CN102876454A - Two-section preparation method for tobacco vanilla flavour - Google Patents
Two-section preparation method for tobacco vanilla flavour Download PDFInfo
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- CN102876454A CN102876454A CN2012103296075A CN201210329607A CN102876454A CN 102876454 A CN102876454 A CN 102876454A CN 2012103296075 A CN2012103296075 A CN 2012103296075A CN 201210329607 A CN201210329607 A CN 201210329607A CN 102876454 A CN102876454 A CN 102876454A
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- xiangjialandou
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- refluxing extraction
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Abstract
The invention discloses a two-section preparation method for a tobacco vanilla flavour. The method comprises the following steps: extracting vanilla beans through a lipid soluble solvent in a reflux manner; then extracting the vanilla beans through a water soluble solvent in a reflux manner; leaching; and concentrating the filtrate at reduced pressure to obtain the vanilla flavour. With the adoption of the two-section preparation method for the tobacco vanilla flavour disclosed by the invention, separation of the lipid soluble components and water soluble components of the vanilla beans can be realized, thereby being convenient to the subsequent treatment of a crude extract; and the total extractum yield of raw materials can be improved, the raw materials can be fully utilized, and effective fragrant components in the raw materials can be fully extracted and separated.
Description
The present invention is that application number is 201010584532.6, the applying date be December 13 in 2010 day, be called the dividing an application of application for a patent for invention of " cigarette with the preparation method of vanilla spices ".
Technical field
The present invention relates to the preparation method of tobacco aromatics using, belong to technical field of tobacco, specifically take XIANGJIALANDOU as raw material, according to the characteristics of XIANGJIALANDOU chemical ingredients, utilize the method for specific extraction and separation technology segmentation production characteristic tobacco aromatics using.
Background technology
Vanilla (
Vanilla planifoliaAndr.) have another name called vanilla, Herba vanillae Planifoliae, Vanilla annamica, have the good reputation of " king of food spice ".The country of origin of vanilla is Mexico, is a kind of large-scale the orchid family spice berry that is grown in the tropical rain forest.At present, the cultivation area of vanilla mainly concentrates on island state or the areas such as Madagascar, Indonesia, Comoros, Liu Wangni, Uganda, Seychelles, Mexico and Tahiti.China introduces vanilla in nineteen sixty from Indonesia, plants in Fujian, the ground such as Hainan, Guangxi and Yunnan, because the advantageous physical environment in Yunnan, vanilla is the most successful in the cultivation in Yunnan, at present existing nearly 1000 mu cultivated area, stable yield, best in quality.
The fragrance of vanilla is fresh and sweet creamy, and human body is had joyful, comfortable impression, many rhythms that give off a strong fragrance, and lasting is lasting, long times of aftertaste.The XIANGJIALANDOU extract uses in tobacco, food, makeup in a large number at present, and the flavouring effect is fairly obvious.What is particularly worth mentioning is that the XIANGJIALANDOU extract is applied on the tobacco, can play pure and mild flue gas, coordinate smoke, it is fragrant to increase cigarette, the just fragrant fine and smooth soft effect of cigarette.
Adopt directly concentrated rear acquisition of solvent-extraction process for the extraction of vanilla spices at present more, this method can not effectively be extracted spices for the characteristics that XIANGJIALANDOU had not only contained fat-soluble ingredient but also contained water soluble ingredient, the total extractives yield of raw material is lower, can not fully utilize and differently in raw material and the abundant extracting and separating raw material effectively cause fragrant component, so that the different spice products of gained are suitable for the reinforced effect characteristics of perfuming cigarette, also be not easy to following process and the processing of crude extract.
Summary of the invention
The objective of the invention is to solve the deficiencies in the prior art, provide a kind of take XIANGJIALANDOU as raw material, can realize separating of XIANGJIALANDOU fat-soluble ingredient and water soluble ingredient, be convenient to following process and the processing of crude extract, can improve the total extractives yield of raw material, reach the preparation method that the cigarette that effectively causes fragrant component in comprehensive utilization raw material and the abundant extracting and separating raw material is used vanilla spices.
The objective of the invention is to be achieved through the following technical solutions.
The cigarette two-part preparation method of vanilla spices, by after the fat-soluble solvent refluxing extraction with XIANGJIALANDOU, to use again the water-soluble solvent refluxing extraction through the XIANGJIALANDOU after the fat-soluble solvent refluxing extraction, then suction filtration, the concentrated vanilla spices that obtains of filtrate decompression.
The inventive method is specially the segment that first XIANGJIALANDOU is cut into 1～2cm, adds to add fat-soluble solvent refluxing extraction three times, each 1～3 hour doubly by 3～6 of XIANGJIALANDOU weight; Then after removing the residual solvent in the XIANGJIALANDOU after fat-soluble solvent extracts, add the adding water soluble solvent doubly by 5～8 of XIANGJIALANDOU weight, refluxing extraction twice each 1～3 hour, gets final product the extracting liquid filtering that obtains by concentrating under reduced pressure.
Fat-soluble solvent of the present invention is sherwood oil or ethyl acetate or propyl carbinol or chloroform or ether; Described water-soluble solvent is the double solvents of water, alcoholic solvent or water and alcoholic solvent.
The inventive method has following characteristics: by the stage extraction of opposed polarity solvent, can realize separating of XIANGJIALANDOU fat-soluble ingredient and water soluble ingredient, be convenient to following process and the processing of crude extract.The method of stage extraction has improved the total extractives yield of raw material, has reached the purpose that effectively causes fragrant component in comprehensive utilization raw material and the abundant extracting and separating raw material.The a whole set of technological process of the inventive method is simple, and required equipment is simple, can be implemented in the wire gauge modelling and produce, and is easy to utilize.The spices that the method is produced can play pure and mild flue gas, coordinates smoke, and it is fragrant to increase cigarette, makes the fragrant fine and smooth soft effect of cigarette.
Embodiment
Embodiment one
Divide in the steps below two sections to prepare the vanilla spice product:
1. take by weighing XIANGJIALANDOU 500g, it is cut into the segment of about 1～2cm, add the sherwood oil of 2000g, refluxing extraction 3 times, each 3 hours;
2. with the 1. the XIANGJIALANDOU behind the section Petroleum ether extraction through dry remove unrecovered oil ether after, add 70% ethanol of 2500g, refluxing extraction 2 times at every turn, each 3 hours, united extraction liquid carries out suction filtration after its natural subsidence, filtrate namely obtains the vanilla spice product behind concentrating under reduced pressure.
Embodiment two
Divide in the steps below two sections to prepare the vanilla spice product:
1. take by weighing XIANGJIALANDOU 500g, it is cut into the segment of 1～2cm, add the ethyl acetate of 3000g, refluxing extraction 3 times, each 2 hours;
2. with the XIANGJIALANDOU after the above-mentioned ethyl acetate extraction through dry remove residual ethyl acetate after, add 70% propylene glycol of 3500g, refluxing extraction 2 times at every turn, each 3 hours, united extraction liquid carries out suction filtration after its natural subsidence, filtrate obtains the vanilla spice product behind concentrating under reduced pressure.
Embodiment three
Divide in the steps below two sections to prepare the vanilla spice product:
1. take by weighing XIANGJIALANDOU 500g, it is cut into the segment of 1～2cm, add the propyl carbinol of 2500g, refluxing extraction 3 times, each 2 hours;
2. with the XIANGJIALANDOU behind the n-butanol extraction through dry remove residual propyl carbinol after, add 95% ethanol of 3000g, refluxing extraction 2 times at every turn, each 2 hours, united extraction liquid carries out suction filtration after its natural subsidence, filtrate obtains the vanilla spice product behind concentrating under reduced pressure.
Embodiment four
Divide in the steps below two sections to prepare the vanilla spice product:
1. take by weighing XIANGJIALANDOU 500g, it is cut into the segment of 1～2cm, add chloroform or the ether of 1500g, refluxing extraction 3 times, each 1 hour;
2. with the XIANGJIALANDOU after chloroform or the ether extraction through dry remove residual chloroform after, add 70% ethanol of 4000g, refluxing extraction 2 times at every turn, each 1 hour, united extraction liquid carries out suction filtration after its natural subsidence, filtrate obtains the vanilla spice product behind concentrating under reduced pressure.
Claims (3)
1. cigarette is with the two-part preparation method of vanilla spices, it is characterized in that, XIANGJIALANDOU by after the fat-soluble solvent refluxing extraction, will be used the water-soluble solvent refluxing extraction again through the XIANGJIALANDOU after the fat-soluble solvent refluxing extraction, then suction filtration, the concentrated vanilla spices that obtains of filtrate decompression.
2. cigarette according to claim 1 is characterized in that with the two-part preparation method of vanilla spices, first XIANGJIALANDOU is cut into the segment of 1～2cm, adds doubly by 3～6 of XIANGJIALANDOU weight to add fat-soluble solvent, refluxing extraction three times, each 1～3 hour; Then after removing the residual solvent in the XIANGJIALANDOU after fat-soluble solvent extracts, add the adding water soluble solvent doubly by 5～8 of XIANGJIALANDOU weight, refluxing extraction twice each 1～3 hour, gets final product the extracting liquid filtering that obtains by concentrating under reduced pressure.
3. cigarette according to claim 1 and 2 is characterized in that with the two-part preparation method of vanilla spices described fat-soluble solvent is sherwood oil or ethyl acetate or propyl carbinol or chloroform or ether; Described water-soluble solvent is the double solvents of water, alcoholic solvent or water and alcoholic solvent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103296075A CN102876454A (en) | 2010-12-13 | 2010-12-13 | Two-section preparation method for tobacco vanilla flavour |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103296075A CN102876454A (en) | 2010-12-13 | 2010-12-13 | Two-section preparation method for tobacco vanilla flavour |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010584532 Division CN102051266B (en) | 2010-12-13 | 2010-12-13 | Preparation method of vanilla perfume for cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102876454A true CN102876454A (en) | 2013-01-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2012103296075A Pending CN102876454A (en) | 2010-12-13 | 2010-12-13 | Two-section preparation method for tobacco vanilla flavour |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242959A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of tobacco chrysanthemum absolute oil |
| CN103404963A (en) * | 2013-05-10 | 2013-11-27 | 湖北中烟工业有限责任公司 | Tobacco perfuming method |
| CN103445286A (en) * | 2013-09-05 | 2013-12-18 | 湖北中烟工业有限责任公司 | Preparing method of tobacco sheets containing black vanilla |
| RU2594174C1 (en) * | 2015-04-28 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
-
2010
- 2010-12-13 CN CN2012103296075A patent/CN102876454A/en active Pending
Non-Patent Citations (2)
| Title |
|---|
| 孙宝国等: "《食用调香术》", 30 September 2003 * |
| 海南布莱特公司香芙兰深加工课题组: "香荚兰豆提纯物生产制备研究", 《2000年中国香料香精学术研讨会》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103404963A (en) * | 2013-05-10 | 2013-11-27 | 湖北中烟工业有限责任公司 | Tobacco perfuming method |
| CN103242959A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of tobacco chrysanthemum absolute oil |
| CN103445286A (en) * | 2013-09-05 | 2013-12-18 | 湖北中烟工业有限责任公司 | Preparing method of tobacco sheets containing black vanilla |
| CN103445286B (en) * | 2013-09-05 | 2015-08-19 | 湖北中烟工业有限责任公司 | A kind of preparation method containing black vanilla reconstituted tobacoo |
| RU2594174C1 (en) * | 2015-04-28 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
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Application publication date: 20130116 |