CN107474658A - A kind of aqueous, environmental protective heat discoloration crackle paint and preparation method thereof - Google Patents

A kind of aqueous, environmental protective heat discoloration crackle paint and preparation method thereof Download PDF

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Publication number
CN107474658A
CN107474658A CN201710702325.8A CN201710702325A CN107474658A CN 107474658 A CN107474658 A CN 107474658A CN 201710702325 A CN201710702325 A CN 201710702325A CN 107474658 A CN107474658 A CN 107474658A
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China
Prior art keywords
aqueous
paint
heat discoloration
rotating speed
min rotating
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Granted
Application number
CN201710702325.8A
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Chinese (zh)
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CN107474658B (en
Inventor
戴家兵
曹琛
祝彬
陈磊
王建元
葛文高
王永乐
唐朋朋
魏念旺
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HEFEI SCISKY TECHNOLOGY Co.,Ltd.
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Lanzhou Ketian New Material Co Ltd
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Publication of CN107474658A publication Critical patent/CN107474658A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/002—Priming paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/02—Emulsion paints including aerosols
    • C09D5/024—Emulsion paints including aerosols characterised by the additives
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/26—Thermosensitive paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/28—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for wrinkle, crackle, orange-peel, or similar decorative effects
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of aqueous, environmental protective heat discoloration crackle paint and preparation method thereof, aqueous, environmental protective heat discoloration crackle paint includes priming paint and finish paint, and priming paint includes component by weight percentage：Aqueous acrylic emulsion 20~60%, nertralizer 0.3~1.5%, coalescents 5~20%, catalyst 0.5~1.5%, levelling agent 0.1~1%, defoamer 0.3~1%, thickener 0.5~2%, mill base 10~25%, deionized water 10~30%, finish paint include component by weight percentage：Aqueous acrylic emulsion 30~60%, nertralizer 0.5~3%, wetting dispersing agent 1~3%, levelling agent 0.1~1%, defoamer 0.3~1%, white carbon 5~30%, heat discoloration pigment 5~10%, mill base 10~30%, thickener 0.5~2%, deionized water 15~40%.Crackle paint of the present invention is environmentally friendly, heat discoloration.

Description

A kind of aqueous, environmental protective heat discoloration crackle paint and preparation method thereof
Technical field
The present invention relates to technical field of coatings, and in particular to a kind of aqueous, environmental protective heat discoloration crackle paint and its preparation side Method.
Background technology
Crackle paint compared with other types product, is applied as a kind of coating products with special aesthetic feeling and style The fields such as furniture, the art work, fitment material for family, the quality that more preferable decorative aesthetics and Geng Gao can be provided to consumer are pursued.But It is that traditional crackle paint uses organic solvent to have too high volatile materials during use as raw material mostly.Meanwhile Although traditional crackle paint has a well-regulated crack effect, but its aesthetic feeling and intelligent more fall behind.Therefore, it is possible to provide one kind It can change with ambient temperature and make crackle paint that the novel environment friendly heat discoloration crackle paint of color change occur, become more intentional Justice.
The content of the invention
For above-mentioned problems of the prior art, the present invention provide a kind of aqueous, environmental protective heat discoloration crackle paint and its Preparation method.
Specifically, the present invention provides a kind of aqueous, environmental protective heat discoloration crackle paint it is characterised in that it includes priming paint and finish paint,
The priming paint count by weight percentage, including following components：
The finish paint count by weight percentage, including following components：
Wherein, the nertralizer is amine multifunctional assistant AMP-95 (Tao Shi)；
Aqueous acrylic emulsion described in priming paint is R4188 (Hua Jinsi), aqueous acrylic emulsion is described in finish paint HD2535 (Hua Jinsi)；
The wetting dispersing agent is Dispers651 (enlightening is high)；
The coalescents are at least one of alcohol ester 12, dipropylene, DPG first mystery；
The catalyst is dibutyl tin laurate；
The levelling agent is RM2020 (ROHM AND HAAS)；
The defoamer is Foamex810 (enlightening is high)；
The mill base is aqueous color paste；
The thickener is TT935 (ROHM AND HAAS)；
The white carbon is micron order aerosil TS100 (Degussa)；
The heat discoloration pigment is #1640 DEG C, at least one in #1828 DEG C (the discoloration Science and Technology Ltd. of Shenzhen thousand) Kind.
The present invention also provides a kind of preparation method of aqueous, environmental protective heat discoloration crackle paint as described above, the preparation of priming paint Comprise the following steps：
A) deionized water is put into material cylinder, aqueous acrylic emulsion, levelling agent, defoamer is then put into material cylinder, 400 Mixing 10 minutes is continuously stirred under~600r/min rotating speed；
B) nertralizer, curing agent coalescents and catalyst are added under 800~1000r/min rotating speed, is continuously stirred Mixing 20 minutes；
C) thickener is put under 400~600r/min rotating speed and adjusts viscosity to 80~120pa.s；
D) mill base is added under 400~600r/min rotating speed to adjust to required color and filter；
The preparation of the finish paint comprises the following steps：
1) by needed for formula ratio portions of de-ionized water put into material cylinder, then by aqueous acrylic emulsion, wetting dispersing agent, disappear Infusion, levelling agent input material cylinder, continuously stir mixing 10 minutes under 400~600r/min rotating speed；
2) nertralizer, curing agent are added under 800~1000r/min rotating speed, continuously stirs mixing 20 minutes；
3) white carbon, heat discoloration pigment are put under 1000~1200r/min rotating speed, thickener, is continuously stirred mixed It is bonded to few 30 minutes and adjusts viscosity to 150pa.s；
4) remaining deionized water, mill base needed for input formula under 400~600r/min rotating speed, reduction viscosity to 80~ 120pa.s, and filtered after continuously stirring mixing 20 minutes.
The present invention has advantages below compared with prior art：
1st, the present invention is coordinated using finish paint with priming paint, because finish paint and primed surface tension force are different with drying shrinkage factor, first Priming paint brush finish again after its drying is brushed, finish paint can gradually be ftractureed in its drying process and the upper amplitude limit that ftractures Height, its crackle degree can be obtained adhesive force well and lines cracking are regular, attractive in appearance by brushing thickness control after its drying Crack effect, it is and simple to operate, easy for construction.
2nd, heat discoloration pigment used herein is a kind of organic compound of microcapsule structure, in different temperatures section Its interior internal organic compound can change with temperature and produce certain receiving and losing electrons phenomenon, and then produce color change.Utilize this One characteristic, using the pigment (such as 28 degree of sky blue bleach, 40 degree of dark blue bleach) in two or more different temperature-sensitive sections as water Property environmental protection heat discoloration crackle paint part simultaneously coordinates the aqueous color paste of certain deal, is fabricated to water-based heat discoloration environmental protection and splits Line finish paint, can be with change (such as zubzero temperature~28 DEG C, 28 DEG C~40 DEG C, more than 40 DEG C) production of the ambient temperature in different sections Add lustre to phase, the depth or light and shade it is different change, it is to be dried after its brushing manufactured goods can vary with temperature and produce respective change.
3rd, each component employed in the present invention is aqueous environment protection material, and unharmful substance volatilization will not be to using Person's body and environment cause any harmful effect.
Embodiment
Technical solution of the present invention is discussed in detail with reference to embodiment, but the present invention is not limited to these embodiments.
Embodiment 1
Prepare aqueous, environmental protective heat discoloration crackle priming paint：
A) 30kg deionized water is put into material cylinder, then by 30kg aqueous acrylic emulsion R4188,1kg levelling agent RM2020,1kg defoamer Foamex810 put into material cylinder, and mixing 10 minutes is continuously stirred under 400~600r/min rotating speed；
B) 1.5kg nertralizer AMP95,4kg coalescents DPG fourths are added under 800~1000r/min rotating speed Ether and 4kg coalescents DPG first mystery, 1.5kg catalyst dibutyltin dilaurylates, continuously stir mixing 20 minutes；
C) 2kg thickener TT935, regulation viscosity to 80~120pa.s are put under 400~600r/min rotating speed；
D) 25kg aqueous color pastes are added under 400~600r/min rotating speed and are filtered, bucket is packaged into after detection is qualified.
Prepare aqueous, environmental protective heat discoloration crackle finish paint：
A) 10kg deionized waters are put into material cylinder, then by 30kg aqueous acrylic emulsion HD2535,1kg wetting dispersing agents Dispers651,0.4kg defoamer Foamex810,0.1kg levelling agent RM2020 put into material cylinder, in turning for 400~600r/min Mixing 10 minutes is continuously stirred under speed；
B) 0.5kg nertralizers AMP95 is added under 800~1000r/min rotating speed and continuously stirs mixing 20 minutes；
C) #1640 DEG C of 15kg white carbon TS100,3kg heat discolorations pigment is put under 1000~1200r/min rotating speed With #1828 DEG C of 4.5kg heat discolorations pigment, 0.5kg thickener TT935, mixing at least 30 minutes is continuously stirred；
D) input 5kg deionized waters and 30kg aqueous color pastes under 400~600r/min rotating speed, regulation viscosity to 80~ 120pa.s, and filtered after continuously stirring mixing at least 20 minutes, it is packaged into bucket after detection is qualified.
Embodiment 2
The aqueous, environmental protective heat discoloration crackle priming paint of the present embodiment includes：
12kg deionized waters, 60kg aqueous acrylic emulsion R4188,1kg levelling agent RM2020,1kg defoamers Foamex810,0.3kg nertralizer AMP95,4.2kg coalescents dipropylene and 8kg coalescents DPG first Mystery, 1.5kg catalyst dibutyltins dilaurylate, 10kg mill bases, 2kg thickeners TT935；
The aqueous, environmental protective heat discoloration crack surface enamel-cover of the present embodiment includes：
24kg deionized waters, 35kg aqueous acrylic emulsion HD2535,1.9kg wetting dispersing agents Dispers651, 0.48kg defoamer Foamex810,0.28kg levelling agent RM2020,0.24kg nertralizer AMP95,18.5kg white carbons TS100, #1640 DEG C of 3.6kg heat discolorations pigment and #1828 DEG C of 5.4kg heat discolorations pigment, 0.6kg thickeners, 10kg aqueous color pastes.
The preparation method of the aqueous, environmental protective heat discoloration crackle paint of the present embodiment is identical with examining embodiment 1.
Embodiment 3
The aqueous, environmental protective heat discoloration crackle priming paint of the present embodiment includes：
15kg deionized waters, 45kg aqueous acrylic emulsion R4188,0.5kg levelling agent RM2020,0.5kg defoamers Foamex810,0.3kg nertralizer AMP95,10kg coalescents dipropylene and 10kg coalescents DPG first Mystery, 0.5kg catalyst dibutyltins dilaurylate, 0.5kg thickener TT935,17.7kg aqueous color pastes；
The aqueous, environmental protective heat discoloration crack surface enamel-cover of the present embodiment includes：
15kg deionized waters, 60kg aqueous acrylic emulsion HD2535,2.2kg wetting dispersing agents Dispers651,0.6kg Defoamer Foamex810,0.3kg levelling agent RM2020,0.5kg nertralizer AMP95,5.65kg white carbon TS100,4.5kg feel #1640 DEG C of warm camouflage paint and #1828 DEG C of 0.5kg heat discolorations pigment, 0.75kg thickeners, 10kg aqueous color pastes.
The preparation method of the aqueous, environmental protective heat discoloration crackle paint of the present embodiment is identical with examining embodiment 1.
In above example 1-3, outside air temperature higher than 40 DEG C then present aqueous color paste colors, as outside air temperature between The blend color of #1640 DEG C of heat discoloration pigment and aqueous color paste is then presented between 28 DEG C~40 DEG C, if outside air temperature is between zero Under~28 DEG C between the blend color of #1640 DEG C of heat discoloration pigment, 1828 DEG C and aqueous color paste is then presented.
Exist according to the aqueous, environmental protective heat discoloration crackle paint prepared by present invention component proportion described above and preparation method After brushing and drying in addition to crackle rule, aqueous, environmental protective, feature easy for construction, can be according to ambient temperature difference Present zubzero temperature~28 DEG C, 28 DEG C~40 DEG C, the color inverible transform between 40 DEG C of temperatures above.As family, household etc. Field construction lifts the aesthetic feeling and decorative value of product by a relatively large margin.

Claims (3)

  1. A kind of 1. aqueous, environmental protective heat discoloration crackle paint, it is characterised in that including priming paint and finish paint, priming paint percentage by weight Than calculating, including following components：
    The finish paint count by weight percentage, including following components：
  2. 2. aqueous, environmental protective heat discoloration crackle paint according to claim 1, it is characterised in that
    The nertralizer is amine multifunctional assistant AMP-95；
    Aqueous acrylic emulsion described in priming paint is R4188, aqueous acrylic emulsion is HD2535 described in finish paint；
    The wetting dispersing agent is Dispers651；
    The coalescents are at least one of alcohol ester 12, dipropylene, DPG first mystery；The catalyst is Dibutyl tin laurate；
    The levelling agent is RM2020；
    The defoamer is Foamex810；
    The mill base is aqueous color paste；
    The thickener is TT935；
    The white carbon is micron order aerosil TS100；
    The heat discoloration pigment is #1640 DEG C, at least one of #1828 DEG C.
  3. A kind of 3. preparation method of aqueous, environmental protective heat discoloration crackle paint as claimed in claim 1 or 2, it is characterised in that
    The preparation of priming paint comprises the following steps：
    A) deionized water is put into material cylinder, aqueous acrylic emulsion, levelling agent, defoamer is then put into material cylinder, 400~ Mixing 10 minutes is continuously stirred under 600r/min rotating speed；
    B) nertralizer, coalescents and catalyst are added under 800~1000r/min rotating speed, continuously stirs mixing 20 minutes；
    C) thickener is put under 400~600r/min rotating speed and adjusts viscosity to 80~120pa.s；
    D) mill base is added under 400~600r/min rotating speed to adjust to required color and filter；
    The preparation of the finish paint comprises the following steps：
    1) portions of de-ionized water needed for formula ratio is put into material cylinder, then by aqueous acrylic emulsion, wetting dispersing agent, defoaming Agent, levelling agent input material cylinder, continuously stir mixing 10 minutes under 400~600r/min rotating speed；
    2) nertralizer is added under 800~1000r/min rotating speed, continuously stirs mixing 20 minutes；
    3) under 1000~1200r/min rotating speed put into white carbon, heat discoloration pigment, thickener, continuously stir mix to Lack 30 minutes and adjust viscosity to 150pa.s；
    4) remaining deionized water, mill base needed for input formula under 400~600r/min rotating speed, reduction viscosity to 80~ 120pa.s, and filtered after continuously stirring mixing 20 minutes.
CN201710702325.8A 2017-08-16 2017-08-16 water-based environment-friendly thermochromic crack paint and preparation method thereof Active CN107474658B (en)

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CN107474658B CN107474658B (en) 2019-12-13

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109229912A (en) * 2018-07-23 2019-01-18 企鹅兰登（北京）文化发展有限公司 A kind of printed matter and its packing container of reversible temperature-sensitive changing content
CN109337455A (en) * 2018-08-14 2019-02-15 广东瓦科新材料有限公司 A kind of production method of aqueous temperature-sensitive skin texture paint
CN109468040A (en) * 2018-10-11 2019-03-15 河北晨阳工贸集团有限公司 A kind of superpower three-dimensional hydronasty orange-peel paint
CN111978867A (en) * 2020-08-25 2020-11-24 上海一田涂料有限公司 Single-component water-based pearl coating and preparation process thereof
CN112852209A (en) * 2021-02-23 2021-05-28 江苏集萃智能液晶科技有限公司 Color-changing crack paint film and preparation method thereof
CN114015289A (en) * 2021-12-09 2022-02-08 温州市品达科装饰材料有限公司 Water-based crack paint, preparation method thereof and application method of crack paint
CN114213921A (en) * 2021-12-31 2022-03-22 三棵树(上海)新材料研究有限公司 Water-based crack artistic coating and preparation method thereof
CN114539859A (en) * 2021-12-31 2022-05-27 苏州弗克技术股份有限公司 Water-based crack paint with adjustable crack width

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CN104130648A (en) * 2014-07-22 2014-11-05 信和新材料股份有限公司 Aqueous crackle paint and coating technology thereof
CN104231814A (en) * 2014-10-17 2014-12-24 晟通科技集团有限公司 Environment-friendly water-based crack lacquer and application method thereof
CN104312339A (en) * 2014-11-19 2015-01-28 上海展辰涂料有限公司 Water-based crack lacquer product and manufacturing method thereof
CN104610820A (en) * 2015-01-13 2015-05-13 武汉怡可漆科技有限公司 Water-based crack lacquer as well as preparation method and construction method thereof
CN106928794A (en) * 2017-02-06 2017-07-07 广州市昌成陶瓷有限公司 A kind of heat discoloration coating and heat discoloration container

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Publication number Priority date Publication date Assignee Title
CN104130648A (en) * 2014-07-22 2014-11-05 信和新材料股份有限公司 Aqueous crackle paint and coating technology thereof
CN104231814A (en) * 2014-10-17 2014-12-24 晟通科技集团有限公司 Environment-friendly water-based crack lacquer and application method thereof
CN104312339A (en) * 2014-11-19 2015-01-28 上海展辰涂料有限公司 Water-based crack lacquer product and manufacturing method thereof
CN104610820A (en) * 2015-01-13 2015-05-13 武汉怡可漆科技有限公司 Water-based crack lacquer as well as preparation method and construction method thereof
CN106928794A (en) * 2017-02-06 2017-07-07 广州市昌成陶瓷有限公司 A kind of heat discoloration coating and heat discoloration container

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109229912A (en) * 2018-07-23 2019-01-18 企鹅兰登（北京）文化发展有限公司 A kind of printed matter and its packing container of reversible temperature-sensitive changing content
CN109337455A (en) * 2018-08-14 2019-02-15 广东瓦科新材料有限公司 A kind of production method of aqueous temperature-sensitive skin texture paint
CN109468040A (en) * 2018-10-11 2019-03-15 河北晨阳工贸集团有限公司 A kind of superpower three-dimensional hydronasty orange-peel paint
CN111978867A (en) * 2020-08-25 2020-11-24 上海一田涂料有限公司 Single-component water-based pearl coating and preparation process thereof
CN112852209A (en) * 2021-02-23 2021-05-28 江苏集萃智能液晶科技有限公司 Color-changing crack paint film and preparation method thereof
WO2022179358A1 (en) * 2021-02-23 2022-09-01 江苏集萃智能液晶科技有限公司 Color-changing crack paint film and preparation method therefor
CN114015289A (en) * 2021-12-09 2022-02-08 温州市品达科装饰材料有限公司 Water-based crack paint, preparation method thereof and application method of crack paint
CN114213921A (en) * 2021-12-31 2022-03-22 三棵树(上海)新材料研究有限公司 Water-based crack artistic coating and preparation method thereof
CN114539859A (en) * 2021-12-31 2022-05-27 苏州弗克技术股份有限公司 Water-based crack paint with adjustable crack width

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