CN107338130A - A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract - Google Patents

A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract Download PDF

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Publication number
CN107338130A
CN107338130A CN201710540707.5A CN201710540707A CN107338130A CN 107338130 A CN107338130 A CN 107338130A CN 201710540707 A CN201710540707 A CN 201710540707A CN 107338130 A CN107338130 A CN 107338130A
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weight
parts
extract
preparation
agitator
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CN201710540707.5A
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Chinese (zh)
Inventor
单筱慧
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Wuhu Hui Yu Commerce Co Ltd
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Wuhu Hui Yu Commerce Co Ltd
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Priority to CN201710540707.5A priority Critical patent/CN107338130A/en
Publication of CN107338130A publication Critical patent/CN107338130A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2082—Polycarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Molecular Biology (AREA)
  • Detergent Compositions (AREA)

Abstract

A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract, belongs to liquid detergent field, including：Prepare camomile extract, and APG, AEO, fatty amide propyl amine-oxides, dodecyl benzyl dimethyl ammonium chloride, potassium sorbate, sodium alginate, chitosan, disodium ethylene diamine tetraacetate, citric acid, essence, Nacl etc. are added, prepare liquid detergent.The liquid detergent of the present invention has good bactericidal effect, and moderate performance, and health environment-friendly, can protect hand skin and preparation method is simple, is adapted to large-scale production and soil removal efficiency is high.

Description

A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract
Technical field
The present invention relates to liquid detergent field, more particularly to a kind of preparation side of the Traditional Chinese medicine laundry detergent containing camomile extract Method.
Background technology
With the pollution getting worse of environment, clothing is positioned over interior, due to indoor environment after the cleaning of common cleaning agent Humidity, tend to grow a large amount of bacteriums, harm to the human body is serious, especially personal clothing and underwear.Exist in the prior art more Chemical bactericide is added in liquid detergent, to reach the effect of sterilization.These chemical addition agents can cause certain journey to human body skin The influence of degree, skin after the immersion of liquid detergent can some influences are caused on skin, cause pachylosis, Carried bacteria or Allergy etc., this is the defects of traditional liquid detergent is present.Chinese herbal medicine has good Disinfection Effect, and is free from side effects.
The content of the invention
According to problems of the prior art, the invention provides a kind of Traditional Chinese medicine laundry detergent containing camomile extract Preparation method, there is good bactericidal effect, and be free of chemical bactericide, health environment-friendly.
The present invention uses following technical scheme：
A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract, comprises the following steps：
Step 1：25kg chamomiles are taken, are ground into coarse powder, volatile ingredient is removed through steam distillation, it is sweet to obtain ocean Chrysanthemum residue, by solid-liquid ratio 1:5 add the ethanol that volumetric concentration is 95%, and stirring extraction 3h, filters to take supernatant under the conditions of 50 DEG C Liquid, repeat extraction 2 times；
Step 2：2 gained supernatants are merged, are concentrated under reduced pressure untill without ethanol, produce the extraction of chamomile ethanol Thing；
Step 3：Take chamomile ethanol extract to add the deionized water of 5 times of volumes thereto and suspension is made, to suspended Add the petroleum ether of 1 times of volume to extract 3h at room temperature in liquid, petroleum ether is mutually concentrated under reduced pressure after removal petroleum ether after layering, produced Camomile extract；
Step 4：90 parts of deionized water is weighed by weight, is divided into 3 parts of equivalent, takes a copy of it to add in agitator, After being heated to 45 DEG C, the parts by weight of APG 10, the parts by weight of AEO 12, fatty acid amide third are added while stirring The parts by weight of base amine-oxides 8, the parts by weight of dodecyl benzyl dimethyl ammonium chloride 3, continue to stir, agitator speed 100r/ Min, stir 35min；
Step 5：2 parts of the potassium sorbate weighed by weight, 1 part of sodium alginate, 1 part of chitosan and 1/3rd Deionized water is added in agitator, agitator speed 80r/min, stirs 20min；
Step 6：Weigh and continue in the deionized water addition agitator of 3 parts of camomile extract and surplus by weight After stirring 35min, rotating speed 50r/min；
Step 7：Agitator is heated to 80 DEG C, is incubated 20min, is cooled to 40 DEG C, adds ethylenediamine by weight 0.2 part of tetraacethyl disodium, 0.1 part of citric acid, 0.1 part of essence, 0.1 part of Nacl, and PH conditioning agents are added, PH to 6-7 is adjusted, Produce liquid detergent.
Preferably, the essence described in step 7 is lemon extract or flavoring rose essence.
Preferably, the crushing described in step 1 is to use LD-Y400A high speed Universal pulverizers.
The beneficial effects of the present invention are：
1) present invention addition camomile extract, chamomile have cleaning, moisten, antibacterial, it is antipruritic, dispel taste the effect of.
2) present invention addition dodecyl benzyl dimethyl ammonium chloride, is a kind of cationic surfactant, is also simultaneously A kind of non oxidizing bactericide, there is wide spectrum, efficient bactericidal effect.
3) liquid detergent moderate performance of the invention, health environment-friendly, can protect hand skin and preparation method is simple, be adapted to rule Modelling produces and soil removal efficiency is high.
Embodiment
Below with reference to specific embodiment, the present invention is described further.
Embodiment 1
A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract, comprises the following steps：
Step 1：25kg chamomiles are taken, are ground into coarse powder, volatile ingredient is removed through steam distillation, it is sweet to obtain ocean Chrysanthemum residue, by solid-liquid ratio 1:5 add the ethanol that volumetric concentration is 95%, and stirring extraction 3h, filters to take supernatant under the conditions of 50 DEG C Liquid, repeat extraction 2 times；
Step 2：2 gained supernatants are merged, are concentrated under reduced pressure untill without ethanol, produce the extraction of chamomile ethanol Thing；
Step 3：Take chamomile ethanol extract to add the deionized water of 5 times of volumes thereto and suspension is made, to suspended Add the petroleum ether of 1 times of volume to extract 3h at room temperature in liquid, petroleum ether is mutually concentrated under reduced pressure after removal petroleum ether after layering, produced Camomile extract；
Step 4：90 parts of deionized water is weighed by weight, is divided into 3 parts of equivalent, takes a copy of it to add in agitator, After being heated to 45 DEG C, the parts by weight of APG 10, the parts by weight of AEO 12, fatty acid amide third are added while stirring The parts by weight of base amine-oxides 8, the parts by weight of dodecyl benzyl dimethyl ammonium chloride 3, continue to stir, agitator speed 100r/ Min, stir 35min；
Step 5：2 parts of the potassium sorbate weighed by weight, 1 part of sodium alginate, 1 part of chitosan and 1/3rd Deionized water is added in agitator, agitator speed 80r/min, stirs 20min；
Step 6：Weigh and continue in the deionized water addition agitator of 3 parts of camomile extract and surplus by weight After stirring 35min, rotating speed 50r/min；
Step 7：Agitator is heated to 80 DEG C, is incubated 20min, is cooled to 40 DEG C, adds ethylenediamine by weight 0.2 part of tetraacethyl disodium, 0.1 part of citric acid, 0.1 part of essence, 0.1 part of Nacl, and PH conditioning agents are added, PH to 6-7 is adjusted, Produce liquid detergent.
Essence described in step 7 is lemon extract or flavoring rose essence.
Crushing described in step 1 is to use LD-Y400A high speed Universal pulverizers.
The detergency ability comparing result of liquid detergent made from the embodiment of the present invention 1 and same type liquid detergent on the market is shown in Table 1 below.
Table 1
Project Soil removal efficiency %
Embodiment 1 More than 85
Same type liquid detergent 70-75

Claims (3)

1. a kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract, it is characterised in that comprise the following steps：
Step 1：25kg chamomiles are taken, are ground into coarse powder, volatile ingredient is removed through steam distillation, it is residual to obtain chamomile Slag, by solid-liquid ratio 1:5 add the ethanol that volumetric concentration is 95%, and stirring extraction 3h, filters to take supernatant under the conditions of 50 DEG C, weight Extract 2 times again；
Step 2：2 gained supernatants are merged, is concentrated under reduced pressure untill without ethanol, produces chamomile ethanol extract；
Step 3：Take chamomile ethanol extract to add the deionized water of 5 times of volumes thereto and suspension is made, into suspension Add the petroleum ether of 1 times of volume to extract 3h at room temperature, petroleum ether is mutually concentrated under reduced pressure after removal petroleum ether after layering, it is sweet to produce ocean Chrysanthemum extract；
Step 4：90 parts of deionized water is weighed by weight, is divided into 3 parts of equivalent, takes a copy of it to add in agitator, heating To after 45 DEG C, the parts by weight of APG 10, the parts by weight of AEO 12, fatty amide propyl oxygen are added while stirring Change the parts by weight of ammonium 8, the parts by weight of dodecyl benzyl dimethyl ammonium chloride 3, continue to stir, agitator speed 100r/min, stir Mix 35min；
Step 5：2 parts of the potassium sorbate weighed by weight, 1 part of sodium alginate, 1 part of chitosan and 1/3rd go from Sub- water is added in agitator, agitator speed 80r/min, stirs 20min；
Step 6：Weigh by weight and continue to stir in the deionized water addition agitator of 3 parts of camomile extract and surplus After 35min, rotating speed 50r/min；
Step 7：Agitator is heated to 80 DEG C, is incubated 20min, is cooled to 40 DEG C, adds ethylenediamine tetrem by weight 0.2 part of acid disodium, 0.1 part of citric acid, 0.1 part of essence, 0.1 part of Nacl, and PH conditioning agents are added, PH to 6-7 is adjusted, is produced Liquid detergent.
A kind of 2. preparation method of Traditional Chinese medicine laundry detergent containing camomile extract according to claim 1, it is characterised in that： Essence described in step 7 is lemon extract or flavoring rose essence.
A kind of 3. preparation method of Traditional Chinese medicine laundry detergent containing camomile extract according to claim 1, it is characterised in that： Crushing described in step 1 is to use LD-Y400A high speed Universal pulverizers.
CN201710540707.5A 2017-07-05 2017-07-05 A kind of preparation method of the Traditional Chinese medicine laundry detergent containing camomile extract Withdrawn CN107338130A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108728261A (en) * 2018-05-15 2018-11-02 贝德氏（上海）健康科技股份有限公司 A kind of environmental protecting physical bacteriostatic lotion and application thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102517164A (en) * 2011-12-06 2012-06-27 江南大学 Sterilizing laundry detergent containing hairyvein agrimony extract
CN104178370A (en) * 2014-08-29 2014-12-03 成都顺发消洗科技有限公司 Bactericidal laundry detergent containing traditional Chinese medicine components and preparation method thereof
CN105997535A (en) * 2016-05-24 2016-10-12 长沙华晨生物科技有限公司 Personal care formula without preservative
CN106244344A (en) * 2016-07-31 2016-12-21 申秋英 Bamboo charcoal low foam laundry liquid and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102517164A (en) * 2011-12-06 2012-06-27 江南大学 Sterilizing laundry detergent containing hairyvein agrimony extract
CN104178370A (en) * 2014-08-29 2014-12-03 成都顺发消洗科技有限公司 Bactericidal laundry detergent containing traditional Chinese medicine components and preparation method thereof
CN105997535A (en) * 2016-05-24 2016-10-12 长沙华晨生物科技有限公司 Personal care formula without preservative
CN106244344A (en) * 2016-07-31 2016-12-21 申秋英 Bamboo charcoal low foam laundry liquid and preparation method thereof

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Title
王昌涛等: "《化妆品植物添加剂的开发与应用》", 30 April 2013, 中国轻工业出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108728261A (en) * 2018-05-15 2018-11-02 贝德氏（上海）健康科技股份有限公司 A kind of environmental protecting physical bacteriostatic lotion and application thereof
CN108728261B (en) * 2018-05-15 2020-09-08 贝德氏（上海）健康科技股份有限公司 Environment-friendly physical bacteriostatic lotion and application thereof

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