CN107927422A - Artificial breeding feed of oyster and preparation method thereof - Google Patents

Artificial breeding feed of oyster and preparation method thereof Download PDF

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CN107927422A
CN107927422A CN201711263090.3A CN201711263090A CN107927422A CN 107927422 A CN107927422 A CN 107927422A CN 201711263090 A CN201711263090 A CN 201711263090A CN 107927422 A CN107927422 A CN 107927422A
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parts
oyster
weight
reaction kettle
bath
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李六秀
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K50/00Feeding-stuffs specially adapted for particular animals
    • A23K50/70Feeding-stuffs specially adapted for particular animals for birds
    • A23K50/75Feeding-stuffs specially adapted for particular animals for birds for poultry
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/10Animal feeding-stuffs obtained by microbiological or biochemical processes
    • A23K10/16Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • A23K10/22Animal feeding-stuffs from material of animal origin from fish
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • A23K10/26Animal feeding-stuffs from material of animal origin from waste material, e.g. feathers, bones or skin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/37Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/111Aromatic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/163Sugars; Polysaccharides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/26Compounds containing phosphorus
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/28Silicates, e.g. perlites, zeolites or bentonites
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/30Oligoelements
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

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  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
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  • Food Science & Technology (AREA)
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  • Fodder In General (AREA)

Abstract

The invention discloses the artificial breeding feed of a seed oyster, include the raw material of following parts by weight:21~25 parts of flour, 10~13 parts of dregs of beans, 7~9 portions of corn flour, 5~10 parts of cuttlefish powders, 8~12 parts of dried silkworm chrysalis meals, 4~6 parts of shrimp shell meals, 3~8 parts of liver powder, 25~28 parts of Isochrysis galbanas, 17~22 parts of Chaetoceros, 15~19 parts of Drilgrasses, 2~9 parts of HERBA HEDYOTIS DIFFUSAEs, 1~6 part of Herba Pteridis Multifidae, 11~15 parts of calcium dihydrogen phosphates, 7~13 parts of zeolite powders, 1~4 part of montmorillonite, 1~4 part of bentonite, 3~6 parts of choline chlorides, 5~7 parts of glycine betaines, 16~22 parts of chitosans, 6~10 parts of lignin, 7~9 parts of composite mineral matters.The present invention can improve oyster artificial breeding survival rate, shorten the culturing time of oyster, improve the yield of oyster.

Description

Artificial breeding feed of oyster and preparation method thereof
Technical field
The present invention relates to oyster culture field.It is more particularly related to the artificial breeding feed of a seed oyster and Its preparation method.
Background technology
Oyster is a kind of most commonly seen shellfish of China coast, is commonly called as oyster, oyster Huang, oyster, contains albumen in its soft body Matter 45%~57%, lipase 37 %~11%, glycogen 19%~38%, additionally grade containing multivitamin, ash, have compared with High nutritive value, there is the title of " ocean milk ".The meat of oyster also has certain medical value, the courage of oyster in addition to delicious flavour Sterol content is low, Zn content is high, helps to improve male's sexual.And oyster shell is the good raw material of lime calcining, it is also possible to Come processing and fabricating button and craftwork, the feed addictive that can also be milled as poultry, domestic animal.Therefore oyster is big-and-middle at some Goods tight valency in city is expensive, and existing oyster culture technology and imperfection, oyster yield cannot fully meet the market demand.
The content of the invention
It is an object of the invention to solve at least the above, and provide the advantages of at least will be described later.
It is a still further object of the present invention to provide a kind of cultivation that can be improved oyster artificial breeding survival rate, shorten oyster Time, the artificial breeding feed of oyster of yield for improving oyster and preparation method thereof.
In order to realize these purposes and further advantage according to the present invention, there is provided the artificial breeding feed of a seed oyster, Include the raw material of following parts by weight:21~25 parts of flour, 10~13 parts of dregs of beans, 7~9 portions of corn flour, 5~10 parts of cuttlefish powders, 8~ 12 parts of dried silkworm chrysalis meals, 4~6 parts of shrimp shell meals, 3~8 parts of liver powder, 25~28 parts of Isochrysis galbanas, 17~22 parts of Chaetoceros, 15~19 Part Drilgrass, 2~9 parts of HERBA HEDYOTIS DIFFUSAEs, 1~6 part of Herba Pteridis Multifidae, 11~15 parts of calcium dihydrogen phosphates, 7~13 parts of zeolite powders, 1~4 part of illiteracy De- soil, 1~4 part of bentonite, 3~6 parts of choline chlorides, 5~7 parts of glycine betaines, 16~22 parts of chitosans, 6~10 parts of lignin, 7~9 Part composite mineral matter.
Preferably, the raw material of following percentage by weight is included in every part of composite mineral matter:13% cupric glycinate, 25% Sodium selenite, 17% calcium iodate, 21% manganese methionine, 9% glycine zine, 15% cobalt methionine.
Preferably, Drilgrass, HERBA HEDYOTIS DIFFUSAE, the weight ratio of Herba Pteridis Multifidae are 4.5:1:1.
Preferably, calcium dihydrogen phosphate, zeolite powder, montmorillonite, bentonite, the weight ratio of composite mineral matter are 1:1:0.25: 0.25:0.67.
The present invention also provides the preparation method of the artificial breeding feed of above-mentioned oyster, including:
Step 1: the Isochrysis galbana of above-mentioned parts by weight, Chaetoceros, Drilgrass, HERBA HEDYOTIS DIFFUSAE and Herba Pteridis Multifidae are shredded, must cut Particle, will shred and fumigates 2~3h with deionized water at a temperature of material is placed in 90~100 DEG C, then will it is stifling after the material that shreds mash, and By 1:10~13 weight ratio adds the hydrolyzate that cellulase is mixed with papain, then by immersed with the water for shredding material Solving liquid and carry out infrared heating, heating time be 1~2h, and heating-up temperature is 38~41 DEG C, while is aided with magnetic agitation, then to reaction The aqueous solution for shredding the mass fraction of 5 times of gross mass of material as 25~30% NaCl is added in kettle, reaction kettle is carried out for the first time Heating water bath, bath temperature be 90~100 DEG C, after reacting kettle inner pressure reaches 220~240kpa keep water-bath 30~ 45min, is then placed in Temperature fall in air by reaction kettle stopping water-bath, liquid therein is left and taken when reaction kettle is cooled to room temperature Body obtains the first diffusate, then the water for shredding the mass fraction of 3 times of gross mass of material as 15~19% NaCl is added into reaction kettle Solution, second of heating water bath is carried out by reaction kettle, and bath temperature is 90~100 DEG C, when reacting kettle inner pressure reaches 190~ 24~28min of water-bath is kept after 210kpa, reaction kettle stopping water-bath is then placed in Temperature fall in air, when reaction kettle drops Liquid therein is left and taken after to room temperature and obtains the second diffusate, at the same by reaction kettle it is remaining shred material and air-dry be crushed into powder, obtain Powder materials;
Step 2, by the choline chloride of above-mentioned parts by weight, glycine betaine, chitosan, lignin and step 1 obtained the One diffusate and the second diffusate mix to obtain soak, then soak is evaporated under reduced pressure, pressure control 65~ 75kpa, temperature control is at 80~90 DEG C, when the volume of soak is decreased to original volumeStop vacuum distillation, then will be upper Powder materials made from stating flour, dregs of beans, corn flour, cuttlefish powder, dried silkworm chrysalis meal, shrimp shell meal, liver powder and the step 1 of parts by weight fall Enter to stir evenly in the soak after vacuum distillation and paste is made, the calcium dihydrogen phosphate of above-mentioned parts by weight, zeolite powder, illiteracy is de- Soil, bentonite, composite mineral matter mix to obtain mixture with the deionized water of 112~120 parts by weight, and mixture is kneaded into a diameter of The graininess of 3~5mm, then put it into Muffle furnace and calcine, calcining heat control at 350~400 DEG C, time control 25~ 35min, must calcine material, will calcine the circumferentially uniform applied paste of particle surface of material, enwrapped granule material is obtained, by enwrapped granule material wind Particulate material must be air-dried after dry;
Step 3: obtained air-dried particulate material in step 2 is carried out disinfection by ultraviolet light, the artificial breeding feed of oyster is obtained.
Preferably, ultrasonication is carried out before soak is evaporated under reduced pressure in step 2, the frequency of ultrasonic wave is 28 ~32KHz.
The present invention includes at least following beneficial effect:
Containing more protein with trace element, can meet comprehensively oyster growth needed for nutrient, and Drilgrass, The active ingredient contained in HERBA HEDYOTIS DIFFUSAE and Herba Pteridis Multifidae can stimulate oyster to grow, and shorten its growth cycle, chitosan, lignin are matched somebody with somebody Wu Houneng improves oyster artificial breeding survival rate.It is long-term to occupy and preparation method provided by the invention is according to the life habit of oyster In sand mud beach, the little particle with coating is fabricated to, is on the one hand easily settled down to sand mud beach bottom, it is not easy to rolled up by tide Walk, while facilitate oyster to ingest after seawater softening decomposes, the component of another aspect surface coatings also can induce oyster and ingest..
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification Word can be implemented according to this.
It should be noted that experimental method described in following embodiments, is conventional method unless otherwise specified, institute Reagent and material are stated, unless otherwise specified, is commercially obtained.
<Embodiment 1>
The artificial breeding feed of one seed oyster, includes the raw material of following parts by weight:21 parts of flour, 10 parts of dregs of beans, 7 parts of corns Powder, 5 parts of cuttlefish powders, 8 parts of dried silkworm chrysalis meals, 4 parts of shrimp shell meals, 3 parts of liver powder, 25 parts of Isochrysis galbanas, 17 parts of Chaetoceros, 15 parts successively Grass, 2 parts of HERBA HEDYOTIS DIFFUSAEs, 1 part of Herba Pteridis Multifidae, 11 parts of calcium dihydrogen phosphates, 7 parts of zeolite powders, 1 part of montmorillonite, 1 part of bentonite, 3 parts of chlorination courages Alkali, 5 parts of glycine betaines, 16 parts of chitosans, 6 parts of lignin, 7 parts of composite mineral matters.
Wherein, the raw material of following percentage by weight is included in every part of composite mineral matter:13% cupric glycinate, 25% Asia Sodium selenate, 17% calcium iodate, 21% manganese methionine, 9% glycine zine, 15% cobalt methionine.
The preparation method of the artificial breeding feed of above-mentioned oyster, including:
Step 1: the Isochrysis galbana of above-mentioned parts by weight, Chaetoceros, Drilgrass, HERBA HEDYOTIS DIFFUSAE and Herba Pteridis Multifidae are shredded, must cut Particle, will shred and fumigates 2h with deionized water at a temperature of material is placed in 90 DEG C, then will it is stifling after the material that shreds mash, and by 1:10 Weight ratio adds the hydrolyzate that cellulase is mixed with papain, then will be carried out immersed with the hydrolyzate for shredding material infrared Heating, heating time 1h, heating-up temperature is 38 DEG C, while is aided with magnetic agitation, then is added into reaction kettle and shred the total matter of material The mass fraction of 5 times of amount is the aqueous solution of 25% NaCl, and reaction kettle is carried out first time heating water bath, bath temperature 90 DEG C, water-bath 30min is kept after reacting kettle inner pressure reaches 220kpa, is then placed in reaction kettle stopping water-bath in air certainly So cooling, leaves and takes liquid therein and obtains the first diffusate when reaction kettle is cooled to room temperature, then adds into reaction kettle that to shred material total The mass fraction that 3 times of quality is the aqueous solution of 15% NaCl, and reaction kettle is carried out second of heating water bath, bath temperature 90 DEG C, water-bath 24min is kept after reacting kettle inner pressure reaches 190kpa, is then placed in reaction kettle stopping water-bath in air certainly So cooling, leaves and takes liquid therein and obtains the second diffusate when reaction kettle is cooled to room temperature, while is shredded remaining in reaction kettle Material is air-dried and is crushed into powder, and obtains powder materials;
Step 2, by the choline chloride of above-mentioned parts by weight, glycine betaine, chitosan, lignin and step 1 obtained the One diffusate and the second diffusate mix to obtain soak, first carry out ultrasonication to soak, and the frequency of ultrasonic wave is 28KHz, then soak is evaporated under reduced pressure, pressure is controlled in 65kpa, and temperature control is at 80 DEG C, when the volume of soak subtracts As low as original volumeI.e. stop vacuum distillation, then by the flour of above-mentioned parts by weight, dregs of beans, corn flour, cuttlefish powder, dried silkworm chrysalis meal, Stirred evenly in the soak that shrimp shell meal, liver powder are poured into after vacuum distillation with powder materials made from step 1 and paste is made, will Calcium dihydrogen phosphate, zeolite powder, montmorillonite, bentonite, the composite mineral matter of above-mentioned parts by weight are mixed with the deionized water of 112 parts by weight Mixture is obtained, the graininess by mixture kneading into a diameter of 3mm, then put it into Muffle furnace and calcine, calcining heat control At 350 DEG C, time control must calcine material, will calcine the circumferentially uniform applied paste of particle surface of material in 25min, must wrap up Pellet, must air-dry particulate material after enwrapped granule material is air-dried;
Step 3: obtained air-dried particulate material in step 2 is carried out disinfection by ultraviolet light, the artificial breeding feed of oyster is obtained.
<Embodiment 2>
The artificial breeding feed of one seed oyster, includes the raw material of following parts by weight:25 parts of flour, 13 parts of dregs of beans, 9 parts of corns Powder, 10 parts of cuttlefish powders, 12 parts of dried silkworm chrysalis meals, 6 parts of shrimp shell meals, 8 parts of liver powder, 28 parts of Isochrysis galbanas, 22 parts of Chaetoceros, 19 parts of sections Knotweed, 9 parts of HERBA HEDYOTIS DIFFUSAEs, 6 parts of Herba Pteridis Multifidaes, 15 parts of calcium dihydrogen phosphates, 13 parts of zeolite powders, 4 parts of montmorillonites, 4 parts of bentonite, 6 parts of chlorinations Choline, 7 parts of glycine betaines, 22 parts of chitosans, 10 parts of lignin, 9 parts of composite mineral matters.
Wherein, the raw material of following percentage by weight is included in every part of composite mineral matter:13% cupric glycinate, 25% Asia Sodium selenate, 17% calcium iodate, 21% manganese methionine, 9% glycine zine, 15% cobalt methionine.
The preparation method of the artificial breeding feed of above-mentioned oyster, including:
Step 1: the Isochrysis galbana of above-mentioned parts by weight, Chaetoceros, Drilgrass, HERBA HEDYOTIS DIFFUSAE and Herba Pteridis Multifidae are shredded, must cut Particle, will shred and fumigates 3h with deionized water at a temperature of material is placed in 100 DEG C, then will it is stifling after the material that shreds mash, and by 1:13 Weight ratio add the hydrolyzate that is mixed with papain of cellulase, then will be red immersed with the hydrolyzate progress for shredding material External heat, heating time 2h, heating-up temperature is 41 DEG C, while is aided with magnetic agitation, then is added into reaction kettle and shred material always The mass fraction that 5 times of quality is the aqueous solution of 30% NaCl, reaction kettle is carried out first time heating water bath, bath temperature is 100 DEG C, water-bath 45min is kept after reacting kettle inner pressure reaches 240kpa, reaction kettle stopping water-bath is then placed in air Middle Temperature fall, leaves and takes liquid therein and obtains the first diffusate when reaction kettle is cooled to room temperature, then adds and shred into reaction kettle The mass fraction for expecting 3 times of gross mass is the aqueous solution of 19% NaCl, and reaction kettle is carried out second of heating water bath, bath temperature For 100 DEG C, water-bath 28min is kept after reacting kettle inner pressure reaches 210kpa, reaction kettle stopping water-bath is then placed in sky Temperature fall in gas, leaves and takes liquid therein and obtains the second diffusate when reaction kettle is cooled to room temperature, while will be left in reaction kettle Shred material air-dry be crushed into powder, obtain powder materials;
Step 2, by the choline chloride of above-mentioned parts by weight, glycine betaine, chitosan, lignin and step 1 obtained the One diffusate and the second diffusate mix to obtain soak, first carry out ultrasonication to soak, and the frequency of ultrasonic wave is 32KHz, then soak is evaporated under reduced pressure, pressure is controlled in 75kpa, and temperature control is at 90 DEG C, when the volume of soak subtracts As low as original volumeI.e. stop vacuum distillation, then by the flour of above-mentioned parts by weight, dregs of beans, corn flour, cuttlefish powder, dried silkworm chrysalis meal, Stirred evenly in the soak that shrimp shell meal, liver powder are poured into after vacuum distillation with powder materials made from step 1 and paste is made, will Calcium dihydrogen phosphate, zeolite powder, montmorillonite, bentonite, the composite mineral matter of above-mentioned parts by weight are mixed with the deionized water of 120 parts by weight Mixture is obtained, the graininess by mixture kneading into a diameter of 5mm, then put it into Muffle furnace and calcine, calcining heat control At 400 DEG C, time control must calcine material, will calcine the circumferentially uniform applied paste of particle surface of material in 35min, must wrap up Pellet, must air-dry particulate material after enwrapped granule material is air-dried;
Step 3: obtained air-dried particulate material in step 2 is carried out disinfection by ultraviolet light, the artificial breeding feed of oyster is obtained.
<Embodiment 3>
The artificial breeding feed of one seed oyster, includes the raw material of following parts by weight:23 parts of flour, 12 parts of dregs of beans, 8 parts of corns Powder, 8 parts of cuttlefish powders, 10 parts of dried silkworm chrysalis meals, 5 parts of shrimp shell meals, 6 parts of liver powder, 27 parts of Isochrysis galbanas, 20 parts of Chaetoceros, 18 parts of sections Knotweed, 4 parts of HERBA HEDYOTIS DIFFUSAEs, 4 parts of Herba Pteridis Multifidaes, 12 parts of calcium dihydrogen phosphates, 12 parts of zeolite powders, 3 parts of montmorillonites, 3 parts of bentonite, 5 parts of chlorinations Choline, 6 parts of glycine betaines, 19 parts of chitosans, 8 parts of lignin, 8 parts of composite mineral matters.
Wherein, the raw material of following percentage by weight is included in every part of composite mineral matter:13% cupric glycinate, 25% Asia Sodium selenate, 17% calcium iodate, 21% manganese methionine, 9% glycine zine, 15% cobalt methionine.
The preparation method of the artificial breeding feed of above-mentioned oyster, including:
Step 1: the Isochrysis galbana of above-mentioned parts by weight, Chaetoceros, Drilgrass, HERBA HEDYOTIS DIFFUSAE and Herba Pteridis Multifidae are shredded, must cut Particle, will shred and fumigates 2.5h with deionized water at a temperature of material is placed in 95 DEG C, then will it is stifling after the material that shreds mash, and by 1:11 Weight ratio add the hydrolyzate that is mixed with papain of cellulase, then will be red immersed with the hydrolyzate progress for shredding material External heat, heating time 1.5h, heating-up temperature is 39 DEG C, while is aided with magnetic agitation, then is added into reaction kettle and shred material The mass fraction that 5 times of gross mass is the aqueous solution of 25~30% NaCl, and reaction kettle is carried out first time heating water bath, water-bath temperature Spend for 95 DEG C, water-bath 39min is kept after reacting kettle inner pressure reaches 230kpa, reaction kettle stopping water-bath is then placed in sky Temperature fall in gas, leaves and takes liquid therein and obtains the first diffusate when reaction kettle is cooled to room temperature, then adds and cut into reaction kettle The mass fraction that 3 times of particle gross mass is the aqueous solution of 17% NaCl, and reaction kettle is carried out second of heating water bath, water-bath temperature Spend for 95 DEG C, water-bath 26min is kept after reacting kettle inner pressure reaches 200kpa, reaction kettle stopping water-bath is then placed in sky Temperature fall in gas, leaves and takes liquid therein and obtains the second diffusate when reaction kettle is cooled to room temperature, while will be left in reaction kettle Shred material air-dry be crushed into powder, obtain powder materials;
Step 2, by the choline chloride of above-mentioned parts by weight, glycine betaine, chitosan, lignin and step 1 obtained the One diffusate and the second diffusate mix to obtain soak, first carry out ultrasonication to soak, and the frequency of ultrasonic wave is 30KHz, then soak is evaporated under reduced pressure, pressure is controlled in 70kpa, and temperature control is at 85 DEG C, when the volume of soak subtracts As low as original volumeI.e. stop vacuum distillation, then by the flour of above-mentioned parts by weight, dregs of beans, corn flour, cuttlefish powder, dried silkworm chrysalis meal, Stirred evenly in the soak that shrimp shell meal, liver powder are poured into after vacuum distillation with powder materials made from step 1 and paste is made, will Calcium dihydrogen phosphate, zeolite powder, montmorillonite, bentonite, the composite mineral matter of above-mentioned parts by weight are mixed with the deionized water of 116 parts by weight Mixture is obtained, the graininess by mixture kneading into a diameter of 4mm, then put it into Muffle furnace and calcine, calcining heat control At 370 DEG C, time control must calcine material, will calcine the circumferentially uniform applied paste of particle surface of material in 30min, must wrap up Pellet, must air-dry particulate material after enwrapped granule material is air-dried;
Step 3: obtained air-dried particulate material in step 2 is carried out disinfection by ultraviolet light, the artificial breeding feed of oyster is obtained.
<Comparative example>
The artificial breeding feed of one seed oyster, includes the raw material of following parts by weight:30~35 parts of flat algaes, 20~30 parts of bottoms are dwelt Diatom, 20~30 portions of chlorellas, 5~15 portions of corn flour, 2~4 parts of mineral matters.
The artificial breeding feed of above-mentioned oyster is mixed into excessively uniform.
The oyster in above-described embodiment 1, embodiment 2, embodiment 3 and comparative example is propagated artificially feed in North Sea oyster Mudflat aquaculture base is tested, and wherein the breeding density of oyster is 100,000/mu, is fed every 3 days 1 time, feeding volume exists 38g, continuously feeds 8 months, then digs out oyster, calculates the average weight of oyster per acre, survival rate and ripe body ratio, as a result It is shown in Table 1.
Table 1, the average weight of oyster per acre, survival rate and ripe body ratio contrast table
It is not difficult to find out in embodiment 1~3 that the average weight of oyster per acre, survival rate and ripe body ratio are above from table 1 Comparative example, illustrate oyster provided by the invention artificial breeding feed can improve oyster artificial breeding survival rate, shorten it is male The culturing time of oyster, the yield for improving oyster.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art Realize other modification, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited In specific details and shown here as the embodiment with description.

Claims (6)

1. the artificial breeding feed of a seed oyster, it is characterised in that include the raw material of following parts by weight:21~25 parts of flour, 10 ~13 parts of dregs of beans, 7~9 portions of corn flour, 5~10 parts of cuttlefish powders, 8~12 parts of dried silkworm chrysalis meals, 4~6 parts of shrimp shell meals, 3~8 parts of livers Powder, 25~28 parts of Isochrysis galbanas, 17~22 parts of Chaetoceros, 15~19 parts of Drilgrasses, 2~9 parts of HERBA HEDYOTIS DIFFUSAEs, 1~6 part of wind tail Grass, 11~15 parts of calcium dihydrogen phosphates, 7~13 parts of zeolite powders, 1~4 part of montmorillonite, 1~4 part of bentonite, 3~6 parts of choline chlorides, 5 ~7 parts of glycine betaines, 16~22 parts of chitosans, 6~10 parts of lignin, 7~9 parts of composite mineral matters.
2. the artificial breeding feed of oyster as claimed in claim 1, it is characterised in that comprising following in every part of composite mineral matter The raw material of percentage by weight:13% cupric glycinate, 25% sodium selenite, 17% calcium iodate, 21% manganese methionine, 9% glycine zine, 15% cobalt methionine.
3. the artificial breeding feed of oyster as claimed in claim 1, it is characterised in that Drilgrass, HERBA HEDYOTIS DIFFUSAE, the weight of Herba Pteridis Multifidae Amount is than being 4.5:1:1.
4. the artificial breeding feed of oyster as claimed in claim 1, it is characterised in that calcium dihydrogen phosphate, zeolite powder, illiteracy are de- Soil, bentonite, the weight ratio of composite mineral matter are 1:1:0.25:0.25:0.67.
A kind of 5. preparation method of the artificial breeding feed of oyster as claimed in claim 1, it is characterised in that including:
Step 1: the Isochrysis galbana of above-mentioned parts by weight, Chaetoceros, Drilgrass, HERBA HEDYOTIS DIFFUSAE and Herba Pteridis Multifidae are shredded, must shred Material, will shred and fumigates 2~3h with deionized water at a temperature of material is placed in 90~100 DEG C, then will it is stifling after the material that shreds mash, and press 1:10~13 weight ratio adds the hydrolyzate that cellulase is mixed with papain, then by immersed with the hydrolysis for shredding material Liquid carries out infrared heating, and heating time be 1~2h, and heating-up temperature is 38~41 DEG C, while is aided with magnetic agitation, then to reaction kettle The aqueous solution for the NaCl that the mass fraction that middle addition shreds 5 times of gross mass of material is 25~30%, first time water is carried out by reaction kettle Bath heating, bath temperature are 90~100 DEG C, and 30~45min of water-bath is kept after reacting kettle inner pressure reaches 220~240kpa, Then reaction kettle stopping water-bath being placed in Temperature fall in air, leaves and takes liquid therein when reaction kettle is cooled to room temperature and obtain the One diffusate, then the aqueous solution for shredding the mass fraction of 3 times of gross mass of material as 15~19% NaCl is added into reaction kettle, will Reaction kettle carries out second of heating water bath, and bath temperature is 90~100 DEG C, after reacting kettle inner pressure reaches 190~210kpa 24~28min of water-bath is kept, reaction kettle stopping water-bath is then placed in Temperature fall in air, when reaction kettle is cooled to room temperature Leave and take liquid therein and obtain the second diffusate, at the same by reaction kettle it is remaining shred material and air-dry be crushed into powder, obtain powder materials;
Step 2, in the choline chloride of above-mentioned parts by weight, glycine betaine, chitosan, lignin and step 1 obtained first is oozed Go out liquid and the second diffusate mixes to obtain soak, then soak is evaporated under reduced pressure, pressure control is in 65~75kpa, temperature Degree control is at 80~90 DEG C, when the volume of soak is decreased to original volumeStop vacuum distillation, then by above-mentioned parts by weight Flour, dregs of beans, corn flour, cuttlefish powder, dried silkworm chrysalis meal, shrimp shell meal, powder materials made from liver powder and step 1 pour into decompression and steam Stirred evenly in soak after evaporating and paste is made, by the calcium dihydrogen phosphate of above-mentioned parts by weight, zeolite powder, montmorillonite, bentonite, multiple Close mineral matter and mix to obtain mixture with the deionized water of 112~120 parts by weight, by mixture kneading into a diameter of 3~5mm Granular, then put it into Muffle furnace and calcine, at 350~400 DEG C, time control must be forged in 25~35min for calcining heat control Imitation frosted glass, will calcine the circumferentially uniform applied paste of particle surface of material, obtains enwrapped granule material, must be air-dried after enwrapped granule material is air-dried Particulate material;
Step 3: obtained air-dried particulate material in step 2 is carried out disinfection by ultraviolet light, the artificial breeding feed of oyster is obtained.
6. the preparation method of the artificial breeding feed of oyster as claimed in claim 5, it is characterised in that soak in step 2 Ultrasonication is carried out before being evaporated under reduced pressure, the frequency of ultrasonic wave is 28~32KHz.
CN201711263090.3A 2017-12-04 2017-12-04 Artificial breeding feed of oyster and preparation method thereof Pending CN107927422A (en)

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Publication number Priority date Publication date Assignee Title
CN108740586A (en) * 2018-06-13 2018-11-06 威海金牌生物科技股份有限公司 A kind of oyster fattening bait and preparation method thereof produced with agriculture marine product waste
CN109566860A (en) * 2018-12-29 2019-04-05 大连海洋大学 One seed oyster special compound feed
CN109699810A (en) * 2018-12-29 2019-05-03 大连海洋大学 One seed oyster Chinese herbal medicine solid state fermentation regulation type feed additive
CN114190498A (en) * 2022-01-24 2022-03-18 威海金牌生物科技有限公司 Selenium-rich oyster feed and preparation method thereof
CN114365711A (en) * 2022-01-24 2022-04-19 威海金牌生物科技有限公司 Selenium-rich oyster cultivation method

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108740586A (en) * 2018-06-13 2018-11-06 威海金牌生物科技股份有限公司 A kind of oyster fattening bait and preparation method thereof produced with agriculture marine product waste
CN109566860A (en) * 2018-12-29 2019-04-05 大连海洋大学 One seed oyster special compound feed
CN109699810A (en) * 2018-12-29 2019-05-03 大连海洋大学 One seed oyster Chinese herbal medicine solid state fermentation regulation type feed additive
CN114190498A (en) * 2022-01-24 2022-03-18 威海金牌生物科技有限公司 Selenium-rich oyster feed and preparation method thereof
CN114365711A (en) * 2022-01-24 2022-04-19 威海金牌生物科技有限公司 Selenium-rich oyster cultivation method

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