CN104971285A - Broad-spectrum anti-bacterial solution and preparation method thereof - Google Patents
Broad-spectrum anti-bacterial solution and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a broad-spectrum anti-bacterial solution and a preparation method thereof. The broad-spectrum anti-bacterial solution is prepared from the following raw materials in parts by weight: 5-10 parts of corn stigma, 15-20 parts of fructus cnidii, 8-10 parts of radix phytolaccae, 10-15 parts of radix angelicae, 10-12 parts of radix stemonae, 20-30 parts of hawthorns, 5-10 parts of rhizoma kaempferiae, 20-30 parts of pilose bushclover herbs, 15-20 parts of folium isatidis, 3-5 parts of citric acid, 10-15 parts of coconut oil, 15-20 parts of orange peel and 400-500 parts of water. The broad-spectrum anti-bacterial solution is nontoxic and harmless to human bodies and the environment, has the effects of sterilizing, disinfecting and deodorizing, is low in cost, good in stability and free of irritation and can be widely used to the life field such as clothes cleaning and disinfection, skin and wound sterilization and disinfection, kitchen ware disinfection and toilets so as to be very wide in application range.
Description
Technical field
The present invention relates to a kind of antibacterial liquid, especially relate to a kind of broad-spectrum antibacterial liquid and preparation method thereof.
Background technology
The sterilized principle for germ of the chemosterilants such as present widely used chlorinated product, Operand, aldehydes preparation and phenols preparation mainly changes bacterial cell membrane permeability, carrys out sterilizing or antibacterial to its protein, peptide chain and amino acid whose destruction or inhibitory action.But the shortcomings such as chemosterilant ubiquity corrosivity is strong, large to skin irritation, environmental pollution is serious or harmful, therefore can not meet the demand that people are general.
Application publication number CN 102113524 A, the Chinese patent of Shen Qing Publication day 2011.07.06 discloses a kind of Traditional Chinese medicine bacteriostatic liquid and processing method thereof, by being prepared from united extraction mixed after Radix Codonopsis, Fructus Zanthoxyli, Flos Lonicerae, Cortex Phellodendri, Flos Lonicerae, withered all rational proportions, there is nonirritant, without toxicity, can effectively kill various pathogenic microorganism, eliminating bacteria is thorough, can grow by anti-bacteria, of many uses, be applicable to the sterilizations such as medicated clothing, skin, kitchen tools.Containing ethanol in this Traditional Chinese medicine bacteriostatic liquid, ethanol is applied on skin and skin can be made after volatilization to produce dry sensation, if ethanol is directly applied to skin wound place simultaneously, can produces strong impulse, cause comfort poor; In addition, containing phosphoric acid in this Traditional Chinese medicine bacteriostatic liquid, phosphoric acid not only has zest to skin, also can to environment.
Summary of the invention
The present invention is the problems referred to above existing for the antibacterial liquid in order to solve prior art, and provide one and have sterilization, sterilization, deodouring effect concurrently, cost is low, good stability, nonirritant, nontoxic to human body, environment, the broad-spectrum antibacterial liquid had wide range of applications.
The invention also discloses a kind of broad-spectrum antibacterial liquid and preparation method thereof, processing step is simple, and low for equipment requirements, workable, preparation efficiency is high.
To achieve these goals, the present invention is by the following technical solutions:
A kind of broad-spectrum antibacterial liquid, is made up of the raw material of following weight portion: 5 ~ 10 parts of Stigma Maydis, 15 ~ 20 parts of Fructus Cnidiis, 8 ~ 10 parts of Radix Phytolaccaes, 10 ~ 15 parts of Radixs Angelicae Dahuricae, 10 ~ 12 parts of Radixs Stemonae, 20 ~ 30 portions of Fructus Crataegis, 5 ~ 10 parts of Rhizoma Kaempferiaes, 20 ~ 30 parts of Herba lespedezae pilosaes, 15 ~ 20 portions of Folium Isatidiss, 3 ~ 5 parts of citric acids, 10 ~ 15 portions of Oleum Cocois, 15 ~ 20 parts of Pericarpium Citri junoriss, 400 ~ 500 parts of water.
The present invention is a kind of complete natural herb preparation made for primary raw material with the plurality of Chinese such as Stigma Maydis, Fructus Cnidii, nontoxic to human body, environment, Stigma Maydis contains saponin, alkaloid, fatty wet goods plurality of active ingredients, its water extract has excellent bactericidal effect, and Stigma Maydis fairly obtains, cheapness, it can be used as the raw materials of antibacterial liquid can greatly improve its economic worth, turn waste into wealth; Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, the mutual coordinated of several Chinese medicine of Folium Isatidis, can effectively kill the various pathogenic microorganisms such as staphylococcus aureus, Candida albicans, Pseudomonas aeruginosa, escherichia coli, mycete, bactericidal effect is good, broad-spectrum bactericidal effect, and nontoxic to human body, environment; Citric acid, to adjust antibacterial liquid pH for faintly acid, strengthens the bactericidal effect of antibacterial liquid of the present invention greatly; Radix Phytolaccae can remove edema, has effect of antiinflammatory; Oleum Cocois is added in the present invention, oils and fats containing a large amount of medium-chain fatty acid composition in Oleum Cocois, medium-chain fatty acid has natural comprehensive antibacterial ability, disinfection effect of the present invention can be improved, the most important thing is, Oleum Cocois has moisturizing, neutralization, the zest to skin and wound of the present invention can be greatly reduced, improve comfort, and Oleum Cocois can also improve stability of the present invention and permeance property, making the present invention when sterilizing for clothes washing, medicated clothing can be infiltrated rapidly and playing effect; Pericarpium Citri junoris not only has bactericidal action, but also containing abundant natural perfume material, and absorption affinity and resistance to oxidation by force, can effectively neutralize and remove antibacterial, fungus grows produced stink, thus make the present invention have deodorizing effect.The present invention is by the mutual Synergistic between each component, have sterilization, sterilization, deodouring effect concurrently, cost is low, good stability, nonirritant, nontoxic to human body, environment, can be widely used in the sphere of lifes such as clothes washing sterilization, skin and wound sterilizing, kitchen tools sterilization, toilet, range of application is very extensive.
A preparation method for broad-spectrum antibacterial liquid, concrete preparation method is:
After taking each component by above-mentioned weight, Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis are added to the water immersion 1 ~ 3h, obtain and just put forward feed liquid, add compound enzyme and carry out step heat preservation lixiviate just carrying in feed liquid again, filter, after adding citric acid and Oleum Cocois in filtrate, stir, obtain antibacterial liquid.The present invention to make the abundant stripping of effective ingredient in each raw material, improves the extraction ratio of effective medicinal components by complex enzyme hydrolysis, step heat preservation lixiviate, and processing step is simple, and low for equipment requirements, workable, preparation efficiency is high.
As preferably, Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis, Pericarpium Citri junoris are soaked after pulverizing.
As preferably, soaking temperature controls at 20 ~ 25 DEG C.Soaking temperature controls to bubble open swelling at 20 ~ 25 DEG C to make quick, abundant raw material, is conducive to the extraction ratio improving effective ingredient in follow-up enzymolysis water extraction.
As preferably, the addition of described compound enzyme is just put forward 1 ~ 3% of feed liquid quality, and in compound enzyme, the mass percentage of each enzyme is: 20 ~ 25% pectases, 20 ~ 25% glucosidase, and surplus is cellulase.The present invention selects pectase, glucosidase and cellulase are as compound enzyme, wherein, pectase coordinates with cellulase synergistic, leniently can decompose the cellulose in cell wall and intercellular substance, hemicellulose, the compositions such as pectic substance, destroy the dense construction of cell wall, cause cell wall and intercellular substance structure to produce local to loosen, expand, the changes such as collapse, reduce the mass transfer such as cell wall and intercellular substance barrier to effective ingredient from born of the same parents to the resistance to mass tranfer of Extraction medium diffusion, thus be conducive to the stripping of effective ingredient, improve dissolution efficiency, be aided with glucosidase, just it has been generally acknowledged that invalid impurity is as decomposition such as starch, be conducive to follow-up filtration to create favorable conditions, improve simultaneously and extract clarity.
As preferably, the concrete steps of step heat preservation lixiviate are: be first warming up to 50 ~ 60 DEG C and keep 40 ~ 50min, then continue to heat to 100 DEG C and keep 10 ~ 15min.The present invention adopts step heat preservation lixiviate, has both ensured that effective ingredient is not destroyed, and ensures extraction efficiency and extraction ratio again.
Therefore, the present invention has following beneficial effect:
(1) the present invention is a kind of complete natural herb preparation made for primary raw material with the plurality of Chinese such as Stigma Maydis, Fructus Cnidii, nontoxic to human body, environment, have sterilization, sterilization, deodouring effect concurrently, cost is low, good stability, nonirritant, can be widely used in the sphere of lifes such as clothes washing sterilization, skin and wound sterilizing, kitchen tools sterilization, toilet, range of application is very extensive;
(2) the present invention is by complex enzyme hydrolysis, step heat preservation lixiviate to make the abundant stripping of effective ingredient in each raw material, improves the extraction ratio of effective medicinal components, and processing step is simple, and low for equipment requirements, workable, preparation efficiency is high.
Detailed description of the invention
Below by detailed description of the invention, the present invention will be further described.
Embodiment 1
By 50g Stigma Maydis, 150g Fructus Cnidii, 80g Radix Phytolaccae, the 100g Radix Angelicae Dahuricae, the 100g Radix Stemonae, 200g Fructus Crataegi, 50g Rhizoma Kaempferiae, 200g Herba lespedezae pilosae, 150g Folium Isatidis, 30g citric acid, 100g Oleum Cocois, 150g Pericarpium Citri junoris, after the proportioning of 4000g water takes each component, by Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis, Pericarpium Citri junoris is pulverized, be added to the water and soak 1h, soaking temperature controls at 25 DEG C, obtain and just put forward feed liquid, add compound enzyme and carry out step heat preservation lixiviate just carrying in feed liquid again, the addition of compound enzyme is just put forward 1% of feed liquid quality, in compound enzyme, the mass percentage of each enzyme is: 20% pectin element enzyme, 20% glucosidase, surplus is cellulase, the concrete steps of step heat preservation lixiviate are: be first warming up to 50 DEG C and keep 50min, continue again to heat to 100 DEG C of maintenance 10min, filter, after adding citric acid and Oleum Cocois in filtrate, stir, obtain antibacterial liquid.
Embodiment 2
By 100g Stigma Maydis, 200g Fructus Cnidii, 100g Radix Phytolaccae, the 150g Radix Angelicae Dahuricae, the 120g Radix Stemonae, 300g Fructus Crataegi, 100g Rhizoma Kaempferiae, 300g Herba lespedezae pilosae, 200g Folium Isatidis, 50g citric acid, 150g Oleum Cocois, 200g Pericarpium Citri junoris, after the proportioning of 5000g water takes each component, by Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis, Pericarpium Citri junoris is pulverized, be added to the water and soak 3h, soaking temperature controls at 20 DEG C, obtain and just put forward feed liquid, add compound enzyme and carry out step heat preservation lixiviate just carrying in feed liquid again, the addition of compound enzyme is just put forward 3% of feed liquid quality, in compound enzyme, the mass percentage of each enzyme is: 25% pectin element enzyme, 25% glucosidase, surplus is cellulase, the concrete steps of step heat preservation lixiviate are: be first warming up to 60 DEG C and keep 40min, continue again to heat to 100 DEG C of maintenance 15min, filter, after adding citric acid and Oleum Cocois in filtrate, stir, obtain antibacterial liquid.
Embodiment 3
By 80g Stigma Maydis, 160g Fructus Cnidii, 890g Radix Phytolaccae, the 120g Radix Angelicae Dahuricae, the 110g Radix Stemonae, 250g Fructus Crataegi, 60g Rhizoma Kaempferiae, 280g Herba lespedezae pilosae, 180g Folium Isatidis, 40g citric acid, 120g Oleum Cocois, 180g Pericarpium Citri junoris, after the proportioning of 4200g water takes each component, by Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis, Pericarpium Citri junoris is pulverized, be added to the water immersion, 2h, soaking temperature controls at 23 DEG C, obtain and just put forward feed liquid, add compound enzyme and carry out step heat preservation lixiviate just carrying in feed liquid again, the addition of compound enzyme is just put forward 2% of feed liquid quality, in compound enzyme, the mass percentage of each enzyme is: 22% pectin element enzyme, 23% glucosidase, surplus is cellulase, the concrete steps of step heat preservation lixiviate are: be first warming up to 55 DEG C and keep 45min, continue again to heat to 100 DEG C of maintenance 12min, filter, after adding citric acid and Oleum Cocois in filtrate, stir, obtain antibacterial liquid.
Antibacterial liquid of the present invention all reaches more than 98% to Candida albicans, staphylococcus aureus and escherichia coli killing rate, bactericidal effect is good, broad-spectrum bactericidal effect, and it is nontoxic to human body, environment, have sterilization, sterilization, deodouring effect concurrently, cost is low, good stability, nonirritant, can be widely used in the sphere of lifes such as clothes washing sterilization, skin and wound sterilizing, kitchen tools sterilization, toilet, range of application is very extensive.
Above-described embodiment is one of the present invention preferably scheme, not does any pro forma restriction to the present invention, also has other variant and remodeling under the prerequisite not exceeding the technical scheme described in claim.
Claims (6)
1. a broad-spectrum antibacterial liquid, is characterized in that, is made up of the raw material of following weight portion: 5 ~ 10 parts of Stigma Maydis, 15 ~ 20 parts of Fructus Cnidiis, 8 ~ 10 parts of Radix Phytolaccaes, 10 ~ 15 parts of Radixs Angelicae Dahuricae, 10 ~ 12 parts of Radixs Stemonae, 20 ~ 30 portions of Fructus Crataegis, 5 ~ 10 parts of Rhizoma Kaempferiaes, 20 ~ 30 parts of Herba lespedezae pilosaes, 15 ~ 20 portions of Folium Isatidiss, 3 ~ 5 parts of citric acids, 10 ~ 15 portions of Oleum Cocois, 15 ~ 20 parts of Pericarpium Citri junoriss, 400 ~ 500 parts of water.
2. the preparation method of a broad-spectrum antibacterial liquid according to claim 1, it is characterized in that the preparation method of this antibacterial liquid is: after taking each component by weight ratio, Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis and Pericarpium Citri junoris are added to the water immersion 1 ~ 3h, obtain and just put forward feed liquid, add compound enzyme and carry out step heat preservation lixiviate just carrying in feed liquid again, filter, after adding citric acid and Oleum Cocois in filtrate, stir, obtain antibacterial liquid.
3. preparation method according to claim 2, is characterized in that, Stigma Maydis, Fructus Cnidii, Radix Phytolaccae, the Radix Angelicae Dahuricae, the Radix Stemonae, Fructus Crataegi, Rhizoma Kaempferiae, Herba lespedezae pilosae, Folium Isatidis, Pericarpium Citri junoris is soaked after pulverizing.
4. preparation method according to claim 2, is characterized in that, soaking temperature controls at 20 ~ 25 DEG C.
5. preparation method according to claim 2, is characterized in that, the addition of described compound enzyme is just put forward 1 ~ 3% of feed liquid quality, and in compound enzyme, the mass percentage of each enzyme is: 20 ~ 25% pectin element enzymes, 20 ~ 25% glucosidase, surplus is cellulase.
6. preparation method according to claim 2, is characterized in that, the concrete steps of step heat preservation lixiviate are: be first warming up to 50 ~ 60 DEG C and keep 40 ~ 50min, then continues to heat to 100 DEG C of maintenance 10 ~ 15min.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107897630A (en) * | 2017-12-11 | 2018-04-13 | 荣成海锐芯生物科技有限公司 | A kind of fresh-keeping method of conch |
| CN110227174A (en) * | 2018-08-16 | 2019-09-13 | 山西艾珂灵环境科技有限公司 | A kind of plant spray agent for the taste that antibacterial can dispel |
| CN110393191A (en) * | 2019-02-22 | 2019-11-01 | 季建萍 | A kind of coconut extractive and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107897630A (en) * | 2017-12-11 | 2018-04-13 | 荣成海锐芯生物科技有限公司 | A kind of fresh-keeping method of conch |
| CN107897630B (en) * | 2017-12-11 | 2021-04-23 | 荣成海锐芯生物科技有限公司 | Method for keeping fresh of conch |
| CN110227174A (en) * | 2018-08-16 | 2019-09-13 | 山西艾珂灵环境科技有限公司 | A kind of plant spray agent for the taste that antibacterial can dispel |
| CN110393191A (en) * | 2019-02-22 | 2019-11-01 | 季建萍 | A kind of coconut extractive and application thereof |
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