CN107629874A - A kind of cinnamomum camphora Verbena officinalis essential oil - Google Patents

A kind of cinnamomum camphora Verbena officinalis essential oil Download PDF

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Publication number
CN107629874A
CN107629874A CN201710933906.2A CN201710933906A CN107629874A CN 107629874 A CN107629874 A CN 107629874A CN 201710933906 A CN201710933906 A CN 201710933906A CN 107629874 A CN107629874 A CN 107629874A
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China
Prior art keywords
parts
cinnamomum camphora
verbena officinalis
essential oil
extract
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Pending
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CN201710933906.2A
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Chinese (zh)
Inventor
梁珑膑
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Guangdong Changli Flavor Co
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Guangdong Changli Flavor Co
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Priority to CN201710933906.2A priority Critical patent/CN107629874A/en
Publication of CN107629874A publication Critical patent/CN107629874A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of cinnamomum camphora Verbena officinalis essential oil, belong to spices manufacture field.The cinnamomum camphora Verbena officinalis essential oil of the present invention includes following raw material in units of parts by weight:12 ~ 35 parts of cinnamomum camphora extract, 10 ~ 30 parts of Herba Verbenae, 5 ~ 25 parts of tea tree extract, 20 ~ 45 parts of Sweet Almond Oil, 40 ~ 110 parts of wheat-germ oil, 5 ~ 15 parts of sandalwood oil, 60 ~ 100 parts of ethanol, 50 ~ 100 parts of glycerine.The cinnamomum camphora Verbena officinalis essential oil that inventive formulation and processing method are prepared into, there is cinnamomum camphora, Verbena officinalis, the fragrance of tea tree, the main aromatic components that cedarwood is adjusted after asing, release is slow, and fragrant atmosphere is lasting, with calm the nerves, be quiet, according to one's conscience the effect of.

Description

A kind of cinnamomum camphora Verbena officinalis essential oil
Technical field
The invention belongs to spices manufacture field, and in particular to a kind of cinnamomum camphora Verbena officinalis essential oil.
Background technology
Cinnamomum camphora, cinnamomum camphora are Laurales, Lauraceae, the evergreen megaphanerophyte of Cinnamomum, high up to 30 meters, and diameter is up to 3 meters, the wide ovum of tree crown Shape;Tree crown is extensively opened up, and is thick with leaves, spectacular, is excellent greening-tree, shade tree and shade tree.Produce southern china and southwest Each provinces and regions.Vietnam, Korea, Japan are also distributed, and often there is introducing and planting other various countries.Plant entirety has camphor fragrance, can carry Camphor processed and extraction camphor oil.
Verbena officinalis(Classification system:Verbena officinalis L.), perennial vertical herbage plant, height is up to 120 Centimetre, base portion lignifying, single leaf is avette to long avette to life, two sides by bristle, below Mao Youmi on arteries and veins.Basidixed or axillary Spike, flower bluish violet, stockless, calyx film quality, tubular, micro- corolla is in two lips, and filigree is extremely short;Ovary is hairless, fruit bag It is hidden in calyx, pyrene.The flowering fruit bearing stage 6-10 months.
The content of the invention
The invention provides it is a kind of have containing cinnamomum camphora, Verbena officinalis, tea tree extract essential oil.
The present invention uses following technical scheme:A kind of cinnamomum camphora Verbena officinalis essential oil, in units of parts by weight, include following original Material:It is 12 ~ 35 parts of cinnamomum camphora extract, 10 ~ 30 parts of Herba Verbenae, 5 ~ 25 parts of tea tree extract, 20 ~ 45 parts of Sweet Almond Oil, small 40 ~ 110 parts of wheat germ oil, 5 ~ 15 parts of sandalwood oil, 60 ~ 100 parts of ethanol, 50 ~ 100 parts of glycerine.
Described cinnamomum camphora Verbena officinalis essential oil, its constitutive material also include:The parts by weight of cedarwood extract 5 ~ 15.
Preferably, the preparation method of described cinnamomum camphora extract is as follows:(1)After leaf of Cortex cinnamomi camphorae is cleaned, drying moisture, put In soxhlet extraction instrument;(2)Absolute ethyl alcohol is added to soxhlet extraction instrument, leaf of Cortex cinnamomi camphorae carried out at being 70 ~ 80 DEG C in temperature Refluxing extraction;(3)1/5 that volume is primary liquid volume is concentrated in vacuo at being 40 ~ 50 DEG C in temperature by gained phegma.
Preferably, the preparation method of the Herba Verbenae is as follows:Verbena officinalis is once purged, drying, crush, be placed in In 75% ethanol, 50 ~ 60 DEG C are heated to, 1 ~ 3h of refluxing extraction;Gained phegma is removed into solvent through being evaporated under reduced pressure, produced.
Preferably, during the vacuum concentration, Stress control is 20 ~ 30kPa.
Preferably, the pressure of the vacuum distillation is 10 ~ 30kPa, and temperature is 60 ~ 80 DEG C.
The cinnamomum camphora Verbena officinalis essential oil that inventive formulation and processing method are prepared into, there is cinnamomum camphora, Verbena officinalis, the perfume (or spice) of tea tree Taste, the main aromatic components that cedarwood is adjusted as after, release is slow, and fragrant atmosphere is lasting, have calm the nerves, be quiet, according to one's conscience the effect of.
Embodiment
The present invention is described in further detail with reference to embodiment.It is emphasized that the description below is only Only it is exemplary, the scope being not intended to be limiting of the invention and its application.
Embodiment 1 prepares the essential oil of the present invention using the raw material of following quality proportioning:30 parts of cinnamomum camphora extract, Verbena officinalis carry Take 12 parts of thing, the parts by weight of cedarwood extract 10,25 parts of tea tree extract, 33 parts of Sweet Almond Oil, 87 parts of wheat-germ oil, santal 11 parts of oil, 60 parts of ethanol, 80 parts of glycerine.
Wherein, the preparation of cinnamomum camphora extract:(1)After leaf of Cortex cinnamomi camphorae is cleaned, drying moisture, it is placed in soxhlet extraction instrument; (2)The absolute ethyl alcohol of 3 times of quality is added to soxhlet extraction instrument, refluxing extraction is carried out to leaf of Cortex cinnamomi camphorae at being 75 DEG C in temperature; (3)1/5 that volume is primary liquid volume is concentrated at being 45 DEG C in temperature by gained phegma, under 25kPa.
It is prepared by Herba Verbenae:Verbena officinalis is cleaned, dry, be crushed to 80 mesh, be placed in 75% ethanol, be heated to 55 DEG C, refluxing extraction 2h;Gained phegma is evaporated under reduced pressure under the conditions of pressure is 20kPa, temperature is 70 DEG C and removes solvent i.e. .
Embodiment 2 prepares the essential oil of the present invention using the raw material of following quality proportioning:35 parts of cinnamomum camphora extract, Verbena officinalis carry Take 30 parts of thing, 5 parts of tea tree extract, 45 parts of Sweet Almond Oil, 40 parts of wheat-germ oil, 5 parts of sandalwood oil, 87 parts of ethanol, glycerine 90 parts.
Wherein, the preparation of cinnamomum camphora extract:(1)After leaf of Cortex cinnamomi camphorae is cleaned, drying moisture, it is placed in soxhlet extraction instrument; (2)The absolute ethyl alcohol of 3 times of quality is added to soxhlet extraction instrument, refluxing extraction is carried out to leaf of Cortex cinnamomi camphorae at being 70 DEG C in temperature; (3)Gained phegma is concentrated in vacuo in the case where temperature is 40 DEG C, pressure is 20kPa to 1/5 that volume is primary liquid volume.
It is prepared by Herba Verbenae:Verbena officinalis is cleaned, dry, be crushed to 80-100 mesh, be placed in 75% ethanol, add Heat is to 50 DEG C, the refluxing extraction 3h in the case where distillation pressure is 10kPa;Gained phegma is removed into solvent through being evaporated under reduced pressure.
Embodiment 3 prepares the essential oil of the present invention using the raw material of following quality proportioning:12 parts of cinnamomum camphora extract, Verbena officinalis carry Take 10 parts of thing, 22 parts of tea tree extract, 20 parts of Sweet Almond Oil, 110 parts of wheat-germ oil, 15 parts of sandalwood oil, 100 parts of ethanol, third 100 parts of triol.
Wherein, the preparation of cinnamomum camphora extract:(1)After leaf of Cortex cinnamomi camphorae is cleaned, drying moisture, it is placed in soxhlet extraction instrument; (2)The absolute ethyl alcohol of 5 times of quality is added to soxhlet extraction instrument, refluxing extraction is carried out to leaf of Cortex cinnamomi camphorae at being 80 DEG C in temperature; (3)By gained phegma in the case where temperature is 50 DEG C, be concentrated into that volume is primary liquid volume in the case where pressure is 30kPa 1/5.
It is prepared by Herba Verbenae:Verbena officinalis is cleaned, dry, be crushed to 100 mesh, be placed in 75% ethanol, be heated to 60 DEG C, the refluxing extraction 1h in the case where pressure is 30kPa;Gained phegma is produced through being evaporated under reduced pressure removing solvent.

Claims (6)

1. a kind of cinnamomum camphora Verbena officinalis essential oil, it is characterised in that in units of parts by weight, include following raw material:Cinnamomum camphora extract 12 ~ 35 parts, 10 ~ 30 parts of Herba Verbenae, 5 ~ 25 parts of tea tree extract, 20 ~ 45 parts of Sweet Almond Oil, 40 ~ 110 parts of wheat-germ oil, 5 ~ 15 parts of sandalwood oil, 60 ~ 100 parts of ethanol, 50 ~ 100 parts of glycerine.
2. cinnamomum camphora Verbena officinalis essential oil according to claim 1, it is characterised in that also include:The weight of cedarwood extract 5 ~ 15 Measure part.
3. cinnamomum camphora Verbena officinalis essential oil according to claim 1, it is characterised in that the preparation method of described cinnamomum camphora extract It is as follows:(1)After leaf of Cortex cinnamomi camphorae is cleaned, drying moisture, it is placed in soxhlet extraction instrument;(2)Absolute ethyl alcohol is added to cable-styled carry Instrument is taken, refluxing extraction is carried out to leaf of Cortex cinnamomi camphorae at being 70 ~ 80 DEG C in temperature;(3)By gained phegma in the case where temperature is 40 ~ 50 DEG C It is concentrated in vacuo to 1/5 that volume is primary liquid volume.
4. cinnamomum camphora Verbena officinalis essential oil according to claim 1, it is characterised in that the preparation method of the Herba Verbenae It is as follows:Verbena officinalis is once purged, drying, crush, be placed in 75% ethanol, be heated to 50 ~ 60 DEG C, 1 ~ 3h of refluxing extraction;By institute Obtain phegma and remove solvent through being evaporated under reduced pressure, produce.
5. cinnamomum camphora Verbena officinalis essential oil according to claim 3, it is characterised in that during the vacuum concentration, Stress control is 20~30kPa。
6. cinnamomum camphora Verbena officinalis essential oil according to claim 3, it is characterised in that the pressure of the vacuum distillation be 10 ~ 30kPa, temperature are 60 ~ 80 DEG C.
CN201710933906.2A 2017-10-10 2017-10-10 A kind of cinnamomum camphora Verbena officinalis essential oil Pending CN107629874A (en)

Priority Applications (1)

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CN201710933906.2A CN107629874A (en) 2017-10-10 2017-10-10 A kind of cinnamomum camphora Verbena officinalis essential oil

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CN201710933906.2A CN107629874A (en) 2017-10-10 2017-10-10 A kind of cinnamomum camphora Verbena officinalis essential oil

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103952240B (en) * 2014-05-19 2015-09-30 安徽科技学院 A kind of preparation method of Flower of Sunset Abelmoschus volatile oil
CN104958774A (en) * 2015-06-11 2015-10-07 北京清科慧谷科技发展有限公司 Air purification plant composition and making method thereof
CN105362137A (en) * 2015-11-28 2016-03-02 刘丽玲 Osmanthus flower perfume
CN105476931A (en) * 2015-12-29 2016-04-13 青岛蓝图文化传播有限公司市南分公司 Lavender fragrance perfume
CN105997812A (en) * 2016-07-07 2016-10-12 青岛艾派克生物科技有限公司 Refreshing perfume

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103952240B (en) * 2014-05-19 2015-09-30 安徽科技学院 A kind of preparation method of Flower of Sunset Abelmoschus volatile oil
CN104958774A (en) * 2015-06-11 2015-10-07 北京清科慧谷科技发展有限公司 Air purification plant composition and making method thereof
CN105362137A (en) * 2015-11-28 2016-03-02 刘丽玲 Osmanthus flower perfume
CN105476931A (en) * 2015-12-29 2016-04-13 青岛蓝图文化传播有限公司市南分公司 Lavender fragrance perfume
CN105997812A (en) * 2016-07-07 2016-10-12 青岛艾派克生物科技有限公司 Refreshing perfume

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
屈娴: "《精油圣经:神奇抗衰、祛疤、瘦身精油》", 30 November 2014, 吉林科学技术出版社 *

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Application publication date: 20180126