CN107382294B - Magnificent jade porcelain and preparation method thereof - Google Patents

Magnificent jade porcelain and preparation method thereof Download PDF

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CN107382294B
CN107382294B CN201710842629.4A CN201710842629A CN107382294B CN 107382294 B CN107382294 B CN 107382294B CN 201710842629 A CN201710842629 A CN 201710842629A CN 107382294 B CN107382294 B CN 107382294B
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china
porcelain
beautiful
beautiful porcelain
glaze
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CN107382294A (en
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张宁
孟莉
李晓亮
王德亮
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Zibo Huaguangguo Porcelain Technology And Culture Co Ltd
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
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    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/04Clay; Kaolin
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    • C04B33/24Manufacture of porcelain or white ware
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/447Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
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    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/447Phosphates or phosphites, e.g. orthophosphate, hypophosphite

Abstract

The present invention relates to beautiful porcelain of a kind of China and preparation method thereof, belong to ceramic technology field.The beautiful porcelain of China of the present invention, green body chemical composition weight percent are as follows: SiO239~43%, Al2O310~15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%, CaF21.2-2%, Pr2O30.02~0.08%, surplus is impurity.The beautiful porcelain of China of the present invention, formula is simple, and the transparency with Bone China, glaze is smooth, glow under light illumination it is faint yellow, also with the bandwagon effect of artistic porcelain;Invention also provides a kind of simple and easy preparation methods.

Description

Magnificent jade porcelain and preparation method thereof
Technical field
The present invention relates to beautiful porcelain of a kind of China and preparation method thereof, belong to ceramic technology field.
Background technique
With the raising of living standards of the people and appreciation level, the appearance and dicoration of domestic ceramics increasingly cause people Concern, emerged many new porcelain kinds, such as steatite ceramic, Shandong jade porcelain, quartz enriched porcelain and Bone China, made domestic ceramic product The development trend of windy lattice, multiscale is presented, the color of porcelain is gradually enriched also with the development of ceramics.
Traditional ceramic whiteware color is single, ornamental value is poor, has had many Ceramics Enterprises to improve the formula of porcelain, but The product developed is only applicable to masses, does not all create exclusively for women a especially soft, brief luxurious without losing Product.
Summary of the invention
The purpose of the present invention is to provide a kind of beautiful porcelain of China, and formula is simple, the transparency with Bone China, glaze light Profit, glow under light illumination it is faint yellow, also with artistic porcelain bandwagon effect;Invention also provides a kind of simple and easy systems Preparation Method.
The beautiful porcelain of China of the present invention, green body chemical composition weight percent are as follows: SiO239~43%, Al2O310~ 15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%, CaF21.2-2%, Pr2O30.02~0.08%, surplus is impurity.
The beautiful porcelain of the China, is made of the raw material of following weight percentage: synthos 38~46%, feldspar 8~ 13%, quartz 8~14%, Datong District's soil 13~18%, elutriation Longyan clay 6~15%, Guangdong black mud 2~8%, Laiyang soil 1~5% With lane soil 1~5%;It is 100% metering, additional CaF with the total weight of the above raw material22-3%, Pr2O30.05~0.1%.
Preferably, the beautiful porcelain of the China, is made of the raw material of following weight percentage: synthos 38~43%, length Stone 8~12%, Datong District's soil 13~15%, eluriates Longyan clay 6~9%, Guangdong black mud 2~6%, Laiyang soil 1 at quartz 8~11% ~4% and lane soil 1~4%;It is 100% metering, additional CaF with the total weight of the above raw material22-3%, Pr2O30.05~ 0.1%.
The preparation method of the beautiful porcelain of the China, comprising the following steps:
(1) after mixing raw material, ball milling is carried out, then removes iron, sieving, filters pressing, pugging, compacting;
(2) step (1) pressed semi-finished product are subjected to biscuiting at 1250-1280 DEG C;
(3) to the green body glazing after step (2) biscuiting;
(4) semi-finished product after step (3) glazing are subjected at 1150-1180 DEG C secondary glaze firing, obtain the Hua Yu Porcelain.
In step (1), Ball-milling Time is 60-70 hours, ball milling fineness >=87%.
In step (1), when pugging, filter cake is practiced to the mud item for being 20-25% at moisture.
In step (3), when glazing, glaze used was Bone China high gloss leadless glaze.
The present invention is using raw materials such as the various clays such as synthos and feldspar, quartz, Datong District's soil as basic raw material, in high temperature Physical reaction is carried out during biscuiting forms solid solution.Then it is generated according to rare earth element Pr is exclusive since its wavelength is long Chromophoric mechanism, by all unique textures of rare earth ion itself and property, under high temperature action enter fluorite lattice, not Under the premise of destroying fluorite octahedron lattice, the calcium in fluorite is substituted by Pr and yellow is wrapped up to the octahedra monocrystalline into fluorite Inside lattice (it uses inorganic coating structure), the package for foring stable color development is yellow, has no effect on the light transmittance of porcelain;And it ties Optical principle is closed, the refraction principle of light is made full use of, further promotes the purity and grade of raw material, adjustment and optimization body recipe In potassium, sodium content, the beautiful porcelain of China developed issues light milk yellow, and translucence with higher, glaze smoothness is bright, Entire body is more glittering and translucent, gentle as beautiful, it is soft in show Huang, brief luxurious without losing, appearance is high-end, generous, is traditional potter Skill combines later perfect product with modern science and technology, can make as the first choice of porcelain for women.
Compared with the prior art, the present invention has the following beneficial effects:
(1) formula is simple, scientific and reasonable, and the beautiful ceramic glaze surface brightness of the China of preparation is high, thermal stability is good, glows under light illumination Faint yellow, Lead and cadmium rate is zero;
(2) the beautiful porcelain of the China of preparation increases the color kind of Bone China, further improves the class of Bone China, has wide General applicability is particularly suitable for doing gift tea set, vase etc., the bandwagon effect with artistic porcelain;
(3) preparation method of the beautiful porcelain of China described in uses oxidizing flame calcining system, and controlling of production process difficulty is small, easily grasps Make, is conducive to large-scale production.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but it is not intended to limit implementation of the invention.
Embodiment 1
A kind of beautiful porcelain of China, is made of the raw material of following weight percentage: synthos 38%, feldspar 12%, Datong District's soil 17%, quartz 12%, elutriation Longyan clay 10%, Guangdong black mud 6%, Laiyang soil 4% and lane soil 1%, additional CaF22%, Pr2O30.05%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 60 hours, and ball milling fineness is 87%, then remove iron, sieving, filters pressing, then with vacuum deairing machine filter cake practiced at moisture be 21% mud item, suppressed with roller press At 8 cun of square positions, in 1265 ± 15 DEG C of at a temperature of biscuiting, the beautiful porcelain biscuit of faint yellow China is obtained, then glazing (Bone China when glazing With high gloss leadless glaze), make color through glaze by high-temperature chemical reaction in 1165 ± 15 DEG C of at a temperature of secondary glaze firing Layer is refracted to product surface, and it is flat to obtain the smooth beautiful porcelain 8 of faint yellow China as beautiful.
Embodiment 2
A kind of beautiful porcelain of China, is made of the raw material of following weight percentage: synthos 42%, feldspar 11%, Datong District's soil 16%, quartz 12%, elutriation Longyan clay 8%, Guangdong black mud 6%, Laiyang soil 4% and lane soil 1%, additional CaF23%, Pr2O30.08%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 65 hours, and ball milling fineness is 90%, then remove iron, sieving, filters pressing, then with vacuum deairing machine filter cake practiced at moisture be 22% mud item, suppressed with roller press At 6 cun of square positions, in 1265 ± 15 DEG C of at a temperature of biscuiting, the beautiful porcelain biscuit of faint yellow China is obtained, then glazing (Bone China when glazing With high gloss leadless glaze), make color through glaze by high-temperature chemical reaction in 1165 ± 15 DEG C of at a temperature of secondary glaze firing Layer is refracted to product surface, and it is flat to obtain the smooth beautiful porcelain 6 of faint yellow China as beautiful.
Embodiment 3
A kind of beautiful porcelain of China, is made of the raw material of following weight percentage: synthos 46%, feldspar 10%, Datong District's soil 15%, quartz 12%, elutriation Longyan clay 8%, Guangdong black mud 5%, Laiyang soil 3% and lane soil 1%, additional CaF22.5%, Pr2O30.1%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 70 hours, and ball milling fineness is 88%, then remove iron, sieving, filters pressing, then with vacuum deairing machine filter cake practiced at moisture be 25% mud item, suppressed with roller press The beautiful porcelain biscuit of faint yellow China is obtained, then glazing (is used when glazing with Bone China in 1265 ± 15 DEG C of at a temperature of biscuiting at 5 cun of bowls High gloss leadless glaze), make color through glaze layer by high-temperature chemical reaction in 1165 ± 15 DEG C of at a temperature of secondary glaze firing It is refracted to product surface, is obtained smooth such as the beautiful flat bowl of the faint yellow beautiful porcelain 5 of China.
Raw materials used chemical weight percentage composition, is shown in Table 1.
The raw materials used chemical weight percentage composition of table 1
The chemical weight percentage composition of the product of embodiment 1-3 preparation, is shown in Table 2.
The chemical weight percentage composition of the product of 2 embodiment 1-3 of table preparation

Claims (6)

1. a kind of beautiful porcelain of China, it is characterised in that: green body chemical composition weight percent are as follows: SiO239~43%, Al2O310~ 15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O3 0.2~0.5%, TiO2 0.05~0.2%, CaF2 1.2-2%、Pr2O3 0.02~0.08%, surplus is impurity.
2. the beautiful porcelain of China according to claim 1, it is characterised in that be made of the raw material of following weight percentage: calcium phosphate Salt 38~46%, feldspar 8~13%, quartz 8~14%, Datong District's soil 13~18%, eluriate Longyan clay 6~15%, Guangdong black mud 2~8%, Laiyang soil 1~5% and lane soil 1~5%;It is 100% metering, additional CaF with the total weight of the above raw material2 2-3%、Pr2O3 0.05 ~0.1%.
3. a kind of preparation method of the beautiful porcelain of China of any of claims 1 or 2, it is characterised in that the following steps are included:
(1) after mixing raw material, ball milling is carried out, then removes iron, sieving, filters pressing, pugging, compacting;
(2) step (1) pressed semi-finished product are subjected to biscuiting at 1250-1280 DEG C;
(3) to the green body glazing after step (2) biscuiting;
(4) semi-finished product after step (3) glazing are subjected at 1150-1180 DEG C secondary glaze firing, obtain the beautiful porcelain of the China.
4. the preparation method of the beautiful porcelain of China according to claim 3, it is characterised in that: in step (1), Ball-milling Time 60- 70 hours, ball milling fineness >=87%.
5. the preparation method of the beautiful porcelain of China according to claim 3, it is characterised in that: in step (1), when pugging, by filter cake Practice the mud item for being 20-25% at moisture.
6. the preparation method of the beautiful porcelain of China according to claim 3, it is characterised in that: in step (3), when glazing glaze used Material is Bone China high gloss leadless glaze.
CN201710842629.4A 2017-09-18 2017-09-18 Magnificent jade porcelain and preparation method thereof Active CN107382294B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112794707B (en) * 2021-04-14 2021-07-20 佛山市东鹏陶瓷有限公司 High-whiteness and high-strength light-transmitting ceramic tile and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1935738A (en) * 2006-10-12 2007-03-28 淄博华光瓷业有限公司 Bone-green porcelain
CN101913843A (en) * 2010-07-23 2010-12-15 华南理工大学 Preparation method of emerald ceramic
CN102515704A (en) * 2011-12-27 2012-06-27 淄博华光陶瓷科技文化有限公司 Hua celadon and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1935738A (en) * 2006-10-12 2007-03-28 淄博华光瓷业有限公司 Bone-green porcelain
CN101913843A (en) * 2010-07-23 2010-12-15 华南理工大学 Preparation method of emerald ceramic
CN102515704A (en) * 2011-12-27 2012-06-27 淄博华光陶瓷科技文化有限公司 Hua celadon and preparation method thereof

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