CN107723081A - 液压支架用乳化油及其制备方法 - Google Patents

液压支架用乳化油及其制备方法 Download PDF

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CN107723081A
CN107723081A CN201710918317.7A CN201710918317A CN107723081A CN 107723081 A CN107723081 A CN 107723081A CN 201710918317 A CN201710918317 A CN 201710918317A CN 107723081 A CN107723081 A CN 107723081A
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hydraulic support
support oil
oil emulsion
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冯妍梅
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XINJIANG MODERN PETROCHEMICAL INDUSTRY CO LTD
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Abstract

本发明涉及乳化油技术领域，是一种液压支架用乳化油及其制备方法；该液压支架用乳化油原料按质量百分含量包括甘油50%至80%、乙二醇8%至30%、乳化剂10%至20%、防锈剂0.1%至0.3%、抗泡剂0.01%至0.05%、极压润滑剂0.1%至0.5%、防腐防霉杀菌剂0.1%至0.3% 、其余为水。本发明液压支架用乳化油较现有液压支架油的稳定性好，且本发明液压支架用乳化油与现有液压支架油的润滑性能相当；同时，本发明液压支架用乳化油较现有液压支架油的生产成本降低15%至20%，大大降低了生产成本。

Description

液压支架用乳化油及其制备方法
技术领域
本发明涉及乳化油技术领域，是一种液压支架用乳化油及其制备方法。
背景技术
现市场常用的液压支架油是皂化乳化油，用井水稀释后与矿物元素发生反应；但现市场常用的液压支架油稳定性差，在70±2℃下检测，24h后出现分层，产生絮状物现象，且有油皂析出；为了解决此问题，通常的做法是加大表面活性剂的加量，加抗硬水剂，但由于表面活性剂价格比较高，从而大大提高了液压支架油的生产成本。
发明内容
本发明提供了一种液压支架用乳化油及其制备方法，克服了上述现有技术之不足，其能有效解决现有液压支架油稳定性差，在70±2℃下检测24h后出现分层、产生絮状物现象、有油皂析出和生产成本高的问题。
本发明的技术方案之一是通过以下措施来实现的：一种液压支架用乳化油，原料按质量百分含量包括甘油50%至80%、乙二醇8%至30%、乳化剂10%至20%、防锈剂0.1%至0.3%、抗泡剂0.01%至0.05%、极压润滑剂0.1%至0.5%、防腐防霉杀菌剂0.1%至0.3% 、其余为水。
下面是对上述发明技术方案之一的进一步优化或/和改进：
上述液压支架用乳化油按下述方法得到：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油。
上述防腐防霉杀菌剂为水性防腐剂卡松或羧酸胺盐。
上述极压润滑剂为硼酸脂或油酸三乙醇胺；或/和，抗泡剂为聚醚或有机硅。
上述防锈剂为聚羧酸盐类或脂肪酸盐或脂肪酸脂；或/和，乳化剂为非离子水性表面活性剂。
本发明的技术方案之二是通过以下措施来实现的：一种液压支架用乳化油的制备方法，按下述方法进行：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油。
下面是对上述发明技术方案之二的进一步优化或/和改进：
上述防腐防霉杀菌剂为水性防腐剂卡松或羧酸胺盐。
上述极压润滑剂为硼酸脂或油酸三乙醇胺；或/和，抗泡剂为聚醚或有机硅。
上述防锈剂为聚羧酸盐类或脂肪酸盐或脂肪酸脂；或/和，乳化剂为非离子水性表面活性剂。
本发明液压支架用乳化油较现有液压支架油的稳定性好，且本发明液压支架用乳化油与现有液压支架油的润滑性能相当；同时，本发明液压支架用乳化油较现有液压支架油的生产成本降低15%至20%，大大降低了生产成本。
具体实施方式
本发明不受下述实施例的限制，可根据本发明的技术方案与实际情况来确定具体的实施方式。
实施例1，该液压支架用乳化油原料按质量百分含量包括甘油50%至80%、乙二醇8%至30%、乳化剂10%至20%、防锈剂0.1%至0.3%、抗泡剂0.01%至0.05%、极压润滑剂0.1%至0.5%、防腐防霉杀菌剂0.1%至0.3% 、其余为水。
实施例2，该液压支架用乳化油原料按质量百分含量包括甘油50%或80%、乙二醇8%或30%、乳化剂10% 或20%、防锈剂0.1%或 0.3%、抗泡剂0.01% 或0.05%、极压润滑剂0.1% 或0.5%、防腐防霉杀菌剂0.1% 或0.3% 、其余为水。
实施例3，该液压支架用乳化油按下述方法得到：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油。
实施例4，该液压支架用乳化油按下述方法得到：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油；原料按质量百分含量包括甘油60%、乙二醇14.5%、乳化剂17.6%、防锈剂0.3%、抗泡剂0.05%、极压润滑剂0.5%、防腐防霉杀菌剂0.3%、水6.75%。
实施例5，该液压支架用乳化油按下述方法得到：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油；原料按质量百分含量包括甘油50%、乙二醇14.6%、乳化剂15%、防锈剂0.3%、抗泡剂0.05%、极压润滑剂0.5%、防腐防霉杀菌剂0.3%、水19.25%。
实施例6，该液压支架用乳化油按下述方法得到：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油；原料按质量百分含量包括甘油50%、乙二醇10%、乳化剂12%、防锈剂0.3%、抗泡剂0.03%、极压润滑剂0.5%、防腐防霉杀菌剂0.3%、水26.87%。
实施例7，作为上述实施例的优化，防腐防霉杀菌剂为水性防腐剂卡松或羧酸胺盐。
实施例8，作为上述实施例的优化，极压润滑剂为硼酸脂或油酸三乙醇胺；或/和，抗泡剂为聚醚或有机硅。
实施例9，作为上述实施例的优化，防锈剂为聚羧酸盐类或脂肪酸盐或脂肪酸脂；或/和，乳化剂为非离子水性表面活性剂。
稳定性测定：
将实施例4、实施例5和实施例6得到的液压支架用乳化油在（70±2℃）下检测结果见表1所示；从表1可以看出，实施例4、实施例5和实施例6得到的液压支架用乳化油在（70±2℃）下168h无分层、无絮状物和无油皂析出，在水中均匀分散，无不良的刺激性气味；说明本发明液压支架用乳化油较现有液压支架油的稳定性好，且本发明液压支架用乳化油与现有液压支架油的润滑性能相当。
综上所述，本发明液压支架用乳化油较现有液压支架油的稳定性好，且本发明液压支架用乳化油与现有液压支架油的润滑性能相当；同时，本发明液压支架用乳化油较现有液压支架油的生产成本降低15%至20%，大大降低了生产成本。
以上技术特征构成了本发明的实施例，其具有较强的适应性和实施效果，可根据实际需要增减非必要的技术特征，来满足不同情况的需求。

Claims (9)

1.一种液压支架用乳化油，其特征在于原料按质量百分含量包括甘油50%至80%、乙二醇8%至30%、乳化剂10%至20%、防锈剂0.1%至0.3%、抗泡剂0.01%至0.05%、极压润滑剂0.1%至0.5%、防腐防霉杀菌剂0.1%至0.3% 、其余为水。
2.根据权利要求1所述的液压支架用乳化油，其特征在于按下述方法得到：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油。
3.根据权利要求1或2所述的液压支架用乳化油，其特征在于防腐防霉杀菌剂为水性防腐剂卡松或羧酸胺盐。
4.根据权利要求1或2或3所述的液压支架用乳化油，其特征在于极压润滑剂为硼酸脂或油酸三乙醇胺；或/和，抗泡剂为聚醚或有机硅。
5.根据权利要求1或2或3或4所述的液压支架用乳化油，其特征在于防锈剂为聚羧酸盐类或脂肪酸盐或脂肪酸脂；或/和，乳化剂为非离子水性表面活性剂。
6.一种根据权利要求1所述的液压支架用乳化油的制备方法，其特征在于按下述方法进行：在所需量的甘油中依次加入所需量的乳化剂、水、乙二醇、防腐防霉杀菌剂、极压润滑剂、防锈剂和抗泡剂，混合均匀后得到液压支架用乳化油。
7.根据权利要求6所述的液压支架用乳化油的制备方法，其特征在于防腐防霉杀菌剂为水性防腐剂卡松或羧酸胺盐。
8.根据权利要求6或7所述的液压支架用乳化油的制备方法，其特征在于极压润滑剂为硼酸脂或油酸三乙醇胺；或/和，抗泡剂为聚醚或有机硅。
9.根据权利要求6或7或8所述的液压支架用乳化油的制备方法，其特征在于极压润滑剂为硼酸脂或油酸三乙醇胺；或/和，抗泡剂为聚醚或有机硅。
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