CN106728340A - Chinese medicine composition with hair care effect and its preparation method and application - Google Patents
Chinese medicine composition with hair care effect and its preparation method and application Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/804—Rehmannia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/63—Arthropods
- A61K35/64—Insects, e.g. bees, wasps or fleas
- A61K35/644—Beeswax; Propolis; Royal jelly; Honey
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/13—Coniferophyta (gymnosperms)
- A61K36/14—Cupressaceae (Cypress family), e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/236—Ligusticum (licorice-root)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/47—Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/539—Scutellaria (skullcap)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses a kind of Chinese medicine composition with hair care effect, the described Chinese medicine composition with hair care effect is mainly contained and takes 1 10 parts of the fleece-flower root, 1 10 parts of cacumen biotae, 1 10 parts of Radix Glycyrrhizae, 1 10 parts of Semen sesami nigrum, 1 10 parts of Radix Angelicae Sinensis, 1 10 parts of Ligusticum wallichii, 1 10 parts of the root of large-flowered skullcap, 1 10 parts of lopseed, 1 10 parts of chrysanthemum, 1 10 parts of Astragalus membranacus root, 1 10 parts of honey, 1 10 parts of glutinous rehmannia, hair nutrition can be increased, blood-activating and qi-promoting, improve skin of head blood circulation and immunity, improve hair quality, promote natural on-off cycles of hair growth development.
Description
Technical field
The invention belongs to cosmetic field, a kind of Chinese medicine composition with hair care effect and its preparation side are specifically related to
Method and application.
Background technology
With expanding economy and the continuous improvement of living standard, people for appearance requirement more and more higher, but with
Cumulative operating pressure and environmental pollution, increasing people is subject to hair to dry, matt, dandruff the problems such as perplex.This
Outward, hair can also be damaged because having hair dyed or perming, thus hair shows the feel as hay after hair washing.
Under the trend of back to nature, people in the urgent need to safety non-toxic, allergic natural hair conditioning will not be caused to produce
Product, these products should be the nursing and protection for being conceived to hair essence, also make every effort in skin of head, hair cell new old generation
Thank, anti-aging aspect receives certain effect, and then reaches young, beautiful and pleasurable purpose.
Chinese patent ZL201110239392.3 discloses a kind of natural Chinese herbal medicine hair caring liquid, using following weight proportion
Raw material：4000~6000 grams of mulberry leaf, 3000~4500 grams of Semen sesami nigrum, 3000~4500 grams of the fleece-flower root, dark plum
2500~3500 grams, 2500~3500 grams of cacumen biotae, 2000~3000 grams of santal, flos caryophylli 2000~
3000 grams；It is made by techniques such as ethanol immersion, distillation, filterings.Declare that natural Chinese herbal medicine hair caring liquid is rich in hair
The favourable protein of growth, amino acid, vitamin, organic acid and its compound and substantial amounts of inorganic microelement, with changing
Kind hair quality, effect of hair conditioning and brain nourishing.
Chinese patent ZL201110263634.2 discloses a kind of hair blackening liquid, including following weight proportion raw material system
Into, 50~60 parts of the fleece-flower root, 40~50 parts of cacumen biotae, 10~20 parts of Eclipta prostrata, 35~45 parts of notopterygium root,
40~50 parts of Radix Angelicae Sinensis, 6~8 parts of Ligusticum wallichii, 10~20 parts of the Radix Astragali, 10~15 parts of garden balsam, indigo naturalis 5~
15 parts.Declare to have that infiltration is subcutaneous white hair blackening, weak hair can be made to become strong, withered hair brighten effect, safe and free of toxic and side effects.
From the foregoing, extracting active component from plant, especially Chinese medicine as conditioning maintenance composition for being pacified
Complete reliable hair care class product has great importance.Based on this, the invention provides a kind of hair care unlike the prior art
Composition and its application, the hair nourishing composition extract active component from different types of Chinese medicinal plant, with significant conditioning
Hair care effect.
The content of the invention
Embodiment of the present invention technical problem to be solved is, there is provided it is a kind of unlike the prior art with hair care
Chinese medicine composition of effect and its preparation method and application.Concrete technical scheme is as follows：
In a first aspect, a kind of Chinese medicine composition with hair care effect is the embodiment of the invention provides, it is described with hair care effect
Chinese medicine composition be prepared via a method which to obtain：
Take fleece-flower root 1-10 parts, cacumen biotae 1-10 parts, Radix Glycyrrhizae 1-10 parts, Semen sesami nigrum 1-10 parts, Radix Angelicae Sinensis 1-10 parts, Ligusticum wallichii 1-10
Part, root of large-flowered skullcap 1-10 parts, lopseed 1-10 parts, chrysanthemum 1-10 parts, 1-10 parts, honey 1-10 parts, glutinous rehmannia 1-10 parts of Astragalus membranacus root
Mixing, crushes, and sifts out, and obtains mixed material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 30-50% in mixed material, low rate mixing,
Then Microwave Extraction is carried out；Filtering obtain extractive juice, to being separated by filtration after the dregs of a decoction carry out squeezing obtain squeezing juice, by extractive juice
With squeezing juice mixing, mixed juice is obtained；
To deionized water is added in mixed juice, the weight of wherein deionized water is 3-5 times of mixed juice, well mixed to be diluted
Concoction；Then, part of dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation obtains one-level
Zymotic fluid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution concoction, increase throughput, fermented, obtained
Obtain second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, takes filtrate, obtains described with hair care effect
Chinese medicine composition.
Specifically, preferably, the mesh number of the sieve is 10-100 mesh.
Specifically, preferably, the low rate mixing time is 3-6 hours；The frequency of the microwave abstracting is 15-
20KHZ, extraction time is 10-15 minutes.
Specifically, preferably, the dilution concoction consumption of the one grade fermemtation is 10%-20% dilutes concoction total amount.
Specifically, preferably, the cultivation temperature of the one grade fermemtation is 30-35 DEG C, incubation time 2-3 days.
Specifically, preferably, the cultivation temperature of the second order fermentation is 35-38 DEG C, incubation time 1-3 days.
Specifically, preferably, the cryogenic temperature of the freezing and filtering is 2-3 DEG C, cooling time is 1-2 days, and is used
Aperture 1-5 microns of filter plant pressure filtration.
Second aspect, the Chinese medicine composition with hair care effect of the present invention can exist as one kind hair care additive
The application of hair care hair care category commodity.Specifically, the hair care hair care category commodity include：Hair care spraying, shampoo, hair care
Su, treatment waxes, scalp nursing solution and Hair-conditioning essential oil.
Present invention also offers a kind of conditioning shampoo, described conditioning shampoo includes each of following weight/mass percentage composition
Component：Laureth sulfuric ester ammonium 10-20%, bay alcohol sulfuric ester ammonium 5-10%, LAA 1-5%, decyl
Glucoside 1-5%, guar hydroxypropyltrimonium chloride 0.5-2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamides acid esters is handed over
Linked polymer 0.1-0.5%, Coco-Hydroxysultaine 1-5%, arginine 0.1-0.5%, panthenol 0.1-1%, tocopherol（Dimension
Raw element E）0.1-0.2%, pungent glycol 0.3-0.6%, 1,2- pentanediol 0.5-1%, the above-mentioned Chinese medicine composition with hair care effect
1-10%, water surplus.
The beneficial effect that technical scheme provided in an embodiment of the present invention is brought is：
Chinese medicine composition with hair care effect provided in an embodiment of the present invention passes through alcohol extracting method and coordinates to be obtained using Microwave Extraction
The Hubeiwan of high activity is obtained, then using fermentation method, is fully improved using microbial metabolism and is discharged their activity, obtained
Obtain the hair nourishing composition of high activity.This is used for the composition of skin and hair maintenance with cacumen biotae, the fleece-flower root as main ingredient, to work as
Return, Ligusticum wallichii, the Radix Astragali, lopseed, Astragalus membranacus root, glutinous rehmannia be ministerial drug, with Radix Glycyrrhizae, honey, Semen sesami nigrum, chrysanthemum as adjuvant.Will
When it is used for hair nursing, hair nutrition can be increased, blood-activating and qi-promoting improves skin of head blood circulation and immunity, improves hair
Matter, promotes natural on-off cycles of hair growth development.
Specific embodiment
With reference to specific embodiment to of the invention for a more detailed description, but embodiments of the present invention are not limited to
This, for especially not dated technological parameter or condition, can refer to routine techniques is carried out.
Involved each Chinese medicine material is described as follows in hair nourishing composition of the present invention：
The fleece-flower root, polygonaceae fleece-flower root platymiscium is bitter, sweet；It is puckery, slightly warm in nature.Return liver, kidney channel.《Compendium of Materia Medica》Record：This thing gas
Warm bitter and puckery flavor, bitter kidney tonifying, temperature compensation liver can restrain vital essence, so energy blood-nourishing benefit liver, controlling nocturnal emission with astringent drugs kidney-nourishing, muscle reinforcing and bone strengthening, black hair is nourishing
Good medicine, does not tremble with fear not dry, and work(is on glutinous rehmannia, all medicines of lucid asparagus.Qi and blood Taihe county, then wind void, carbuncle swells, all diseases of scrofula understand（Remove）
.
Cacumen biotae, Chinese medicine is that cupressaceae plant arbor-vitae dries branch and leaf, and return lung, liver, the spleen channel, with cooling blood and hemostasis, change
Phlegm and relieving cough, effect of growing and blacking hair.
Radix Glycyrrhizae, pulse family Glycyrrhiza perennial herb, root is sturdy with root-like stock, is a kind of help Chinese herbal medicine.Containing variousization
Study point, glycyrrhizin and Flavonoid substances are most important physiological activators in Radix Glycyrrhizae.Radix Glycyrrhizae is invigorated the spleen and benefited qi, moistening lung stops
Cough, purging intense heat and detonicating, relieving spasm to stop pain, many effects such as coordinating the drug actions of a prescription.
Semen sesami nigrum, is the black seeds of Pedaliaceae sesame, containing substantial amounts of fat and protein, also contains carbohydrate, dimension life
The nutritional ingredients such as plain A, vitamin E, lecithin, calcium, iron, chromium.There are stomach invigorating, liver protection, promote red blood cell growth, while can
To increase internal melanin, be conducive to natural on-off cycles of hair growth.
Radix Angelicae Sinensis, the root of Umbelliferae herbaceos perennial Radix Angelicae Sinensis.The traditional Chinese medical science thinks that Radix Angelicae Sinensis is sweet and weighs, therefore can specially enrich blood, its
Gas is light and pungent, thus again can promoting circulation of blood, bowl spares has, has benefit in row, is the key medicine in blood.Thus, it can enrich blood, and can invigorate blood circulation,
Both can stimulate the menstrual flow, and can be active.
A kind of Ligusticum wallichii, Chinese medicinal plant is usually used in blood-activating and qi-promoting, and wind-expelling pain-stopping, Ligusticum wallichii pungent-warm perfume (or spice) is dry, walks without keeping, can
Row dissipates, up up to mountain peak top；Enter blood system again, it is descending up to the sea of blood.Promoting blood circulation effect is extensive, the suitable various diseases of stagnation of blood stasis
Disease；Wind-expelling pain-stopping, effectiveness is favourable, can control the diseases such as head wind headache, arthralgia pain due to rheumatism.Former times people meaning Ligusticum wallichii is the gas medicine in blood, nearly says it
The functions such as the pungent scattered, Xie Yu of residence, sensible, analgesic.
The root of large-flowered skullcap, lamiaceae labiatae scutellaria herbaceos perennial, root is used as medicine.It is bitter, cold in nature, have heat-clearing and damp-drying drug, purging intense heat and detonicating,
Hemostasis, it is antiabortive the effects such as.
There is promoting blood circulation and removing blood stasis, diuresis removing toxic substances lopseed, part of being used as medicine, stimulates the menstrual flow deep for plant herb.
Chrysanthemum, the dry capitulum of feverfew,《This warp》Described in：" all public attention are dizzy to swell and ache, and mesh is intended to take off, lacrimation, skin
The dead flesh of skin, foul wind arthritis with fixed pain caused by dampness.Long term usage profit vim and vigour, resistance to old macrobiosis of making light of one's life by commiting suicide ".
Astragalus membranacus root, a kind of Chinese medicine, with tonifying Qi and lifting yang, benefit defends the effect such as solid table, inducing diuresis for removing edema, torr sore myogenic.
The honey that the nectar that honey is honeybee to be adopted from the spending of flowering plant is brewed in honeycomb, its main component is fruit
Sugar and glucose, both contents are total to account for 70%, and plurality of inorganic salt and vitamin, iron, calcium, copper, manganese, potassium, phosphorus etc. are more
Plant the trace element of organic acid and beneficial health.《This warp》Described in：" main trusted subordinate's perverse trend, all frightened epilepsies, five viscera settling is all not
Foot, invigorating middle warmer and replenishing QI, analgesic antidotal, and hundred medicines ".
Glutinous rehmannia, Scrophulariaceae glutinous rehmannia belongs to the underground root tuber of herbaceos perennial, and cool in nature, sweet-bitter flavor with enriching yin and nourishing kidney, is supported
Blood is enriched blood, effect of cool blood.
Embodiment 1
A kind of Chinese medicine composition with hair care effect, is prepared via a method which to obtain：
Take fleece-flower root 1kg, cacumen biotae 10kg, Radix Glycyrrhizae 1kg, Semen sesami nigrum 10kg, Radix Angelicae Sinensis 1kg, Ligusticum wallichii 10kg, root of large-flowered skullcap 1kg, lopseed
10kg, chrysanthemum 1kg, Astragalus membranacus root 10kg, honey 1kg, glutinous rehmannia 10kg mixing, crush, and cross 10 mesh sieve, obtain mixing former
Material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 50% in mixed material, and low rate mixing 3 is small
When, Microwave Extraction is then carried out, frequency is 20KHZ, and extraction time is 10 minutes；Filtering obtains extractive juice, after being separated by filtration
The dregs of a decoction carry out squeezing and obtain squeezing juice, extractive juice and squeezing juice are mixed, obtain mixed juice；
To deionized water is added in mixed juice, the weight of wherein deionized water is 5 times of mixed juice, is well mixed and obtains diluent
Juice；Then, 10% dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation, cultivation temperature
It it is 35 DEG C, incubation time 2 days obtains one grade fermemtation liquid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution
Concoction, increases throughput, is fermented, and cultivation temperature is 38 DEG C, and incubation time 1 day obtains second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, cryogenic temperature is 3 DEG C, and cooling time is 1 day, and
Using 5 microns of the filter plant pressure filtration in aperture, filtrate is taken, obtain the Chinese medicine composition with hair care effect.
Embodiment 2
A kind of Chinese medicine composition with hair care effect, is prepared via a method which to obtain：
Take fleece-flower root 10kg, cacumen biotae 1kg, Radix Glycyrrhizae 10kg, Semen sesami nigrum 1kg, Radix Angelicae Sinensis 10kg, Ligusticum wallichii 1kg, root of large-flowered skullcap 10kg, deep
Careless 1kg, chrysanthemum 10kg, Astragalus membranacus root 1kg, honey 10kg, glutinous rehmannia 1kg mixing, crush, and cross 100 mesh sieve, obtain mixing former
Material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 30% in mixed material, and low rate mixing 6 is small
When, Microwave Extraction is then carried out, frequency is 15KHZ, and extraction time is 15 minutes；Filtering obtains extractive juice, after being separated by filtration
The dregs of a decoction carry out squeezing and obtain squeezing juice, extractive juice and squeezing juice are mixed, obtain mixed juice；
To deionized water is added in mixed juice, the weight of wherein deionized water is 3 times of mixed juice, is well mixed and obtains diluent
Juice；Then, 20% dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation, cultivation temperature
It it is 30 DEG C, incubation time 3 days obtains one grade fermemtation liquid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution
Concoction, increases throughput, is fermented, and cultivation temperature is 35 DEG C, and incubation time 3 days obtains second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, cryogenic temperature is 2 DEG C, and cooling time is 2 days, and
Using aperture 1-5 microns of filter plant pressure filtration, filtrate is taken, obtain the Chinese medicine composition with hair care effect.
Embodiment 3
A kind of Chinese medicine composition with hair care effect, is prepared via a method which to obtain：
Take fleece-flower root 8kg, cacumen biotae 8kg, Radix Glycyrrhizae 2kg, Semen sesami nigrum 2kg, Radix Angelicae Sinensis 3kg, Ligusticum wallichii 5kg, root of large-flowered skullcap 5kg, lopseed
6kg, chrysanthemum 3kg, Astragalus membranacus root 7kg, honey 8kg, glutinous rehmannia 3kg mixing, crush, and cross 50 mesh sieve, obtain mixed material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 40% in mixed material, and low rate mixing 5 is small
When, Microwave Extraction is then carried out, frequency is 20KHZ, and extraction time is 12 minutes；Filtering obtains extractive juice, after being separated by filtration
The dregs of a decoction carry out squeezing and obtain squeezing juice, extractive juice and squeezing juice are mixed, obtain mixed juice；
To deionized water is added in mixed juice, the weight of wherein deionized water is 4 times of mixed juice, is well mixed and obtains diluent
Juice；Then, 15% dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation, cultivation temperature
It it is 32 DEG C, incubation time 2 days obtains one grade fermemtation liquid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution
Concoction, increases throughput, is fermented, and cultivation temperature is 37 DEG C, and incubation time 2 days obtains second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, cryogenic temperature is 3 DEG C, and cooling time is 1 day, and
Using 5 microns of the filter plant pressure filtration in aperture, filtrate is taken, obtain the Chinese medicine composition with hair care effect.
Embodiment 4
A kind of conditioning shampoo, described conditioning shampoo includes each component of following weight/mass percentage composition：Laureth sulphur
Acid esters ammonium 10%, bay alcohol sulfuric ester ammonium 10%, LAA 1%, Plantacare 818 5%, melon glue hydroxypropyl three
Ammonio methacrylate 0.5%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.5%, cocoyl weight ratio
Glycine betaine 1%, arginine 0.5%, panthenol 0.1%, tocopherol（Vitamin E）0.2%th, pungent glycol 0.3%, 1,2- pentanediols 1%, reality
Apply the Chinese medicine composition 1%, water surplus with hair care effect obtained by example 1.
Embodiment 5
A kind of conditioning shampoo, described conditioning shampoo includes each component of following weight/mass percentage composition：Laureth sulphur
Acid esters ammonium 20%, bay alcohol sulfuric ester ammonium 5%, LAA 5%, Plantacare 818 1%, melon glue hydroxypropyl trimethylammonium
Ammonium chloride 2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.1%, cocoyl weight ratio beet
Alkali 5%, arginine 0.1%, panthenol 1%, tocopherol（Vitamin E）0.1%th, pungent glycol 0.6%, 1,2- pentanediols 0.5%, embodiment 2
The obtained Chinese medicine composition 10%, water surplus with hair care effect.
Embodiment 6
A kind of conditioning shampoo, described conditioning shampoo includes each component of following weight/mass percentage composition：Laureth sulphur
Acid esters ammonium 15%, bay alcohol sulfuric ester ammonium 7%, LAA 2%, Plantacare 818 3%, melon glue hydroxypropyl trimethylammonium
Ammonium chloride 1%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.3%, cocoyl weight ratio beet
Alkali 3%, arginine 0.3%, panthenol 0.5%, tocopherol（Vitamin E）0.15%th, pungent glycol 0.5%, 1,2- pentanediols 0.7%, implementation
The Chinese medicine composition 5%, water surplus with hair care effect obtained by example 3.
Comparative example 1
A kind of conditioning shampoo, described conditioning shampoo includes each component of following weight/mass percentage composition：Laureth sulphur
Acid esters ammonium 15%, bay alcohol sulfuric ester ammonium 7%, LAA 2%, Plantacare 818 3%, melon glue hydroxypropyl trimethylammonium
Ammonium chloride 1%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.3%, cocoyl weight ratio beet
Alkali 3%, arginine 0.3%, panthenol 0.5%, tocopherol（Vitamin E）0.15%th, pungent glycol 0.5%, 1,2- pentanediols 0.7%, have
The Chinese medicine composition 5%, water surplus of hair care effect；
The Chinese medicine composition with hair care effect, is prepared via a method which to obtain：
Take cacumen biotae 8kg, Radix Glycyrrhizae 2kg, Radix Angelicae Sinensis 3kg, Ligusticum wallichii 5kg, root of large-flowered skullcap 5kg, lopseed 6kg, chrysanthemum 3kg, Astragalus membranacus root
7kg, honey 8kg, glutinous rehmannia 3kg mixing, crush, and cross 50 mesh sieve, obtain mixed material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 40% in mixed material, and low rate mixing 5 is small
When, Microwave Extraction is then carried out, frequency is 20KHZ, and extraction time is 12 minutes；Filtering obtains extractive juice, after being separated by filtration
The dregs of a decoction carry out squeezing and obtain squeezing juice, extractive juice and squeezing juice are mixed, obtain mixed juice；
To deionized water is added in mixed juice, the weight of wherein deionized water is 4 times of mixed juice, is well mixed and obtains diluent
Juice；Then, 15% dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation, cultivation temperature
It it is 32 DEG C, incubation time 2 days obtains one grade fermemtation liquid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution
Concoction, increases throughput, is fermented, and cultivation temperature is 37 DEG C, and incubation time 2 days obtains second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, cryogenic temperature is 3 DEG C, and cooling time is 1 day, and
Using 5 microns of the filter plant pressure filtration in aperture, filtrate is taken, obtain the Chinese medicine composition with hair care effect.
Comparative example 2
A kind of conditioning shampoo, described conditioning shampoo includes each component of following weight/mass percentage composition：Laureth sulphur
Acid esters ammonium 15%, bay alcohol sulfuric ester ammonium 7%, LAA 2%, Plantacare 818 3%, melon glue hydroxypropyl trimethylammonium
Ammonium chloride 1%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.3%, cocoyl weight ratio beet
Alkali 3%, arginine 0.3%, panthenol 0.5%, tocopherol（Vitamin E）0.15%th, pungent glycol 0.5%, 1,2- pentanediols 0.7%, have
The Chinese medicine composition 5%, water surplus of hair care effect；
The Chinese medicine composition with hair care effect, is prepared via a method which to obtain：
Take fleece-flower root 8kg, Radix Glycyrrhizae 2kg, Semen sesami nigrum 2kg, Ligusticum wallichii 5kg, root of large-flowered skullcap 5kg, lopseed 6kg, chrysanthemum 3kg, Astragalus membranacus
Root 7kg, honey 8kg, glutinous rehmannia 3kg mixing, crush, and cross 50 mesh sieve, obtain mixed material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 40% in mixed material, and low rate mixing 5 is small
When, Microwave Extraction is then carried out, frequency is 20KHZ, and extraction time is 12 minutes；Filtering obtains extractive juice, after being separated by filtration
The dregs of a decoction carry out squeezing and obtain squeezing juice, extractive juice and squeezing juice are mixed, obtain mixed juice；
To deionized water is added in mixed juice, the weight of wherein deionized water is 4 times of mixed juice, is well mixed and obtains diluent
Juice；Then, 15% dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation, cultivation temperature
It it is 32 DEG C, incubation time 2 days obtains one grade fermemtation liquid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution
Concoction, increases throughput, is fermented, and cultivation temperature is 37 DEG C, and incubation time 2 days obtains second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, cryogenic temperature is 3 DEG C, and cooling time is 1 day, and
Using 5 microns of the filter plant pressure filtration in aperture, filtrate is taken, obtain the Chinese medicine composition with hair care effect.
Comparative example 3
A kind of conditioning shampoo, described conditioning shampoo includes each component of following weight/mass percentage composition：Laureth sulphur
Acid esters ammonium 15%, bay alcohol sulfuric ester ammonium 7%, LAA 2%, Plantacare 818 3%, melon glue hydroxypropyl trimethylammonium
Ammonium chloride 1%, acrylic acid（Ester）Class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.3%, cocoyl weight ratio beet
Alkali 3%, arginine 0.3%, panthenol 0.5%, tocopherol（Vitamin E）0.15%th, pungent glycol 0.5%, 1,2- pentanediols 0.7%, have
The Chinese medicine composition 5%, water surplus of hair care effect；
The Chinese medicine composition with hair care effect, is prepared via a method which to obtain：
Take fleece-flower root 8kg, cacumen biotae 8kg, Radix Glycyrrhizae 2kg, Semen sesami nigrum 2kg, Radix Angelicae Sinensis 3kg, Ligusticum wallichii 5kg, root of large-flowered skullcap 5kg, lopseed
6kg, chrysanthemum 3kg, Astragalus membranacus root 7kg, honey 8kg, glutinous rehmannia 3kg mixing, crush, and cross 50 mesh sieve, obtain mixed material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 40% in mixed material, and low rate mixing 5 is small
When, then filtering obtain extractive juice, to being separated by filtration after the dregs of a decoction carry out squeezing obtain squeezing juice, extractive juice and squeezing juice are mixed
Close, obtain composition.
Embodiment 7
Carry out efficacy test to the conditioning shampoo obtained by embodiment 4-6 and comparative example 1-3, and with one it is commercially available declare to have support
Send out the shampoo as a comparison case 4 of effect.
Specific method of testing is as follows：Each experimental group chooses 20 volunteers, age 20-50 Sui, all dried by hair,
The problems such as tarnish, dandruff, is perplexed；Application method：It is dry to seventy percent using the clean hair post processing of conditioning shampoo, then gently press
Rub 3-5 minutes, with horn comb combing.It is 1 time every night, continuous on probation 12 weeks, mug, and trier is paid a return visit.
Evaluation method：The 0th day and the 12nd week photo are contrasted, wherein hair becomes substantially glossy black, and hair is dried, matt, dandruff problem
Be resolved for effective；Hair becomes glossy black, hair is dried, matt, dandruff problem obtain part solution for effective；Head
Dry dry, matt, dandruff problem be not changed in for invalid.Specific test result such as table 1.Trier is entered after on probation 12 weeks
Row is paid a return visit, and does not occur allergic phenomenon, shows the shampoo safety non-toxic.
The test result record sheet of table 1
| It is effective | Effectively | It is invalid | |
| Embodiment 4 | 8 | 9 | 3 |
| Embodiment 5 | 10 | 6 | 4 |
| Embodiment 6 | 7 | 11 | 2 |
| Comparative example 1 | 1 | 6 | 13 |
| Comparative example 2 | 0 | 9 | 11 |
| Comparative example 3 | 3 | 8 | 9 |
| Comparative example 4 | 0 | 5 | 15 |
From the result of table 1：
Embodiment 4-6 and comparative example 1-4 contrasts are visible, the hair care and nourishing of the shampoo with hair care effect obtained by the present invention
Effect is significant is better than comparative example；
Embodiment 6 contrasts visible, the fleece-flower root of the invention, cacumen biotae, Radix Glycyrrhizae, Semen sesami nigrum, Radix Angelicae Sinensis, Ligusticum wallichii, Huang with comparative example 1-2
Hair care and nourishing is better when a kind of reed mentioned in ancient books, lopseed, chrysanthemum, Astragalus membranacus root, honey, glutinous rehmannia share, and each plant component is according to specific
Ratio compatibility after play the role of Synergistic.
Embodiment 6 contrasts visible with comparative example 3, with Chinese medicine composition obtained in preparation method disclosed in this invention, its
Hair care and nourishing effect is than composition obtained in common extracting method more preferably.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality
Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, the scope of this specification record is all considered to be.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously
Can not therefore be construed as limiting the scope of the patent.It should be pointed out that coming for one of ordinary skill in the art
Say, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to present invention protection model
Enclose.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (9)
1. a kind of Chinese medicine composition with hair care effect, it is characterised in that the Chinese medicine composition with hair care effect leads to
Following method is crossed to prepare：
Take fleece-flower root 1-10 parts, cacumen biotae 1-10 parts, Radix Glycyrrhizae 1-10 parts, Semen sesami nigrum 1-10 parts, Radix Angelicae Sinensis 1-10 parts, Ligusticum wallichii 1-10
Part, root of large-flowered skullcap 1-10 parts, lopseed 1-10 parts, chrysanthemum 1-10 parts, 1-10 parts, honey 1-10 parts, glutinous rehmannia 1-10 parts of Astragalus membranacus root
Mixing, crushes, and sifts out, and obtains mixed material；
To adding edible alcohol in mixed material so that the volumetric concentration of alcohol reaches 30-50% in mixed material, low rate mixing,
Then Microwave Extraction is carried out；Filtering obtain extractive juice, to being separated by filtration after the dregs of a decoction carry out squeezing obtain squeezing juice, by extractive juice
With squeezing juice mixing, mixed juice is obtained；
To deionized water is added in mixed juice, the weight of wherein deionized water is 3-5 times of mixed juice, well mixed to be diluted
Concoction；Then, part of dilution concoction is first poured into one grade fermemtation tank, is passed through filtrated air, inoculation acetic acid bacteria fermentation obtains one-level
Zymotic fluid；One grade fermemtation liquid is pumped into second order fermentation tank, and adds remaining dilution concoction, increase throughput, fermented, obtained
Obtain second order fermentation liquid；
By the sterilizing of second order fermentation liquid, at normal temperatures ageing, then freezing and filtering, takes filtrate, obtains described with hair care effect
Chinese medicine composition.
2. the Chinese medicine composition with hair care effect according to claim 1, it is characterised in that the mesh number of the sieve is
10-100 mesh.
3. the Chinese medicine composition with hair care effect according to claim 1, it is characterised in that the low rate mixing time
It is 3-6 hours；The frequency of the microwave abstracting is 15-20KHZ, and extraction time is 10-15 minutes.
4. the Chinese medicine composition with hair care effect according to claim 1, it is characterised in that the one grade fermemtation it is dilute
Drug release juice consumption is that 10%-20% dilutes concoction total amount.
5. the Chinese medicine composition with hair care effect according to claim 1, it is characterised in that the training of the one grade fermemtation
It is 30-35 DEG C, incubation time 2-3 days to support temperature.
6. the Chinese medicine composition with hair care effect according to claim 1, it is characterised in that the training of the second order fermentation
It is 35-38 DEG C, incubation time 1-3 days to support temperature.
7. the Chinese medicine composition with hair care effect according to claim 1, it is characterised in that the freezing and filtering it is cold
It is 2-3 DEG C to freeze temperature, and cooling time is 1-2 days, and using aperture 1-5 microns of filter plant pressure filtration.
8. the Chinese medicine composition with hair care effect described in any one of claim 1-7 is taken care of hair as hair care additive in hair care
The application of class commodity, the hair care hair care category commodity include：Hair care spraying, shampoo, hair conditioner, treatment waxes, scalp shield
Reason liquid and Hair-conditioning essential oil.
9. a kind of conditioning shampoo, it is characterised in that each component including following weight/mass percentage composition：
Laureth sulfuric ester ammonium 10-20%, bay alcohol sulfuric ester ammonium 5-10%, LAA 1-5%, decyl
Glucoside 1-5%, guar hydroxypropyltrimonium chloride 0.5-2%, acrylic acid（Ester）Class/C10-30 alkylol acrylamides acid esters is handed over
Linked polymer 0.1-0.5%, Coco-Hydroxysultaine 1-5%, arginine 0.1-0.5%, panthenol 0.1-1%, tocopherol（Dimension
Raw element E）Described in 0.1-0.2%, pungent glycol 0.3-0.6%, 1,2- pentanediol 0.5-1%, claim any one of 1-7 with support
Send out the Chinese medicine composition 1-10%, water surplus of effect.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107998211A (en) * | 2018-01-15 | 2018-05-08 | 富延辉 | Hair tonic composition and its preparation method and application |
| CN109646672A (en) * | 2019-01-10 | 2019-04-19 | 石家庄正扬头道生物科技有限公司 | A kind of STM black hair medicament |
| CN111991284A (en) * | 2020-08-14 | 2020-11-27 | 侯春艳 | Health-care shampoo and production method thereof |
| CN112023017A (en) * | 2020-10-14 | 2020-12-04 | 段晓剑 | Traditional Chinese medicine preparation for treating alopecia and preparation method thereof |
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| CN103721144A (en) * | 2014-01-11 | 2014-04-16 | 广州丹奇日用化工厂有限公司 | Natural plant hair blackening solution and preparation method thereof |
| CN106074306A (en) * | 2016-08-04 | 2016-11-09 | 碌柚葉（香港）有限公司 | A kind of for skin and the compositions of hair maintenance and application |
| CN106265385A (en) * | 2016-10-20 | 2017-01-04 | 广州臻颜化妆品有限公司 | A kind of submissive glossy shampoo composite and application thereof |
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2017
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103721144A (en) * | 2014-01-11 | 2014-04-16 | 广州丹奇日用化工厂有限公司 | Natural plant hair blackening solution and preparation method thereof |
| CN106074306A (en) * | 2016-08-04 | 2016-11-09 | 碌柚葉（香港）有限公司 | A kind of for skin and the compositions of hair maintenance and application |
| CN106265385A (en) * | 2016-10-20 | 2017-01-04 | 广州臻颜化妆品有限公司 | A kind of submissive glossy shampoo composite and application thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107998211A (en) * | 2018-01-15 | 2018-05-08 | 富延辉 | Hair tonic composition and its preparation method and application |
| CN107998211B (en) * | 2018-01-15 | 2020-10-30 | 富延辉 | Hair nourishing composition and preparation method and application thereof |
| CN109646672A (en) * | 2019-01-10 | 2019-04-19 | 石家庄正扬头道生物科技有限公司 | A kind of STM black hair medicament |
| CN111991284A (en) * | 2020-08-14 | 2020-11-27 | 侯春艳 | Health-care shampoo and production method thereof |
| CN112023017A (en) * | 2020-10-14 | 2020-12-04 | 段晓剑 | Traditional Chinese medicine preparation for treating alopecia and preparation method thereof |
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