CN1079646A - " Ganson maifanshi " bath-lotion - Google Patents

" Ganson maifanshi " bath-lotion Download PDF

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Publication number
CN1079646A
CN1079646A CN 93102635 CN93102635A CN1079646A CN 1079646 A CN1079646 A CN 1079646A CN 93102635 CN93102635 CN 93102635 CN 93102635 A CN93102635 A CN 93102635A CN 1079646 A CN1079646 A CN 1079646A
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China
Prior art keywords
maifanshi
bath
ganson
radix
soluble
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CN 93102635
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Chinese (zh)
Inventor
朱颉安
章丽云
童兵
付黄浦
何胜宏
尉孟龙
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DONGHU MATERIAL COMPOUND NEW TECHNOLOGY CORP WUHAN CITY
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DONGHU MATERIAL COMPOUND NEW TECHNOLOGY CORP WUHAN CITY
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Priority to CN 93102635 priority Critical patent/CN1079646A/en
Publication of CN1079646A publication Critical patent/CN1079646A/en
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Abstract

" Ganson maifanshi " bath-lotion, it is to be primary raw material with the Maifanitum, the mineral YAOSHI that is aided with other is mixed, sintering, technology such as concentrate and make full water-soluble maifanshi " bath essence, add the full water-soluble pressed powder that extracts with in tens kinds of Chinese herbal medicine such as Radix Et Rhizoma Nardostachyos, Radix Ginseng, Rhizoma Chuanxiong, mix according to a certain percentage with the maifanshi " bath essence then, make " Ganson maifanshi " bath-lotion.
The multiple inorganic nutritive element of energy stripping after this product balneation, percutaneous osmosis, further increase the nutrient of skin, thereby make it that effects such as allaying tiredness, Palmitoleic Acid, soothing the channels and quicking the network vessels be arranged, simultaneously tinea manus and pedis, skin eczema, arthritis etc. are had certain curative effect.

Description

" Ganson maifanshi " bath-lotion
" Ganson maifanshi " bath-lotion belongs to the domestic health-care product category.
Maifanitum is the medicinal Ore that a kind of utmost point has therapeuticing and health effect in the traditional medicine, and at present, there are many reports the extraction and the production method aspect of relevant Maifanitum.As invention disclosed patent CN87105061 " Maifanitum active ingredient enrichment extracting method and equipment ", CN1036335 " productive method of China medicine stone extract ".The Maifanitum of above-mentioned two patent introductions is that the trace element enrichment with the contained needed by human body of Maifanitum extracts, its common characteristic is to adopt the method for Maifanitum raw ore (or original ore powder) with single acid solution leaching, and " China medicine stone extract " made in the neutralization of reuse alkali.
Above-mentioned two kinds of production methods without any processing, are just used single acid leach solution to raw ore, because in the acid treatment process, the structure of Maifanitum raw ore is suffered partial destruction, so the harmful element stripping quantity increases greatly; Handle with the solution leaching of single acid simultaneously, make some that human body beneficial's trace element is formed precipitation easily, can not effectively utilize.The present invention has overcome the Maifanitum application limit; Make full use of the various trace elements that Maifanitum is rich in needed by human body, with the Maifanitum is primary raw material, Calamina, Natrii Sulfas, Gypsum Fibrosum, four kinds of YAOSHI of Magnetitum mix simultaneously through overdoping, sintering, technology such as concentrate, make full water-soluble maifanshi " bath essence, the full water-soluble pressed powder of 11 kinds of Chinese medicine extraction such as Radix Et Rhizoma Nardostachyos, Radix Ginseng, Rhizoma Chuanxiong, Herba Dendranthematis indici, Flos Chrysanthemi, Cortex Moutan, Radix Salviae Miltiorrhizae, red luxuriant growth, Fructus Schisandrae Chinensis, Rhizoma Acori Graminei, Radix Notoginseng mixes the maifanshi " bath essence by certain proportioning simultaneously.
The technological process of production of the present invention is seen Fig. 1, Fig. 2.
Fig. 1: the molten essence of full water-soluble Maifanitum
Fig. 2: dipping essence in the full water-soluble.
(1) medical stone, calamine, saltcake, gypsum, five kinds of mineral remedies difference of magnetite pulverizing and jevigating, passing-screen size is 120 orders~325 orders.
(2) above-mentioned five kinds of ores are prepared burden with certain proportion, ratio is as follows:
Maifanitum 50~70wt%
Calamina 5~10wt%
Awns sand 5~10wt%
Gypsum Fibrosum 10~15wt%
Magnetitum 10~15wt%
Batching inserted in the batch mixer mixed 0.5 hour~2 hours, to evenly.
(3) above-mentioned compound is contained in the potter's clay system saggar, the mineral sintered body is made in 800 ℃~1200 ℃ calcinings of high temperature furnace 2 hours~8 hours; Again it is broken into 0.5cm~1cm granule.
(4) compound acid preparation: sulphuric acid (chemical pure, concentration 0.1M~2M), hydrochloric acid (CP, (food usefulness, concentration 10wt%~30wt%), above-mentioned three kinds of acid are with volume ratio (0.5~1): (0.5~1): fully mix for concentration 0.1~2M), citric acid by the ratio of (8~15).
(5) in ceramic vessel with compound acid and mineral sintered body particle, part by weight is (3~5): 1, be heated to 80~95 ℃, leached 4 hours~8 hours, left standstill again 1 hour~4 hours, take out the supernatant, and three times repeatedly, above-mentioned solution is mixed.
(6) with soda (in the solution of CP, concentration 0.5M~3M) and the above-mentioned solution of going up, to pH value be 5~6, filter, with solution spray dryer drying, make full water-soluble Maifanitum solid essence.
(7) get Chinese herbal medicine, 11 kinds of Chinese medicine proportionings following (percentage by weight):
Radix Et Rhizoma Nardostachyos 20~50wt%
Radix Ginseng 2~5wtt
Rhizoma Chuanxiong 8~11wt%
Herba Dendranthematis indici 10~13wt%
Flos Chrysanthemi 6~9wt%
Cortex Moutan 5~8wt%
Radix Salviae Miltiorrhizae 4~7wt%
Red luxuriant growth 5~8wt%
Fructus Schisandrae Chinensis 3~6wt%
Rhizoma Acori Graminei 4~8wt%
Radix Notoginseng 3~7wt%
Mix above former medicine, leach 50 ℃~80 ℃ heating with alcoholic solution (volume by volume concentration 30%~70%), 4~8 hours, filter, get solution.
(8) above-mentioned solution decompression is concentrated (volume concentrates 3~5 times) and precipitation dope (volume concentrates 5~10 times), dry on spray dryer again, make full water-soluble Radix Et Rhizoma Nardostachyos solid essence.
(9) be (8~15) with the smart weight ratio of the full water-soluble Maifanitum solid of certain proportioning with full water-soluble Radix Et Rhizoma Nardostachyos solid essence: 1, uniform mixing is made " Ganson maifanshi " bath-lotion.
Invention characteristics of the present invention are:
Adopt new prescription and calcine technology, make the easy stripping of beneficial element in the Maifanitum, and wherein harmful element is limited in the structure, is difficult for stripping.Adopt compound acid treatment simultaneously, make healthy trace elements with household can not form precipitation, cause waste.
Utilize the effect of Chinese herbal medicine to combine, significant curative effect is arranged for clean skin, skin protection, skin moistening, beauty treatment with the effect of Maifanitum trace element.
The embodiment of the invention comprises the preparation technology of " " Ganson maifanshi " bath-lotion ".
Preparation technology:
(1) preparation of full water-soluble Maifanitum solid essence.
Proportioning raw materials (percentage by weight):
Maifanitum 62wt%
Calamina 8wt%
Natrii Sulfas 7wt%
Gypsum Fibrosum 12wt%
Magnetitum 11wt%
More than five kinds of raw material pulverizing and jevigatings, granularity is respectively:
Maifanitum 200 orders that sieve
Calamina 180 orders that sieve
Natrii Sulfas 150 orders that sieve
Gypsum Fibrosum 325 orders that sieve
Magnetitum 250 orders that sieve
Batching with its mixing, is contained in the potter's clay saggar in the batch mixer, and calcining 6 hours under 1100 ℃ of conditions in high temperature furnace is taken out saggar when being cooled to 400 ℃ of furnace temperature, obtains the mineral sintered body, is broken into 0.5cm~1cm granule again.
Acid material:
Sulphuric acid (chemical pure, concentration 0.5M)
Hydrochloric acid (chemical pure, concentration 0.5M)
Citric acid (food usefulness, concentration 10.wt%)
Above-mentioned three kinds of acidic aqueous solutions with 1: 1: 10 uniform mixing of volume ratio, are inserted this compound acid in the ceramic pot then, pour mineral sintered body (0.5cm~1cm granule) into, cooperate at 1: 3 with solid-to-liquid ratio, to make that this solution is little to boil 6 hours with electrical heating, leave standstill 3 hours, get the clear solution in upper strata.Handle 3 times with acid solution repeatedly, above-mentioned solution is collected in together.
(chemical pure, 1M) the above-mentioned solution of solution titration to pH value is between 5~6 with soda.Filter, obtain full water-soluble Maifanitum solid essence with spray drying method.
(2) preparation of full water-soluble Radix Et Rhizoma Nardostachyos solid essence
Proportioning raw materials (percentage by weight)
Radix Et Rhizoma Nardostachyos 39wt%
Radix Ginseng 2wt%
Rhizoma Chuanxiong 9wt%
Herba Dendranthematis indici 10wt%
Flos Chrysanthemi 9wt%
Cortex Moutan 6wt%
Radix Salviae Miltiorrhizae 5wt%
Red luxuriant growth 7wt%
Fructus Schisandrae Chinensis 3wt%
Rhizoma Acori Graminei 6wt%
Radix Notoginseng 4wt%
Levigate (extract with alcoholic solution under 0.1~0.5cm), 57 ℃ of conditions, filtered concentrating under reduced pressure then 2 hours, precipitation concentrates 3 hours, makes full water-soluble Radix Et Rhizoma Nardostachyos solid essence with spray drying method at last above-mentioned 11 kinds of Chinese herbal medicine.
(3) with full water-soluble Maifanitum solid essence, full water-soluble Radix Et Rhizoma Nardostachyos stone solid essence promptly gets the present invention with 10: 1 ratio uniform mixing of weight ratio, with " Ganson maifanshi " bath-lotion by the actual condition of using, with solid-to-liquid ratio=1: 10 4When being dissolved in distilled water, record essential element and micronutrient levels sees the following form:
Sequence number Element or ion Concentration PPm Sequence number Element or ion Concentration PPm
1 Ca 15.52 10 Cd 〈0.002
2 Mg 0.0498 11 Fe 0.30
3 Na 11.9 12 Hg 〈0.0001
4 K 27.3 13 Mn 0.0004
5 SO 4 2- 55.4 14 Sr 0.21
6 Cu 〈0.01 15 V 0.00022
7 Zn 0.49 16 Mo 0.00001
8 HCO - 3 10.1 17 Pb 〈0.02
9 As 0.00001

Claims (8)

1, a kind of " Ganson maifanshi " bath-lotion, it is characterized in that with the Maifanitum being primary raw material, mix other 4 kinds of mineral YAOSHI and make full dissolubility China medicine stone extract, again full water-soluble pressed powder and the China medicine stone extract that puts forward in the Chinese herbal medicine mixed through technologies such as fragmentation, fine grindings.
2, " Ganson maifanshi " bath-lotion according to claim 1 is characterized in that 4 kinds of mineral YAOSHI are Natrii Sulfas, Calamina, Magnetitum, Gypsum Fibrosum, and ratio is:
Maifanitum 50-70wt%
Awns sand 5~10wt%
Calamina 5~10wt%
Magnetitum 10~15wt%
Gypsum Fibrosum 10~15wt%
3, " Ganson maifanshi " bath-lotion according to claim 1 is characterized in that Chinese herbal medicine is to adopt Radix Et Rhizoma Nardostachyos, Radix Ginseng, Rhizoma Chuanxiong, Herba Dendranthematis indici, anti-chrysanthemum, Cortex Moutan, Radix Salviae Miltiorrhizae, red luxuriant growth, Fructus Schisandrae Chinensis, Rhizoma Acori Graminei, Radix Notoginseng.
Material rate is: (percentage by weight)
Radix Et Rhizoma Nardostachyos 20~50wt%
Radix Ginseng 2~5wtt
Rhizoma Chuanxiong 8~11wt%
Herba Dendranthematis indici 10~13wt%
Flos Chrysanthemi 6~9wt%
Cortex Moutan 5~8wt%
Radix Salviae Miltiorrhizae 4~7wt%
Red luxuriant growth 5~8wt%
Fructus Schisandrae Chinensis 3~6wt%
Rhizoma Acori Graminei 4~8wt%
Radix Notoginseng 3~7wt%
4, " Ganson maifanshi " bath-lotion according to claim 1, the preparation that it is characterized in that full water-soluble solid essence are fragmentation, proportioning, calcining, fragmentation, acidic aqueous solution heating leaching.
5, " Ganson maifanshi " bath-lotion according to claim 4 is characterized in that ore sintering body crushed particles is 0.5~1cm, 800~1200 ℃ of sintering temperatures.
6, " Ganson maifanshi " bath-lotion according to claim 1, acidic aqueous solution adopts sulphuric acid, hydrochloric acid, citric acid, and its ratio is:
Sulphuric acid (chemical pure, concentration 0.5M)
Hydrochloric acid (chemical pure, concentration 0.5M)
Citric acid (food usefulness, concentration 10.wt%)
7, three kinds of acidic aqueous solution ratios of " Ganson maifanshi " bath-lotion according to claim 6 are 1: 1: 10.
8, " Ganson maifanshi " bath-lotion according to claim 1 is characterized in that the smart weight ratio with full water-soluble Radix Et Rhizoma Nardostachyos solid essence of full water-soluble Maifanitum solid is 8~15: 1.
CN 93102635 1993-03-10 1993-03-10 " Ganson maifanshi " bath-lotion Pending CN1079646A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 93102635 CN1079646A (en) 1993-03-10 1993-03-10 " Ganson maifanshi " bath-lotion

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 93102635 CN1079646A (en) 1993-03-10 1993-03-10 " Ganson maifanshi " bath-lotion

Publications (1)

Publication Number Publication Date
CN1079646A true CN1079646A (en) 1993-12-22

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1049137C (en) * 1994-11-09 2000-02-09 温长路 Skin-warming body-building bath lotion containing Chinese medicine
WO2005011716A1 (en) * 2003-07-21 2005-02-10 Henkel Kommanditgesellschaft Auf Aktien Prebiotically active plant extracts
CN102552089A (en) * 2012-01-18 2012-07-11 江苏同源堂生物工程有限公司 Gingko bath powder and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1049137C (en) * 1994-11-09 2000-02-09 温长路 Skin-warming body-building bath lotion containing Chinese medicine
WO2005011716A1 (en) * 2003-07-21 2005-02-10 Henkel Kommanditgesellschaft Auf Aktien Prebiotically active plant extracts
CN102552089A (en) * 2012-01-18 2012-07-11 江苏同源堂生物工程有限公司 Gingko bath powder and preparation method thereof

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