CN107996627A - The preparation method of textile thimerosal - Google Patents
The preparation method of textile thimerosal Download PDFInfo
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- CN107996627A CN107996627A CN201711194642.XA CN201711194642A CN107996627A CN 107996627 A CN107996627 A CN 107996627A CN 201711194642 A CN201711194642 A CN 201711194642A CN 107996627 A CN107996627 A CN 107996627A
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- China
- Prior art keywords
- textile
- thimerosal
- herbal medicine
- chinese herbal
- extracts
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- Pending
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- 239000004753 textile Substances 0.000 title claims abstract description 39
- RTKIYNMVFMVABJ-UHFFFAOYSA-L thimerosal Chemical compound [Na+].CC[Hg]SC1=CC=CC=C1C([O-])=O RTKIYNMVFMVABJ-UHFFFAOYSA-L 0.000 title claims abstract description 29
- 229940033663 thimerosal Drugs 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000284 extract Substances 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 28
- 241000411851 herbal medicine Species 0.000 claims abstract description 27
- 238000000605 extraction Methods 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 239000000706 filtrate Substances 0.000 claims abstract description 9
- 239000012535 impurity Substances 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 14
- 240000007849 Macleaya cordata Species 0.000 claims description 8
- 241001499733 Plantago asiatica Species 0.000 claims description 8
- 240000006688 Telosma cordata Species 0.000 claims description 8
- 235000017352 Telosma cordata Nutrition 0.000 claims description 8
- 239000010495 camellia oil Substances 0.000 claims description 8
- 238000004140 cleaning Methods 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 8
- 125000005909 ethyl alcohol group Chemical group 0.000 claims description 8
- 239000002893 slag Substances 0.000 claims description 8
- PXFBZOLANLWPMH-UHFFFAOYSA-N 16-Epiaffinine Natural products C1C(C2=CC=CC=C2N2)=C2C(=O)CC2C(=CC)CN(C)C1C2CO PXFBZOLANLWPMH-UHFFFAOYSA-N 0.000 claims description 7
- 235000015763 Artemisia ludoviciana Nutrition 0.000 claims description 7
- 241000608847 Gnaphalium Species 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 241000196324 Embryophyta Species 0.000 claims description 6
- 238000007738 vacuum evaporation Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 4
- 230000001954 sterilising effect Effects 0.000 abstract description 3
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 2
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 230000002779 inactivation Effects 0.000 abstract description 2
- 206010022000 influenza Diseases 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 241000345998 Calamus manan Species 0.000 description 6
- 235000012950 rattan cane Nutrition 0.000 description 6
- 239000004744 fabric Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 241000186227 Corynebacterium diphtheriae Species 0.000 description 1
- 241000192041 Micrococcus Species 0.000 description 1
- 241000607768 Shigella Species 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- 208000037386 Typhoid Diseases 0.000 description 1
- 230000000249 desinfective effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Botany (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Medicines Containing Plant Substances (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The present invention relates to a kind of preparation method of textile thimerosal, comprise the following steps:(1)After taking natural plants to clean removal of impurities, drying and crushing, it is separately added into absolute ethyl alcohol and extracts at room temperature, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, then evaporate under vacuum, obtain natural botanical extraction liquid;(2)The Chinese herbal medicine of equivalent is taken, is added water to cook, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtains extracts of Chinese herbal medicine;(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.Obtained textile disinfection uses natural plants and Chinese herbal medicine, have no toxic side effect to human body, and infected by influenza has certain inactivation capacity, there is stronger antibacterial action to staphylococcus aureus etc., sterilizing power is strong, the feel of textile in itself etc. will not be impacted, the daily disinfection suitable for textiles such as clothing, bedding, towels uses.
Description
Technical field
The present invention relates to textile field, more particularly, to a kind of preparation method of textile thimerosal.
Background technology
Textile is a kind of product that textile fabric is formed by processing weaving, is commonly applied to clothes, bedding etc., is made
For the article for wearing next to the skin or using, for the requirement in terms of disinfecting also higher, and due to frequent and human contact, sweat
Bacterium is easily grown with secretion, harmful effect is caused to human body health, and daily washing can only remove dust and spot,
Have no the effect of sterilizing, it is therefore desirable to carry out disinfection to textile.Also there are some textile thimerosals currently on the market, but
Chemical assistant is added with mostly, has certain toxic side effect to human body, is not suitable for being commonly used.
The content of the invention
The object of the present invention is to provide a kind of preparation method of textile thimerosal.
The object of the invention is achieved by the following technical programs:
A kind of preparation method of textile thimerosal is provided, is comprised the following steps:
(1)Each 5~10 parts of natural plants are taken, after cleaning removal of impurities, drying and crushing respectively, are separately added into 3~4 times of absolute ethyl alcohols, point
Do not extract 10~15h at room temperature, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, then under vacuum
Evaporation, obtains the natural botanical extraction liquid that mass percentage concentration is 50~70%;
(2)Totally 20~30 parts of the Chinese herbal medicine of equivalent is taken, 7~12 times of water is added and decocts 50~70min, the dregs of a decoction are filtered out after cooling, will
Liquid evaporates under vacuum after crossing 200 mesh sieves, obtains the extracts of Chinese herbal medicine that mass percentage concentration is 50~70%;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.
Further, the step(3)After natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and
Activated carbon decolorizing, is filtered after stirring 10~15min, is crossed 300 mesh sieves, is obtained textile thimerosal.
Further, the natural plants include elscholtiza, leached tea oil slag, flagger and Jin Zhongteng.
Further, the Chinese herbal medicine is by bent including Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and mouse
Grass.
Application method:Take obtained textile thimerosal in mass ratio 1:30~100 are diluted with water, then by textile
20~30min of immersion is put into, better at 40~70 DEG C, then washing drying.
Compared with prior art, the invention has the advantages that:
The present invention provides a kind of preparation method of textile thimerosal, using natural plants and Chinese herbal medicine, to the nontoxic pair of human body
Effect, and infected by influenza has certain inactivation capacity, to staphylococcus aureus, beta streptococcus, typhoid bacillus, Freund dysentery
Shigella, corynebacterium diphtheriae, diplococcus meningitidis, micrococcus catarrhalis, there is stronger antibacterial action, and sterilizing power is strong, to spinning
The feel of fabric in itself etc. will not impact, and the daily disinfection suitable for textiles such as clothing, bedding, towels makes
With.
Embodiment
With reference to specific embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)10 parts of elscholtiza, 5 parts of leached tea oil slag, 7 parts of flagger and golden 9 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively
3 times of absolute ethyl alcohols are added, extract 15h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, so
Evaporate under vacuum afterwards, obtain the natural botanical extraction liquid that mass percentage concentration is 50%;
(2)Totally 30 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 7 times of decoctings
70min is boiled, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is
50% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.
Embodiment 2
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)8 parts of elscholtiza, 6 parts of leached tea oil slag, 5 parts of flagger and golden 10 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively
4 times of absolute ethyl alcohols are added, extract 10h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, so
Evaporate under vacuum afterwards, obtain the natural botanical extraction liquid that mass percentage concentration is 70%;
(2)Totally 20 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 12 times of water
50min is decocted, the dregs of a decoction is filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is
70% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 10min,
300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 3
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)5 parts of elscholtiza, 9 parts of leached tea oil slag, 8 parts of flagger and golden 6 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively
3.5 times of absolute ethyl alcohols are added, extract 12h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves,
Then evaporate under vacuum, obtain the natural botanical extraction liquid that mass percentage concentration is 60%;
(2)Totally 25 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 10 times of water
60min is decocted, the dregs of a decoction is filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is
60% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 15min,
300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 4
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)7 parts of elscholtiza, 5 parts of leached tea oil slag, 8 parts of flagger and golden 5 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively
3 times of absolute ethyl alcohols are added, extract 13h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, so
Evaporate under vacuum afterwards, obtain the natural botanical extraction liquid that mass percentage concentration is 55%;
(2)Totally 22 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 8 times of decoctings
65min is boiled, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is
65% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 12min,
300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 5
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)9 parts of elscholtiza, 10 parts of leached tea oil slag, 10 parts of flagger and golden 8 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, point
Not Jia Ru 4 times of absolute ethyl alcohols, extract 11h at room temperature respectively, respectively filter after separated, merging filtrate, cross 200 mesh sieves,
Then evaporate under vacuum, obtain the natural botanical extraction liquid that mass percentage concentration is 58%;
(2)Totally 28 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 9 times of decoctings
68min is boiled, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is
62% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 14min,
300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 6
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)5 parts of elscholtiza, 7 parts of leached tea oil slag, 5 parts of flagger and golden 8 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively
3.5 times of absolute ethyl alcohols are added, extract 14h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves,
Then evaporate under vacuum, obtain the natural botanical extraction liquid that mass percentage concentration is 55%;
(2)Totally 24 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 11 times of water
55min is decocted, the dregs of a decoction is filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is
55% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 13min,
300 mesh sieves are crossed, obtain textile thimerosal.
Claims (4)
1. a kind of preparation method of textile thimerosal, it is characterised in that comprise the following steps:
(1)Each 5~10 parts of natural plants are taken, after cleaning removal of impurities, drying and crushing respectively, are separately added into 3~4 times of absolute ethyl alcohols, point
Do not extract 10~15h at room temperature, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, then under vacuum
Evaporation, obtains the natural botanical extraction liquid that mass percentage concentration is 50~70%;
(2)Totally 20~30 parts of the Chinese herbal medicine of equivalent is taken, 7~12 times of water is added and decocts 50~70min, the dregs of a decoction are filtered out after cooling, will
Liquid evaporates under vacuum after crossing 200 mesh sieves, obtains the extracts of Chinese herbal medicine that mass percentage concentration is 50~70%;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.
2. the preparation method of textile thimerosal according to claim 1, it is characterised in that the step(3)To naturally it plant
After thing extracting solution and extracts of Chinese herbal medicine merge, diatomite and activated carbon are added, is filtered after stirring 10~15min, crosses 300 mesh
Sieve, obtains textile thimerosal.
3. the preparation method of textile thimerosal according to claim 1 or claim 2, it is characterised in that the natural plants include
Elscholtiza, leached tea oil slag, flagger and Jin Zhongteng.
4. according to the preparation method of the textile thimerosal of claim 1 or 3, it is characterised in that the Chinese herbal medicine by including
Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and affine cudweed.
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CN201711194642.XA CN107996627A (en) | 2017-11-24 | 2017-11-24 | The preparation method of textile thimerosal |
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CN103651607A (en) * | 2013-12-18 | 2014-03-26 | 青岛百瑞吉生物工程有限公司 | Biopesticide for vegetables and preparation method of biopesticide |
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CN104082353A (en) * | 2014-07-04 | 2014-10-08 | 李钟� | Pure traditional Chinese medicine disinfectant and preparation method thereof |
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2017
- 2017-11-24 CN CN201711194642.XA patent/CN107996627A/en active Pending
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---|---|---|---|---|
CN101317585A (en) * | 2007-06-04 | 2008-12-10 | 孙克来 | Broad spectrum environment friendly pesticide and preparation thereof |
CN103444801A (en) * | 2013-08-19 | 2013-12-18 | 河北省科学技术情报研究院 | Traditional Chinese medicinal bactericidal freshening preparation for sterilizing library |
CN103721286A (en) * | 2013-10-24 | 2014-04-16 | 青岛华仁技术孵化器有限公司 | Air freshener with disinfection function |
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