CN107653032A - 一种环保型润滑脂及其制备方法 - Google Patents

一种环保型润滑脂及其制备方法 Download PDF

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CN107653032A
CN107653032A CN201610597290.1A CN201610597290A CN107653032A CN 107653032 A CN107653032 A CN 107653032A CN 201610597290 A CN201610597290 A CN 201610597290A CN 107653032 A CN107653032 A CN 107653032A
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lubricating grease
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周丽
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
    • C10M2207/044—Cyclic ethers having four or more ring atoms, e.g. furans, dioxolanes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
    • C10M2207/123—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms polycarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C10M2229/0415—Siloxanes with specific structure containing aliphatic substituents used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08—Resistance to extreme temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/02—Bearings
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

本发明公开了一种环保型润滑脂及其制备方法，该润滑脂包括：乙基硅油基础油70‑130份、磺酸镁40‑60份、丙二酸35‑51份、四氢呋喃49‑72份及焦磷酸二三聚氰胺18‑36份；其制法为将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在25～50℃下搅拌混合1‑10h，利用三辊机研磨均化0.5‑3h使之均匀，即可。优点为该环保型润滑脂具有良好的氧化安定性、耐高温和极压抗磨性，能够用作高速轴承的润滑脂；同时，本发明的制备工艺简单，无需复杂的合成设备，降低了生产成本，并减轻了对环境的负荷。

Description

一种环保型润滑脂及其制备方法
技术领域
本发明属于润滑脂领域，尤其涉及一种环保型润滑脂及其制备方法。
背景技术
润滑脂是工业润滑剂的重要组成部分，由于其本身固有的优良性能，不仅能满足一般的润滑要求，而且还具有良好的极压、抗磨和密封性能。广泛应用于钢铁、汽车、航空航天和军事等工业。
发明内容
发明目的：本发明的第一目的是提供一种具有良好的氧化安定性、耐高温性能和极压抗磨性的环保型润滑脂；
本发明的第二目的是提供该润滑脂的制备方法。
技术方案：本发明的环保型润滑脂，按重量份数计包括如下原料：乙基硅油基础油70-130份、磺酸镁40-60份、丙二酸35-51份、四氢呋喃49-72份及焦磷酸二三聚氰胺18-36份。优选的，乙基硅油基础油90-120份；磺酸镁45-55份；丙二酸40-50份；四氢呋喃55-65份。
本发明制备环保型润滑脂的方法，包括如下步骤：将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在25～50℃下搅拌混合1-10h，利用三辊机研磨均化0.5-3h使之均匀，即可。
有益效果：与现有技术相比，本发明的显著优点为：该环保型润滑脂具有良好的氧化安定性、耐高温性能和极压抗磨性，能够用作高速轴承的润滑脂；同时，本发明的制备工艺简单，无需复杂的合成设备，降低了生产成本，并减轻了对环境的负荷。
具体实施方式
实施例1
原料：乙基硅油基础油90份、磺酸镁45份、丙二酸40份、四氢呋喃55份及焦磷酸二三聚氰胺18份。
制备方法：将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在25℃下搅拌混合10h，利用三辊机研磨均化0.5h使之均匀，即可。
实施例2
原料：乙基硅油基础油120份、磺酸镁55份、丙二酸50份、四氢呋喃65份及焦磷酸二三聚氰胺36份。
制备方法：将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在50℃下搅拌混合1h，利用三辊机研磨均化3h使之均匀，即可。
实施例3
原料：乙基硅油基础油130份、磺酸镁60份、丙二酸51份、四氢呋喃72份及焦磷酸二三聚氰胺36份。
制备方法：将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在25℃下搅拌混合10h，利用三辊机研磨均化0.5h使之均匀，即可。
实施例4
原料：乙基硅油基础油70份、磺酸镁40份、丙二酸35份、四氢呋喃49份及焦磷酸二三聚氰胺18份。
制备方法：将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在50℃下搅拌混合1h，利用三辊机研磨均化3h使之均匀，即可。

Claims (6)

1.一种环保型润滑脂，其特征在于按重量份数计包括如下原料：乙基硅油基础油70-130份、磺酸镁40-60份、丙二酸35-51份、四氢呋喃49-72份及焦磷酸二三聚氰胺18-36份。
2.根据权利要求1所述的环保型润滑脂，其特征在于：所述乙基硅油基础油90-120份。
3.根据权利要求1所述的环保型润滑脂，其特征在于：所述磺酸镁45-55份。
4.根据权利要求1所述的环保型润滑脂，其特征在于：所述丙二酸40-50份。
5.根据权利要求1所述的环保型润滑脂，其特征在于：所述四氢呋喃55-65份。
6.一种制备权利要求1所述环保型润滑脂的方法，其特征在于包括如下步骤：将乙基硅油基础油、磺酸镁、丙二酸、四氢呋喃及焦磷酸二三聚氰胺在25～50℃下搅拌混合1-10h，利用三辊机研磨均化0.5-3h使之均匀，即可。
CN201610597290.1A 2016-07-26 2016-07-26 一种环保型润滑脂及其制备方法 Pending CN107653032A (zh)

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Application publication date: 20180202