CN107996621A - A kind of composition for preventing cockroach - Google Patents
A kind of composition for preventing cockroach Download PDFInfo
- Publication number
- CN107996621A CN107996621A CN201711234226.8A CN201711234226A CN107996621A CN 107996621 A CN107996621 A CN 107996621A CN 201711234226 A CN201711234226 A CN 201711234226A CN 107996621 A CN107996621 A CN 107996621A
- Authority
- CN
- China
- Prior art keywords
- ethiprole
- eucalyptus oil
- cockroach
- composition according
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/002—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits
- A01N25/006—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits insecticidal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The present invention relates to a kind of composition for preventing cockroach, it is made of the active ingredient and phagostimulant, excipient, preservative, moisturizer, the uniform mixture of water that are formed with ethiprole and eucalyptus oil, the weight ratio of ethiprole and eucalyptus oil is 3:1~1:5.It is high-efficiency low-toxicity of the present invention, safe and reliable, it can effectively control the cockroach harm in the indoor place such as residence, dining room, hotel, office.
Description
Technical field
The present invention relates to daily chemical product, hygienic insecticide, more particularly to a kind of composition for preventing cockroach.
Background technology
Blattaria (being commonly called as cockroach) likes appearing in the place of human lives, and the health hazard to the mankind is serious, it takes everywhere
Eat, creeping spreads the disease, cockroach can also be from a kind of grease of special stench be secreted, in food and tableware and day in vivo in addition
Peculiar smell and multiple pathogens are left when creeping on common tool, it has also become maximum city pest.
At present, the prevention of cockroach is still based on chemical prevention, and ethiprole (fipronil) is used as most of Cockroach-killing drugs
The main component of agent, because of long-term single use, has there is urban reflection cockroach resistance increase, the phenomenon that drug effect reduces.
Therefore the resistance of cockroach how is delayed, extend ethiprole is a reality and asking urgently as the life cycle of hygienic insecticide
Topic.
With reference to the characteristics of chemical prevention, compounded by using the component of different mechanism of action, be to solve chemical pesticide resistance
One quick and simple approach of problem.Screened by formulation of pesticide, draw and mixed in certain ratio range between heterogeneity
With with synergistic function, it is possible to increase actual prevention effect, is the important means for administering pest and disease damage resistance.
Eucalyptus oil, English name：Oil of eucalyptus, are the fragrance essences that the oil droplet cell of eucalyptus leaves is secreted
Oil, has special aromatic odor, and main chemical compositions are terpenoid and its containing oxygen derivative, have antibiotic and sterilizing, resist
Oxidation, promote infiltration, the effect of desinsection mosquito-expelling and antipruritic.
At present, relevant report is not shown in the research for ethiprole and eucalyptus oil mixture being used to prevent to sanitary insect pest also.
The content of the invention
The technical problem to be solved in the present invention is, there is provided a kind of composition for preventing cockroach, its high-efficiency low-toxicity, safety can
Lean on, can effectively control the cockroach harm in the indoor place such as residence, dining room, hotel, office.
The present invention uses following technical scheme：A kind of composition for preventing cockroach, by what is formed with ethiprole and eucalyptus oil
Active ingredient and the uniform mixture of phagostimulant, excipient, preservative, moisturizer, water are made, and the weight ratio of ethiprole and eucalyptus oil is
3:1~1:5.
Preferably, the weight ratio of ethiprole and eucalyptus oil is 1:2.
The composition, the percentage by weight of ethiprole is 0.02-0.1%, and the percentage by weight of eucalyptus oil is 0.02-
0.2%.
The phagostimulant is selected from one or more combinations of fish meal, cracker meal, analysis for soybean powder, corn flour, starch, white sugar.
One or more combinations of the excipient in guar gum, hydroxyethyl cellulose.
One or more combinations of the preservative in Nipagin complex esters, potassium sorbate, sodium benzoate.
One or more combinations of the moisturizer in glycerine, propane diols, polyethylene glycol.
The composition prepares glue bait formulation common in any art, and preparation method is：According to recipe requirements, claim respectively
Take the weight of active ingredient, phagostimulant, excipient, preservative, moisturizer.Excipient and moisturizer are thoroughly mixed scattered
30 minutes, addition water fully dissolved spare；Phagostimulant, preservative, active ingredient are put into the solution above prepared again, then
Stir, up to the cockroach-killing gel bait of the present invention.
Compared with prior art, the present invention possesses following technique effect：
(1) active ingredient of the invention is used with rational ratio range, synergistic notable, can greatly improve medicine
Effect, reduces pesticide cost, is conducive to delay pest resistance to develop, and extends Life Cycle of the ethiprole in health pest control field
Phase.
(2) palatability of the present invention is good, and allure is strong, safe, and appearance is fine and smooth, is unlikely to deteriorate and distributes unhappy gas
Taste.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail, and percentage of the present invention is
Percentage by weight.
First, embodiment is prepared
Embodiment 1：0.06% ethiprole eucalyptus oil cockroach-killing gel bait
Formula：Ethiprole 0.02%, eucalyptus oil 0.04%, Nipagin complex esters 0.2g, hydroxyethyl cellulose are weighed according to quantity
0.4%, glycerine 15.0%, starch 12.0%, white sugar 5.0%, water complements to 100%.
Embodiment 2：0.15% ethiprole eucalyptus oil cockroach-killing gel bait
Formula：Ethiprole 0.05%, eucalyptus oil 0.1%, potassium sorbate 0.2g, guar gum 0.5%, propane diols are weighed according to quantity
15.0%, fish meal 12.0%, white sugar 3.0%, water complements to 100%.
Embodiment 3：0.3% ethiprole eucalyptus oil cockroach-killing gel bait
Formula：Weigh ethiprole 0.1% according to quantity, eucalyptus oil 0.2%, sodium benzoate 0.5g, hydroxyethyl cellulose 0.5%,
Polyethylene glycol 10.0%, cracker meal 15.0%, white sugar 2.0%, water complements to 100%.
Embodiment 4：0.04% ethiprole eucalyptus oil cockroach-killing gel bait
Formula：Ethiprole 0.02%, eucalyptus oil 0.02%, Nipagin complex esters 0.2g, hydroxyethyl cellulose are weighed according to quantity
0.5%, glycerine 12.0%, analysis for soybean powder 10.0%, corn flour 5.0%, water complements to 100%.
The preparation method of the cockroach-killing gel bait of the present invention is as follows：According to the part by weight of above-mentioned each raw material, weigh respectively effectively
Component, phagostimulant, excipient, preservative, the weight of moisturizer.Excipient and moisturizer are thoroughly mixed scattered 30 points
Clock, addition water fully dissolve spare；Phagostimulant, preservative, active ingredient are put into the solution above prepared again, then fully
Stir evenly, up to the cockroach-killing gel bait of the present invention.
2nd, Toxicity Determination is tested
Embodiment 1：The indoor pharmacodynamic test of ethiprole, eucalyptus oil and its mixture to Groton bug
Experimental design：Indoor pharmacodynamic test, using stomach toxicity method, square box device.The valid density of each medicament is determined through prerun
After scope, using ethiprole, eucalyptus oil and its mixture by 5 concentration of active constituent content gradient dilution as glue bait medicament to be measured.
120 Groton bugs are put into the square box device for being turned off door by putting worm channel, stoppers and puts worm channel.Treat that test worm recovers normal activity
Afterwards, diagonal places glue bait medicament to be measured respectively in the case, and center, which is placed, fills immersion cotton balls culture dish.Day by day it is dead to observe test worm
Situation is died, and dead test worm is taken out, numeration, is continuously observed to the 12nd day after bait throwing in.If using chow diet raising as blank pair
According to.Each off-test, cleans experimental rig.
Using drug concentration (mg/kg) to numerical value as independent variable x, using the probit value of corrected mortality as y, with DPS softwares
Calculate LC50And virulence regression equation, the co-toxicity coefficient (CTC) of each mixed ratio is obtained using the method for Sun Yunpei, and evaluate two
When the synergistic effect that person uses with, i.e. co-toxicity coefficient (CTC) >=120, composition shows as synergistic effect；As CTC≤80, combination
Thing shows as antagonism；As 80 ＜ CTC ＜ 120, composition shows as summation action.
3rd, result of the test is shown in Table 1.
The Toxicity Determination table of 1 ethiprole of table, eucalyptus oil and mixture to Groton bug
| Reagent agent | Proportioning | LD50(mg/kg) | Survey toxicity index | Theoretical toxicity index | Co-toxicity coefficient (CTC) |
| Ethiprole (A) | / | 0.82 | 430.37 | / | / |
| Eucalyptus oil (B) | / | 3.52 | 100.00 | / | / |
| A:B | 3:1 | 0.74 | 474.64 | 347.78 | 136.5 |
| A:B | 2:1 | 0.75 | 469.92 | 320.25 | 146.7 |
| A:B | 1:1 | 0.73 | 483.14 | 265.19 | 182.2 |
| A:B | 1:2 | 0.66 | 532.47 | 210.12 | 253.4 |
| A:B | 1:3 | 1.02 | 346.36 | 182.59 | 189.7 |
| A:B | 1:5 | 1.35 | 260.70 | 155.06 | 168.1 |
| A:B | 10:1 | 0.99 | 350.80 | 447.62 | 78.4 |
1 joint toxicity measuring of table the result shows that, ethiprole and eucalyptus oil are 3 in weight ratio:1~1:Mixture pair in the range of 5
The co-toxicity coefficient (CTC) of Groton bug is all higher than 120, has synergistic function；When the weight ratio of ethiprole and eucalyptus oil is
1:When 2, co-toxicity coefficient is maximum, is 253.4, synergy is more notable, there is good application value in the prevention of sanitary insect pest.
3rd, field efficacy experiment is simulated
Embodiment 1：Preparation (0.06% ethiprole eucalyptus oil cockroach-killing gel bait) the prevention Germany for preparing the gained of embodiment 1 is small
The simulation field efficacy experiment of Lian
Experimental design：Simulation sets cockroach to conceal place in scene.100 Groton bugs of the same size are discharged in simulation
In scene.After test worm recovers normal activity, to be measured kill diagonally is placed in the room for recommending dosage throughout to manage according to the present invention
In roach glue bait medicament and two culture dishes, the culture dish of cockroach feed is contained in another diagonal placement, is placed in parallel by each culture dish
One culture dish for filling immersion cotton balls.The method and weight of the launched cockroach-killing gel bait of each processing are consistent, close the doors and windows, and count
When.Check daily and record dead borer population, continuous observation to 12d after bait throwing in.
The medicament of the cockroach-killing gel bait respectively handled is as follows：
Handle 1#：Prepare the preparation of the gained of embodiment 1, i.e. 0.06% ethiprole eucalyptus oil cockroach-killing gel bait.
Handle 2#：0.06% ethiprole cockroach-killing gel bait.
Handle 3#：0.15% eucalyptus oil cockroach-killing gel bait.
Handle 4#：Blank control (CK), not delivering medicament.
Result of the test is shown in Table 2.
Table 2：Test of pesticide effectiveness statistical form of the 0.06% ethiprole eucalyptus oil cockroach-killing gel bait to Groton bug
From indoor harmacological effect result (table 2), tried according to the agriculture chemical registration of GB/T 13917.7-2009 with hygienic insecticide in
The test of pesticide effectiveness and evaluation criterion, 0.06% ethiprole eucalyptus oil cockroach-killing gel bait of the invention are to the indoor harmacological effect of Groton bug
A grades.The synergistic effect of two kinds of components of the invention at the same time, helps to reduce the dosage of chemical composition ethiprole.
Claims (7)
1. a kind of composition for preventing cockroach, it is characterised in that by the active ingredient and food calling formed with ethiprole and eucalyptus oil
Agent, excipient, preservative, moisturizer, the uniform mixture of water are made, and the weight ratio of ethiprole and eucalyptus oil is 3:1~1:5.
2. composition according to claim 1, it is characterised in that the weight ratio of ethiprole and eucalyptus oil is 1:2.
3. composition according to claim 1 or 2, it is characterised in that the percentage by weight of ethiprole is 0.02-0.1%,
The percentage by weight of eucalyptus oil is 0.02-0.2%.
4. composition according to claim 1, it is characterised in that the phagostimulant is selected from fish meal, cracker meal, soya bean
One or more combinations of powder, corn flour, starch, white sugar.
5. composition according to claim 1, it is characterised in that the excipient is selected from guar gum, hydroxyethyl cellulose
In one or more combinations.
6. composition according to claim 1, it is characterised in that the preservative is selected from Nipagin complex esters, sorbic acid
One or more combinations in potassium, sodium benzoate.
7. composition according to claim 1, it is characterised in that the moisturizer is selected from glycerine, propane diols, polyethylene glycol
In one or more combinations.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711234226.8A CN107996621A (en) | 2017-11-30 | 2017-11-30 | A kind of composition for preventing cockroach |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711234226.8A CN107996621A (en) | 2017-11-30 | 2017-11-30 | A kind of composition for preventing cockroach |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107996621A true CN107996621A (en) | 2018-05-08 |
Family
ID=62055185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711234226.8A Pending CN107996621A (en) | 2017-11-30 | 2017-11-30 | A kind of composition for preventing cockroach |
Country Status (1)
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102834471A (en) * | 2009-10-15 | 2012-12-19 | 玛丽亚·皮拉尔·马特奥·埃雷罗 | Insecticide and acaricide paints that inhibit chitin synthesis, regulate insect juvenile hormone and repel arthropods, for controlling endemic diseases, pests and allergens |
| CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
| CN103503927A (en) * | 2013-10-17 | 2014-01-15 | 太仓欧锐智能化工程有限公司 | Cockroach bait agent and preparation method thereof |
| CN104521950A (en) * | 2014-12-16 | 2015-04-22 | 广西科技大学 | Long-acting bait for killing cockroach and preparation method |
| CN105688168A (en) * | 2016-03-19 | 2016-06-22 | 上海申亚动物保健品阜阳有限公司 | Pet all-in-one insect expelling spray and preparation method thereof |
-
2017
- 2017-11-30 CN CN201711234226.8A patent/CN107996621A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102834471A (en) * | 2009-10-15 | 2012-12-19 | 玛丽亚·皮拉尔·马特奥·埃雷罗 | Insecticide and acaricide paints that inhibit chitin synthesis, regulate insect juvenile hormone and repel arthropods, for controlling endemic diseases, pests and allergens |
| CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
| CN103503927A (en) * | 2013-10-17 | 2014-01-15 | 太仓欧锐智能化工程有限公司 | Cockroach bait agent and preparation method thereof |
| CN104521950A (en) * | 2014-12-16 | 2015-04-22 | 广西科技大学 | Long-acting bait for killing cockroach and preparation method |
| CN105688168A (en) * | 2016-03-19 | 2016-06-22 | 上海申亚动物保健品阜阳有限公司 | Pet all-in-one insect expelling spray and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 陈默等: "桉叶油的化学成分及其生物活性研究进展", 《中国现代医学杂志》 * |
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