CN107794758A - 一种刺绣用整理剂的制备方法 - Google Patents
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Abstract
本申请公开了一种刺绣用整理剂的制备方法，称取蒸馏水、羧甲基纤维素钠、分散剂、橡胶大红、丝素、氧化铝、二甲基硅氧烷、氯化镁、磷酸钾、聚醚和盐酸；制备方法简单，防霉效果好，抗拉强度2‑4MPa，抗潮气性优良；增加光泽，附着力1级，耐腐蚀性好，耐洗刷性6000‑8000次；耐水洗性50‑90次螨虫趋避率90‑94%，柔韧性1mm，光泽度好；延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率95‑99%，可以广泛生产并不断代替现有材料。
Description
技术领域
本申请属于刺绣材料领域，尤其涉及一种刺绣用整理剂的制备方法。
背景技术
刺绣是针线在织物上绣制的各种装饰图案的总称。刺绣分丝线刺绣和羽毛两种。就是用针将丝线或其他纤维、纱线以一定图案和色彩在绣料上穿刺，以绣迹构成花纹的装饰织物。它是用针和线把人的设计和制作添加在任何存在的织物上的一种艺术。刺绣是中国民间传统手工艺之一，在中国至少有二三千年历史。中国刺绣主要有苏绣、湘绣、蜀绣和粤绣四大门类。刺绣的技法有：错针绣、乱针绣、网绣、满地绣、锁丝、纳丝、纳锦、平金、影金、盘金、铺绒、刮绒、戳纱、洒线、挑花等等，刺绣的用途主要包括生活和艺术装饰，如服装、床上用品、台布、舞台、艺术品装饰。
树脂整理剂旨在防止或改善织物在穿着过程中出现的收缩或折皱现象，在其印染加工后用合成树脂进行化学整理(俗称树脂整理)，如防缩、防皱树脂整理。所用的物质称为树脂整理剂。
织物整理是在织物上施加一种整理剂，它能改变织物的表面性能，从而赋予织物特殊的功能。例如憎水憎油整理是以具有低表面张力的整理剂处理织物，改变纤维的表面特性，使织物表面不易被水或油润湿和铺展，从而达到憎水憎油的目的。防污整理和易去污整理是通过改变纤维的表面性能或表面状态，使织物在穿着、使用条件下不易沾附污垢，或将已沾附的污垢易于洗涤并不再沾污的加工工艺。
三防整理剂是一种适用于棉、毛、丝、化纤及混纺纤维等织物的面料，赋予其具有超拒水拒油和防污功能的纺织后整理剂。
中国刺绣又称丝绣、针绣，是中国优秀的民族传统工艺之一。中国是世界上发现与使用蚕丝最早的国家，人们在四五千年前就已经开始养蚕、缫丝了。
随着蚕丝的使用，丝织品的产生与发展，刺绣工艺也逐渐兴起，据《尚书》记载在四千前的章服制度，就规定“衣画而裳绣”。宋代时期崇尚刺绣服装的风气，已逐渐在民间广泛流行，这也促使了中国丝绣工艺的发展。
发明内容
解决的技术问题：
本申请针对上述技术问题，提供一种刺绣用整理剂的制备方法，解决现有刺绣用整理剂防霉效果差、光泽度低和阻燃性差等技术问题。
技术方案：
一种刺绣用整理剂的制备方法，包括如下步骤：
第一步：按照重量份数配比称取蒸馏水100份、羧甲基纤维素钠10-50份、分散剂0.8-1.2份、橡胶大红0.5-4.5份、丝素5-25份、氧化铝10-30份、二甲基硅氧烷15-35份、氯化镁1-5份、磷酸钾2-6份、聚醚10-30份和盐酸1-5份；
第二步：将氧化铝、氯化镁和磷酸钾投入研磨机中研磨10-20min，在带有温度计、搅拌机和加热装置的反应釜中依次加入丝素、蒸馏水和羧甲基纤维素钠，打开搅拌机混合，升温至60-100℃，混合速度为400-600r/min，混合1-3h；
第三步：加入剩余原料，调节混合速度至1000-1200 r/min，混合6-10h，搅拌均匀，溶解完全后将混合均匀的产物投入砂磨机中，砂磨30-50min，过滤清液后，静置20-24h后即得。
作为本发明的一种优选技术方案：所述第一步中刺绣用整理剂的原料按重量份数配比如下：蒸馏水100份、羧甲基纤维素钠10份、分散剂0.8份、橡胶大红0.5份、丝素5份、氧化铝10份、二甲基硅氧烷15份、氯化镁1份、磷酸钾2份、聚醚10份和盐酸1份。
作为本发明的一种优选技术方案：所述第一步中刺绣用整理剂的原料按重量份数配比如下：蒸馏水100份、羧甲基纤维素钠50份、分散剂1.2份、橡胶大红4.5份、丝素25份、氧化铝30份、二甲基硅氧烷35份、氯化镁5份、磷酸钾6份、聚醚30份和盐酸5份。
作为本发明的一种优选技术方案：所述第一步中刺绣用整理剂的原料按重量份数配比如下：蒸馏水100份、羧甲基纤维素钠30份、分散剂1份、橡胶大红2.5份、丝素15份、氧化铝20份、二甲基硅氧烷25份、氯化镁3份、磷酸钾4份、聚醚20份和盐酸3份。
作为本发明的一种优选技术方案：所述分散剂采用甲基二萘磺酸钠。
有益效果：
本发明所述一种刺绣用整理剂的制备方法采用以上技术方案与现有技术相比，具有以下技术效果：1、制备方法简单，防霉效果好，抗拉强度2-4MPa，抗潮气性优良；2、增加光泽，附着力1级，耐腐蚀性好，耐洗刷性6000-8000次；3、耐水洗性50-90次螨虫趋避率90-94%，柔韧性1mm，光泽度好；4、延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率95-99%，可以广泛生产并不断代替现有材料。
具体实施方式
实施例1:
按照重量份数配比称取蒸馏水100份、羧甲基纤维素钠10份、甲基二萘磺酸钠0.8份、橡胶大红0.5份、丝素5份、氧化铝10份、二甲基硅氧烷15份、氯化镁1份、磷酸钾2份、聚醚10份和盐酸1份。
将氧化铝、氯化镁和磷酸钾投入研磨机中研磨10min，在带有温度计、搅拌机和加热装置的反应釜中依次加入丝素、蒸馏水和羧甲基纤维素钠，打开搅拌机混合，升温至60℃，混合速度为400r/min，混合1h。
加入剩余原料，调节混合速度至1000 r/min，混合6h，搅拌均匀，溶解完全后将混合均匀的产物投入砂磨机中，砂磨30min，过滤清液后，静置20h后即得。
制备方法简单，防霉效果好，抗拉强度2MPa，抗潮气性优良；增加光泽，附着力1级，耐腐蚀性好，耐洗刷性6000次；耐水洗性50次螨虫趋避率90%，柔韧性1mm，光泽度好；延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率95%，可以广泛生产并不断代替现有材料。
实施例2:
按照重量份数配比称取蒸馏水100份、羧甲基纤维素钠50份、甲基二萘磺酸钠1.2份、橡胶大红4.5份、丝素25份、氧化铝30份、二甲基硅氧烷35份、氯化镁5份、磷酸钾6份、聚醚30份和盐酸5份。
将氧化铝、氯化镁和磷酸钾投入研磨机中研磨20min，在带有温度计、搅拌机和加热装置的反应釜中依次加入丝素、蒸馏水和羧甲基纤维素钠，打开搅拌机混合，升温至100℃，混合速度为600r/min，混合3h。
加入剩余原料，调节混合速度至1200 r/min，混合10h，搅拌均匀，溶解完全后将混合均匀的产物投入砂磨机中，砂磨50min，过滤清液后，静置24h后即得。
制备方法简单，防霉效果好，抗拉强度3MPa，抗潮气性优良；增加光泽，附着力1级，耐腐蚀性好，耐洗刷性7000次；耐水洗性70次螨虫趋避率92%，柔韧性1mm，光泽度好；延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率97%，可以广泛生产并不断代替现有材料。
实施例3:
按照重量份数配比称取蒸馏水100份、羧甲基纤维素钠30份、甲基二萘磺酸钠1份、橡胶大红2.5份、丝素15份、氧化铝20份、二甲基硅氧烷25份、氯化镁3份、磷酸钾4份、聚醚20份和盐酸3份。
将氧化铝、氯化镁和磷酸钾投入研磨机中研磨15min，在带有温度计、搅拌机和加热装置的反应釜中依次加入丝素、蒸馏水和羧甲基纤维素钠，打开搅拌机混合，升温至80℃，混合速度为500r/min，混合2h。
加入剩余原料，调节混合速度至1100 r/min，混合8h，搅拌均匀，溶解完全后将混合均匀的产物投入砂磨机中，砂磨30-50min，过滤清液后，静置22h后即得。
制备方法简单，防霉效果好，抗拉强度4MPa，抗潮气性优良；增加光泽，附着力1级，耐腐蚀性好，耐洗刷性8000次；耐水洗性90次螨虫趋避率94%，柔韧性1mm，光泽度好；延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99%，可以广泛生产并不断代替现有材料。
以上实施例中的组合物所有组分均可以商业购买。
上述实施例只是用于对本发明的内容进行阐述，而不是限制，因此在与本发明的权利要求书相当的含义和范围内的任何改变，都应该认为是包括在权利要求书的范围内。
Claims (5)
1.一种刺绣用整理剂的制备方法，其特征在于，包括如下步骤：
第一步：按照重量份数配比称取蒸馏水100份、羧甲基纤维素钠10-50份、分散剂0.8-1.2份、橡胶大红0.5-4.5份、丝素5-25份、氧化铝10-30份、二甲基硅氧烷15-35份、氯化镁1-5份、磷酸钾2-6份、聚醚10-30份和盐酸1-5份；
第二步：将氧化铝、氯化镁和磷酸钾投入研磨机中研磨10-20min，在带有温度计、搅拌机和加热装置的反应釜中依次加入丝素、蒸馏水和羧甲基纤维素钠，打开搅拌机混合，升温至60-100℃，混合速度为400-600r/min，混合1-3h；
第三步：加入剩余原料，调节混合速度至1000-1200 r/min，混合6-10h，搅拌均匀，溶解完全后将混合均匀的产物投入砂磨机中，砂磨30-50min，过滤清液后，静置20-24h后即得。
2.根据权利要求1所述的刺绣用整理剂的制备方法，其特征在于：所述第一步中刺绣用整理剂的原料按重量份数配比如下：蒸馏水100份、羧甲基纤维素钠10份、分散剂0.8份、橡胶大红0.5份、丝素5份、氧化铝10份、二甲基硅氧烷15份、氯化镁1份、磷酸钾2份、聚醚10份和盐酸1份。
3.根据权利要求1所述的刺绣用整理剂的制备方法，其特征在于：所述第一步中刺绣用整理剂的原料按重量份数配比如下：蒸馏水100份、羧甲基纤维素钠50份、分散剂1.2份、橡胶大红4.5份、丝素25份、氧化铝30份、二甲基硅氧烷35份、氯化镁5份、磷酸钾6份、聚醚30份和盐酸5份。
4.根据权利要求1所述的刺绣用整理剂的制备方法，其特征在于：所述第一步中刺绣用整理剂的原料按重量份数配比如下：蒸馏水100份、羧甲基纤维素钠30份、分散剂1份、橡胶大红2.5份、丝素15份、氧化铝20份、二甲基硅氧烷25份、氯化镁3份、磷酸钾4份、聚醚20份和盐酸3份。
5.根据权利要求1所述的刺绣用整理剂的制备方法，其特征在于：所述分散剂采用甲基二萘磺酸钠。
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101070678A (zh) * | 2007-05-25 | 2007-11-14 | 上海赛博化工有限公司 | 一种吸湿速干排汗织物整理剂及其制备方法和用途 |
| CN102002854A (zh) * | 2010-12-06 | 2011-04-06 | 中原工学院 | 一种多功能织物整理剂及其制备方法和棉织物整理方法 |
| CN102220694A (zh) * | 2010-04-16 | 2011-10-19 | 香港纺织及成衣研发中心 | 用于织物多功能整理的组合物及使用其的织物多功能整理方法 |
-
2017
- 2017-11-30 CN CN201711239192.1A patent/CN107794758A/zh not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101070678A (zh) * | 2007-05-25 | 2007-11-14 | 上海赛博化工有限公司 | 一种吸湿速干排汗织物整理剂及其制备方法和用途 |
| CN102220694A (zh) * | 2010-04-16 | 2011-10-19 | 香港纺织及成衣研发中心 | 用于织物多功能整理的组合物及使用其的织物多功能整理方法 |
| CN102002854A (zh) * | 2010-12-06 | 2011-04-06 | 中原工学院 | 一种多功能织物整理剂及其制备方法和棉织物整理方法 |
Non-Patent Citations (2)
| Title |
|---|
| 中国香料香精化妆品工业协会编: "《化妆品原料规格实用手册》", 31 March 2002, 中国标准出版社 * |
| 张学铭等: "《化学小辞典》", 31 August 1994, 科学技术文献出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108691203A (zh) * | 2018-05-07 | 2018-10-23 | 贵州西江阿幼民族文化博物馆有限公司 | 一种刺绣用杀菌防虫整理剂的制备方法 |
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