CN107406807B - 制备对映体混合物的方法和对映体混合物 - Google Patents

制备对映体混合物的方法和对映体混合物 Download PDF

Info

Publication number
CN107406807B
CN107406807B CN201680014500.8A CN201680014500A CN107406807B CN 107406807 B CN107406807 B CN 107406807B CN 201680014500 A CN201680014500 A CN 201680014500A CN 107406807 B CN107406807 B CN 107406807B
Authority
CN
China
Prior art keywords
mono
salts
mixtures
acid
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201680014500.8A
Other languages
English (en)
Chinese (zh)
Other versions
CN107406807A (zh
Inventor
C·弗兰兹克
M·莱诺索加西亚
R·巴曼
T·格赖因德尔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN107406807A publication Critical patent/CN107406807A/zh
Application granted granted Critical
Publication of CN107406807B publication Critical patent/CN107406807B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/06—Preparation of carboxylic acid nitriles from N-formylated amino compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/26—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing carboxyl groups by reaction with HCN, or a salt thereof, and amines, or from aminonitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/24—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the same saturated acyclic carbon skeleton
    • C07C255/25—Aminoacetonitriles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201680014500.8A 2015-03-12 2016-03-02 制备对映体混合物的方法和对映体混合物 Active CN107406807B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP15158841 2015-03-12
EP15158841.5 2015-03-12
PCT/EP2016/054375 WO2016142228A1 (en) 2015-03-12 2016-03-02 Process for making mixtures of enantiomers, and mixtures of enantiomers

Publications (2)

Publication Number Publication Date
CN107406807A CN107406807A (zh) 2017-11-28
CN107406807B true CN107406807B (zh) 2021-03-23

Family

ID=52648924

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201680014500.8A Active CN107406807B (zh) 2015-03-12 2016-03-02 制备对映体混合物的方法和对映体混合物

Country Status (12)

Country Link
US (1) US10619125B2 (https=)
EP (1) EP3268348B1 (https=)
JP (1) JP6727225B2 (https=)
KR (1) KR102694078B1 (https=)
CN (1) CN107406807B (https=)
BR (1) BR112017019108A2 (https=)
CA (1) CA2976716A1 (https=)
ES (1) ES2881309T3 (https=)
MX (1) MX2017011725A (https=)
MY (1) MY189265A (https=)
RU (1) RU2722803C2 (https=)
WO (1) WO2016142228A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2882568T3 (es) * 2017-04-27 2021-12-02 Basf Se Recipiente que comprende una composición detergente que contiene sales de mgda y glda
JP7245337B2 (ja) * 2018-12-21 2023-03-23 ヌーリオン ケミカルズ インターナショナル ベスローテン フェノーツハップ メチルグリシンｎ，ｎ二酢酸の脆弱相組成物
WO2021175701A1 (en) * 2020-03-03 2021-09-10 Basf Se Process for manufacture of a complexing agent
CN117658857B (zh) * 2022-08-25 2025-11-04 万华化学集团股份有限公司 存储稳定的甲基甘氨酸-n,n-二乙腈组合物、制备方法及其用途

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010139755A1 (en) * 2009-06-05 2010-12-09 Akzo Nobel Chemicals International B.V. Process to prepare a chelating agent or precursor thereof using a cyanide salt
WO2011080540A1 (en) * 2009-12-30 2011-07-07 Ecolab Inc. Phosphate substitutes for membrane-compatible cleaning and/or detergent compositions
WO2011100344A1 (en) * 2010-02-09 2011-08-18 Basf Se Detergent composition
WO2012150155A1 (de) * 2011-05-03 2012-11-08 Basf Se Verfahren zur herstellung eines kristallinen l-mgda-trialkalimetallsalzes

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5837663A (en) 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
DE19819187A1 (de) 1998-04-30 1999-11-11 Henkel Kgaa Festes maschinelles Geschirrspülmittel mit Phosphat und kristallinen schichtförmigen Silikaten
DE102005021055A1 (de) * 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
GB0522659D0 (en) * 2005-11-07 2005-12-14 Reckitt Benckiser Nv Delivery cartridge
DE102007019458A1 (de) * 2007-04-25 2008-10-30 Basf Se Phosphatfreies Maschinengeschirrspülmittel mit ausgezeichneter Klarspülleistung
CA2696669C (en) * 2007-08-17 2016-05-24 Akzo Nobel N.V. Alkali metal salt of glutamic acid n,n-diacetic acid, a process to prepare such salt, and the use thereof
GB0716228D0 (en) * 2007-08-20 2007-09-26 Reckitt Benckiser Nv Detergent composition
US20110080540A1 (en) * 2008-07-08 2011-04-07 Sharp Kabushiki Kaisha Lighting device and liquid crystal display device
WO2011076769A1 (en) 2009-12-24 2011-06-30 Akzo Nobel Chemicals International B.V. Coated particles of a glumatic acid n,n-diacetate chelating agent
EP2568808B1 (de) * 2010-05-14 2016-06-22 COMPO GmbH Köderformulierungen zur bekämpfung von schnecken
CA2820944C (en) 2010-12-17 2018-11-27 Akzo Nobel Chemicals International B.V. Fluid suitable for treatment of carbonate formations containing a chelating agent
AU2011200525B8 (en) 2010-12-17 2016-10-13 Akzo Nobel Chemicals International B.V. Environmentally friendly stimulation fluids, processes to create wormholes in carbonate reservoirs, and processes to remove wellbore damage in carbonate reservoirs
RU2598850C2 (ru) * 2011-04-04 2016-09-27 Басф Се Способ получения водных растворов трехосновных солей щелочного металла метилглицин-n,n-диуксусной кислоты
US8802894B2 (en) * 2011-04-04 2014-08-12 Basf Se Process for the preparation of aqueous solutions of methylglycine-N,N-diacetic acid trialkali metal salts
US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
DE102011084934A1 (de) 2011-10-21 2013-04-25 Henkel Ag & Co. Kgaa Klarspül- und Geschirrspülmittel
US9738594B2 (en) 2012-12-14 2017-08-22 Akzo Nobel Chemicals International B.V. Crystalline particles of salts of glutamic acid N,N-diacetic acid
WO2014090942A1 (en) 2012-12-14 2014-06-19 Akzo Nobel Chemicals International B.V. Crystalline particles of glutamic acid n,n-diacetic acid
PL2997121T3 (pl) 2013-05-17 2019-05-31 Unilever Nv Kompozycja detergentowa do automatycznego mycia naczyń
KR20160012209A (ko) 2013-05-27 2016-02-02 바스프 에스이 고농도의 착물화제를 함유하는 수용액
BR112015029557A2 (pt) 2013-05-27 2020-03-10 Basf Se solução aquosa, processo para fabricação de uma solução aquosa, e, uso de uma solução aquosa
CN105358669A (zh) * 2013-07-04 2016-02-24 巴斯夫欧洲公司 清洗器皿的方法
CA2921800C (en) * 2013-09-09 2018-10-02 Ecolab Usa Inc. Synergistic stain removal through novel chelator combination
MX394036B (es) 2013-09-09 2025-03-24 Ecolab Usa Inc Eliminacion sinergica de manchas a traves de una combinacion de quelacion novedosa.
US9802884B2 (en) * 2013-09-13 2017-10-31 Basf Se Mixtures of MGDA enantiomers, and process for making such mixtures

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010139755A1 (en) * 2009-06-05 2010-12-09 Akzo Nobel Chemicals International B.V. Process to prepare a chelating agent or precursor thereof using a cyanide salt
WO2011080540A1 (en) * 2009-12-30 2011-07-07 Ecolab Inc. Phosphate substitutes for membrane-compatible cleaning and/or detergent compositions
WO2011100344A1 (en) * 2010-02-09 2011-08-18 Basf Se Detergent composition
WO2012150155A1 (de) * 2011-05-03 2012-11-08 Basf Se Verfahren zur herstellung eines kristallinen l-mgda-trialkalimetallsalzes

Also Published As

Publication number Publication date
MX2017011725A (es) 2017-11-13
CN107406807A (zh) 2017-11-28
WO2016142228A1 (en) 2016-09-15
KR20170128398A (ko) 2017-11-22
JP2018507898A (ja) 2018-03-22
BR112017019108A2 (pt) 2018-04-17
ES2881309T3 (es) 2021-11-29
JP6727225B2 (ja) 2020-07-22
RU2722803C2 (ru) 2020-06-03
RU2017136081A3 (https=) 2019-07-29
US20180237728A1 (en) 2018-08-23
US10619125B2 (en) 2020-04-14
CA2976716A1 (en) 2016-09-15
KR102694078B1 (ko) 2024-08-09
EP3268348A1 (en) 2018-01-17
MY189265A (en) 2022-01-31
RU2017136081A (ru) 2019-04-12
EP3268348B1 (en) 2021-05-12

Similar Documents

Publication Publication Date Title
KR102360294B1 (ko) 거울상이성질체의 혼합물, 및 이러한 혼합물의 제조 방법
CN109072135B (zh) 螯合剂的混合物和制备该类混合物的方法
CN107406807B (zh) 制备对映体混合物的方法和对映体混合物
JP6847034B2 (ja) アミノカルボン酸のトリアルカリ金属塩の溶液、その製造及び使用方法
JP6808637B2 (ja) キレート剤の混合物、及び該混合物の製造方法
EP3216781A1 (en) Mixtures containing potassium salts of methyl glycine diacetic acid

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant