecular Devices). As a result of the measurement, the absorption of wavelengths of all samples showed the highest absorbance at 310 to 350 nm, and in particular, in the case of the 5th algae repellent composition, which showed the strongest algae repellent effect, the absorbance at 320 to 330 nms was the highest in the present invention It was confirmed that the algae repellent composition exhibits a UV-A wavelength that algae avoid (FIG. 4).

본 발명 제 5차 조류기피제 조성물을 증류수로 103배, 102배 및 10배 희석하고 대조군으로 증류수를 사용하여 석영 Cuvette에 각각 1 mL 씩 분주하고 이에 자외선을 투과시켜 측정한 결과 농도가 낮아짐에 따라 흡광도 역시 낮아짐을 확인하였다(도 5).The fifth algae repellent composition of the present invention was diluted 10 3 times, 10 2 times, and 10 times with distilled water, and 1 mL each was dispensed into a quartz cuvette using distilled water as a control. Accordingly, it was confirmed that the absorbance was also lowered (FIG. 5).

따라서, 본 발명의 적용예로서 상기 실시예 1 내지 7에서 제조한 조류기피제 조성물을 이용하여 조류피해 방지용 조류기피제를 제조할 수 있었다(도 6).
Therefore, as an application example of the present invention, it was possible to prepare a bird repellent for preventing damage to birds by using the bird repellent compositions prepared in Examples 1 to 7 (FIG. 6).

이상 설명한 바와 같이 본 발명은 천연 오일성분을 유효성분으로 함유하는 신규한 조류기피제 조성물을 제공하는 효과가 있고 아울러 점증성과 기피성이 뛰어난 조류기피제의 제조방법을 제공하는 효과가 있어 조류피해로 인한 농작물 및 주변 시설물의 피해를 현저히 저하시키는 뛰어난 효과가 있으므로 농산업 및 환경산업상 매우 유용한 발명인 것이다.
As described above, the present invention has the effect of providing a novel bird repellent composition containing a natural oil component as an active ingredient, and also has the effect of providing a method for manufacturing a bird repellent excellent in thickening properties and repellent properties. And it is a very useful invention in the agricultural and environmental industries because it has an excellent effect of significantly reducing the damage to the surrounding facilities.

Claims (9)

(a) 캡시컴, 타임(Thyme), 페퍼민트, 라벤더, 시더우드, 님(Neem), 시나몬, 멘톨, 메틸안드라닐레이트 및 시너메이트로 구성된 군에서 선택되는 둘 이상의 천연 오일성분 및 계면활성제를 혼합하는 단계;
(b) 은행잎 추출물, 어성초 추출물, 불가사리 추출물 및 녹차 추출물의 천연 액상성분을 제오라이트 침출수와 함께 혼합하는 단계;
(c) 상기 (a)단계에서 얻은 혼합물을 알코올과 혼합하는 단계;
(d) 카보풀(CARBOPOL)을 증류수에 용해하는 단계;
(e) 상기 (b) 내지 (d)단계에서 얻은 혼합물을 동일한 부피비로 배합하고 다시 혼합하는 단계;
(f) 상기 (e)단계에서 얻은 혼합물에 페녹시에탄올 및 TEA를 첨가하여 점도를 증진시키는 단계;
(g) 상기 (f)단계에서 얻은 증점성 혼합물에 전체 조성물의 100 부피%가 되도록 정제수를 첨가하고 다시 혼합하여 제품화하는 단계를 포함하는 조류기피제 조성물 제조방법에 있어서,
상기 (b)단계에서 은행잎 추출물은 전체 조성물의 0.25 부피%, 어성초 추출물은 전체 조성물의 0.1 부피%, 불가사리 추출물은 전체 조성물의 1 내지 5 부피% 및 녹차 추출물은 전체 조성물의 0.1 내지 0.12 부피%로 첨가되는 것이 특징인 조류기피제 조성물 제조방법
(a) Capsicum, thyme, peppermint, lavender, cedarwood, neem, cinnamon, menthol, methylandranilate and cinnamate are mixed with two or more natural oil components and surfactants to do;
(b) mixing the natural liquid components of ginkgo leaf extract, eoseongcho extract, starfish extract and green tea extract with zeolite leachate;
(c) mixing the mixture obtained in step (a) with alcohol;
(d) dissolving CARBOPOL in distilled water;
(e) mixing the mixture obtained in steps (b) to (d) in the same volume ratio and mixing again;
(f) increasing the viscosity by adding phenoxyethanol and TEA to the mixture obtained in step (e);
(g) in the algae repellent composition manufacturing method comprising the step of adding purified water to the thickening mixture obtained in step (f) so as to be 100% by volume of the total composition and mixing again to commercialize,
In step (b), the ginkgo leaf extract is 0.25% by volume of the total composition, the eosinthia extract is 0.1% by volume of the total composition, the starfish extract is 1 to 5% by volume of the total composition, and the green tea extract is 0.1 to 0.12% by volume of the total composition. Method for producing a bird repellent composition characterized in that it is added
제 1항에 있어서, (a)단계의 캡시컴은 전체 조성물의 0.04 내지 1 부피%, 타임(Thyme)은 전체 조성물의 0.05 내지 0.44 부피%, 페퍼민트는 전체 조성물의 0.05 내지 0.46 부피%, 라벤더는 전체 조성물의 0.2 내지 0.44 부피%, 시더우드는 전체 조성물의 0.02 부피%, 님(Neem)은 전체 조성물의 0.1 부피%, 시나몬은 전체 조성물의 0.03 내지 0.10 부피%, 멘톨은 전체 조성물의 0.1 부피%, 메틸안드라닐레이트는 전체 조성물의 0.5 내지 3 부피% 및 시너메이트는 전체 조성물의 0.03 부피%를 첨가하는 것이 특징인 조류기피제 조성물 제조방법According to claim 1, wherein the capsicum of step (a) is 0.04 to 1% by volume of the total composition, Thyme is 0.05 to 0.44% by volume of the total composition, Peppermint is 0.05 to 0.46% by volume of the total composition, Lavender is 0.2 to 0.44% by volume of the total composition, cedarwood is 0.02% by volume of the total composition, Neem is 0.1% by volume of the total composition, cinnamon is 0.03 to 0.10% by volume of the total composition, menthol is 0.1% by volume of the total composition , methylandranilate is 0.5 to 3% by volume of the total composition, and cinnamate is a method for producing a bird repellent composition, characterized in that adding 0.03% by volume of the total composition 삭제delete 제 1항에 있어서, (c)단계의 알코올은 전체 조성물의 2.25 내지 10 부피%를 첨가하여 혼합하는 것이 특징인 조류기피제 조성물 제조방법The method according to claim 1, wherein the alcohol in step (c) is mixed by adding 2.25 to 10% by volume of the total composition. 제 1항에 있어서, (d) 단계의 증류수에 용해한 카보풀은 0.1 내지 0.2 부피%인 것이 특징인 조류기피제 조성물 제조방법The method according to claim 1, wherein the amount of carbopool dissolved in distilled water in step (d) is 0.1 to 0.2% by volume. 제 1항에 있어서, (f)단계의 페녹시에탄올은 전체 조성물의 0.5 부피%를 첨가하는 것이 특징인 조류기피제 조성물 제조방법The method according to claim 1, wherein the phenoxyethanol in step (f) is added in an amount of 0.5% by volume of the total composition. 제 1항에 있어서, (f)단계의 TEA는 전체 조성물의 0.1 내지 0.2 부피%를 첨가하는 것이 특징인 조류기피제 조성물 제조방법The method according to claim 1, wherein the TEA in step (f) is added in an amount of 0.1 to 0.2% by volume of the total composition. 제 1항에 있어서, (a) 단계의 계면활성제는 전체 조성물의 2.70 내지 12 부피%를 첨가하는 것이 특징인 조류기피제 조성물 제조방법The method according to claim 1, wherein the surfactant in step (a) is added in an amount of 2.70 to 12% by volume of the total composition. 삭제delete
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JP2010202570A (en) 2009-03-03 2010-09-16 Seiji Nakazato Repellent, method for producing the same, and production system
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JP2006096685A (en) * 2004-09-28 2006-04-13 Kazuyoshi Hoshino Composition for repelling small animal and small animal-repelling sheet
KR100798290B1 (en) 2007-05-28 2008-02-04 전진바이오팜 주식회사 Gel-type bird aversion compositions
JP2010202570A (en) 2009-03-03 2010-09-16 Seiji Nakazato Repellent, method for producing the same, and production system
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KR101192980B1 (en) * 2012-02-02 2012-10-24 (주)바이오디펜스 Manufacturing method of wildlife animal repellent composition

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