CN107382294A - Beautiful porcelain of China and preparation method thereof - Google Patents
Beautiful porcelain of China and preparation method thereof Download PDFInfo
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- CN107382294A CN107382294A CN201710842629.4A CN201710842629A CN107382294A CN 107382294 A CN107382294 A CN 107382294A CN 201710842629 A CN201710842629 A CN 201710842629A CN 107382294 A CN107382294 A CN 107382294A
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- 229910052573 porcelain Inorganic materials 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 210000000988 bone and bone Anatomy 0.000 claims abstract description 10
- 229910001634 calcium fluoride Inorganic materials 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 239000000126 substance Substances 0.000 claims abstract description 7
- 239000000758 substrate Substances 0.000 claims abstract description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 3
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 3
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 3
- 239000012535 impurity Substances 0.000 claims abstract description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 3
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 3
- 239000002689 soil Substances 0.000 claims description 22
- 239000002994 raw material Substances 0.000 claims description 21
- 238000000498 ball milling Methods 0.000 claims description 12
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
- 239000010453 quartz Substances 0.000 claims description 9
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical class [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 8
- 239000004927 clay Substances 0.000 claims description 7
- 239000010433 feldspar Substances 0.000 claims description 7
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 6
- 239000012065 filter cake Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 238000010304 firing Methods 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 239000011265 semifinished product Substances 0.000 claims description 4
- 239000000919 ceramic Substances 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000005286 illumination Methods 0.000 abstract description 3
- 239000003973 paint Substances 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 9
- 239000002932 luster Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000010436 fluorite Substances 0.000 description 4
- 235000015895 biscuits Nutrition 0.000 description 3
- 229910052761 rare earth metal Inorganic materials 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- -1 rare earth ion Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/447—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/447—Phosphates or phosphites, e.g. orthophosphate or hypophosphite
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Materials Engineering (AREA)
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- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Glass Compositions (AREA)
Abstract
The present invention relates to a kind of beautiful porcelain of China and preparation method thereof, belong to ceramic technology field.The beautiful porcelain of China of the present invention, its base substrate chemical composition percentage by weight are：SiO239~43%, Al2O310~15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%, CaF21.2 2%, Pr2O30.02~0.08%, surplus is impurity.The beautiful porcelain of China of the present invention, formula is simple, has the transparency of Bone China, and glaze paint is smooth, glows faint yellow, the also bandwagon effect with artistic porcelain under light illumination；Invention also provides a kind of simple and easy preparation method.
Description
Technical field
The present invention relates to a kind of beautiful porcelain of China and preparation method thereof, belong to ceramic technology field.
Background technology
With the raising of living standards of the people and appreciation level, the outward appearance and dicoration of domestic ceramics increasingly cause people
Concern, emerged many new porcelain kinds, such as steatite ceramic, Shandong jade porcelain, quartz enriched porcelain and Bone China, made domestic ceramic product
More styles, the development trend of multiscale are presented, the color of porcelain gradually enriches also with the development of ceramics.
Traditional ceramic whiteware color and luster is single, sight is poor, has had many Ceramics Enterprises to be improved the formula of porcelain, but
The product developed is only applicable to masses, all not exclusively for women create it is a it is especially soft, brief without lose it is luxurious
Product.
The content of the invention
It is an object of the invention to provide a kind of beautiful porcelain of China, and it is formulated simple, the transparency with Bone China, glaze paint light
Profit, faint yellow, the also bandwagon effect with artistic porcelain is glowed under light illumination；Invention also provides a kind of simple and easy system
Preparation Method.
The beautiful porcelain of China of the present invention, its base substrate chemical composition percentage by weight are：SiO239~43%, Al2O310~
15%th, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%,
CaF21.2-2%, Pr2O30.02~0.08%, surplus is impurity.
Described magnificent beautiful porcelain, is made up of the raw material of following weight percentage：Synthos 38~46%, feldspar 8~
13%th, quartz 8~14%, Datong District's soil 13~18%, elutriation Longyan clay 6~15%, Guangdong black mud 2~8%, Laiyang soil 1~5%
With lane soil 1~5%；Using the gross weight of above raw material as 100% metering, additional CaF22-3%, Pr2O30.05~0.1%.
Preferably, described magnificent beautiful porcelain, is made up of the raw material of following weight percentage：Synthos 38~43%, length
Stone 8~12%, quartz 8~11%, Datong District's soil 13~15%, elutriation Longyan clay 6~9%, Guangdong black mud 2~6%, Laiyang soil 1
~4% and lane soil 1~4%；Using the gross weight of above raw material as 100% metering, additional CaF22-3%, Pr2O30.05~
0.1%.
The preparation method of described magnificent beautiful porcelain, comprises the following steps：
(1) after raw material is mixed, ball milling, then iron removaling, sieving, press filtration, pugging, compacting are carried out；
(2) semi-finished product after step (1) is suppressed carry out biscuiting at 1250-1280 DEG C；
(3) to the base substrate glazing after step (2) biscuiting；
(4) semi-finished product after step (3) glazing are subjected to secondary glaze firing at 1150-1180 DEG C, obtain described Hua Yu
Porcelain.
In step (1), Ball-milling Time is 60-70 hours, ball milling fineness >=87%.
In step (1), during pugging, by filter cake white silk into the mud bar that moisture is 20-25%.
In step (3), glaze used is Bone China high gloss leadless glaze during glazing.
Present invention raw material based on the raw materials such as the various clays such as synthos and feldspar, quartz, Datong District's soil, in high temperature
Physical reaction is carried out during biscuiting and forms solid solution.Then produced according to rare earth element Pr is exclusive because its wavelength is long
Chromophoric mechanism, by rare earth ion all unique texture and property in itself, fluorite lattice is entered under high temperature action, not
On the premise of destroying fluorite octahedron lattice, the calcium in fluorite is substituted by Pr and yellow is wrapped up to the octahedra monocrystalline into fluorite
Inside lattice (it uses inorganic coating structure), the parcel Huang of stable color development is formd, it has no effect on the light transmittance of porcelain；And tie
Optical principle is closed, makes full use of the refraction principle of light, further lifts the purity and grade of raw material, adjustment and optimization body recipe
In potassium, sodium content, the magnificent beautiful porcelain developed sends light milk yellow, has higher translucence, and glaze paint is smooth bright,
Entire body is more glittering and translucent, gentle as beautiful, Huang is shown in soft, brief luxurious without losing, outward appearance is high-end, generous, is traditional potter
Skill is combined later perfect product with modern science and technology, can make as the first choice of porcelain for women.
The present invention compared with prior art, has the advantages that：
(1) formula is simple, scientific and reasonable, and the magnificent beautiful ceramic glaze surface brightness height of preparation, heat endurance are good, glow under light illumination
Faint yellow, Lead and cadmium rate is zero；
(2) the magnificent beautiful porcelain prepared adds the color and luster kind of Bone China, further improves the class of Bone China, has wide
General applicability, it is particularly suitable for doing gift tea set, vase etc., there is the bandwagon effect of artistic porcelain；
(3) preparation method of the magnificent beautiful porcelain described in employs oxidizing flame calcining system, and controlling of production process difficulty is small, easily behaviour
Make, beneficial to large-scale production.
Embodiment
With reference to embodiment, the present invention is further illustrated, but it is not intended to limit the implementation of the present invention.
Embodiment 1
A kind of beautiful porcelain of China, is made up of the raw material of following weight percentage：Synthos 38%, feldspar 12%, Datong District's soil
17%th, quartz 12%, elutriation Longyan clay 10%, Guangdong black mud 6%, Laiyang soil 4% and lane soil 1%, additional CaF22%th,
Pr2O30.05%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 60 hours, and ball milling fineness is
87%, then iron removaling, sieving, press filtration, then with vacuum deairing machine be 21% mud bar into moisture filter cake white silk, suppressed with roller press
Into 8 cun of square positions, the biscuiting at a temperature of 1265 ± 15 DEG C, the beautiful porcelain biscuit of faint yellow China is obtained, then glazing (Bone China during glazing
With high gloss leadless glaze), the secondary glaze firing at a temperature of 1165 ± 15 DEG C, by high-temperature chemical reaction, color and luster is passed through glaze
Layer is refracted to product surface, and it is flat to obtain the smooth beautiful porcelain 8 of faint yellow China as beautiful.
Embodiment 2
A kind of beautiful porcelain of China, is made up of the raw material of following weight percentage：Synthos 42%, feldspar 11%, Datong District's soil
16%th, quartz 12%, elutriation Longyan clay 8%, Guangdong black mud 6%, Laiyang soil 4% and lane soil 1%, additional CaF23%th,
Pr2O30.08%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 65 hours, and ball milling fineness is
90%, then iron removaling, sieving, press filtration, then with vacuum deairing machine be 22% mud bar into moisture filter cake white silk, suppressed with roller press
Into 6 cun of square positions, the biscuiting at a temperature of 1265 ± 15 DEG C, the beautiful porcelain biscuit of faint yellow China is obtained, then glazing (Bone China during glazing
With high gloss leadless glaze), the secondary glaze firing at a temperature of 1165 ± 15 DEG C, by high-temperature chemical reaction, color and luster is passed through glaze
Layer is refracted to product surface, and it is flat to obtain the smooth beautiful porcelain 6 of faint yellow China as beautiful.
Embodiment 3
A kind of beautiful porcelain of China, is made up of the raw material of following weight percentage：Synthos 46%, feldspar 10%, Datong District's soil
15%th, quartz 12%, elutriation Longyan clay 8%, Guangdong black mud 5%, Laiyang soil 3% and lane soil 1%, additional CaF22.5%th,
Pr2O30.1%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 70 hours, and ball milling fineness is
88%, then iron removaling, sieving, press filtration, then with vacuum deairing machine be 25% mud bar into moisture filter cake white silk, suppressed with roller press
Into 5 cun of bowls, the biscuiting at a temperature of 1265 ± 15 DEG C obtains the beautiful porcelain biscuit of faint yellow China, and then glazing (is used during glazing with Bone China
High gloss leadless glaze), the secondary glaze firing at a temperature of 1165 ± 15 DEG C, by high-temperature chemical reaction, color and luster is passed through glaze layer
Product surface is refracted to, is obtained smooth such as the beautiful beautiful 5 flat bowl of porcelain of faint yellow China.
Raw materials used chemical weight percentage composition, is shown in Table 1.
The raw materials used chemical weight percentage composition of table 1
The chemical weight percentage composition of product prepared by embodiment 1-3, is shown in Table 2.
The chemical weight percentage composition of product prepared by the embodiment 1-3 of table 2
Claims (7)
- A kind of 1. beautiful porcelain of China, it is characterised in that：Base substrate chemical composition percentage by weight is：SiO239~43%, Al2O310~ 15%th, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%, CaF21.2-2%, Pr2O30.02~0.08%, surplus is impurity.
- 2. the beautiful porcelain of China according to claim 1, it is characterised in that be made up of the raw material of following weight percentage：Calcium phosphate Salt 38~46%, feldspar 8~13%, quartz 8~14%, Datong District's soil 13~18%, elutriation Longyan clay 6~15%, Guangdong black mud 2 ~8%, Laiyang soil 1~5% and lane soil 1~5%；Using the gross weight of above raw material as 100% metering, additional CaF2 2- 3%th, Pr2O30.05~0.1%.
- 3. the beautiful porcelain of China according to claim 1, it is characterised in that be made up of the raw material of following weight percentage：Calcium phosphate Salt 38~46%, feldspar 8~13%, quartz 8~14%, Datong District's soil 13~18%, elutriation Longyan clay 6~15%, Guangdong black mud 2 ~8%, Laiyang soil 1~5% and lane soil 1~5%；Using the gross weight of above raw material as 100% metering, additional CaF2 2- 3%th, Pr2O30.05~0.1%.
- 4. the preparation method of any described magnificent beautiful porcelain of a kind of claim 1-3, it is characterised in that comprise the following steps：(1) after raw material is mixed, ball milling, then iron removaling, sieving, press filtration, pugging, compacting are carried out；(2) semi-finished product after step (1) is suppressed carry out biscuiting at 1250-1280 DEG C；(3) to the base substrate glazing after step (2) biscuiting；(4) semi-finished product after step (3) glazing are subjected to secondary glaze firing at 1150-1180 DEG C, obtain described magnificent beautiful porcelain.
- 5. the preparation method of the beautiful porcelain of China according to claim 4, it is characterised in that：In step (1), Ball-milling Time 60- 70 hours, ball milling fineness >=87%.
- 6. the preparation method of the beautiful porcelain of China according to claim 4, it is characterised in that：In step (1), during pugging, by filter cake Practice into the mud bar that moisture is 20-25%.
- 7. the preparation method of the beautiful porcelain of China according to claim 4, it is characterised in that：In step (3), glaze used during glazing Expect for Bone China high gloss leadless glaze.
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| CN201710842629.4A CN107382294B (en) | 2017-09-18 | 2017-09-18 | Magnificent jade porcelain and preparation method thereof |
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| CN201710842629.4A CN107382294B (en) | 2017-09-18 | 2017-09-18 | Magnificent jade porcelain and preparation method thereof |
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| CN107382294B CN107382294B (en) | 2019-06-11 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112794707A (en) * | 2021-04-14 | 2021-05-14 | 佛山市东鹏陶瓷有限公司 | High-whiteness and high-strength light-transmitting ceramic tile and preparation method thereof |
| CN114262207A (en) * | 2021-12-31 | 2022-04-01 | 四川美术学院 | Composite material health-care ceramic tea set and preparation method thereof |
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|---|---|---|---|---|
| CN1935738A (en) * | 2006-10-12 | 2007-03-28 | 淄博华光瓷业有限公司 | Bone-green porcelain |
| CN101913843A (en) * | 2010-07-23 | 2010-12-15 | 华南理工大学 | Preparation method of emerald ceramic |
| CN102515704A (en) * | 2011-12-27 | 2012-06-27 | 淄博华光陶瓷科技文化有限公司 | Hua celadon and preparation method thereof |
-
2017
- 2017-09-18 CN CN201710842629.4A patent/CN107382294B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1935738A (en) * | 2006-10-12 | 2007-03-28 | 淄博华光瓷业有限公司 | Bone-green porcelain |
| CN101913843A (en) * | 2010-07-23 | 2010-12-15 | 华南理工大学 | Preparation method of emerald ceramic |
| CN102515704A (en) * | 2011-12-27 | 2012-06-27 | 淄博华光陶瓷科技文化有限公司 | Hua celadon and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112794707A (en) * | 2021-04-14 | 2021-05-14 | 佛山市东鹏陶瓷有限公司 | High-whiteness and high-strength light-transmitting ceramic tile and preparation method thereof |
| CN114262207A (en) * | 2021-12-31 | 2022-04-01 | 四川美术学院 | Composite material health-care ceramic tea set and preparation method thereof |
| CN114262207B (en) * | 2021-12-31 | 2022-08-12 | 四川美术学院 | Composite material health-care ceramic tea set and preparation method thereof |
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