CN107628827A - A kind of method that foliar fertilizer is made using wild jujube as raw material - Google Patents

A kind of method that foliar fertilizer is made using wild jujube as raw material Download PDF

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Publication number
CN107628827A
CN107628827A CN201711061101.XA CN201711061101A CN107628827A CN 107628827 A CN107628827 A CN 107628827A CN 201711061101 A CN201711061101 A CN 201711061101A CN 107628827 A CN107628827 A CN 107628827A
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China
Prior art keywords
wild jujube
raw material
foliar fertilizer
fertilizer
potassium
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CN201711061101.XA
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Chinese (zh)
Inventor
郭家宏
陈文烨
贾小茜
焦义然
郭卜语
郭晋君
杜进民
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Individual
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Individual
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Abstract

A kind of method that foliar fertilizer is made using wild jujube as raw material, preparation process are as follows:(1) crush (2) fermentative degradation (3) filtering, neutralize (4) dispensing (5) neutralization (6) finished product.The present invention compared with prior art the advantages of have:(1) solves the problems, such as the recycling of wild jujube eluate.(2) targetedly the high nitrogen of nutrient, high phosphorus, the blade face fertilizer product of high potassium can timely and effectively correct crop and lack nutrient symptom.(3) eluate is processed as raw material using spina date seed, it is green, the effect of increasing income is notable.(4) science compounding can be carried out according to the nutritional need of Different Crop under optimum conditions.

Description

A kind of method that foliar fertilizer is made using wild jujube as raw material
Technical field
The present invention relates to foliar fertilizer preparation method field, particularly a kind of high nitrogen, height formed using wild jujube as Raw material processing The foliar fertilizer preparation method of phosphorus, high potassium.
Background technology
In the forties in 19th century, it has been found that crop is except that in addition to the nutriment needed for Root Absorption, can also lead to The cauline leaf for crossing crop absorbs nutrient, and the mode that this cauline leaf cell by plant absorbs nutriment is referred to as Foliage Absorption.Make The fertilizing method that thing absorbs nutrient by blade face (including part stem surface) diffusion mode is referred to as plant foliage fertilization, also It is foliage dressing generally.Fertilizer for foliage dressing is referred to as foliar fertilizer.Nutrient symptom is lacked according to crop leaf, it is different Type foliar fertilizer can be directly fed crop and absorbed quickly, to supplement deficiency of the root to Nutrient Absorption, be realized by foliage-spray Volume increase increases the effect of matter again.
Why foliar fertilizer is widely deployed and applies, and is because foliar fertilizer has many outstanding features:1. specific aim By force.According to crop leaf nutritional deficiency feature, the element lacked can be sprayed in time and improves symptom.2. Nutrient Absorption is fast, fertilizer efficiency is good.According to Experiment, sprays calcium superphosphate leaching liquor, can be transported to each position of plant after 5 minutes, and soil application calcium superphosphate, 15 days After can be only achieved this effect.3. nutrient is avoided to fix.Foliage-spray can avoid fixed and improve fertilizer efficiency and utilization rate of fertilizer.④ Dosage is few, saves fertilizer, reduces cost.Compared with soil application, the fertilizer amount for foliage dressing is only that soil is applied for foliage dressing The 1/10~1/5 of fertilizer.5. reduce environmental pollution.To micro- fertilizer of soil application, once excessive heavy metal element residues in soil In, it is possible to pollute;And the micro- fertilizer of foliage-spray, concentration are low, quantity is few, will not cause soil pollution.6. spraying method It is easy., can operation by spraying apparatus as long as there is water source.Foliage dressing has economic, efficient, safety and without dirt as can be seen here The characteristics of dye.
Currently, foliar fertilizer Main Trends of The Development is:1. some targetedly single nutrient class product in market On more welcome, such as prominent potassium, calcium, iron, the foliar fertilizer of zinc.2. the addition of natural plant extracts is more and more, this Kind product is more environmentally-friendly and safe, such as humic acid, seaweed amino acid, chitin.3. the concentration of product is higher, the use of product Process is more convenient.
Research shows, N containing a great number of elements, P, K leaf are sprayed during the cereal crops such as soybean, corn, wheat seed fills oar Leaven can improve the quality grain represented with protein content, cause obvious volume increase, but crops it is big to element requirement and The each dosage of foliage-spray is limited, and cereal crops a great number of elements foliage-spray is not also widely used in production.
Wild jujube category Rhamnaceae zizyphus, is distributed widely in northern China mountain area, is the spy in China containing abundant nutriment Color advantage wild fruit tree and important medicinal plant.Wild jujube has very high economic use value, its pulp, benevolence, leaf, root, skin Deng can be used as medicine, pulp is nutritious, special taste, is the ideal material for making natural health drink.But it is used for fertilizer production Case it is seldom.Therefore, as the development of innovation fertilizer technology, the value of the product of new-type fertilizer are increasingly lifted, wild jujube are used as Fertilizer production, good economic value and resource profit can be realized by inventing a kind of high nitrogen, high phosphorus, the foliar fertilizer preparation method of high potassium With value.
The content of the invention
The defects of existing for prior art, there is provided a kind of high nitrogen formed using wild jujube as Raw material processing, high phosphorus, high potassium Foliar fertilizer preparation method.
Therefore, the present invention uses following technical scheme:A kind of method that foliar fertilizer is made using wild jujube as raw material, its feature exist In comprising the following steps:
(1) later wild jujube will be enucleated and selects cleaning, then crushed;
(2) by way of biofermentation by wild jujube eluate be degraded to containing low-molecular polysaccharide, peptide, amino acid solution;
(3) above-mentioned reaction product is subjected to filter cleaner, its filtrate ammoniacal liquor and/or potassium hydroxide solution and/or clarification Aqua calcis neutralize, make its pH value be 3~5;Or neutralized using the waste mother liquor of production amino acid, at 80 DEG C Dehydration concentration is carried out below, is higher than 30% to hydrolysis amino acid total amount, is obtained several amino acids Solutions Solution;
(4) polypeptide of gained, Freamine Ⅲ solution liquid are heated to 60~80 DEG C, phosphoric acid is sequentially added under stirring Hydrogen dipotassium, humic acid, reaction is stirred in reaction vessel, is completely dissolved to material is added, it is solution-stabilized;
(5) it is 5~7 with ammoniacal liquor and/or potassium hydroxide solution and/or the aqua calcis of clarification regulation pH value, produces Foliar fertilizer.
As the supplement to above-mentioned technical proposal and perfect, present invention additionally comprises following technical characteristic.
Thing is enucleated in step (1) to wild jujube by industrial pulverizer to crush.
The humic acid in step (4) is 10~12g/L, and available nitrogen is 0.70~0.82g/L, available phosphorus is 2.88~ 3.06g/L, effective potassium are 35.20~36.16g/L.
It can reach following beneficial effect using the present invention:Foliar fertilizer can be prepared in batches by the present invention, can be with It is widely used on crop.Nitrogen of the present invention, phosphorus, potassium content are high, so as to improve the grain protein content of crop and yield, Also the big work pattern of traditional root system fertilising is replaced.The foliar fertilizer of the present invention can be compounded as composite foliage fertilizer, in suitable bar Science compounding can be carried out according to the nutritional need of Different Crop under part, series of products can be prepared as needed.On the other hand, this hair The bright recycling for solving the problems, such as wild jujube eluate, targetedly the high nitrogen of nutrient, high phosphorus, high potassium blade face fertilizer product can Timely and effectively correct crop and lack nutrient symptom.The present invention processes eluate as raw material using spina date seed, and green, volume increase increases Receive significant effect.
Embodiment
Embodiment 1
A kind of method that foliar fertilizer is made using wild jujube as raw material comprises the following steps:
(1) later wild jujube will be enucleated and selects cleaning, then wild jujube eluate is crushed by industrial pulverizer;
(2) wild jujube eluate is degraded to Freamine Ⅲ by way of biofermentation;
(3) above-mentioned reaction product is subjected to filter cleaner, its filtrate ammoniacal liquor and potassium hydroxide solution neutralize, and make its pH value For 3~5;
(4) the several amino acids solution solution liquid of gained is heated to 80 DEG C, phosphoric acid hydrogen two is sequentially added under stirring Potassium, humic acid, reaction is stirred in reaction vessel, is completely dissolved to material is added, it is solution-stabilized;
(5) it is 5~7 with ammoniacal liquor and potassium hydroxide solution regulation pH value, produces foliar fertilizer.
Embodiment 2
A kind of method that foliar fertilizer is made using wild jujube as raw material comprises the following steps:
(1) later wild jujube will be enucleated and selects cleaning, then wild jujube eluate is crushed by industrial pulverizer;
(2) wild jujube eluate is degraded to Freamine Ⅲ by way of biofermentation;
(3) above-mentioned reaction product is subjected to filter cleaner, neutralized using the waste mother liquor of production amino acid, at 80 DEG C Dehydration concentration is carried out below, is higher than 30% to hydrolysis amino acid total amount, it is 3~5 to make its pH value, and it is molten to obtain several amino acids Liquid;
(4) the several amino acids solution solution liquid of gained is heated to 60 DEG C, phosphoric acid hydrogen two is sequentially added under stirring Potassium, humic acid, reaction is stirred in reaction vessel, is completely dissolved to material is added, it is solution-stabilized;
(5) it is 5~7 with ammoniacal liquor and potassium hydroxide solution, the aqua calcis regulation pH value of clarification, produces foliar fertilizer.
Embodiment 3
A kind of method that foliar fertilizer is made using wild jujube as raw material comprises the following steps:
(1) later wild jujube will be enucleated and selects cleaning, then crushed;
(2) wild jujube eluate is degraded to Freamine Ⅲ by way of biofermentation;
(3) above-mentioned reaction product is subjected to filter cleaner, its filtrate is neutralized with ammoniacal liquor, and it is 3~5 to make its pH value;
(4) the several amino acids solution solution liquid of gained is heated to 70 DEG C, phosphoric acid hydrogen two is sequentially added under stirring Potassium, humic acid are stirred reaction in reaction vessel, and its content of humic acid is 10~12g/L, and effective nitrogen content is 0.70~ 0.82g/L, available phosphorus content are 2.88~3.06g/L, and effective potassium content is 35.20~36.16g/L, and to adding, material is complete Dissolving, it is solution-stabilized;
(5) it is 5~7 with ammoniacal liquor regulation pH value, produces foliar fertilizer.
Embodiment 4
A kind of method that foliar fertilizer is made using wild jujube as raw material comprises the following steps:
(1) later wild jujube will be enucleated and selects cleaning, then crushed;
(2) wild jujube eluate is degraded to Freamine Ⅲ by way of biofermentation;
(3) above-mentioned reaction product is subjected to filter cleaner, its filtrate ammoniacal liquor and potassium hydroxide solution, the hydroxide of clarification Calcium solution neutralizes, and it is 3~5 to make its pH value;
(4) the several amino acids solution solution liquid of gained is heated to 60 DEG C, phosphoric acid hydrogen two is sequentially added under stirring Potassium, humic acid, reaction is stirred in reaction vessel, is completely dissolved to material is added, it is solution-stabilized;
(5) it is 5~7 with the aqua calcis regulation pH value of clarification, produces foliar fertilizer.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (3)

  1. A kind of 1. method that foliar fertilizer is made using wild jujube as raw material, it is characterised in that comprise the following steps:
    (1) later wild jujube will be enucleated and selects cleaning, then crushed;
    (2) by way of biofermentation by wild jujube eluate be degraded to containing low-molecular polysaccharide, peptide, amino acid solution;
    (3) above-mentioned reaction product is subjected to filter cleaner, its filtrate ammoniacal liquor and/or potassium hydroxide solution and/or the hydrogen of clarification Calcium oxide solution neutralizes, and it is 3~5 to make its pH value;Or neutralized using the waste mother liquor of production amino acid, below 80 DEG C Dehydration concentration is carried out, is higher than 30% to hydrolysis amino acid total amount.
    (4) polypeptide of gained, Freamine Ⅲ solution liquid are heated to 60~80 DEG C, phosphoric acid hydrogen two is sequentially added under stirring Potassium, humic acid, reaction is stirred in reaction vessel, is completely dissolved to material is added;
    (5) it is 5~7 with ammoniacal liquor and/or potassium hydroxide solution and/or the aqua calcis of clarification regulation pH value, produces blade face Fertilizer.
  2. A kind of 2. method that foliar fertilizer is made using wild jujube as raw material according to claim 1, it is characterised in that:Step (1) In by industrial pulverizer to wild jujube be enucleated thing crush.
  3. A kind of 3. method that foliar fertilizer is made using wild jujube as raw material according to claim 1, it is characterised in that:Step (4) Described in content of humic acid be 10~12g/L, effective nitrogen content is 0.70~0.82g/L, available phosphorus content is 2.88~ 3.06g/L, effective potassium content are 35.20~36.16g/L.
CN201711061101.XA 2017-11-02 2017-11-02 A kind of method that foliar fertilizer is made using wild jujube as raw material Pending CN107628827A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109232127A (en) * 2018-10-24 2019-01-18 河北省农林科学院遗传生理研究所(河北省农林科学院农产品质量安全研究中心) A kind of Zizyphus Spinosa Hu Flesh organic fertilizer and its preparation method and application

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1154352A (en) * 1996-01-06 1997-07-16 北京市思达尔化工新技术公司 Plant leaves fertilizer
KR100283959B1 (en) * 1999-01-27 2001-02-15 채명칠 Manufacturing method of tonic for cultivation melon using medicinal decoction dregs
CN106008047A (en) * 2016-05-14 2016-10-12 安徽新天地生物肥业有限公司 Amino acid rice leaf fertilizer

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1154352A (en) * 1996-01-06 1997-07-16 北京市思达尔化工新技术公司 Plant leaves fertilizer
KR100283959B1 (en) * 1999-01-27 2001-02-15 채명칠 Manufacturing method of tonic for cultivation melon using medicinal decoction dregs
CN106008047A (en) * 2016-05-14 2016-10-12 安徽新天地生物肥业有限公司 Amino acid rice leaf fertilizer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109232127A (en) * 2018-10-24 2019-01-18 河北省农林科学院遗传生理研究所(河北省农林科学院农产品质量安全研究中心) A kind of Zizyphus Spinosa Hu Flesh organic fertilizer and its preparation method and application

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Application publication date: 20180126