CN107338129A - A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E - Google Patents

A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E Download PDF

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Publication number
CN107338129A
CN107338129A CN201710540706.0A CN201710540706A CN107338129A CN 107338129 A CN107338129 A CN 107338129A CN 201710540706 A CN201710540706 A CN 201710540706A CN 107338129 A CN107338129 A CN 107338129A
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Prior art keywords
weight
parts
honegsukle flower
preparation
agitator
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CN201710540706.0A
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Chinese (zh)
Inventor
单筱慧
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Wuhu Hui Yu Commerce Co Ltd
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Wuhu Hui Yu Commerce Co Ltd
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Priority to CN201710540706.0A priority Critical patent/CN107338129A/en
Publication of CN107338129A publication Critical patent/CN107338129A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2082—Polycarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Molecular Biology (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E, belongs to liquid detergent field, including：Prepare Honegsukle flower P.E, and APG, AEO, fatty amide propyl amine-oxides, dodecyl benzyl dimethyl ammonium chloride, potassium sorbate, sodium alginate, chitosan, disodium ethylene diamine tetraacetate, citric acid, essence, Nacl etc. are added, prepare liquid detergent.The liquid detergent of the present invention has good bactericidal effect, and moderate performance, and health environment-friendly, can protect hand skin and preparation method is simple, is adapted to large-scale production and soil removal efficiency is high.

Description

A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E
Technical field
The present invention relates to liquid detergent field, more particularly to a kind of preparation side of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E Method.
Background technology
With the pollution getting worse of environment, clothing is positioned over interior, due to indoor environment after the cleaning of common cleaning agent Humidity, tend to grow a large amount of bacteriums, harm to the human body is serious, especially personal clothing and underwear.Exist in the prior art more Chemical bactericide is added in liquid detergent, to reach the effect of sterilization.These chemical addition agents can cause certain journey to human body skin The influence of degree, skin after the immersion of liquid detergent can some influences are caused on skin, cause pachylosis, Carried bacteria or Allergy etc., this is the defects of traditional liquid detergent is present.Chinese herbal medicine has good Disinfection Effect, and is free from side effects.
The content of the invention
According to problems of the prior art, the invention provides a kind of Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E Preparation method, there is good bactericidal effect, and be free of chemical bactericide, health environment-friendly.
The present invention uses following technical scheme：
A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E, comprises the following steps：
Step 1：Honeysuckle is placed in drying machine, 30min is dried at 60 DEG C；
Step 2：The whole flower of dried honeysuckle is taken, is crushed after removing insect pest, part of going mouldy, crosses 80 mesh sieves；
Step 3：According to 1:10 solid-liquid ratios, with the ethanol solution of volumetric concentration 80%, ultrasound extraction is golden at a temperature of 50 DEG C Honeysuckle flower, time 30min, resulting solution 5000r/min centrifugal treating 20min, supernatant liquid filtering is taken, then remove through vacuum rotary steam Ethanol, obtain Honegsukle flower P.E；
Step 4：90 parts of deionized water is weighed by weight, is divided into 3 parts of equivalent, takes a copy of it to add in agitator, After being heated to 45 DEG C, the parts by weight of APG 10, the parts by weight of AEO 12, fatty acid amide third are added while stirring The parts by weight of base amine-oxides 8, the parts by weight of dodecyl benzyl dimethyl ammonium chloride 3, continue to stir, agitator speed 100r/ Min, stir 35min；
Step 5：2 parts of the potassium sorbate weighed by weight, 1 part of sodium alginate, 1 part of chitosan and 1/3rd Deionized water is added in agitator, agitator speed 80r/min, stirs 20min；
Step 6：Weigh and continue in 3 parts of Honegsukle flower P.E and the deionized water addition agitator of surplus by weight After stirring 35min, rotating speed 50r/min；
Step 7：Agitator is heated to 80 DEG C, is incubated 20min, is cooled to 40 DEG C, adds ethylenediamine by weight 0.2 part of tetraacethyl disodium, 0.1 part of citric acid, 0.1 part of essence, 0.1 part of Nacl, and PH conditioning agents are added, PH to 6-7 is adjusted, Produce liquid detergent.
Preferably, the essence described in step 7 is lemon extract or flavoring rose essence.
Preferably, the crushing described in step 2 is to use LD-Y400A high speed Universal pulverizers.
The beneficial effects of the present invention are：
1) present invention addition Honegsukle flower P.E, honeysuckle have the effect of good restraining and sterilizing bacteria.
2) present invention addition dodecyl benzyl dimethyl ammonium chloride, is a kind of cationic surfactant, is also simultaneously A kind of non oxidizing bactericide, there is wide spectrum, efficient bactericidal effect.
3) liquid detergent moderate performance of the invention, health environment-friendly, can protect hand skin and preparation method is simple, be adapted to rule Modelling produces and soil removal efficiency is high.
Embodiment
Below with reference to specific embodiment, the present invention is described further.
Embodiment 1
A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E, comprises the following steps：
Step 1：Honeysuckle is placed in drying machine, 30min is dried at 60 DEG C；
Step 2：The whole flower of dried honeysuckle is taken, is crushed after removing insect pest, part of going mouldy, crosses 80 mesh sieves；
Step 3：According to 1:10 solid-liquid ratios, with the ethanol solution of volumetric concentration 80%, ultrasound extraction is golden at a temperature of 50 DEG C Honeysuckle flower, time 30min, resulting solution 5000r/min centrifugal treating 20min, supernatant liquid filtering is taken, then remove through vacuum rotary steam Ethanol, obtain Honegsukle flower P.E；
Step 4：90 parts of deionized water is weighed by weight, is divided into 3 parts of equivalent, takes a copy of it to add in agitator, After being heated to 45 DEG C, the parts by weight of APG 10, the parts by weight of AEO 12, fatty acid amide third are added while stirring The parts by weight of base amine-oxides 8, the parts by weight of dodecyl benzyl dimethyl ammonium chloride 3, continue to stir, agitator speed 100r/ Min, stir 35min；
Step 5：2 parts of the potassium sorbate weighed by weight, 1 part of sodium alginate, 1 part of chitosan and 1/3rd Deionized water is added in agitator, agitator speed 80r/min, stirs 20min；
Step 6：Weigh and continue in 3 parts of Honegsukle flower P.E and the deionized water addition agitator of surplus by weight After stirring 35min, rotating speed 50r/min；
Step 7：Agitator is heated to 80 DEG C, is incubated 20min, is cooled to 40 DEG C, adds ethylenediamine by weight 0.2 part of tetraacethyl disodium, 0.1 part of citric acid, 0.1 part of essence, 0.1 part of Nacl, and PH conditioning agents are added, PH to 6-7 is adjusted, Produce liquid detergent.
Essence described in step 7 is lemon extract or flavoring rose essence.
Crushing described in step 2 is to use LD-Y400A high speed Universal pulverizers.
The detergency ability comparing result of liquid detergent made from the embodiment of the present invention 1 and same type liquid detergent on the market is shown in Table 1 below.
Table 1
Project Soil removal efficiency %
Embodiment 1 More than 85
Same type liquid detergent 70-75

Claims (3)

1. a kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E, it is characterised in that comprise the following steps：
Step 1：Honeysuckle is placed in drying machine, 30min is dried at 60 DEG C；
Step 2：The whole flower of dried honeysuckle is taken, is crushed after removing insect pest, part of going mouldy, crosses 80 mesh sieves；
Step 3：According to 1:10 solid-liquid ratios, with the ethanol solution of volumetric concentration 80%, ultrasound extracts honeysuckle at a temperature of 50 DEG C, Time is 30min, resulting solution 5000r/min centrifugal treating 20min, takes supernatant liquid filtering, then removes ethanol through vacuum rotary steam, Obtain Honegsukle flower P.E；
Step 4：90 parts of deionized water is weighed by weight, is divided into 3 parts of equivalent, takes a copy of it to add in agitator, heating To after 45 DEG C, the parts by weight of APG 10, the parts by weight of AEO 12, fatty amide propyl oxygen are added while stirring Change the parts by weight of ammonium 8, the parts by weight of dodecyl benzyl dimethyl ammonium chloride 3, continue to stir, agitator speed 100r/min, stir Mix 35min；
Step 5：2 parts of the potassium sorbate weighed by weight, 1 part of sodium alginate, 1 part of chitosan and 1/3rd go from Sub- water is added in agitator, agitator speed 80r/min, stirs 20min；
Step 6：Weigh by weight and continue to stir in 3 parts of Honegsukle flower P.E and the deionized water addition agitator of surplus After 35min, rotating speed 50r/min；
Step 7：Agitator is heated to 80 DEG C, is incubated 20min, is cooled to 40 DEG C, adds ethylenediamine tetrem by weight 0.2 part of acid disodium, 0.1 part of citric acid, 0.1 part of essence, 0.1 part of Nacl, and PH conditioning agents are added, PH to 6-7 is adjusted, is produced Liquid detergent.
A kind of 2. preparation method of Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E according to claim 1, it is characterised in that： Essence described in step 7 is lemon extract or flavoring rose essence.
A kind of 3. preparation method of Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E according to claim 1, it is characterised in that： Crushing described in step 2 is to use LD-Y400A high speed Universal pulverizers.
CN201710540706.0A 2017-07-05 2017-07-05 A kind of preparation method of the Traditional Chinese medicine laundry detergent containing Honegsukle flower P.E Withdrawn CN107338129A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108060027A (en) * 2017-12-20 2018-05-22 陈景芳 A kind of multifuctional cleaning agent
CN108795593A (en) * 2018-05-21 2018-11-13 李均辉 A kind of anti-antibacterial honeysuckle liquid detergent

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104178370A (en) * 2014-08-29 2014-12-03 成都顺发消洗科技有限公司 Bactericidal laundry detergent containing traditional Chinese medicine components and preparation method thereof
CN104403844A (en) * 2014-12-09 2015-03-11 韦爱琴 Bactericidal and aromatic washing soap
CN104403831A (en) * 2014-12-09 2015-03-11 韦爱琴 High-performance bactericidal detergent
CN104403833A (en) * 2014-12-09 2015-03-11 韦爱琴 Bactericidal and aromatic washing liquid
CN104498238A (en) * 2014-12-09 2015-04-08 韦爱琴 High-efficient sterilization washing soap

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104178370A (en) * 2014-08-29 2014-12-03 成都顺发消洗科技有限公司 Bactericidal laundry detergent containing traditional Chinese medicine components and preparation method thereof
CN104403844A (en) * 2014-12-09 2015-03-11 韦爱琴 Bactericidal and aromatic washing soap
CN104403831A (en) * 2014-12-09 2015-03-11 韦爱琴 High-performance bactericidal detergent
CN104403833A (en) * 2014-12-09 2015-03-11 韦爱琴 Bactericidal and aromatic washing liquid
CN104498238A (en) * 2014-12-09 2015-04-08 韦爱琴 High-efficient sterilization washing soap

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108060027A (en) * 2017-12-20 2018-05-22 陈景芳 A kind of multifuctional cleaning agent
CN108795593A (en) * 2018-05-21 2018-11-13 李均辉 A kind of anti-antibacterial honeysuckle liquid detergent

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Application publication date: 20171110