CN107788019A - A kind of hygienic insecticide for being used to prevent and treat cockroach - Google Patents
A kind of hygienic insecticide for being used to prevent and treat cockroach Download PDFInfo
- Publication number
- CN107788019A CN107788019A CN201711240357.7A CN201711240357A CN107788019A CN 107788019 A CN107788019 A CN 107788019A CN 201711240357 A CN201711240357 A CN 201711240357A CN 107788019 A CN107788019 A CN 107788019A
- Authority
- CN
- China
- Prior art keywords
- ethiprole
- peppermint oil
- cockroach
- hygienic insecticide
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/002—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits
- A01N25/006—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits insecticidal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Food Science & Technology (AREA)
- Toxicology (AREA)
- Insects & Arthropods (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of hygienic insecticide for being used to prevent and treat cockroach, it is made up of the active ingredient and phagostimulant, excipient, preservative, NMF, the uniform mixture of water that are formed with ethiprole and peppermint oil, the weight ratio of ethiprole and peppermint oil is 3:1~1:5.It is high-efficiency low-toxicity of the present invention, safe and reliable, it can effectively control the cockroach in the indoor place such as residence, dining room, hotel, office to endanger.
Description
Technical field
The present invention relates to daily chemical product, hygienic insecticide, more particularly to a kind of hygienic biocide for being used to prevent and treat cockroach
Agent.
Background technology
Cockroach has become one of important sanitary insect pest at present, and it prevents and treats the great attention for having caused people.But due to
Long-term a large amount of to use chemical prevention, the common insecticide roach that goes out is ineffective.Ethiprole (fipronil) is used as most of Cockroach-killing drugs
The main component of agent, because of long-term single use, there are urban reflection cockroach resistance increase, the phenomenon that drug effect reduces.
Therefore the resistance of cockroach how is delayed, extend ethiprole is a reality and asking urgently as the life cycle of hygienic insecticide
Topic.
With reference to the characteristics of chemical prevention, compounded by using the composition of different mechanism of action, be to solve chemical pesticide resistance
One quick and simple approach of problem.Screened by formulation of pesticide, draw and mixed in certain ratio range between heterogeneity
With with synergistic function, it is possible to increase actual prevention effect, be the important means for administering pest and disease damage resistance.
Peppermint oil (Mentha arvensis oil) is colourless or flaxen supernatant liquid, has special aroma
Taste, main chemical compositions are terpenoid and its containing oxygen derivative, have antibiotic and sterilizing, anti-oxidant, rush infiltration, desinsection mosquito repellent
Antipruritic effect.
At present, related report is not shown in the research for ethiprole being used to prevent and treat to sanitary insect pest to peppermint oil mixture also.
The content of the invention
The technical problem to be solved in the present invention be to provide it is a kind of be used to preventing and treating the hygienic insecticide of cockroach, its high-efficiency low-toxicity,
Securely and reliably, the cockroach in the indoor place such as residence, dining room, hotel, office can be effectively controlled to endanger.
The present invention uses following technical scheme：A kind of hygienic insecticide for being used to prevent and treat cockroach, by with ethiprole and peppermint
The active ingredient and the uniform mixture of phagostimulant, excipient, preservative, NMF, water of oil composition are made, ethiprole and peppermint oil
Weight ratio is 3:1~1:5.
Preferably, the weight of ethiprole and peppermint oil ratio is 1:2.
Described hygienic insecticide, the percentage by weight of ethiprole is 0.02-0.1%, and the percentage by weight of peppermint oil is
0.02-0.2%.
Described phagostimulant is selected from one or more combinations of fish meal, cracker meal, analysis for soybean powder, corn flour, starch, white sugar.
One or more combinations of the excipient in guar gum, hydroxyethyl cellulose.
One or more combinations of the preservative in Nipagin complex esters, potassium sorbate, sodium benzoate.
One or more combinations of the NMF in glycerine, propane diols, polyethylene glycol.
Described hygienic insecticide prepares glue bait formulation common in any art, and compound method is：According to recipe requirements, divide
Also known as take active ingredient, phagostimulant, excipient, preservative, the weight of NMF.Excipient and NMF are thoroughly mixed
Scattered 30 minutes, addition water fully dissolves standby；Phagostimulant, preservative, active ingredient are put into the solution above prepared again
In, then stir, produce the cockroach-killing gel bait of the present invention.
Compared with prior art, the present invention possesses following technique effect：
(1) active ingredient of the invention is used with rational ratio range, and Synergistic is notable, can greatly improve medicine
Effect, pesticide cost is reduced, is advantageous to delay pest resistance to develop, extend Life Cycle of the ethiprole in health pest control field
Phase.
(2) palatability of the present invention is good, and allure is strong, safe, and outward appearance is fine and smooth, is unlikely to deteriorate and distributes unhappy gas
Taste.
Embodiment
Below in conjunction with embodiment, the present invention is further detailed explanation, and percentage of the present invention is
Percentage by weight.
First, embodiment is prepared
Embodiment 1：0.06% ethiprole peppermint oil cockroach-killing gel bait
Formula：Ethiprole 0.02%, peppermint oil 0.04%, Nipagin complex esters 0.2g, hydroxyethyl cellulose are weighed according to quantity
0.4%, glycerine 15.0%, starch 12.0%, white sugar 5.0%, water complements to 100%.
Embodiment 2：0.15% ethiprole peppermint oil cockroach-killing gel bait
Formula：Ethiprole 0.05%, peppermint oil 0.1%, potassium sorbate 0.2g, guar gum 0.5%, propane diols are weighed according to quantity
15.0%, fish meal 12.0%, white sugar 3.0%, water complements to 100%.
Embodiment 3：0.3% ethiprole peppermint oil cockroach-killing gel bait
Formula：Weigh ethiprole 0.1% according to quantity, peppermint oil 0.2%, sodium benzoate 0.5g, hydroxyethyl cellulose 0.5%,
Polyethylene glycol 10.0%, cracker meal 15.0%, white sugar 2.0%, water complements to 100%.
Embodiment 4：0.04% ethiprole peppermint oil cockroach-killing gel bait
Formula：Ethiprole 0.02%, peppermint oil 0.02%, Nipagin complex esters 0.2g, hydroxyethyl cellulose are weighed according to quantity
0.5%, glycerine 12.0%, analysis for soybean powder 10.0%, corn flour 5.0%, water complements to 100%.
The preparation method of the cockroach-killing gel bait of the present invention is as follows：According to the part by weight of above-mentioned each raw material, weigh respectively effectively
Composition, phagostimulant, excipient, preservative, the weight of NMF.Excipient and NMF are thoroughly mixed scattered 30 points
Clock, addition water fully dissolve standby；Phagostimulant, preservative, active ingredient are put into the solution above prepared again, then fully
Stir, produce the cockroach-killing gel bait of the present invention.
2nd, Toxicity Determination is tested
Embodiment 1：The indoor pharmacodynamic test of ethiprole, peppermint oil and its mixture to Groton bug
Experimental design：Indoor pharmacodynamic test, using stomach toxicity method, square box device.The valid density of each medicament is determined through prerun
After scope, ethiprole, peppermint oil and its mixture are pressed into 5 concentration of active constituent content gradient dilution as glue bait medicament to be measured.
120 Groton bugs are put into the square box device for being turned off door by putting worm channel, stoppers and puts worm channel.Treat that test worm recovers normal activity
Afterwards, glue bait medicament to be measured is placed respectively in case inner opposite angle line, center, which is placed, fills immersion cotton balls culture dish.Day by day it is dead to observe test worm
Situation is died, and dead test worm is taken out, numeration, the 12nd day after Continuous Observation to bait throwing in.If using chow diet raising as blank pair
According to.Each off-test, clean experimental rig.
Using the logarithm value of drug concentration (mg/kg) as independent variable x, using the probit value of corrected mortality as y, with DPS softwares
Calculate LC50And virulence regression equation, the co-toxicity coefficient (CTC) of each mixed ratio is obtained using Sun Yunpei method, and evaluate two
When the synergistic effect that person uses with, i.e. co-toxicity coefficient (CTC) >=120, hygienic insecticide shows as synergistic effect；As CTC≤80,
Hygienic insecticide shows as antagonism；As 80 ＜ CTC ＜ 120, hygienic insecticide shows as summation action.
3rd, result of the test is shown in Table 1.
The Toxicity Determination table of the ethiprole of table 1, peppermint oil and mixture to Groton bug
| Reagent agent | Proportioning | LD50(mg/kg) | Survey toxicity index | Theoretical toxicity index | Co-toxicity coefficient (CTC) |
| Ethiprole (A) | / | 0.73 | 488.04 | / | / |
| Peppermint oil (B) | / | 3.56 | 100.00 | / | / |
| A:B | 3:1 | 0.73 | 486.51 | 391.03 | 124.4 |
| A:B | 2:1 | 0.75 | 476.04 | 358.69 | 132.7 |
| A:B | 1:1 | 0.73 | 489.42 | 294.02 | 166.5 |
| A:B | 1:2 | 0.61 | 580.47 | 229.35 | 253.1 |
| A:B | 1:3 | 1.10 | 323.25 | 197.01 | 164.1 |
| A:B | 1:5 | 1.46 | 244.59 | 164.67 | 148.5 |
| A:B | 20:1 | 0.98 | 362.45 | 469.56 | 77.2 |
The joint toxicity measuring result of table 1 shows, ethiprole and peppermint oil are 3 in weight ratio:1~1:Mixture pair in the range of 5
The co-toxicity coefficient (CTC) of Groton bug is all higher than 120, has synergistic function；When the weight of ethiprole and peppermint oil ratio is
1:When 2, co-toxicity coefficient is maximum, is 253.1, synergy is more notable, there is good application value in the preventing and treating of sanitary insect pest.
3rd, field efficacy experiment is simulated
Embodiment 1：Preparation (0.06% ethiprole peppermint oil cockroach-killing gel bait) the preventing and treating Germany for preparing the gained of embodiment 1 is small
Lian simulation field efficacy experiment
Experimental design：Simulation sets cockroach to conceal place in scene.100 Groton bugs of the same size are discharged in simulation
In scene.After test worm recovers normal activity, to be measured kill diagonally is placed in the room for recommending dosage throughout to manage according to the present invention
In roach glue bait medicament and two culture dishes, the culture dish of cockroach feed is contained in another diagonal placement, is placed in parallel by each culture dish
One culture dish for filling immersion cotton balls.The method and weight of the launched cockroach-killing gel bait of each processing are consistent, close the doors and windows, and count
When.Check daily and record dead borer population, 12d after Continuous Observation to bait throwing in.
The medicament of the cockroach-killing gel bait respectively handled is as follows：
Handle 1#：Prepare the preparation of the gained of embodiment 1, i.e. 0.06% ethiprole peppermint oil cockroach-killing gel bait.
Handle 2#：0.06% ethiprole cockroach-killing gel bait.
Handle 3#：0.15% peppermint oil cockroach-killing gel bait.
Handle 4#：Blank control (CK), not delivering medicament.
Result of the test is shown in Table 2.
Table 2：Test of pesticide effectiveness statistical form of the 0.06% ethiprole peppermint oil cockroach-killing gel bait to Groton bug
From indoor harmacological effect result (table 2), tried according to GB/T 13917.7-2009 agriculture chemical registration with hygienic insecticide in
The test of pesticide effectiveness and evaluation criterion, 0.06% ethiprole peppermint oil cockroach-killing gel bait of the invention are to the indoor harmacological effect of Groton bug
A levels.The synergistic effect of two kinds of compositions of the invention simultaneously, help to reduce the dosage of chemical composition ethiprole.
Claims (7)
1. a kind of be used to prevent and treat the hygienic insecticide of cockroach, it is characterised in that by with ethiprole and peppermint oil form it is effective into
Divide and phagostimulant, excipient, preservative, NMF, the uniform mixture of water are made, the weight ratio of ethiprole and peppermint oil is 3:1~
1:5。
2. hygienic insecticide according to claim 1, it is characterised in that the weight of ethiprole and peppermint oil ratio is 1:2.
3. hygienic insecticide according to claim 1 or 2, it is characterised in that the percentage by weight of ethiprole is 0.02-
0.1%, the percentage by weight of peppermint oil is 0.02-0.2%.
4. hygienic insecticide according to claim 1, it is characterised in that described phagostimulant is selected from fish meal, cracker meal, Huang
One or more combinations of bean powder, corn flour, starch, white sugar.
5. hygienic insecticide according to claim 1, it is characterised in that it is fine that the excipient is selected from guar gum, ethoxy
One or more combinations in dimension element.
6. hygienic insecticide according to claim 1, it is characterised in that the preservative is selected from Nipagin complex esters, mountain
One or more combinations in potassium sorbate, sodium benzoate.
7. hygienic insecticide according to claim 1, it is characterised in that the NMF is selected from glycerine, propane diols, poly- second
One or more combinations in glycol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711240357.7A CN107788019A (en) | 2017-11-30 | 2017-11-30 | A kind of hygienic insecticide for being used to prevent and treat cockroach |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711240357.7A CN107788019A (en) | 2017-11-30 | 2017-11-30 | A kind of hygienic insecticide for being used to prevent and treat cockroach |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107788019A true CN107788019A (en) | 2018-03-13 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711240357.7A Pending CN107788019A (en) | 2017-11-30 | 2017-11-30 | A kind of hygienic insecticide for being used to prevent and treat cockroach |
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| Country | Link |
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| CN (1) | CN107788019A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115191433A (en) * | 2022-07-22 | 2022-10-18 | 中国人民解放军海军特色医学中心 | Application of functional additive in cockroach killing composition, cockroach killing composition and application of cockroach killing composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731202A (en) * | 2008-11-25 | 2010-06-16 | 李伟 | Method for processing and preparing granular fresh bait for killing cockroaches |
| CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
| CN104521950A (en) * | 2014-12-16 | 2015-04-22 | 广西科技大学 | Long-acting bait for killing cockroach and preparation method |
-
2017
- 2017-11-30 CN CN201711240357.7A patent/CN107788019A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731202A (en) * | 2008-11-25 | 2010-06-16 | 李伟 | Method for processing and preparing granular fresh bait for killing cockroaches |
| CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
| CN104521950A (en) * | 2014-12-16 | 2015-04-22 | 广西科技大学 | Long-acting bait for killing cockroach and preparation method |
Non-Patent Citations (1)
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| 王东等: "环境友好型卫生杀虫剂的研究进展", 《中国媒介生物学及控制杂志》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115191433A (en) * | 2022-07-22 | 2022-10-18 | 中国人民解放军海军特色医学中心 | Application of functional additive in cockroach killing composition, cockroach killing composition and application of cockroach killing composition |
| CN115191433B (en) * | 2022-07-22 | 2024-05-28 | 中国人民解放军海军特色医学中心 | Application of functional auxiliary agent in cockroach killing composition, cockroach killing composition and application thereof |
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