CA2976716A1 - Process for making mixtures of enantiomers, and mixtures of enantiomers - Google Patents

Process for making mixtures of enantiomers, and mixtures of enantiomers Download PDF

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Publication number
CA2976716A1
CA2976716A1 CA2976716A CA2976716A CA2976716A1 CA 2976716 A1 CA2976716 A1 CA 2976716A1 CA 2976716 A CA2976716 A CA 2976716A CA 2976716 A CA2976716 A CA 2976716A CA 2976716 A1 CA2976716 A1 CA 2976716A1
Authority
CA
Canada
Prior art keywords
mono
mixtures
range
acid
tri
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2976716A
Other languages
English (en)
French (fr)
Inventor
Constanze FRANZKE
Marta Reinoso Garcia
Robert Baumann
Thomas Greindl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CA2976716A1 publication Critical patent/CA2976716A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/26—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing carboxyl groups by reaction with HCN, or a salt thereof, and amines, or from aminonitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/06—Preparation of carboxylic acid nitriles from N-formylated amino compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/24—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the same saturated acyclic carbon skeleton
    • C07C255/25—Aminoacetonitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA2976716A 2015-03-12 2016-03-02 Process for making mixtures of enantiomers, and mixtures of enantiomers Abandoned CA2976716A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP15158841 2015-03-12
EP15158841.5 2015-03-12
PCT/EP2016/054375 WO2016142228A1 (en) 2015-03-12 2016-03-02 Process for making mixtures of enantiomers, and mixtures of enantiomers

Publications (1)

Publication Number Publication Date
CA2976716A1 true CA2976716A1 (en) 2016-09-15

Family

ID=52648924

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2976716A Abandoned CA2976716A1 (en) 2015-03-12 2016-03-02 Process for making mixtures of enantiomers, and mixtures of enantiomers

Country Status (12)

Country Link
US (1) US10619125B2 (https=)
EP (1) EP3268348B1 (https=)
JP (1) JP6727225B2 (https=)
KR (1) KR102694078B1 (https=)
CN (1) CN107406807B (https=)
BR (1) BR112017019108A2 (https=)
CA (1) CA2976716A1 (https=)
ES (1) ES2881309T3 (https=)
MX (1) MX2017011725A (https=)
MY (1) MY189265A (https=)
RU (1) RU2722803C2 (https=)
WO (1) WO2016142228A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110582558B (zh) * 2017-04-27 2021-10-26 巴斯夫欧洲公司 包含含有mgda和glda的盐的洗涤剂组合物的容器
WO2020127349A1 (en) * 2018-12-21 2020-06-25 Nouryon Chemicals International B.V. Crumbly phase composition of methylglycine n,n diacetic acid
EP4114822B1 (en) * 2020-03-03 2024-04-17 Basf Se Process for manufacture of a complexing agent
CN117658857B (zh) * 2022-08-25 2025-11-04 万华化学集团股份有限公司 存储稳定的甲基甘氨酸-n,n-二乙腈组合物、制备方法及其用途

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5837663A (en) 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
DE19819187A1 (de) 1998-04-30 1999-11-11 Henkel Kgaa Festes maschinelles Geschirrspülmittel mit Phosphat und kristallinen schichtförmigen Silikaten
DE102005021055A1 (de) * 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
GB0522659D0 (en) * 2005-11-07 2005-12-14 Reckitt Benckiser Nv Delivery cartridge
DE102007019458A1 (de) * 2007-04-25 2008-10-30 Basf Se Phosphatfreies Maschinengeschirrspülmittel mit ausgezeichneter Klarspülleistung
US9080133B2 (en) * 2007-08-17 2015-07-14 Akzo Nobel N.V. Glutamic acid N,N-diacetic amide, glutamic acid N-acetic amide N-acetonitrile, alkali metal salts thereof, process to prepare them and their use
GB0716228D0 (en) * 2007-08-20 2007-09-26 Reckitt Benckiser Nv Detergent composition
US20110080540A1 (en) * 2008-07-08 2011-04-07 Sharp Kabushiki Kaisha Lighting device and liquid crystal display device
BRPI1009084A2 (pt) * 2009-06-05 2016-03-01 Akzo Nobel Chemicals Int Bv processo compreendendo a reação de cianeto com um aminoacido e um aldeido
US9096820B2 (en) 2009-12-24 2015-08-04 Akzo Nobel Chemicals International B.V. Coated particles of a glumatic acid N,N-diacetate chelating agent
EP2519623B2 (en) 2009-12-30 2019-03-20 Ecolab Inc. Phosphate substitutes for membrane-compatible cleaning and/or detergent compositions
MX2012009162A (es) * 2010-02-09 2012-10-03 Basf Se Composicion detergente.
WO2011141566A2 (de) * 2010-05-14 2011-11-17 Compo Gmbh & Co. Kg Köderformulierungen zur bekämpfung von schnecken
JP2014504321A (ja) 2010-12-17 2014-02-20 アクゾ ノーベル ケミカルズ インターナショナル ベスローテン フエンノートシャップ キレート剤を含有する炭酸塩地層の処理に適した流体
AU2011200525B8 (en) 2010-12-17 2016-10-13 Akzo Nobel Chemicals International B.V. Environmentally friendly stimulation fluids, processes to create wormholes in carbonate reservoirs, and processes to remove wellbore damage in carbonate reservoirs
BR112013023846A2 (pt) * 2011-04-04 2020-11-10 Basf Se processo para a preparação de soluções aquosas de sais de tri-metal-alcalino de ácido metilglicina-n,n-diacético
US8802894B2 (en) * 2011-04-04 2014-08-12 Basf Se Process for the preparation of aqueous solutions of methylglycine-N,N-diacetic acid trialkali metal salts
ES2660773T5 (es) 2011-05-03 2021-11-25 Basf Se Procedimiento para la preparación de una sal cristalina trialcalino-metálica de L-MGDA
US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
DE102011084934A1 (de) 2011-10-21 2013-04-25 Henkel Ag & Co. Kgaa Klarspül- und Geschirrspülmittel
EP2931699A1 (en) 2012-12-14 2015-10-21 Akzo Nobel Chemicals International B.V. Crystalline particles of glutamic acid n,n-diacetic acid
US9738594B2 (en) 2012-12-14 2017-08-22 Akzo Nobel Chemicals International B.V. Crystalline particles of salts of glutamic acid N,N-diacetic acid
WO2014184280A1 (en) 2013-05-17 2014-11-20 Unilever N.V. Machine dishwash detergent composition
EP3004316B1 (en) * 2013-05-27 2017-03-22 Basf Se Aqueous solutions containing a complexing agent in high concentration
RU2656211C2 (ru) * 2013-05-27 2018-06-01 Басф Се Водные растворы, содержащие комплексообразующий агент в высокой концентрации
US9938489B2 (en) * 2013-07-04 2018-04-10 Basf Se Process for cleaning dishware
AU2013399899B2 (en) * 2013-09-09 2016-10-13 Ecolab Usa Inc. Synergistic stain removal through novel chelator combination
ES2982202T3 (es) * 2013-09-09 2024-10-15 Ecolab Usa Inc Método de lavado de vajilla basado en la eliminación sinérgica de manchas mediante una nueva combinación de quelantes
ES2646288T3 (es) 2013-09-13 2017-12-13 Basf Se Mezclas de enantiómeros y procedimiento para elaborar dichas mezclas

Also Published As

Publication number Publication date
RU2017136081A (ru) 2019-04-12
EP3268348B1 (en) 2021-05-12
ES2881309T3 (es) 2021-11-29
MY189265A (en) 2022-01-31
US20180237728A1 (en) 2018-08-23
KR20170128398A (ko) 2017-11-22
US10619125B2 (en) 2020-04-14
CN107406807B (zh) 2021-03-23
KR102694078B1 (ko) 2024-08-09
WO2016142228A1 (en) 2016-09-15
EP3268348A1 (en) 2018-01-17
JP2018507898A (ja) 2018-03-22
RU2017136081A3 (https=) 2019-07-29
CN107406807A (zh) 2017-11-28
JP6727225B2 (ja) 2020-07-22
RU2722803C2 (ru) 2020-06-03
BR112017019108A2 (pt) 2018-04-17
MX2017011725A (es) 2017-11-13

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EP3268348B1 (en) Process for making mixtures of enantiomers, and mixtures of enantiomers
EP3207025B1 (en) Solutions of trialkali metal salts of aminocarboxylic acids, their manufacture and use
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Legal Events

Date Code Title Description
FZDE Discontinued

Effective date: 20220525