CN107996627A - The preparation method of textile thimerosal - Google Patents

The preparation method of textile thimerosal Download PDF

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Publication number
CN107996627A
CN107996627A CN201711194642.XA CN201711194642A CN107996627A CN 107996627 A CN107996627 A CN 107996627A CN 201711194642 A CN201711194642 A CN 201711194642A CN 107996627 A CN107996627 A CN 107996627A
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CN
China
Prior art keywords
textile
thimerosal
herbal medicine
chinese herbal
extracts
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201711194642.XA
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Chinese (zh)
Inventor
杨海峰
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Huzhou Zhili Plastic Plastic Technology Co Ltd
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Huzhou Zhili Plastic Plastic Technology Co Ltd
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Priority to CN201711194642.XA priority Critical patent/CN107996627A/en
Publication of CN107996627A publication Critical patent/CN107996627A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/22Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/38Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The present invention relates to a kind of preparation method of textile thimerosal, comprise the following steps:(1)After taking natural plants to clean removal of impurities, drying and crushing, it is separately added into absolute ethyl alcohol and extracts at room temperature, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, then evaporate under vacuum, obtain natural botanical extraction liquid;(2)The Chinese herbal medicine of equivalent is taken, is added water to cook, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtains extracts of Chinese herbal medicine;(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.Obtained textile disinfection uses natural plants and Chinese herbal medicine, have no toxic side effect to human body, and infected by influenza has certain inactivation capacity, there is stronger antibacterial action to staphylococcus aureus etc., sterilizing power is strong, the feel of textile in itself etc. will not be impacted, the daily disinfection suitable for textiles such as clothing, bedding, towels uses.

Description

The preparation method of textile thimerosal
Technical field
The present invention relates to textile field, more particularly, to a kind of preparation method of textile thimerosal.
Background technology
Textile is a kind of product that textile fabric is formed by processing weaving, is commonly applied to clothes, bedding etc., is made For the article for wearing next to the skin or using, for the requirement in terms of disinfecting also higher, and due to frequent and human contact, sweat Bacterium is easily grown with secretion, harmful effect is caused to human body health, and daily washing can only remove dust and spot, Have no the effect of sterilizing, it is therefore desirable to carry out disinfection to textile.Also there are some textile thimerosals currently on the market, but Chemical assistant is added with mostly, has certain toxic side effect to human body, is not suitable for being commonly used.
The content of the invention
The object of the present invention is to provide a kind of preparation method of textile thimerosal.
The object of the invention is achieved by the following technical programs:
A kind of preparation method of textile thimerosal is provided, is comprised the following steps:
(1)Each 5~10 parts of natural plants are taken, after cleaning removal of impurities, drying and crushing respectively, are separately added into 3~4 times of absolute ethyl alcohols, point Do not extract 10~15h at room temperature, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, then under vacuum Evaporation, obtains the natural botanical extraction liquid that mass percentage concentration is 50~70%;
(2)Totally 20~30 parts of the Chinese herbal medicine of equivalent is taken, 7~12 times of water is added and decocts 50~70min, the dregs of a decoction are filtered out after cooling, will Liquid evaporates under vacuum after crossing 200 mesh sieves, obtains the extracts of Chinese herbal medicine that mass percentage concentration is 50~70%;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.
Further, the step(3)After natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and Activated carbon decolorizing, is filtered after stirring 10~15min, is crossed 300 mesh sieves, is obtained textile thimerosal.
Further, the natural plants include elscholtiza, leached tea oil slag, flagger and Jin Zhongteng.
Further, the Chinese herbal medicine is by bent including Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and mouse Grass.
Application method:Take obtained textile thimerosal in mass ratio 1:30~100 are diluted with water, then by textile 20~30min of immersion is put into, better at 40~70 DEG C, then washing drying.
Compared with prior art, the invention has the advantages that:
The present invention provides a kind of preparation method of textile thimerosal, using natural plants and Chinese herbal medicine, to the nontoxic pair of human body Effect, and infected by influenza has certain inactivation capacity, to staphylococcus aureus, beta streptococcus, typhoid bacillus, Freund dysentery Shigella, corynebacterium diphtheriae, diplococcus meningitidis, micrococcus catarrhalis, there is stronger antibacterial action, and sterilizing power is strong, to spinning The feel of fabric in itself etc. will not impact, and the daily disinfection suitable for textiles such as clothing, bedding, towels makes With.
Embodiment
With reference to specific embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)10 parts of elscholtiza, 5 parts of leached tea oil slag, 7 parts of flagger and golden 9 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively 3 times of absolute ethyl alcohols are added, extract 15h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, so Evaporate under vacuum afterwards, obtain the natural botanical extraction liquid that mass percentage concentration is 50%;
(2)Totally 30 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 7 times of decoctings 70min is boiled, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is 50% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.
Embodiment 2
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)8 parts of elscholtiza, 6 parts of leached tea oil slag, 5 parts of flagger and golden 10 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively 4 times of absolute ethyl alcohols are added, extract 10h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, so Evaporate under vacuum afterwards, obtain the natural botanical extraction liquid that mass percentage concentration is 70%;
(2)Totally 20 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 12 times of water 50min is decocted, the dregs of a decoction is filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is 70% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 10min, 300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 3
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)5 parts of elscholtiza, 9 parts of leached tea oil slag, 8 parts of flagger and golden 6 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively 3.5 times of absolute ethyl alcohols are added, extract 12h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, Then evaporate under vacuum, obtain the natural botanical extraction liquid that mass percentage concentration is 60%;
(2)Totally 25 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 10 times of water 60min is decocted, the dregs of a decoction is filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is 60% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 15min, 300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 4
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)7 parts of elscholtiza, 5 parts of leached tea oil slag, 8 parts of flagger and golden 5 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively 3 times of absolute ethyl alcohols are added, extract 13h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, so Evaporate under vacuum afterwards, obtain the natural botanical extraction liquid that mass percentage concentration is 55%;
(2)Totally 22 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 8 times of decoctings 65min is boiled, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is 65% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 12min, 300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 5
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)9 parts of elscholtiza, 10 parts of leached tea oil slag, 10 parts of flagger and golden 8 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, point Not Jia Ru 4 times of absolute ethyl alcohols, extract 11h at room temperature respectively, respectively filter after separated, merging filtrate, cross 200 mesh sieves, Then evaporate under vacuum, obtain the natural botanical extraction liquid that mass percentage concentration is 58%;
(2)Totally 28 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 9 times of decoctings 68min is boiled, the dregs of a decoction are filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is 62% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 14min, 300 mesh sieves are crossed, obtain textile thimerosal.
Embodiment 6
Present embodiment discloses a kind of preparation method of textile thimerosal, comprise the following steps:
(1)5 parts of elscholtiza, 7 parts of leached tea oil slag, 5 parts of flagger and golden 8 parts of clock rattan are taken, after cleaning removal of impurities, drying and crushing respectively, respectively 3.5 times of absolute ethyl alcohols are added, extract 14h at room temperature respectively, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, Then evaporate under vacuum, obtain the natural botanical extraction liquid that mass percentage concentration is 55%;
(2)Totally 24 parts of Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and the affine cudweed of equivalent are taken, adds 11 times of water 55min is decocted, the dregs of a decoction is filtered out after cooling, liquid is crossed after 200 mesh sieves and is evaporated under vacuum, obtaining mass percentage concentration is 55% extracts of Chinese herbal medicine;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, add diatomite and activated carbon, is filtered after stirring 13min, 300 mesh sieves are crossed, obtain textile thimerosal.

Claims (4)

1. a kind of preparation method of textile thimerosal, it is characterised in that comprise the following steps:
(1)Each 5~10 parts of natural plants are taken, after cleaning removal of impurities, drying and crushing respectively, are separately added into 3~4 times of absolute ethyl alcohols, point Do not extract 10~15h at room temperature, separated after filtering respectively, merging filtrate, crosses 200 mesh sieves, then under vacuum Evaporation, obtains the natural botanical extraction liquid that mass percentage concentration is 50~70%;
(2)Totally 20~30 parts of the Chinese herbal medicine of equivalent is taken, 7~12 times of water is added and decocts 50~70min, the dregs of a decoction are filtered out after cooling, will Liquid evaporates under vacuum after crossing 200 mesh sieves, obtains the extracts of Chinese herbal medicine that mass percentage concentration is 50~70%;
(3)Natural botanical extraction liquid and extracts of Chinese herbal medicine are merged, stirs evenly, obtains textile thimerosal.
2. the preparation method of textile thimerosal according to claim 1, it is characterised in that the step(3)To naturally it plant After thing extracting solution and extracts of Chinese herbal medicine merge, diatomite and activated carbon are added, is filtered after stirring 10~15min, crosses 300 mesh Sieve, obtains textile thimerosal.
3. the preparation method of textile thimerosal according to claim 1 or claim 2, it is characterised in that the natural plants include Elscholtiza, leached tea oil slag, flagger and Jin Zhongteng.
4. according to the preparation method of the textile thimerosal of claim 1 or 3, it is characterised in that the Chinese herbal medicine by including Herba Andrographitis, Chinese violet, macleaya cordata, Asiatic plantain, folium panacis japonici cum caule and affine cudweed.
CN201711194642.XA 2017-11-24 2017-11-24 The preparation method of textile thimerosal Pending CN107996627A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101317585A (en) * 2007-06-04 2008-12-10 孙克来 Broad spectrum environment friendly pesticide and preparation thereof
CN103444801A (en) * 2013-08-19 2013-12-18 河北省科学技术情报研究院 Traditional Chinese medicinal bactericidal freshening preparation for sterilizing library
CN103651607A (en) * 2013-12-18 2014-03-26 青岛百瑞吉生物工程有限公司 Biopesticide for vegetables and preparation method of biopesticide
CN103721286A (en) * 2013-10-24 2014-04-16 青岛华仁技术孵化器有限公司 Air freshener with disinfection function
CN104082353A (en) * 2014-07-04 2014-10-08 李钟� Pure traditional Chinese medicine disinfectant and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101317585A (en) * 2007-06-04 2008-12-10 孙克来 Broad spectrum environment friendly pesticide and preparation thereof
CN103444801A (en) * 2013-08-19 2013-12-18 河北省科学技术情报研究院 Traditional Chinese medicinal bactericidal freshening preparation for sterilizing library
CN103721286A (en) * 2013-10-24 2014-04-16 青岛华仁技术孵化器有限公司 Air freshener with disinfection function
CN103651607A (en) * 2013-12-18 2014-03-26 青岛百瑞吉生物工程有限公司 Biopesticide for vegetables and preparation method of biopesticide
CN104082353A (en) * 2014-07-04 2014-10-08 李钟� Pure traditional Chinese medicine disinfectant and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李江英,张亚军主编: "《芦荟大揭密 一部有关"申请植物"的百科全书》", 中国农业出版社 *

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Application publication date: 20180508

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