CN107998211A - Hair tonic composition and its preparation method and application - Google Patents
Hair tonic composition and its preparation method and application Download PDFInfo
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/236—Ligusticum (licorice-root)
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/47—Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/539—Scutellaria (skullcap)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/804—Rehmannia
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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Abstract
The present invention provides a kind of hair tonic composition and its preparation method and application, it is related to hair-care technical field.The hair tonic composition is mainly with cacumen biotae, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, lopseed, chrysanthemum, radix astragali, glutinous rehmannia etc. is raw material, according to the natural pharmacology of each raw material, collaboration compatibility effect between pharmacological property and each raw material, and it is directed to skin of head hair physiological structure feature and outside environmental elements, utilize the osmosis of herbal plant itself, hair follicle pathological tissues are cleared up, repair, supplement nutrition needed for hair growth, improve peripheral blood circulation, improve influence of the extraneous growing environment to hair follicle tissue, hair growth is set to recover normal, the hair tonic composition has good Anti-hair loss, the effect of promoting kainogenesis long, and without obvious toxicity, it is undesirable to improve existing product Anti-hair loss effect, and there are the problem of toxicity for part；Present invention also offers the preparation method and application of hair tonic composition.
Description
Technical field
The present invention relates to hair-care technical field, in particular to a kind of hair tonic composition and its preparation side
Method and application.
Background technology
With social progress and development, the stress of modern increasingly increases.Substantial amounts of clinical and experimental data table
Bright, excessive in stress, liquid, which is adjusted, under the influence of the mental element such as depressed, irritated, oppressive, insomnia, in human body easily occurs
Stress reaction, triggers hidrosis, hypersteatosis, and male sex hormone produces the symptom such as excessive, so that cause hair follicle disease, it is such as common
Fatigue can induce nervous baldness or alopecia seborrheica.Nervous baldness or alopecia seborrheica directly influence people
Image, undoubtedly brought very big puzzlement.
At present, occurs the product of a variety of prevention nervous baldness or alopecia seborrheica on the market, but such product is prevented
Alopecia (especially alopecia late period) effect is bad, and there are toxicity for part.
In view of this, it is special to propose the present invention to solve above-mentioned technical problem.
The content of the invention
The present invention first purpose be to provide a kind of hair tonic composition, mainly by plurality of Chinese material combination and
Into being acted on by coordinated between each Chinese medicine material so that obtained hair tonic composition to nervous baldness or
Alopecia seborrheica has good effect, and without obvious toxic-side effects, improves existing product Anti-hair loss effect on the market and pay no attention to
Think, and there are the problem of toxicity for part.
Second object of the present invention is to provide a kind of preparation method of hair tonic composition, by using specific system
Standby step extracts the active ingredient in each raw material so that and component obtains reservation as much as possible the effect of in each raw material, meanwhile, should
Preparation method is simple, easy, is suitable for industrially mass producing.
Third object of the present invention is to provide a kind of application of hair tonic composition.
In order to realize the above-mentioned purpose of the present invention, spy uses following technical scheme：
The present invention provides a kind of hair tonic composition, includes the raw material of following parts by weight：15-25 parts of cacumen biotae, it is sweet
It is 10-20 parts careless, 20-30 parts of Semen sesami nigrum, 15-25 parts of Angelica sinensis, 15-25 parts of rhizome of chuanxiong, 20-30 parts of radix scutellariae, 20-30 parts of lopseed, chrysanthemum
2500-3500 parts of 5-15 parts of flower, 5-15 parts of radix astragali, 15-25 parts of glutinous rehmannia and solvent.
Further, the hair tonic composition, includes the raw material of following parts by weight：16-24 parts of cacumen biotae, it is sweet
It is 12-20 parts careless, 22-30 parts of Semen sesami nigrum, 16-25 parts of Angelica sinensis, 16-25 parts of rhizome of chuanxiong, 22-30 parts of radix scutellariae, 22-30 parts of lopseed, chrysanthemum
2500-3500 parts of 6-15 parts of flower, 6-15 parts of radix astragali, 16-24 parts of glutinous rehmannia and solvent.
Further, the hair tonic composition, includes the raw material of following parts by weight：Including following parts by weight
Raw material：18-22 parts of cacumen biotae, 12-18 parts of radix glycyrrhizae, 22-28 parts of Semen sesami nigrum, 18-24 parts of Angelica sinensis, 18-24 parts of rhizome of chuanxiong, radix scutellariae
22-28 parts, 22-28 parts of lopseed, 7-14 parts of chrysanthemum, 6-14 parts of radix astragali, 2600-3400 parts of 18-22 parts of glutinous rehmannia and solvent；
Preferably, the hair tonic composition, includes the raw material of following parts by weight：20 parts of cacumen biotae, radix glycyrrhizae 15
Part, 25 parts of Semen sesami nigrum, 20 parts of Angelica sinensis, 20 parts of rhizome of chuanxiong, 25 parts of radix scutellariae, 25 parts of lopseed, 10 parts of chrysanthemum, 10 parts of radix astragali, glutinous rehmannia 20
3000 parts of part and solvent.
Further, the solvent is ethanol water, wherein, the weight ratio of ethanol and water is 1 in ethanol water：
(0.5-1.5)。
Further, the hair tonic composition, further includes the preservative that parts by weight are 1-10 parts；
Preferably, the preservative includes Phenoxyethanol or Sensiva SC50；
Preferably, the preservative includes Phenoxyethanol and Sensiva SC50, and the Phenoxyethanol and ethylhexyl are sweet
The weight ratio of oil is (1-10)：1.
Further, each raw material of the hair tonic composition is deposited in the form of Chinese medicine or Chinese medicinal material extract
.
Further, the hair tonic composition is creme, emulsion agent, solution, film or Sprayable.
Present invention also offers a kind of preparation method of hair tonic composition, comprise the following steps：
By the cacumen biotae of formula ratio existing in the form of Chinese medicine, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, lopseed,
Preservative mixes with solvent and optionally for chrysanthemum, radix astragali, glutinous rehmannia, soaks more than 40 days, and separation, obtains hair tonic composition；
Or, by the cacumen biotae of formula ratio existing in the form of Chinese medical extract, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae,
Preservative mixes with solvent and optionally for lopseed, chrysanthemum, radix astragali, glutinous rehmannia, is warming up to each dissolution of raw material, and insulation, obtains hair
Tonic composition.
Further, when prepared by each raw material existing for use in the form of Chinese medical extract, warming temperature 60-65
℃；
Preferably, soaking time 15-40min.
Present invention also offers application of the above-mentioned hair tonic composition in Anti-hair loss, the long field of promotion kainogenesis.
Compared with prior art, hair tonic composition provided by the invention and preparation method thereof has below beneficial to effect
Fruit：
(1) the present invention provides a kind of hair tonic composition, mainly with cacumen biotae, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong,
The Chinese herbal medicines such as radix scutellariae, lopseed, chrysanthemum, radix astragali, glutinous rehmannia are raw material, according to the natural pharmacology, pharmacological property and each raw material of each raw material
Between compatibility synergistic effect, and be directed to skin of head hair physiological structure feature and outside environmental elements, utilize book on Chinese herbal medicine to plant
The osmosis of thing itself, clears up hair follicle pathological tissues, is repaired, supplementing nutrition needed for hair growth, improving Peripheral blood
Liquid circulates, and improves influence of the extraneous growing environment to hair follicle tissue, hair growth is recovered normal, hair tonic composition tool
There is good Anti-hair loss, promote the performance of kainogenesis length, clinical laboratory data shows, smears the hair tonic composition on request
Afterwards, have good effect for nervous baldness or alopecia seborrheica, 7 days or so can Anti-hair loss, 20 days or so visible new hairs are again
Raw, and without obvious toxicity, it is undesirable to improve existing product Anti-hair loss effect on the market, and there are toxicity for part
The problem of.
(2) the present invention provides the preparation method of hair tonic composition, it is carefully dished up by special process so that each original
Active ingredient in material is sufficiently reserved, meanwhile, the preparation method is simple and practicable, is suitable for industrially mass producing.
(3) present invention also offers the application of hair tonic composition, in view of possessed by above-mentioned hair tonic composition
Advantage so that it has good application in Anti-hair loss, the long field of promotion kainogenesis.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person, the condition suggested according to normal condition or manufacturer carry out.Reagents or instruments used without specified manufacturer, is
The conventional products that can be obtained by commercially available purchase.
According to the first aspect of the invention, there is provided a kind of hair tonic composition, includes the original of following parts by weight
Material：15-25 parts of cacumen biotae, 10-20 parts of radix glycyrrhizae, 20-30 parts of Semen sesami nigrum, 15-25 parts of Angelica sinensis, 15-25 parts of rhizome of chuanxiong, radix scutellariae 20-30
2500-3500 parts of part, 20-30 parts of lopseed, 5-15 parts of chrysanthemum, 5-15 parts of radix astragali, 15-25 parts of glutinous rehmannia and solvent.
Hair tonic composition provided by the invention, mainly with cacumen biotae, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, thoroughly
The Chinese herbal medicines such as bone grass, chrysanthemum, radix astragali, glutinous rehmannia are raw material, according to matching somebody with somebody between the natural pharmacology, pharmacological property and each raw material of each raw material
5 synergistic effects, and skin of head hair physiological structure feature and outside environmental elements are directed to, utilize herbal plant itself
Osmosis, clears up hair follicle pathological tissues, is repaired, supplementing nutrition needed for hair growth, improves peripheral blood circulation, changes
Influence of the kind external world's growing environment to hair follicle tissue, makes hair growth recover normal, which has good
Anti-hair loss, the performance for promoting kainogenesis length, there is good effect for nervous baldness or alopecia seborrheica, and secondary without obvious poison
Reaction, it is undesirable to improve existing product Anti-hair loss effect on the market, and there are the problem of toxicity for part.
Specifically, cacumen biotae is the drying branch and leaf of cupressaceae plant arbor-vitae.Contain volatile oil in cacumen biotae, be mainly in oil
Fenchone, camphor, Bronyl acetate, terpene alcohol；And Quercetin containing juniperic acid, poplar luteoxanthin, Kaempferide, hinokiflavone, wax etc..
Its is cold in nature, bitter and puckery flavor, cures mainly cooling blood and hemostasis, growing and blacking hair.The parts by weight of cacumen biotae are preferably 16-24 parts, further preferably
For 18-22 parts.The typical but non-limiting parts by weight of cacumen biotae are 15 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts or 25
Part.
Radix glycyrrhizae, perennial herb, root is sturdy with root-like stock, is a kind of help Chinese herbal medicine.The parts by weight of radix glycyrrhizae are preferably
12-20 parts, more preferably 12-18 parts.The typical but non-limiting parts by weight of radix glycyrrhizae for 10 parts, 11 parts, 12 parts, 13
Part, 14 parts, 15 parts, 16 parts, 18 parts, 19 parts or 20 parts.
Semen sesami nigrum beneficial to liver, kidney tonifying, blood-nourishing, moisturize, black hair, beautification function.The parts by weight of Semen sesami nigrum are preferably 22-30
Part, more preferably 22-28 parts.The typical but non-limiting parts by weight of Semen sesami nigrum for 30 parts, 31 parts, 32 parts, 33 parts,
34 parts, 35 parts, 36 parts, 37 parts, 38 parts, 39 parts or 40 parts.
Angelica sinensis has expansion blood vessel, improves the effect such as microcirculation, anti-inflammatory, can improve the nutrition of scalp and hair follicle, promote
The growth of hair.The parts by weight of Angelica sinensis are preferably 16-25 parts, and more preferably 18-24 parts, Angelica sinensis is typical but non-limiting
Parts by weight be 15 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts or 25 parts.
Rhizome of chuanxiong, is irregular nodular pattern fist shape agglomerate, gas giving off a strong fragrance, bitter, pungent, can expanded head capillary, promote blood
Liquid circulates, and increases hair, and hair can be made to have good pliability, is not easy to become fragile, and white hair can be delayed to grow, and keeps hair profit
The parts by weight of sliding gloss rhizome of chuanxiong are preferably 16-25 parts, more preferably 18-24 parts.Rhizome of chuanxiong is typical but non-limiting heavy
It is 15 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts or 25 parts to measure number.
Radix scutellariae, alias Radix Scutellariae, tsuchikane tea root, are lamiaceae labiatae scutellaria herbaceos perennials.The parts by weight of radix scutellariae
Preferably 22-30 parts, more preferably 22-28 parts.The typical but non-limiting parts by weight of radix scutellariae for 20 parts, 21 parts, 22
Part, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts or 30 parts.
Lopseed also known as medicine Anacamptis pyromaidalis, perennial herb, acrid flavour, hardship are warm-natured, have effects that dispelling wind and eliminating dampness, promoting blood circulation and stopping pain.
The parts by weight of lopseed are preferably 22-30 parts, more preferably 22-28 parts.The typical but non-limiting weight of lopseed
Number is 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts or 30 parts.
Chrysanthemum is the perennial herb plant of composite family, Chrysanthemum in Plant Taxonomy.The parts by weight of chrysanthemum are preferred
For 6-15 parts, more preferably 7-14 parts.Typical but non-limiting parts by weight for 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10
Part, 11 parts, 12 parts, 13 parts, 14 parts or 15 parts.
Radix astragali, also known as continuous stilbene, perennial herb is sweet, tepor, can mend the gas of the whole body, have rising Yang, strengthening exterior and reducing sweat, apocenosis concurrently
Myogenic, inducing diuresis for removing edema effect.In the present invention, radix astragali is preferably Astragalus membranacus.The parts by weight of radix astragali are preferably 6-15 parts, into
One step is preferably 6-14 parts.The typical but non-limiting parts by weight of radix astragali for 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts,
12 parts, 13 parts, 14 parts or 15 parts.
Glutinous rehmannia Scrophulariaceae glutinous rehmannia category herbaceos perennial, clearing heat and promoting fluid, cooling blood and hemostasis.Available for consumption of YIN caused by febrile disease, polydipsia,
Spot dermexanthesis, spits blood, bleeding from five sense organs or subcutaneous tissue, abscess of throat etc..The parts by weight of glutinous rehmannia are preferably 16-24 parts, more preferably 18-22
Part.The typical but non-limiting parts by weight of glutinous rehmannia are 15 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts or 25 parts.
It should be noted that each raw material of above-mentioned hair tonic composition can exist in the form of Chinese medicine, can also
Exist in the form of Chinese medicinal material extract.
It should be noted that Chinese medicinal material extract of the present invention, for example, it is Cacumen Platycladi extract, licorice, black
Seed of Sesamum indicum L. extract, angelica extract, rhizome of chuanxiong extract, Baical Skullcap root P.E, Herba speranskiae tuberculatae extract, chrysanthemum extract, astragalus extraction
Thing, glutinous rehmannia extract etc. can extract to obtain by method well known to those skilled in the art.For example, take cacumen biotae appropriate, with
Appropriate vehicle soaks, and is extracted with suitable extracting method, supernatant liquid is obtained by filtration.Suitable extracting method and purification process choosing
From following one or several kinds：Immersion, decoction, reflux, overcritical, alcohol precipitation, extraction, column chromatography and UF membrane.
The effect of solvent mainly extracts the active ingredient in Chinese herbal medicine.The typical but non-limiting weight of solvent
Number for 2500 parts, 2600 parts, 2700 parts, 2800 parts, 2900 parts, 3000 parts, 3100 parts, 3200 parts, 3300 parts, 3400 parts or
3500 parts.
As a kind of preferred embodiment of the present invention, the hair tonic composition includes the original of following parts by weight
Material：16-24 parts of cacumen biotae, 12-20 parts of radix glycyrrhizae, 22-30 parts of Semen sesami nigrum, 16-25 parts of Angelica sinensis, 16-25 parts of rhizome of chuanxiong, radix scutellariae 22-30
2500-3500 parts of part, 22-30 parts of lopseed, 6-15 parts of chrysanthemum, 6-15 parts of radix astragali, 16-24 parts of glutinous rehmannia and solvent.
Preferably, the hair tonic composition includes the raw material of following parts by weight：18-22 parts of cacumen biotae, radix glycyrrhizae
12-18 parts, 22-28 parts of Semen sesami nigrum, 18-24 parts of Angelica sinensis, 18-24 parts of rhizome of chuanxiong, 22-28 parts of radix scutellariae, 22-28 parts of lopseed, chrysanthemum
7-14 parts, 6-14 parts of radix astragali, 2600-3400 parts of 18-22 parts of glutinous rehmannia and solvent；
It is further preferred that the hair tonic composition, include the raw material of following parts by weight：20 parts of cacumen biotae, it is sweet
15 parts of grass, 25 parts of Semen sesami nigrum, 20 parts of Angelica sinensis, 20 parts of rhizome of chuanxiong, 25 parts of radix scutellariae, 25 parts of lopseed, 10 parts of chrysanthemum, 10 parts of radix astragali, ground
Yellow 20 parts and 3000 parts of solvent.
By limiting the further of each raw material dosage in the hair tonic composition so that the collaboration between each raw material is made
With more notable, Anti-hair loss, the effect of promoting kainogenesis long, are obvious.
" comprising " of the present invention, it is intended that it can also include other components in addition to the component, such as preservative,
Excipient etc..These other components assign the hair tonic composition different characteristics.In addition, it is of the present invention
" comprising ", may be replaced by enclosed " for " or " by ... form ".
As a kind of preferred embodiment of the present invention, the hair tonic composition, it is 1- to further include parts by weight
10 parts of preservative.
Preferably, the preservative includes Phenoxyethanol or Sensiva SC50.Phenoxyethanol is traditional preservative, second
Base hexyl glycerine be widely recognized as, be flexible, multi-functional additive, it can play the role of antibacterial and corrosion-resistant in formula.
Preferably, the preservative includes Phenoxyethanol and Sensiva SC50, and the Phenoxyethanol and ethylhexyl are sweet
The weight ratio of oil is (1-10)：1.Phenoxyethanol and the typical but non-limiting weight ratio of Sensiva SC50 are 1:1、2:1、3:
1、4:1、5:1、6:1、7:1、8:1、9:1 or 10:1.
Phenoxyethanol and Sensiva SC50 are used in combination, while good preservative efficacy is obtained, also had higher
Security.
It should be noted that further include diluent, moisturizer, wetting agent, solubilizer, thickening in the hair tonic composition
Any one in agent, spices, dyestuff, pH adjusting agent, antiseptic, stabilizer, emulsifying agent, buffer or excipient or at least two
The combination of kind.
As a kind of preferred embodiment of the present invention, the solvent is ethanol water, wherein, second in ethanol water
The weight ratio of alcohol and water is 1:(0.5-1.5).
Ethanol is mainly used to dissolve the medicinal ingredient in Chinese medicine.Ethanol and water are typical but non-limiting in ethanol water
Weight ratio is 1:0.5、1:0.6、1:0.7、1:0.8、1:0.9、1:1.0、1:1.1、1:1.2、1:1.3、1:1.4 or 1:1.5.
It should be noted that due in hair nourishing liquid provided by the invention alcohol content it is higher, it is careful to alcohol intolerance person
With.
Hair tonic composition provided by the invention is not particularly limited herein there are a variety of type of service.It is used as this hair
A kind of bright preferred embodiment, the hair tonic composition are paste, emulsion agent, solution, film or spray form,
Preferably spray form medication.Easy to use using spray form medication, effect is good.
According to the second aspect of the invention, the preparation method of hair tonic composition is additionally provided, is comprised the following steps：
By the cacumen biotae of formula ratio existing in the form of Chinese medicine, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, lopseed,
Preservative mixes with solvent and optionally for chrysanthemum, radix astragali, glutinous rehmannia, soaks more than 40 days, and separation, obtains hair tonic composition.
The preparation method is suitable for small-scale manual production process.
Alternatively, the Cacumen Platycladi extract, licorice, Semen sesami nigrum of formula ratio existing in the form of Chinese medical extract are carried
Thing, angelica extract, rhizome of chuanxiong extract, Baical Skullcap root P.E, Herba speranskiae tuberculatae extract, chrysanthemum extract, astragalus root powder, glutinous rehmannia is taken to carry
Take thing with solvent and optionally preservative mixes, be warming up to each dissolution of raw material, keep the temperature, obtain hair tonic composition.The preparation
Method is suitable for large-scale commercial process.
The preparation method of above-mentioned hair tonic composition, by using specific preparation process extract in each raw material it is effective into
Point so that component obtains reservation as much as possible the effect of in each raw material, meanwhile, the preparation method is simple, easy, is suitable for work
Mass produced in industry.
As a kind of preferred embodiment of the present invention, each raw material system existing for use in the form of Chinese medical extract
When standby, warming temperature is 60-65 DEG C, and typical but non-limiting warming temperature is 60 DEG C, 61 DEG C, 62 DEG C, 63 DEG C, 64 DEG C or 65
℃。
Preferably, soaking time 15-40min, typical but non-limiting soaking time for 15min, 20min,
25min, 30min, 35min or 40min.
Preferably, the preparation method of hair tonic composition comprises the following steps：
By the Cacumen Platycladi extract of formula ratio existing in the form of Chinese medical extract, licorice, Semen Sesami Nigrum extract,
Angelica extract, rhizome of chuanxiong extract, Baical Skullcap root P.E, Herba speranskiae tuberculatae extract, chrysanthemum extract, astragalus root powder, glutinous rehmannia extract
With solvent and optionally preservative mixes, and mixes slowly, and after 60-65 DEG C of heating to each dissolution of raw material, keeps the temperature 15-40min, cooling
To 45 DEG C, censorship, filling after micro- inspection is qualified, packaging, obtains hair tonic composition.
Involved tankage is required to carry out cleaning and sterilizing in the preparation process.
According to the third aspect of the present invention, the application of hair tonic composition is additionally provided.In view of above-mentioned hair nourishes
Effect possessed by composition so that it has good application in Anti-hair loss, the long field of promotion kainogenesis.
With reference to specific embodiment and comparative example, the invention will be further described.
Embodiment 1
A kind of hair tonic composition provided in this embodiment, includes the raw material of following parts by weight：15 parts of cacumen biotae, it is sweet
20 parts of grass, 28 parts of Semen sesami nigrum, 18 parts of Angelica sinensis, 15 parts of rhizome of chuanxiong, 20 parts of radix scutellariae, 22 parts of lopseed, 8 parts of chrysanthemum, 5 parts of radix astragali, glutinous rehmannia
15 parts and 2500 parts of solvent.
Wherein, solvent is ethanol water, and the weight ratio of ethanol and water in ethanol water is 1:0.5.
Embodiment 2
A kind of hair tonic composition provided in this embodiment, includes the raw material of following parts by weight：18 parts of cacumen biotae, it is sweet
12 parts of grass, 20 parts of Semen sesami nigrum, 15 parts of Angelica sinensis, 18 parts of rhizome of chuanxiong, 24 parts of radix scutellariae, 30 parts of lopseed, 5 parts of chrysanthemum, 15 parts of radix astragali, glutinous rehmannia
18 parts and 2800 parts of solvent.
Wherein, solvent is ethanol water, and the weight ratio of ethanol and water in ethanol water is 1:0.75.
Embodiment 3
A kind of hair tonic composition provided in this embodiment, includes the raw material of following parts by weight：20 parts of cacumen biotae, it is sweet
15 parts of grass, 25 parts of Semen sesami nigrum, 20 parts of Angelica sinensis, 20 parts of rhizome of chuanxiong, 25 parts of radix scutellariae, 25 parts of lopseed, 10 parts of chrysanthemum, 10 parts of radix astragali, ground
Yellow 20 parts and 3000 parts of solvent.Wherein, solvent is ethanol water, and the weight ratio of ethanol and water in ethanol water is 1:1.
Embodiment 4
A kind of hair tonic composition provided in this embodiment, includes the raw material of following parts by weight：22 parts of cacumen biotae, it is sweet
10 parts of grass, 22 parts of Semen sesami nigrum, 22 parts of Angelica sinensis, 22 parts of rhizome of chuanxiong, 28 parts of radix scutellariae, 27 parts of lopseed, 12 parts of chrysanthemum, 7 parts of radix astragali, glutinous rehmannia
22 parts and 3200 parts of solvent.
Wherein, solvent is ethanol water, and the weight ratio of ethanol and water in ethanol water is 1:1.2.
Embodiment 5
A kind of hair tonic composition provided in this embodiment, includes the raw material of following parts by weight：25 parts of cacumen biotae, it is sweet
18 parts of grass, 30 parts of Semen sesami nigrum, 25 parts of Angelica sinensis, 25 parts of rhizome of chuanxiong, 30 parts of radix scutellariae, 20 parts of lopseed, 15 parts of chrysanthemum, 12 parts of radix astragali, ground
Yellow 25 parts and 3500 parts of solvent.
Wherein, solvent is ethanol water, and the weight ratio of ethanol and water in ethanol water is 1:1.5.
Embodiment 6
A kind of hair tonic composition provided in this embodiment, except being 10 parts of preservative comprising parts by weight, remaining
Raw material and composition are same as Example 5.
Wherein, preservative includes Phenoxyethanol and Sensiva SC50, the weight of the Phenoxyethanol and Sensiva SC50
Amount is than being 5:1.
The preparation method for the hair tonic composition that embodiment 1-6 is provided, comprises the following steps：
By the Cacumen Platycladi extract of formula ratio existing in the form of Chinese medical extract, licorice, Semen Sesami Nigrum extract,
Angelica extract, rhizome of chuanxiong extract, Baical Skullcap root P.E, Herba speranskiae tuberculatae extract, chrysanthemum extract, astragalus root powder, glutinous rehmannia extract
With solvent and optionally preservative mixes, and mixes slowly, and after 60 DEG C of heating to each dissolution of raw material, keeps the temperature 20min, is cooled to 45
DEG C, censorship, filling after micro- inspection is qualified, packaging, obtains hair tonic composition.
Embodiment 7
A kind of hair tonic composition provided in this embodiment, raw material and composition are same as Example 3.
The preparation method of the hair tonic composition, comprises the following steps：
By the cacumen biotae of formula ratio existing in the form of Chinese medicine, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, lopseed,
Preservative mixes with solvent and optionally for chrysanthemum, radix astragali, glutinous rehmannia, soaks more than 40 days, and separation, obtains hair tonic composition.
Embodiment 8
A kind of hair tonic composition provided in this embodiment, raw material and composition are same as Example 3.
The preparation method of the hair tonic composition, comprises the following steps：
By the Cacumen Platycladi extract of formula ratio existing in the form of Chinese medical extract, licorice, Semen Sesami Nigrum extract,
Angelica extract, rhizome of chuanxiong extract, Baical Skullcap root P.E, Herba speranskiae tuberculatae extract, chrysanthemum extract, astragalus root powder, glutinous rehmannia extract
With solvent and optionally preservative mixes, and mixes slowly, and after 65 DEG C of heating to each dissolution of raw material, keeps the temperature 40min, is cooled to 45
DEG C, censorship, filling after micro- inspection is qualified, packaging, obtains hair tonic composition.
Comparative example 1
A kind of hair tonic composition that this comparative example provides, except the parts by weight of cacumen biotae in raw material are 5 parts, remaining
Raw material and dosage are same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 2
A kind of hair tonic composition that this comparative example provides, except the parts by weight of radix scutellariae in raw material are 15 parts, remaining
Raw material and dosage are same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 3
A kind of hair tonic composition that this comparative example provides, except the parts by weight of lopseed in raw material are 15 parts, its
Remaining raw material and dosage are same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 4
A kind of hair tonic composition that this comparative example provides, except the parts by weight of glutinous rehmannia in raw material are 8 parts, remaining is former
Material and dosage are same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 5
A kind of hair tonic composition that this comparative example provides, except being not added with cacumen biotae in raw material, remaining raw material and use
Measure same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 6
A kind of hair tonic composition that this comparative example provides, except being not added with radix glycyrrhizae in raw material, remaining raw material and dosage
It is same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 7
A kind of hair tonic composition that this comparative example provides, except being not added with Semen sesami nigrum in raw material, remaining raw material and use
Measure same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 8
A kind of hair tonic composition that this comparative example provides, except being not added with radix scutellariae in raw material, remaining raw material and dosage
It is same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 9
A kind of hair tonic composition that this comparative example provides, except being not added with lopseed in raw material, remaining raw material and use
Measure same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
Comparative example 10
A kind of hair tonic composition that this comparative example provides, except being not added with glutinous rehmannia in raw material, remaining raw material and dosage
It is same as Example 3.
The preparation method for the hair tonic composition that this comparative example provides is same as Example 3.
For the further effect of verification above-described embodiment and comparative example, ad hoc following experimental example.
Experimental example 1
First, general information
396 alopecia seborrheica patients are screened, between the age is 18-60 Sui, sufferer is randomly divided into 18 groups, every group 20
Example, first group of hair tonic composition for using embodiment 1, second group of hair tonic composition for using embodiment 2, the 3rd group
Using the hair tonic composition of embodiment 3, the 4th group of hair tonic composition for using embodiment 4, the 5th group using implementation
The hair tonic composition of example 5, the 6th group of hair tonic composition for using embodiment 6, the 7th group of hair for using embodiment 7
Tonic composition, the 8th group of hair tonic composition for using embodiment 8, the 9th group of hair using comparative example 1 nourish combination
Thing, the tenth group of hair tonic composition for using comparative example 2, the 11st group of hair tonic composition for using comparative example 3, the tenth
Two groups of hair tonic compositions for using comparative example 4, the 13rd group of hair tonic composition for using comparative example 5, the 14th group
Using the hair tonic composition of comparative example 6, the 15th group of hair tonic composition for using comparative example 7, the 16th group of use
The hair tonic composition of comparative example 8, the 17th group of hair tonic composition for using comparative example 9, the 18th group using contrast
The hair tonic composition of example 10.
2nd, standard is treated
Recovery from illness：Alopecia stops, and grows new hair；
Effectively：Depilation phenomenon mitigates, and a small amount of new hair is grown；
It is invalid：Depilation phenomenon persistently exists, and does not mitigate.
3rd, treatment method
15mL is smeared daily, it is continuous to smear 21 days.
4th, treatment results
After 21 days, clinical observation statistical result is as shown in table 1 below, wherein, total effective rate=(cure number of cases+effective example
Number)/total number of cases × 100%.
1 clinical test statistical result of table
From table 1 it follows that hair nourishing liquid provided by the invention has the effect of notable for alopecia seborrheica.
Specifically, comparative example 1-10 is the contrast experiment of embodiment 3, and it is different from embodiment 3, provided in comparative example 1-4
Hair tonic composition in a certain raw material dosage beyond the raw material number range that limits of the present invention, and provided in comparative example 5-10
Hair tonic composition lack certain raw material.It can be seen from the data in Table 1 that when certain raw material dosage in hair tonic composition
During beyond the raw material number range that the present invention limits, hair tonic composition is under the therapeutic effect of alopecia seborrheica patient
Drop, and when hair tonic composition lacks certain raw material, its therapeutic effect further reduces.As it can be seen that only limited in the present invention
In the range of fixed raw material and dosage, hair tonic composition can be only achieved good effect for alopecia seborrheica.
Experimental example 2
First, general information
Screen 200 patients' neural's property hair loss patients (wherein, including general alopecia, alopecia areata, whole alopecia, postpartum alopecia patient), year
Between age is 20-65 Sui, sufferer is randomly divided into 18 groups, every group 20, first group of hair using embodiment 1 nourishes combination
Thing, second group of hair tonic composition for using embodiment 2, the 3rd group of hair tonic composition for using embodiment 3, the 4th group
Using the hair tonic composition of embodiment 4, the 5th group of hair tonic composition for using embodiment 5, the 6th group using implementation
The hair tonic composition of example 6, the 7th group of hair tonic composition for using embodiment 7, the 8th group of hair for using embodiment 8
Tonic composition, the 9th group of hair tonic composition for using comparative example 1, the tenth group of hair using comparative example 2 nourish combination
Thing, the 11st group of hair tonic composition for using comparative example 3, the 12nd group of hair tonic composition for using comparative example 4, the
13 groups of hair tonic compositions for using comparative example 5, the 14th group of hair tonic composition for using comparative example 6, the 15th
Group is using the hair tonic composition of comparative example 7, and the 16th group of hair tonic composition for using comparative example 8, the 17th group is adopted
With the hair tonic composition of comparative example 9, the 18th group of hair tonic composition for using comparative example 10.
2nd, standard is treated
Recovery from illness：Alopecia stops, and grows new hair；
Effectively：Depilation phenomenon mitigates, and a small amount of new hair is grown；
It is invalid：Depilation phenomenon persistently exists, and does not mitigate.
3rd, treatment method
15mL is smeared daily, it is continuous to smear 21 days.
4th, treatment results
After 21 days, clinical observation statistical result is as shown in table 2 below, wherein, total effective rate=(cure number of cases+effective example
Number)/total number of cases × 100%.
2 clinical test statistical result of table
From Table 2, it can be seen that hair nourishing liquid provided by the invention has remarkable efficacy for nervous baldness.
Specifically, comparative example 1-10 is the contrast experiment of embodiment 3, and it is different from embodiment 3, provided in comparative example 1-4
Hair tonic composition in a certain raw material dosage beyond the raw material number range that limits of the present invention, and provided in comparative example 5-10
Hair tonic composition lack certain raw material.It can be seen from the data in Table 2 that when certain raw material dosage in hair tonic composition
During beyond the raw material number range that the present invention limits, hair tonic composition is under the therapeutic effect of nervous baldness patient
Drop, and when hair tonic composition lacks certain raw material, its therapeutic effect further reduces.As it can be seen that only limited in the present invention
In the range of fixed raw material and dosage, hair tonic composition can be only achieved good effect for nervous baldness.
In conclusion the hair tonic composition has good Anti-hair loss, promotes the performance of kainogenesis length, for nerve
Property alopecia or alopecia seborrheica have good effect, and without obvious toxicity.
Finally it should be noted that：The above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe is described in detail the present invention with reference to foregoing embodiments, it will be understood by those of ordinary skill in the art that：Its according to
Can so modify to the technical solution described in foregoing embodiments, either to which part or all technical characteristic into
Row equivalent substitution；And these modifications or replacement, the essence of appropriate technical solution is departed from various embodiments of the present invention technology
The scope of scheme.
Claims (10)
1. a kind of hair tonic composition, it is characterised in that include the raw material of following parts by weight：15-25 parts of cacumen biotae, radix glycyrrhizae
10-20 parts, 20-30 parts of Semen sesami nigrum, 15-25 parts of Angelica sinensis, 15-25 parts of rhizome of chuanxiong, 20-30 parts of radix scutellariae, 20-30 parts of lopseed, chrysanthemum
5-15 parts, 5-15 parts of radix astragali, 2500-3500 parts of 15-25 parts of glutinous rehmannia and solvent.
2. hair tonic composition according to claim 1, it is characterised in that include the raw material of following parts by weight：Side
16-24 parts of CedarLeaves, 12-20 parts of radix glycyrrhizae, 22-30 parts of Semen sesami nigrum, 16-25 parts of Angelica sinensis, 16-25 parts of rhizome of chuanxiong, 22-30 parts of radix scutellariae, thoroughly
2500-3500 parts of 22-30 parts of bone grass, 6-15 parts of chrysanthemum, 6-15 parts of radix astragali, 16-24 parts of glutinous rehmannia and solvent.
3. hair tonic composition according to claim 1, it is characterised in that include the raw material of following parts by weight：Side
18-22 parts of CedarLeaves, 12-18 parts of radix glycyrrhizae, 22-28 parts of Semen sesami nigrum, 18-24 parts of Angelica sinensis, 18-24 parts of rhizome of chuanxiong, 22-28 parts of radix scutellariae, thoroughly
2600-3400 parts of 22-28 parts of bone grass, 7-14 parts of chrysanthemum, 6-14 parts of radix astragali, 18-22 parts of glutinous rehmannia and solvent；
Preferably, the hair tonic composition, includes the raw material of following parts by weight：20 parts of cacumen biotae, 15 parts of radix glycyrrhizae, black sesame
25 parts of fiber crops, 20 parts of Angelica sinensis, 20 parts of rhizome of chuanxiong, 25 parts of radix scutellariae, 25 parts of lopseed, 10 parts of chrysanthemum, 10 parts of radix astragali, 20 parts of glutinous rehmannia and solvent
3000 parts.
4. according to the hair tonic composition described in claim 1-3 any one, it is characterised in that the solvent is ethanol water
Solution, wherein, the weight ratio of ethanol and water is 1 in ethanol water：(0.5-1.5).
5. according to the hair tonic composition described in claim 1-3 any one, it is characterised in that further including parts by weight is
1-10 parts of preservative；
Preferably, the preservative includes Phenoxyethanol or Sensiva SC50；
Preferably, the preservative includes Phenoxyethanol and Sensiva SC50, the Phenoxyethanol and Sensiva SC50
Weight ratio is (1-10)：1.
6. according to the hair tonic composition described in claim 1-3 any one, it is characterised in that the hair nourishes combination
Each raw material of thing exists in the form of Chinese medicine or Chinese medicinal material extract.
7. according to the hair tonic composition described in claim 1-3 any one, it is characterised in that the hair nourishes combination
Thing is paste, emulsion agent, solution, film or spray form.
8. the preparation method of the hair tonic composition described in claim 1-7 any one, it is characterised in that including following step
Suddenly：
By cacumen biotae, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, lopseed, the chrysanthemum of formula ratio existing in the form of Chinese medicine
Preservative mixes with solvent and optionally for flower, radix astragali, glutinous rehmannia, soaks more than 40 days, and separation, obtains hair tonic composition；
Or, by the cacumen biotae of formula ratio existing in the form of Chinese medical extract, radix glycyrrhizae, Semen sesami nigrum, Angelica sinensis, rhizome of chuanxiong, radix scutellariae, deep
Preservative mixes with solvent and optionally for grass, chrysanthemum, radix astragali, glutinous rehmannia, is warming up to each dissolution of raw material, insulation, obtains hair nourishing
Composition.
9. the preparation method of hair tonic composition according to claim 8, it is characterised in that when using with traditional Chinese medicine extraction
When existing for thing form prepared by each raw material, warming temperature is 60-65 DEG C；
Preferably, soaking time 15-40min.
10. hair tonic composition described in claim 1-7 any one Anti-hair loss, promote the long field of kainogenesis should
With.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115252506A (en) * | 2022-09-09 | 2022-11-01 | 姚燕容 | Anti-hair loss and hair-growing composition and preparation method and application thereof |
| CN115252506B (en) * | 2022-09-09 | 2024-05-10 | 姚燕容 | Hair loss preventing and hair growing composition and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102973727A (en) * | 2012-12-27 | 2013-03-20 | 赵龙伟 | Hair follicle nutrient activating liquid and preparation method thereof |
| CN106728340A (en) * | 2017-03-11 | 2017-05-31 | 广州煜明生物科技有限公司 | Chinese medicine composition with hair care effect and its preparation method and application |
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2018
- 2018-01-15 CN CN201810035852.2A patent/CN107998211B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102973727A (en) * | 2012-12-27 | 2013-03-20 | 赵龙伟 | Hair follicle nutrient activating liquid and preparation method thereof |
| CN106728340A (en) * | 2017-03-11 | 2017-05-31 | 广州煜明生物科技有限公司 | Chinese medicine composition with hair care effect and its preparation method and application |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115252506A (en) * | 2022-09-09 | 2022-11-01 | 姚燕容 | Anti-hair loss and hair-growing composition and preparation method and application thereof |
| CN115252506B (en) * | 2022-09-09 | 2024-05-10 | 姚燕容 | Hair loss preventing and hair growing composition and preparation method and application thereof |
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