CN107687993B - 通过光衍射来表征悬浮于流体分散剂中的颗粒的方法 - Google Patents
通过光衍射来表征悬浮于流体分散剂中的颗粒的方法 Download PDFInfo
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- CN107687993B CN107687993B CN201710655133.6A CN201710655133A CN107687993B CN 107687993 B CN107687993 B CN 107687993B CN 201710655133 A CN201710655133 A CN 201710655133A CN 107687993 B CN107687993 B CN 107687993B
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- 239000002245 particle Substances 0.000 title claims abstract description 57
- 239000002270 dispersing agent Substances 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 30
- 239000012530 fluid Substances 0.000 title claims abstract description 6
- 238000005259 measurement Methods 0.000 claims abstract description 74
- 238000005286 illumination Methods 0.000 claims abstract description 50
- 238000012545 processing Methods 0.000 claims abstract description 9
- 238000000926 separation method Methods 0.000 claims description 4
- 230000008859 change Effects 0.000 claims description 3
- 238000002474 experimental method Methods 0.000 claims description 2
- 238000009499 grossing Methods 0.000 description 5
- 238000011192 particle characterization Methods 0.000 description 5
- 230000002123 temporal effect Effects 0.000 description 5
- 238000012544 monitoring process Methods 0.000 description 4
- 239000000356 contaminant Substances 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000002296 dynamic light scattering Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 238000001370 static light scattering Methods 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 238000003491 array Methods 0.000 description 1
- 238000004422 calculation algorithm Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000013178 mathematical model Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
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- 238000012800 visualization Methods 0.000 description 1
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Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/02—Investigating particle size or size distribution
- G01N15/0205—Investigating particle size or size distribution by optical means
- G01N15/0211—Investigating a scatter or diffraction pattern
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/47—Scattering, i.e. diffuse reflection
- G01N21/49—Scattering, i.e. diffuse reflection within a body or fluid
- G01N21/53—Scattering, i.e. diffuse reflection within a body or fluid within a flowing fluid, e.g. smoke
- G01N21/532—Scattering, i.e. diffuse reflection within a body or fluid within a flowing fluid, e.g. smoke with measurement of scattering and transmission
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/02—Investigating particle size or size distribution
- G01N15/0205—Investigating particle size or size distribution by optical means
- G01N15/0211—Investigating a scatter or diffraction pattern
- G01N2015/0222—Investigating a scatter or diffraction pattern from dynamic light scattering, e.g. photon correlation spectroscopy
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/47—Scattering, i.e. diffuse reflection
- G01N2021/4704—Angular selective
- G01N2021/4711—Multiangle measurement
- G01N2021/4716—Using a ring of sensors, or a combination of diaphragm and sensors; Annular sensor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/47—Scattering, i.e. diffuse reflection
- G01N2021/4704—Angular selective
- G01N2021/4711—Multiangle measurement
- G01N2021/4721—Multiangle measurement using a PSD
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Dispersion Chemistry (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP16182896.7A EP3279635B1 (en) | 2016-08-04 | 2016-08-04 | Method, processor and machine-readable, non-transient storage medium for characterising particles suspended in a fluid dispersant |
| EP16182896.7 | 2016-08-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107687993A CN107687993A (zh) | 2018-02-13 |
| CN107687993B true CN107687993B (zh) | 2022-11-22 |
Family
ID=56683745
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710655133.6A Active CN107687993B (zh) | 2016-08-04 | 2017-08-03 | 通过光衍射来表征悬浮于流体分散剂中的颗粒的方法 |
Country Status (4)
| Country | Link |
|---|---|
| US (2) | US10422734B2 (enExample) |
| EP (2) | EP3279635B1 (enExample) |
| JP (1) | JP7058478B2 (enExample) |
| CN (1) | CN107687993B (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3279635B1 (en) * | 2016-08-04 | 2022-06-01 | Malvern Panalytical Limited | Method, processor and machine-readable, non-transient storage medium for characterising particles suspended in a fluid dispersant |
| WO2020011949A1 (en) * | 2018-07-13 | 2020-01-16 | Adolphe Merkle Institut, University Of Fribourg | Devices and methods for analyzing and filtering light scattering data from a sample potentially containing a non-target compound |
| EP4312016A1 (en) | 2022-07-25 | 2024-01-31 | Malvern Panalytical Limited | Data quality |
Citations (9)
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| US5416580A (en) * | 1993-07-07 | 1995-05-16 | General Signal Corporation | Methods and apparatus for determining small particle size distribution utilizing multiple light beams |
| US5621523A (en) * | 1992-08-27 | 1997-04-15 | Kowa Company Ltd. | Method and apparatus for measuring particles in a fluid |
| GB2340936A (en) * | 1998-08-22 | 2000-03-01 | Malvern Instr Ltd | Particle size distribution measurement using dual sources of different wavelengths |
| CN101072997A (zh) * | 2003-08-14 | 2007-11-14 | 塞通诺米公司 | 用于粒子分类系统的光学检测器 |
| CN101118210A (zh) * | 2006-08-04 | 2008-02-06 | 株式会社岛津制作所 | 光散射检测器 |
| CN102109454A (zh) * | 2011-03-17 | 2011-06-29 | 上海理工大学 | 同时测量多颗粒的动态光散射纳米颗粒粒度的装置及方法 |
| CN104067105A (zh) * | 2011-09-14 | 2014-09-24 | 马尔文仪器有限公司 | 用于通过光散射测量颗粒尺寸分布的设备和方法 |
| CN104568683A (zh) * | 2014-12-25 | 2015-04-29 | 上海理工大学 | 一种纳米颗粒粒度测量装置及方法 |
| CN105492887A (zh) * | 2013-03-15 | 2016-04-13 | 理查德·哈理·特纳 | 用于体液中的颗粒和可溶性化学实体的体外检测的系统和方法 |
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| US3966332A (en) * | 1974-09-12 | 1976-06-29 | Schering Corporation | Method and apparatus for inspecting liquids in transparent containers |
| US3941479A (en) * | 1974-09-26 | 1976-03-02 | G. D. Searle & Co. | Use of modulated stimulus to improve detection sensitivity for signals from particles in a flow chamber |
| GB2040443B (en) * | 1978-12-07 | 1983-01-12 | English Electric Co Ltd | Optical particle size analyser |
| US4263508A (en) * | 1979-04-20 | 1981-04-21 | Research Corporation | Pulse edge measurement for determining particle dimensional characteristics |
| US4385830A (en) * | 1980-11-26 | 1983-05-31 | Cornell Research Foundation, Inc. | Direct measurement of vorticity by optical probe |
| JPS6238345A (ja) * | 1985-08-14 | 1987-02-19 | Hitachi Ltd | 固形粒子の分析方法及び装置 |
| JPH0786455B2 (ja) * | 1986-07-18 | 1995-09-20 | 興和株式会社 | 粒子測定方法及び装置 |
| JP2635992B2 (ja) * | 1988-03-24 | 1997-07-30 | 興和株式会社 | 微粒子測定装置 |
| US5104221A (en) * | 1989-03-03 | 1992-04-14 | Coulter Electronics Of New England, Inc. | Particle size analysis utilizing polarization intensity differential scattering |
| US4953978A (en) | 1989-03-03 | 1990-09-04 | Coulter Electronics Of New England, Inc. | Particle size analysis utilizing polarization intensity differential scattering |
| US4984889A (en) * | 1989-03-10 | 1991-01-15 | Pacific Scientific Company | Particle size measuring system with coincidence detection |
| AU655216B2 (en) * | 1990-11-28 | 1994-12-08 | Ge Aviation Uk | System and method for monitoring debris in a fluid |
| US5133602A (en) * | 1991-04-08 | 1992-07-28 | International Business Machines Corporation | Particle path determination system |
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| GB9818351D0 (en) | 1998-08-22 | 1998-10-14 | Malvern Instr Ltd | Improvements relating to the measurement of particle size distribution |
| DE69938992D1 (de) * | 1998-09-29 | 2008-08-14 | Horiba Ltd | Vorrichtung und Verfahren zur Messung der Teilchengrössenverteilung |
| US6519033B1 (en) * | 2001-11-19 | 2003-02-11 | Point Source Technologies, Llc | Identification of particles in fluid |
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| EP3279635B1 (en) * | 2016-08-04 | 2022-06-01 | Malvern Panalytical Limited | Method, processor and machine-readable, non-transient storage medium for characterising particles suspended in a fluid dispersant |
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-
2016
- 2016-08-04 EP EP16182896.7A patent/EP3279635B1/en active Active
- 2016-08-04 EP EP22169348.4A patent/EP4050322B1/en active Active
-
2017
- 2017-08-03 CN CN201710655133.6A patent/CN107687993B/zh active Active
- 2017-08-03 US US15/668,552 patent/US10422734B2/en active Active
- 2017-08-04 JP JP2017151926A patent/JP7058478B2/ja active Active
-
2019
- 2019-06-13 US US16/440,208 patent/US11187639B2/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5621523A (en) * | 1992-08-27 | 1997-04-15 | Kowa Company Ltd. | Method and apparatus for measuring particles in a fluid |
| US5416580A (en) * | 1993-07-07 | 1995-05-16 | General Signal Corporation | Methods and apparatus for determining small particle size distribution utilizing multiple light beams |
| GB2340936A (en) * | 1998-08-22 | 2000-03-01 | Malvern Instr Ltd | Particle size distribution measurement using dual sources of different wavelengths |
| CN101072997A (zh) * | 2003-08-14 | 2007-11-14 | 塞通诺米公司 | 用于粒子分类系统的光学检测器 |
| CN101118210A (zh) * | 2006-08-04 | 2008-02-06 | 株式会社岛津制作所 | 光散射检测器 |
| CN102109454A (zh) * | 2011-03-17 | 2011-06-29 | 上海理工大学 | 同时测量多颗粒的动态光散射纳米颗粒粒度的装置及方法 |
| CN104067105A (zh) * | 2011-09-14 | 2014-09-24 | 马尔文仪器有限公司 | 用于通过光散射测量颗粒尺寸分布的设备和方法 |
| CN105492887A (zh) * | 2013-03-15 | 2016-04-13 | 理查德·哈理·特纳 | 用于体液中的颗粒和可溶性化学实体的体外检测的系统和方法 |
| CN104568683A (zh) * | 2014-12-25 | 2015-04-29 | 上海理工大学 | 一种纳米颗粒粒度测量装置及方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP4050322B1 (en) | 2024-05-29 |
| EP4050322A1 (en) | 2022-08-31 |
| EP3279635B1 (en) | 2022-06-01 |
| US20180038782A1 (en) | 2018-02-08 |
| JP7058478B2 (ja) | 2022-04-22 |
| CN107687993A (zh) | 2018-02-13 |
| EP3279635A1 (en) | 2018-02-07 |
| US11187639B2 (en) | 2021-11-30 |
| US10422734B2 (en) | 2019-09-24 |
| JP2018059905A (ja) | 2018-04-12 |
| US20190383718A1 (en) | 2019-12-19 |
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