CN108048107A - It is a kind of for renovation agent of crops soil and preparation method thereof - Google Patents
It is a kind of for renovation agent of crops soil and preparation method thereof Download PDFInfo
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- CN108048107A CN108048107A CN201711363260.5A CN201711363260A CN108048107A CN 108048107 A CN108048107 A CN 108048107A CN 201711363260 A CN201711363260 A CN 201711363260A CN 108048107 A CN108048107 A CN 108048107A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K17/00—Soil-conditioning materials or soil-stabilising materials
- C09K17/40—Soil-conditioning materials or soil-stabilising materials containing mixtures of inorganic and organic compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
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- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Soil Sciences (AREA)
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Abstract
The invention discloses a kind of for renovation agent of crops soil and preparation method thereof, include the raw material of following parts by weight：46 parts of 1.6 3.4 parts of beta cyclodextrin, 36 parts of acrylamide, 16 24 parts of Tourmaline stone, 48 parts of chitosan, 8 12 parts of degradable resin, 68 parts of weathered coal, 47 parts of land plaster, 10 20 parts of stone needle, 5 10 parts of plant ash, 22 26 parts of butanol, 69 parts of precipitated calcium carbonate, 20 27 parts of bed-silt and fennel seeds.The present invention is by the interaction between various raw materials and is aided with suitable technique, and the finished product of preparation can enhance crops soil active soil stratum, improve soil physico-chemical property, increase soil trace element and rare earth element, promote crop growth, improve crop yield, improve the quality of agricultural product.
Description
Technical field
The present invention relates to soil remediation fields, are specifically a kind of renovation agent for crops soil.
Background technology
Crops refer to the various plants agriculturally cultivated, and are one kind of biology, including Liang food Zuo Wu ﹑ industrial crops (oil
Expect crop, vegetable crop, flower, grass, trees) two major classes.Edible crops are one of sources of the basic food of the mankind, " the people
To eat as day ", the relation of people and food is expressed, rational meals, which are arranged in pairs or groups, to bring health to the mankind.The self-sufficiency of food is certainly
Foot is only the basis of a national sustainable development.
The growth of crops be unable to do without soil, and soil refers to that top has fertility, the loose table for being capable of growing plant
Layer, thickness is generally in 2m or so.Soil is the basis of plant growth, for growth and development of plants provide required water, fertilizer,
The increase of the substances such as the fertility element such as air and heat, the pesticide used with people, chemical fertilizer, soil are contaminated, the soil being contaminated
Earth will cause crop production reduction, and quality reduces, it could even be possible to cause pollutant in agricultural product exceeded, and then harmful to human is good for
Health, so needing to repair the soil of crops.
The content of the invention
It is an object of the invention to provide a kind of renovation agent for crops soil, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical solution：
A kind of renovation agent for crops soil includes the raw material of following parts by weight：1.6-3.4 parts of beta-cyclodextrin, third
3-6 parts of acrylamide, 16-24 parts of Tourmaline stone, 4-8 parts of chitosan, 8-12 parts of degradable resin, 6-8 parts of weathered coal, land plaster 4-
7 parts, 10-20 parts of stone needle, 5-10 parts of plant ash, 22-26 parts of butanol, 6-9 parts of precipitated calcium carbonate, 20-27 parts of bed-silt and small
4-6 parts of fennel.
As further embodiment of the present invention：Degradable resin uses wheat stalk, broomcorn straw, sugarcane stalk and soybean
The preparation of at least one of stalk.
As further embodiment of the present invention：The granularity of Tourmaline stone, land plaster and stone needle is 50-60 mesh, weathered coal
Granularity is 10-20 mesh.
The preparation method of the renovation agent for crops soil, is as follows：
Fennel seeds are crushed and add in the ethyl alcohol of 6-8 times of its times of weight by step 1, when sealing immersion 8-12 is small, then
Ultrasonic extraction 10-15 minutes is extracted 2-4 times, and filtering and merging filtrate obtain fennel seeds extracting solution, by filter residue dries pulverizing
Into powder, fennel is obtained, it is spare；
Degradable resin and chitosan are crushed and are uniformly mixed, obtain the first mixture by step 2, by the first mixing
Object is immersed in 45-52 degrees Celsius of fennel seeds extracting solution and ultrasonic wave disperses 5-8 minutes, obtains the first mixed solution；
The mass percent that beta-cyclodextrin is dissolved in equivalent weight is in the ammonium hydroxide of 25-34%, obtains β-ring by step 3
Dextrin aqueous slkali；
Step 4 mixes Tourmaline stone, weathered coal, land plaster, stone needle, plant ash, precipitated calcium carbonate and bed-silt
And acrylamide is added dropwise, is stirred 20-30 minutes with the rotating speed of 600-1200rpm again after being added dropwise completely, it is mixed to obtain second
Close object；
Step 5 is abundant by the first mixed solution, butanol, fennel, beta-cyclodextrin aqueous slkali and the second mixture
Mixing adds in suitable quantity of water and when 880-960 degrees Celsius of heat preservation 4-6 is small, you can obtain finished product.
As further embodiment of the present invention：The mass fraction of ethyl alcohol is 75-85% in step 1, ultrasonic wave in step 1
The power of extraction is 800-1000W.
As further embodiment of the present invention：The temperature mixed in step 4 is 56-75 degrees Celsius.
Compared with prior art, the beneficial effects of the invention are as follows：Raw material sources of the present invention are extensive, by between various raw materials
Interaction and be aided with suitable technique, the finished product of preparation can enhance crops soil active soil stratum, improve soil physical chemistry
Property increases soil trace element and rare earth element, promotes crop growth, improves crop yield, improves the product of agricultural product
Matter meets the use demand of people.
Specific embodiment
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of renovation agent for crops soil includes the raw material of following parts by weight：1.6 parts of beta-cyclodextrin, acryloyl
3 parts of amine, 16 parts of Tourmaline stone, 4 parts of chitosan, 8 parts of degradable resin, 6 parts of weathered coal, 4 parts of land plaster, 10 parts of stone needle, vegetation
4 parts of 5 parts of ash, 22 parts of butanol, 6 parts of precipitated calcium carbonate, 20 parts of bed-silt and fennel seeds.Degradable resin uses wheat stalk system
It is standby.
The preparation method of the renovation agent for crops soil, is as follows：
Fennel seeds are crushed and add in the ethyl alcohol of 6 times of its times of weight by step 1, then ultrasonic when sealing immersion 10 is small
Extraction 12 minutes is extracted 3 times, and filtering and merging filtrate obtain fennel seeds extracting solution, by filter residue dries pulverizing into powder, obtain
It is spare to fennel；
Degradable resin and chitosan are crushed and are uniformly mixed, obtain the first mixture by step 2, by the first mixing
Object is immersed in 48 degrees Celsius of fennel seeds extracting solution and ultrasonic wave disperses 6 minutes, obtains the first mixed solution；
The mass percent that beta-cyclodextrin is dissolved in equivalent weight is in 27% ammonium hydroxide, obtains β-ring paste by step 3
Smart aqueous slkali；
Step 4 mixes Tourmaline stone, weathered coal, land plaster, stone needle, plant ash, precipitated calcium carbonate and bed-silt
And acrylamide is added dropwise, is stirred 24 minutes with the rotating speed of 800rpm again after being added dropwise completely, obtains the second mixture；
Step 5 is abundant by the first mixed solution, butanol, fennel, beta-cyclodextrin aqueous slkali and the second mixture
Mixing adds in suitable quantity of water and when 890 degrees Celsius of heat preservations 5 are small, you can obtain finished product.
Embodiment 2
A kind of renovation agent for crops soil includes the raw material of following parts by weight：2.5 parts of beta-cyclodextrin, acryloyl
4.5 parts of amine, 19 parts of Tourmaline stone, 5.5 parts of chitosan, 10 parts of degradable resin, 6.8 parts of weathered coal, 5.5 parts of land plaster, stone needle
5.2 parts of 14 parts, 7 parts of plant ash, 24 parts of butanol, 7.5 parts of precipitated calcium carbonate, 23 parts of bed-silt and fennel seeds.Tourmaline stone, stone
The granularity of cream powder and stone needle is 50 mesh, and the granularity of weathered coal is 10 mesh.
The preparation method of the renovation agent for crops soil, is as follows：
Fennel seeds are crushed and add in the ethyl alcohol of 8 times of its times of weight by step 1, then ultrasonic when sealing immersion 12 is small
Extraction 13 minutes is extracted 4 times, and filtering and merging filtrate obtain fennel seeds extracting solution, by filter residue dries pulverizing into powder, obtain
It is spare to fennel；
Degradable resin and chitosan are crushed and are uniformly mixed, obtain the first mixture by step 2, by the first mixing
Object is immersed in 50 degrees Celsius of fennel seeds extracting solution and ultrasonic wave disperses 7 minutes, obtains the first mixed solution；
The mass percent that beta-cyclodextrin is dissolved in equivalent weight is in 32% ammonium hydroxide, obtains β-ring paste by step 3
Smart aqueous slkali；
Step 4, by Tourmaline stone, weathered coal, land plaster, stone needle, plant ash, precipitated calcium carbonate and bed-silt 64
It degree Celsius mixes and acrylamide is added dropwise, stirred 26 minutes with the rotating speed of 1050rpm again after being added dropwise completely, obtain second
Mixture；
Step 5 is abundant by the first mixed solution, butanol, fennel, beta-cyclodextrin aqueous slkali and the second mixture
Mixing adds in suitable quantity of water and when 930 degrees Celsius of heat preservations 4 are small, you can obtain finished product.
Embodiment 3
A kind of renovation agent for crops soil includes the raw material of following parts by weight：2.9 parts of beta-cyclodextrin, acryloyl
5 parts of amine, 22 parts of Tourmaline stone, 7 parts of chitosan, 11 parts of degradable resin, 7.8 parts of weathered coal, 6 parts of land plaster, 18 parts of stone needle, grass
5.5 parts of 8 parts of wood ash, 24.6 parts of butanol, 8 parts of precipitated calcium carbonate, 25 parts of bed-silt and fennel seeds.Degradable resin uses wheat
It is prepared by the mixture in stalk, sugarcane stalk and soybean stalk.
The preparation method of the renovation agent for crops soil, is as follows：
The mass fraction that fennel seeds crushed and added in 7 times of its times of weight is 80% ethyl alcohol by step 1, and sealing is impregnated
10 it is small when, then carry out ultrasonic extraction 14 minutes in 860W power, extract 2 times, filter and merging filtrate, obtain fennel seeds and carry
Liquid is taken, by filter residue dries pulverizing into powder, obtains fennel, it is spare；
Degradable resin and chitosan are crushed and are uniformly mixed, obtain the first mixture by step 2, by the first mixing
Object is immersed in 50 degrees Celsius of fennel seeds extracting solution and ultrasonic wave disperses 6 minutes, obtains the first mixed solution；
The mass percent that beta-cyclodextrin is dissolved in equivalent weight is in 32% ammonium hydroxide, obtains β-ring paste by step 3
Smart aqueous slkali；
Step 4 mixes Tourmaline stone, weathered coal, land plaster, stone needle, plant ash, precipitated calcium carbonate and bed-silt
And acrylamide is added dropwise, is stirred 28 minutes with the rotating speed of 750rpm again after being added dropwise completely, obtains the second mixture；
Step 5 is abundant by the first mixed solution, butanol, fennel, beta-cyclodextrin aqueous slkali and the second mixture
Mixing adds in suitable quantity of water and when 920 degrees Celsius of heat preservations 5 are small, you can obtain finished product.
Embodiment 4
A kind of renovation agent for crops soil includes the raw material of following parts by weight：3.4 parts of beta-cyclodextrin, acryloyl
6 parts of amine, 24 parts of Tourmaline stone, 8 parts of chitosan, 12 parts of degradable resin, 8 parts of weathered coal, 7 parts of land plaster, 20 parts of stone needle, vegetation
6 parts of 10 parts of ash, 26 parts of butanol, 9 parts of precipitated calcium carbonate, 27 parts of bed-silt and fennel seeds.Degradable resin using wheat stalk,
It is prepared by the mixture of broomcorn straw, sugarcane stalk and soybean stalk.The granularity of Tourmaline stone, land plaster and stone needle be 60 mesh, wind
The granularity for changing coal is 10 mesh.
The preparation method of the renovation agent for crops soil, is as follows：
The mass fraction that fennel seeds crushed and added in 8 times of its times of weight is 85% ethyl alcohol by step 1, and sealing is impregnated
12 it is small when, then carry out ultrasonic extraction 15 minutes in the power of 950W, extract 4 times, filter and merging filtrate, obtain fennel seeds
Extracting solution by filter residue dries pulverizing into powder, obtains fennel, spare；
Degradable resin and chitosan are crushed and are uniformly mixed, obtain the first mixture by step 2, by the first mixing
Object is immersed in 52 degrees Celsius of fennel seeds extracting solution and ultrasonic wave disperses 8 minutes, obtains the first mixed solution；
The mass percent that beta-cyclodextrin is dissolved in equivalent weight is in 30% ammonium hydroxide, obtains β-ring paste by step 3
Smart aqueous slkali；
Step 4, by Tourmaline stone, weathered coal, land plaster, stone needle, plant ash, precipitated calcium carbonate and bed-silt 72
It degree Celsius mixes and acrylamide is added dropwise, stirred 28 minutes with the rotating speed of 1200rpm again after being added dropwise completely, obtain second
Mixture；
Step 5 is abundant by the first mixed solution, butanol, fennel, beta-cyclodextrin aqueous slkali and the second mixture
Mixing adds in suitable quantity of water and when 950 degrees Celsius of heat preservations 5 are small, you can obtain finished product.
Comparative example 1
Except fennel seeds are not contained, remaining component and preparation method are same as Example 2.
The product of embodiment 1-4 and the product of comparative example 1 spread same Chinese cabbage according to 130kg/ mus of amount
It applies, site preparation and plough, the Chinese cabbage of yield and harvest is detected, testing result is shown in Table 1.
Table 1
From table 1 it follows that under Isodose, the Chinese cabbage yield that the product of embodiment 1-4 obtains is more than comparative example 1
The obtained Chinese cabbage yield of product, do not detect in the Chinese cabbage that the product of embodiment 1-4 obtains harmful mercury, lead,
Chromium, arsenic and cadmium, edible safety, detect in the Chinese cabbage that the product of comparative example 1 obtains harmful mercury, lead, chromium, arsenic and
Cadmium has hidden danger to the health of human body.
Stone needle is a kind of micrite minerals, contains strontium, calcium oxide, silica, sodium oxide molybdena, chromium, manganese, nickel, copper, yttrium etc.
The trace element beneficial to human body more than 36 kinds and rare earth element, while penetrated in stone needle containing metallicses far infrareds such as copper, iron
Line can generate extra-far infrared radiation, and frequency band is extremely wide, and Far-Infrared Frequency coverage is 7-20 microns, and far infrared can ooze
Thoroughly to crops deep layer position, fortification of plants cell, promotion Nutrient Cycle.Tourmaline is also known as tourmaline, tourmaline, is silicate
Class-borosilicate substance in all-transparent, translucent, has piezoelectric effect.Tourmaline is containing there are many necessary micro members of the mankind
Element is splendid mineral origin, can generate a large amount of negative oxygen ions, can adjust soil ion balance, have reactivity.Make soil
The a large amount of anions (OH) of earth generation-, anion and hydrone (H2O)-combine to form hydroxyl ion water (H3O2)-, forms small point
Son group water, so as to obtain soil ion active function.This product changes degradable resin with chitosan in fennel seeds extracting solution
Property, then be attached in the main bodys of formation such as acrylic amide modified Tourmaline stone, stone needle, bed-silt, there is slow releasing function, it can
To enhance crops soil active soil stratum, improve soil physico-chemical property, increase soil trace element and rare earth element, promote crops
Growth improves crop yield, improves the quality of agricultural product, long action time.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requirement rather than above description limit, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
Moreover, it will be appreciated that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
Using specification as an entirety, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (6)
1. a kind of renovation agent for crops soil, which is characterized in that include the raw material of following parts by weight：Beta-cyclodextrin 1.6-
3.4 parts, 3-6 parts of acrylamide, 16-24 parts of Tourmaline stone, 4-8 parts of chitosan, 8-12 parts of degradable resin, 6-8 parts of weathered coal,
4-7 parts of land plaster, 10-20 parts of stone needle, 5-10 parts of plant ash, 22-26 parts of butanol, 6-9 parts of precipitated calcium carbonate, bed-silt 20-
27 parts and 4-6 parts of fennel seeds.
2. the renovation agent according to claim 1 for crops soil, which is characterized in that the degradable resin uses
The preparation of at least one of wheat stalk, broomcorn straw, sugarcane stalk and soybean stalk.
3. the renovation agent according to claim 1 for crops soil, which is characterized in that the Tourmaline stone, gypsum
The granularity of powder and stone needle is 50-60 mesh, and the granularity of weathered coal is 10-20 mesh.
4. a kind of preparation method of renovation agent for crops soil as described in claim 1-3 is any, which is characterized in that
It is as follows：
Fennel seeds are crushed and add in the ethyl alcohol of 6-8 times of its times of weight by step 1, then ultrasonic when sealing immersion 8-12 is small
Extraction 10-15 minute is extracted 2-4 times, and filtering and merging filtrate obtain fennel seeds extracting solution, by filter residue dries pulverizing into powder
End obtains fennel, spare；
Degradable resin and chitosan are crushed and are uniformly mixed, obtained the first mixture, the first mixture is soaked by step 2
Bubble is in 45-52 degrees Celsius of fennel seeds extracting solution and ultrasonic wave disperses 5-8 minutes, obtains the first mixed solution；
The mass percent that beta-cyclodextrin is dissolved in equivalent weight is in the ammonium hydroxide of 25-34%, obtains beta-cyclodextrin by step 3
Aqueous slkali；
Step 4, by Tourmaline stone, weathered coal, land plaster, stone needle, plant ash, precipitated calcium carbonate and bed-silt mix and
Acrylamide is added dropwise, is stirred 20-30 minutes with the rotating speed of 600-1200rpm again after being added dropwise completely, obtains the second mixture；
First mixed solution, butanol, fennel, beta-cyclodextrin aqueous slkali and the second mixture are sufficiently mixed by step 5,
Add in suitable quantity of water and when 880-960 degrees Celsius of heat preservation 4-6 is small, you can obtain finished product.
5. the preparation method of the renovation agent according to claim 4 for crops soil, which is characterized in that the step
The mass fraction of ethyl alcohol is 75-85% in one, and the power of ultrasonic wave extraction is 800-1000W in step 1.
6. the preparation method of the renovation agent according to claim 4 for crops soil, which is characterized in that the step
The temperature mixed in four is 56-75 degrees Celsius.
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| CN108728109A (en) * | 2018-06-01 | 2018-11-02 | 湖南图强科技开发有限公司 | A kind of soil sanitation agent and preparation method thereof for Rice Cropping |
| CN109336345A (en) * | 2018-11-29 | 2019-02-15 | 福州宇澄环保工程设计有限公司 | A kind of black and odorous water bed mud biological modification agent |
| CN114262245A (en) * | 2020-09-16 | 2022-04-01 | 通海县金元有机肥有限公司 | Organic fertilizer capable of preventing soil hardening damage and production method thereof |
| CN114606008A (en) * | 2022-03-04 | 2022-06-10 | 深圳瑞新达新能源科技有限公司 | Soil modifier |
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| CN114262245A (en) * | 2020-09-16 | 2022-04-01 | 通海县金元有机肥有限公司 | Organic fertilizer capable of preventing soil hardening damage and production method thereof |
| CN114606008A (en) * | 2022-03-04 | 2022-06-10 | 深圳瑞新达新能源科技有限公司 | Soil modifier |
| CN114606008B (en) * | 2022-03-04 | 2023-12-08 | 深圳瑞新达新能源科技有限公司 | Soil modifier |
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Application publication date: 20180518 |