CN103451036A - Safe and environment-friendly tea seed washing liquid and preparation method thereof - Google Patents
Safe and environment-friendly tea seed washing liquid and preparation method thereof Download PDFInfo
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- CN103451036A CN103451036A CN2013103840919A CN201310384091A CN103451036A CN 103451036 A CN103451036 A CN 103451036A CN 2013103840919 A CN2013103840919 A CN 2013103840919A CN 201310384091 A CN201310384091 A CN 201310384091A CN 103451036 A CN103451036 A CN 103451036A
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Landscapes
- Detergent Compositions (AREA)
Abstract
The invention discloses a safe and environment-friendly tea seed washing liquid and a preparation method thereof. The preparation method comprises the following steps: step 1, taking 12-14 parts of camellia seed dregs, 3-6 parts of Chinese honey locust, 1-2 parts of cacumen biotae, 0.1-0.6 parts of cortex albiziae, 0.1-0.6 parts of pomegranate bark and 0.1-0.5 parts of natural borneol, and crushing, mixing and stirring the materials so as to obtain washing powder; step 2, taking 10-20 parts of the washing powder prepared in the step 1, and 180-190 parts of deionized water, mixing and stirring, extracting the liquid, and concentrating the liquid to be a concentrated liquid meeting a condition that each milliliter of the concentrated liquid contains 0.105-0.161g of washing powder; step 3, taking 85-95 parts of the concentrated liquid prepared in the step 2, 2-8 parts of cocamidopropyl propyl glycine betaine, 2-4 parts of coconut oil fatty acid biglycollic amide, and 0.3-3 parts of sodium carboxymethylcellulose, and mixing and stirring so as to obtain the safe and environment-friendly tea seed washing liquid. The safe and environment-friendly tea seed washing liquid is high in stability, good in sterilization effect, high in detergency, high in biodegradation degree, tender and smooth for hands, low in foam and waster-saving.
Description
Technical field
The present invention relates to a kind of articles for washing and preparation method thereof, particularly a kind of safety and environmental protection tea seed detergent liquid and preparation method thereof.
Background technology
The daily use chemicals cleaning product that the liquid detergent of take is representative is closely bound up with us in the modern life, and we almost will carry out cleaning food (fruit, vegetables etc.) with liquid detergent everyday, cleans tableware.And, after we use, most liquid detergent can flow to Jiang,He,Hu, sea with water drain.Contain strong carcinogen in liquid detergent, inevitably HUMAN HEALTH is produced to injury.
The main component of liquid detergent is secondary derivative---the Sodium dodecylbenzene sulfonate of oil.Everybody should know that three grades of derivatives of oil are pitch, feels sick poisonous; The Sodium dodecylbenzene sulfonate ratio is easier to volatilization, so just added 10% adhesion agent, when people buy the liquid detergent of barreled, chooses specially thick buying, and in fact thicker, the decontamination composition Sodium dodecylbenzene sulfonate that it contains is few on the contrary.After having added adhesion agent, the taste of Sodium dodecylbenzene sulfonate is very pungent, if smell bad is heard, everybody can not go to buy yet, so producer has added again 10% industrial essence, allows liquid detergent that orange flavor lemon is arranged, and everybody just likes using like this; Along with the use of tableware, these compositions such as essence have part can enter human body, and human body is not had to benefit.Liquid detergent is easily oxidation also, and the liquid detergent after oxidation can become green, blueness.Does not but how the liquid detergent of our family have variable color? because producer has added 10% sanitas inside, do not have variable color.We have a meal sometimes in refreshment bar, and in his kitchen, there is green some barrel of the inside, and blue liquid, be exactly the liquid detergent that there is no adding preservative agent in fact, and along with the use of tableware, the compositions such as sanitas have part can enter human body, and human body is not had to benefit.Jilin television station once did an investigation, 9 kinds of liquid detergents on market, after washing tableware, tap water rinses 12 times, can also detect average 0.03% residual, do not look down upon this 0.03%, we are using liquid detergent every day, and we on average rinse and there is no 12 times at all, we have a meal every day, eat soup and just this residue are had in body, one day two days out of question, one or two years, problem was also little, but 10 years, after 20 years, use along with tableware, after these toxin enter human body, can accumulate the health borough chief phase at us, poison health.
Therefore, life-time service chemosynthesis cleaning product, not only to the stimulation of skin, cause pachylosis dry and cracked, and clean not exclusively, residually causes endangering health, simultaneously because being difficult for decomposition, quite serious to the pollution of ambient soil and water body.
Summary of the invention
The preparation method who the objective of the invention is to overcome the above-mentioned deficiency of prior art and a kind of safety and environmental protection tea seed detergent liquid is provided, its technique is simple, and its raw material is common, cheap; By the safety and environmental protection tea seed detergent liquid of its making, stability is high, and sterilization effect is good, detergent power is strong, and biological degradability is high, gentle refreshing hand, low bubble, water-saving; Its nontoxicity, nonirritant, without supersensitivity, can be used as the desirable safety and environmental protection washing products such as cleaning food Work tool, tableware and vegetables, fruit in people's daily life.
Technical scheme of the present invention is: a kind of preparation method of safety and environmental protection tea seed detergent liquid, and it comprises following processing step:
One, produce safety and environmental protection tea seed detergent powder
Take raw material by following proportion by weight: 12～14 parts of camellia seed meals, 3～6 parts, Chinese honey locust, 1～2 part of Leafy twigs of Oriental Arborvitae, 0.1～0.6 part of Silktree Albizzia Bark, 0.1～0.6 part of pomegranate rind, 0.1～0.5 part of natural Broneolum Syntheticum; The raw material of obtaining is pulverized respectively, crossed 55～65 mesh sieves, obtained each raw material powder; By each raw material powder mixing and stirring, obtain mixing meal; By the sterilization of gained mixing meal, obtain safety and environmental protection tea seed detergent powder;
Two, produce concentrated solution
Take raw material by following proportion by weight: 10～20 parts of the safety and environmental protection tea seed detergent powders of step 1 gained, 180～190 parts of deionized waters; The deionized water of 25～35 quality % is added in safety and environmental protection tea seed detergent powder, water temperature is controlled to 36～38 ℃ of stirrings, get supernatant liquor, obtain extracting solution for the first time; Add again 45～55 quality % of remaining deionized water, water temperature is controlled to 36～38 ℃ of stirrings, get supernatant liquor, obtain extracting solution for the second time; Add remaining deionized water, water temperature is controlled to 36～38 ℃ of stirrings, get the liquid after stirring, obtain extracting solution for the third time; Above No. three extracting solutions are mixed, and in the water temperature of 93～97 ℃, water-bath is concentrated into the concentrated solution that concentration is 0.105～0.161 gram effective ingredient/milliliter, to be concentrated in every milliliter of concentrated solution, contains 0.105～0.161 gram safety and environmental protection tea seed detergent powder;
Three, produce safety and environmental protection tea seed detergent liquid
Take raw material by following proportion by weight: 85～95 parts of the concentrated solutions that step 2 obtains, 2～8 parts of AMONYL 380LC, 2～4 parts of cocoanut fatty acid diethanolamides, 0.3～3 part of Xylo-Mucine; After concentrated solution is heated to 75～80 ℃, then other raw material that will obtain adds in concentrated solution, stirs and dissolves fully, is down to normal temperature, and sterilization, obtain safety and environmental protection tea seed detergent liquid.
The further technical scheme of the present invention is: the raw material of step 1 is pulverized by pulverizer respectively; Each raw material powder mix and blend in stirred pot of step 1, churning time is 20～40min; The mixing meal of step 1 is by ultraviolet or microwave disinfection;
The present invention further technical scheme is: while in step 2, producing extracting solution, safety and environmental protection tea seed detergent powder and deionized water are all stirred in stirred pot; Obtaining the churning time of extracting solution for the first time is 2.5～3.5 hours, and obtaining the churning time of extracting solution for the second time is 2.5～3.5 hours, and obtaining the churning time of extracting solution for the third time is 1.5～2.5 hours; Extracting solution in step 2 is concentrated in every milliliter of concentrated solution and contains 0.138 gram safety and environmental protection tea seed detergent powder.
The present invention further technical scheme is: the stirring of step 3 is all carried out in stirred pot; Safety and environmental protection tea seed detergent liquid also will pack after ultraviolet-sterilization.
The present invention also further technical scheme is: step 1 takes raw material by following proportion by weight: 12.5～13.5 parts of camellia seed meals, 3.76～5.26 parts, Chinese honey locust, 1.26～1.76 parts of Leafy twigs of Oriental Arborvitae, 0.24～0.48 part of Silktree Albizzia Bark, 0.22～0.48 part of pomegranate rind, 0.2～0.4 part of natural Broneolum Syntheticum;
Step 2 takes raw material by following proportion by weight: 13～17 parts of safety and environmental protection tea seed detergent powders, 183～187 parts of deionized waters;
Step 3 takes raw material by following proportion by weight: 87.7～92.7 parts of the concentrated solutions that step 2 obtains, 3.5～6.5 parts of AMONYL 380LC, 2.5～3.5 parts of cocoanut fatty acid diethanolamides, 1～2.4 part of Xylo-Mucine.
The further technical scheme of the present invention is: step 1 takes raw material by following proportion by weight: 13 parts of camellia seed meals, 4.5 parts, Chinese honey locust, 1.5 parts of Leafy twigs of Oriental Arborvitae, 0.36 part of Silktree Albizzia Bark, 0.34 part of pomegranate rind, 0.3 part of natural Broneolum Syntheticum;
Step 2 takes raw material by following proportion by weight: 15 parts of safety and environmental protection tea seed detergent powders, 185 parts of deionized waters;
Step 3 takes raw material by following proportion by weight: 90.3 parts of the concentrated solutions that step 2 obtains, 5 parts of AMONYL 380LC, 3 parts of cocoanut fatty acid diethanolamides, 1.7 parts of Xylo-Mucines.
Another technical scheme of the present invention is: a kind of safety and environmental protection tea seed detergent liquid, it makes by aforesaid method.
Main symbol and name resolving that the present invention uses are as follows:
～: numerical range, for example 1～5 means 1 to 5.
The main raw material that the present invention uses is described as follows:
Camellia seed meal: camellia seed kernel is after squeezing, extract technology extract, and residual bits, be referred to as camellia seed meal, and it is containing having an appointment 10% protein, 10% tea polysaccharide, 12% tea saponin, 50% Mierocrystalline cellulose and xylogen.
Leafy twigs of Oriental Arborvitae: (formal name used at school: browse Platycladus orientalis (L.) Franco), the medicinal material Leafy twigs of Oriental Arborvitae has branch to Cupressaceae plant arbor-vitae more, little and different in size, is flakey.Color is sorrel.The visible leaf in surface is mutually to life, the section yellow-white.Quality is crisp, easily fractureed.The micro-perfume (or spice) of gas, a kind of in the blood-cooling hemostatic of bitter and puckery flavor Chinese medicine hemostatic drug, the effect that has hemostasis, black beard and hair, cough-relieving to breathe heavily.[medicine name] Leafy twigs of Oriental Arborvitae [another name] CedarLeaves, Japan cypress leaf, Cong Baiye.Branch and leaf that [medicinal material Ji Yuan] is Cupressaceae plant arbor-vitae.[section's genus] Cupressaceae.[nature and flavor] hardship; Puckery; Cold nature.[return through] lung; Liver; Large intestine channel.[effect] cooling blood for hemostasis; Cough-relieving apophlegmatic; Wind-damp dispelling; Loose pyogenic infections.[effect classification] blood-cooling hemostatic; Medicine for rheumatism.[curing mainly] controls spitting of blood; Spit blood; Bleeding from five sense organs or subcutaneous tissue; Hematuria; Bloody flux; Discharging fresh blood stool; Uterine bleeding is more than; Coughing with a lot of sputum; Rheumatic arthralgia; Erysipelas; Mumps, scald.[attention] " property of medicine opinion ": suitable with wine." book on Chinese herbal medicine is stated ": many foods also can fall stomach.Chemical composition: containing volatile oil, be mainly fenchone (fenchone), camphor, Bornyl acetate, terpene alcohol in oil; And containing juniperic acid (juniperic acid) Quercetin, poplar luteoxanthin (myricetin), kaempferol, hinokiflavone (hinokiflavone), wax etc.; In Leafy twigs of Oriental Arborvitae, containing volatile oil 0.26%, in oil, main component is α-thujone, thujene, fenchone etc.; Other is still containing flavones ingredient, as aromadendrin, Quercetin, myricetin, hinokiflavone etc.; Also contain the trace elements such as potassium, sodium, nitrogen, phosphorus, calcium, magnesium, manganese and zinc in leaf.Pharmacological action: the Leafy twigs of Oriental Arborvitae decoction can obviously shorten bleeding time and clotting time, and its hemostasis effective constituent is Quercetin and tannin.In addition, effects such as antibechic still being arranged, eliminate the phlegm, relieving asthma, be calm; Experiment in vitro shows, these product all have restraining effect to streptococcus aureus, micrococcus catarrhalis, dysentery bacterium, Corynebacterium diphtheriae, diphtheria corynebacterium etc.
Silktree Albizzia Bark: the dry bark for pulse family (Legumin0sae) plant silk tree is curling tubular or half tubular, long 40～80cm, thick Silktree Albizzia Bark 0.1～0.3cm.The outside surface taupe brown is to beige, and nature and flavor are sweet, flat.The merit that Xie Yu and blood, the peaceful heart, subduing inflammation are arranged.English name: Silktree Albizia Bark; Latin literary fame: Cortex Albiziae; Another name: close confused skin (Thousand Golden Prescriptions), CORTEX ALBIZIAE (" side of walking alone "), albizzia skin (" detailed outline ").The effect of Silktree Albizzia Bark: the bark that Silktree Albizzia Bark is the leguminous plants silk tree, Silktree Albizzia Bark another name closes confused skin, night platform skin, albizzia skin, Silktree Albizzia Bark has the Xie Yu that calms the nerves, the effect of carbuncle of disappearing of invigorating blood circulation, Silktree Albizzia Bark has the effect of confused and worried, melancholy, the egersis for the treatment of, inside and outside large carbuncle, wound, Peptic Ulcers and gastritis sufferer be careful takes Silktree Albizzia Bark, and wind-heat spontaneous perspiration, diseases caused by external factors egersis person prohibit and take Silktree Albizzia Bark.
Chinese honey locust: " Chinese medicine voluminous dictionary " record: Chinese honey locust, [different name] chicken son (" wide will) of dwelling }), Chinese honey locust (" Handbook of Prescriptions for Emergencies "), large Chinese honey locust (" prescriptions worth thousand gold "), long Chinese honey locust (" Bencao Tujing "), outstanding cutter (" outer red book on Chinese herbal medicine "), long Chinese honey locust (" side of directing at ").Fruit or sterile fruit that [base is former] is pulse family Gleditsia plant Chinese honey locust.The former claims Chinese honey locust, and the latter claims Fructus Gleditsiae Abnormalis.[processing of gathering] cultivates after 5～6 years is result, during autumn fruit maturation blackening, plucks, and dries.[pharmacology] be phlegm-dispelling functions 1., and this product can stimulate gastric mucosa containing saponin(e, causes that reflectingly the respiratory mucosa secretion increases.Belong to nauseous expectorant.2. anti-microbial effect, the Chinese honey locust preserved material has restraining effect to trichophyton, star-shaped nocardia and some dermatophytes in vitro.
Pomegranate rind: be the pericarp of Punicaceae plant pomegranate.Autumn, the pomegranate fruit maturation, plucked during the cracking of top, removes seed and reach every flesh, and valve cutting is dried, or low baking temperature is dried.Function cures mainly: puckery intestines, hemostasis, expelling parasite.Control for a long time and rush down, protracted dysentery, have blood in stool, prolapse of the anus, and involuntary emission, uterine bleeding, under band, abdominal pain due to worm stagnation, mange.
Natural Broneolum Syntheticum: another name: d-Bomeol, English name: BORNEOLUM, the fresh branch that this product is canella camphor tree Cinnamomumcamphora (L.) Presl, the crystallization that leaf is processed into through extraction, this product is containing d-Bomeol (C
10h
18o) must not be less than 95.0%.[nature and flavor] are hot, bitter, cool.[function with the cure mainly] inducing resuscitation of having one's ideas straightened out, clearing away heat to and alleviating pain.For pyreticosis coma, convulsion, faint, apoplexy coma due to blocking of the respiratory system, frightened epilepsy phlegm fan, larynx numbness dentalgia, aphtha large carbuncle, hot eyes.
Deionized water: deionized water refers to and has removed the pure water be after ionic species impurity.
AMONYL 380LC: be a kind of zwitterionics, all there is good stability under acidity and alkaline condition, present respectively sun and anionic property, normal and yin, yang ion and nonionogenic tenside use, its compatibility is good.Pungency is little, soluble in water, and to ph stability, foam is many, and strong detergency has good thickening property, flexibility, bactericidal properties, static resistance, anti-hard water.Can significantly improve softness, conditioning and the low-temperature stability of washing series products.Production technique: take Oleum Cocois as raw material, by the condensation with N, N dimethylated propyl diethylenetriamine, generate PKO again and the quaternized two-step reaction of sodium chloroacetate (Monochloro Acetic Acid and sodium carbonate make), produce AMONYL 380LC, productive rate reaches 90% left and right.Molecular formula: C
19h
38n
2o
3.Product performance: 1. good solvability and compatibleness are arranged; 2. there is good foaminess and significant thickening property; 3. have low irritant and bactericidal properties, compatibility is used softness, conditioning and the low-temperature stability that can significantly improve the washing series products; 4. there is good anti-hard water, static resistance and biological degradability.5. adopt the natural raw material preparation be easy to get, the performance gentleness, have good security, and its toxicity index all belongs to advanced index, to human body and environment, can not cause risk.
Cocoanut fatty acid diethanolamide: English name: Coconutt Diethanol Amide; Be called for short: CDEA; Trade(brand)name: 6501, Ninol; Another name: N.N-double hydroxyethyl alkylamide, lauric acid amide of ethanol, coconut oil diethanol amide, alkylol amide; Molecular formula: C
11h
23cON (CH
2cH
2oH)
2; Purposes: can strengthen cleaning effect, can be used as additive, foam tranquilizer, foaming aids, be mainly used in the manufacture of shampoo and liquid washing agent.Form a kind of opaque vaporific solution in water, can be fully transparent under certain stirring, under finite concentration, can be dissolved in fully in different types of tensio-active agent, in low-carbon (LC) and high-carbon, also can dissolve fully.Its biological degradability can reach 99%.
Xylo-Mucine: being the widest, the maximum Mierocrystalline cellulose kind of consumption of use range in the world today, is also to generally acknowledge safest foodstuff additive.Claim again: sodium carboxymethyl-cellulose, carboxymethyl cellulose, CMC, Carboxymethyl, Cellulose Sodium, Sodium salt of Caboxy Methyl Cellulose.Chinese another name: CMC salt; Sodium carboxymethyl-cellulose; Carmethose; English name: Carboxymethylcellulose sodium.Molecular formula: C
8h
16naO
8.Its sodium salt that is carboxymethyl cellulose ether, belong to the anionic ether of cellulose, is white or oyster white fibrous powder or particle, density 0.5-0.7 g/cc, odorless, tasteless almost, tool water absorbability.Be easy to be dispersed in water into transparent colloidal solution, insoluble in the organic solvents such as ethanol.1% aqueous solution pH is 6.5～8.5, as pH > 10 or<5 the time, rubber cement viscosity significantly reduces, performance the best when pH=7.To thermally-stabilised, 20 ℃ of following viscosity, rise rapidly, in the time of 45 ℃, change slowlyer, more than 80 ℃, long-time heating can make its colloid sex change and viscosity and performance obviously descend.Soluble in water, solution is transparent; Very stable in basic solution, meet facile hydrolysis of acid, pH value there will be precipitation while being 2-3, meet polyvalent metal salt and also can react the appearance precipitation.Be used as thickening material in foodstuffs industry, be used as pharmaceutical carrier in medicine industry, be used as cakingagent in daily chemical industry, resist dignified dose again.Be used as the protective colloid of sizing agent and printing gum etc. in printing and dyeing industry.Can be used as oil recovery fracturing liquid composition in petrochemical complex.
" Chinese medicine voluminous dictionary ": " Chinese medicine voluminous dictionary " second edition is write by Nanjing University of Traditional Chinese Medicine, and Shanghai Century publishes limited-liability company and Shanghai science tech publishing house publishes and distributes.
Usage and dosage:
Safety and environmental protection tea seed detergent liquid of the present invention adds tablewares such as splashing in right amount dish, then cleans with rag, and then clear water washes down; Or directly be poured into water stirring, immersion, after washing with rag, then wash with Qing Shui Red.
The present invention compared with prior art has following features:
1. safety and environmental protection tea seed detergent liquid of the present invention adopts plant and phytosynthesis preparation of raw material, and its biological degradability and stability are high.
2. safety and environmental protection tea seed detergent liquid of the present invention is after use, the gentle refreshing hand of hand sensation, the care of its any one single raw material that ratio adopts or other current chemical washing product is eager to excel (in using practice, testing crew has all confirmed this advantage, but not concrete index and the detection data of detecting).
3. to have a detergent power strong for safety and environmental protection tea seed detergent liquid of the present invention, low bubble, water-saving advantage.
Safety and environmental protection tea seed detergent liquid of the present invention to the antibacterial of Salmonella typhi, staphylococcus epidermidis, streptococcus aureus, beta hemolytic streptococcus with and germicidal action be better than camellia seed meal, that is to say that safety and environmental protection tea seed detergent liquid of the present invention has improved germicidal action with respect to its main raw material camellia seed meal, safety and environmental protection tea seed detergent liquid of the present invention is better as the washes disinfectant properties than using separately camellia seed meal.
5. safety and environmental protection tea seed detergent liquid of the present invention is without obvious animal toxicity, harmless, safety.
6. safety and environmental protection tea seed detergent liquid percutaneous drug delivery of the present invention, to complete normal skin and the equal nonirritant of damaged skin, environmental protection.
7. safety and environmental protection tea seed detergent liquid of the present invention without supersensitivity.
Safety and environmental protection tea seed detergent liquid stability of the present invention is high in sum, and sterilization effect is good, detergent power is strong, and biological degradability is high, gentle refreshing hand, low bubble, water-saving.Nontoxicity, nonirritant, without supersensitivity, it adopts plant and phytosynthesis preparation of raw material fully, not containing any chemical industry essence, sanitas, whitening agent, hand is not hindered in washing, after washing, can not cause anything to pollute to environment yet, can be used as safety and environmental protection washing product desirable in people's daily life and use.
In order to be illustrated more clearly in the present invention, enumerate following examples and detect test situation, but it to be without any restrictions to scope of invention.
Embodiment
embodiment 1
A kind of preparation method of safety and environmental protection tea seed detergent liquid, it mainly comprises following processing step:
One, produce safety and environmental protection tea seed detergent powder
Get 13 kilograms of camellia seed meals, 4.5 kilograms, Chinese honey locust, 1.5 kilograms of Leafy twigs of Oriental Arborvitae, 0.36 kilogram of Silktree Albizzia Bark, 0.34 kilogram of pomegranate rind, 0.3 kilogram of natural Broneolum Syntheticum; These raw material compositions are all the quality after drying; To obtain raw material and be pulverized by pulverizer respectively, cross 55～65 mesh sieves, obtain each raw material powder; Each raw material powder is put into to stirred pot, mix and blend, churning time is 20～40min, obtains mixing meal; Gained mixing meal, by ultraviolet or microwave disinfection, is obtained to safety and environmental protection tea seed detergent powder;
Two, produce safety and environmental protection tea seed detergent powder concentrated solution
Get 15 kilograms of safety and environmental protection tea seed detergent powders, 185 kilograms of the deionized waters of step 1 gained;
Get the safety and environmental protection tea seed detergent powder of step 1 gained and put into stirred pot, by 25～35 quality %(185 kilograms of deionized water 25～35%) add and put into stirred pot, water temperature is controlled to 36～38 ℃ (being preferably 37 ℃) and stirs 2.5～3.5 hours (being generally 3 hours), get supernatant liquor, obtain extracting solution for the first time; 45～55 quality % to adding again remaining deionized water in stirred pot, be controlled at 36～38 ℃ (being preferably 37 ℃) by water temperature and stir 2.5～3.5 hours (being generally 3 hours), gets supernatant liquor, obtains extracting solution for the second time; Add remaining deionized water in stirred pot, water temperature is controlled to 36～38 ℃ (being preferably 37 ℃) and stirs 1.5～2.5 hours (being generally 2 hours), get the liquid (having there is no what slag) in stirred pot, obtain extracting solution for the third time; By the liquid mixing obtained for above three times, being concentrated into concentration 93～97 ℃ of (being preferably 95 ℃) waters bath with thermostatic control is that 0.105～0.161(is preferably 0.138) concentrated solution of gram effective ingredient/milliliter, effective ingredient refers to the safety and environmental protection tea seed detergent powder obtained in the first step, is concentrated into to contain 0.105～0.161(in every milliliter of concentrated solution and be preferably 0.138) gram safety and environmental protection tea seed detergent powder;
Three, produce safety and environmental protection tea seed detergent liquid
Get 3 kilograms of 5 kilograms of 90.3 kilograms of concentrated solutions, AMONYL 380LC, cocoanut fatty acid diethanolamides, 1.7 kilograms of Xylo-Mucines that step 2 obtains; Concentrated solution is put into to stirred pot, and after being heated to 75～80 ℃ (being preferably 78 ℃), then other raw material that will obtain adds in stirred pot, stirs and dissolves fully, is down to normal temperature, after ultraviolet-sterilization, packs, and finally obtains safety and environmental protection tea seed detergent liquid.
embodiment 2-12
The raw material that embodiment 2-12 is used is all kinds of identical with embodiment 1, and its step of preparation process is also identical with embodiment 1, is only the functional quality of raw material and embodiment 1 difference to some extent; Following table 1 shows the raw material that each embodiment step 1 is used, and table 2 shows the raw material that each embodiment step 2 is used, and table 3 shows the raw material that each embodiment step 3 is used.
Table 1
Table 2
Table 3
detect and test
The applicant delivers to by the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention detection and the test that special detection mechanism has carried out system, and it is as follows that it mainly detects test-results.
One. by the safety and environmental protection tea seed detergent liquid of above each embodiment gained, by check active matter content, detergent power (GB 9985-2000 detection) etc., obtain the detected result shown in following table 4:
Table 4
Can find out that from above table 4 the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention has advantages of that detersive power is good, nontoxic etc.
Two. anti-microbial effect detects
1. antibacterial range detects (mensuration of inhibition zone diameter size)
Purpose: the utilization agar diffusion method detects the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention and camellia seed meal is wide to distributing in environment, resistibility is strong, can cause that the pathogenic bacterium of food spoilage, food poisoning, pyogenic infection have anti-microbial effect, clear and definite its antibacterial range.
Method: cut-off footpath 12cm plate, impouring substratum 15ml, the cotton swab with sterilizing after condensation dips the test organisms bacterium liquid for the logarithmic phase of specialized range density, is uniformly coated on media surface.Then be put in flat board with aseptic nipper gripping sterilizing Oxford cup, add the safety and environmental protection tea seed detergent liquid 200ul of various embodiments of the present invention in each Oxford cup, and carry out three parallel tests.Take out after 24 hours of 37 ℃ of cultivations, survey inhibition zone diameter, and obtain the mean value of three parallel test inhibition zone diameters.Use the same method and adopt the camellia seed meal solution of same concentrations to carry out the comparison and detection test.
Result: see the following form shown in 5.
The comparison and detection result of table 5. antibacterial range
2. antibiotic degree detecting (MIC; The mensuration of MBC)
Purpose: the antibiotic degree of pathogenic bacterium that utilization liquid diluting method detects the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention and 8 above different concns points of camellia seed meal are wide to distributing in environment, resistibility is strong, can cause food spoilage, food poisoning, pyogenic infection, detect minimum inhibitory concentration (MIC) and minimum bactericidal concentration (MBC), clear and definite its antibiotic degree.
Method: get some of sterile test tube, after doubly diluting the safety and environmental protection tea seed detergent powder liquid of various embodiments of the present invention with liquid nutrient medium etc., each pipe adds 0.1ml for examination bacterium liquid, establish substratum control tube and bacterium liquid control tube simultaneously, take out and see result after 37 ℃ of cultivation 24h, in the satisfactory situation of control tube, observe one by one each developmental tube, take can inhibition test the high dilution of powder liquid of bacteria growing be minimum inhibitory concentration (MIC), and the culture in the test tube of each asepsis growth is forwarded on the agar plate of corresponding substratum, take out and see result after 37 ℃ of cultivation 24h, the high dilution of safety and environmental protection tea seed detergent powder liquid of the various embodiments of the present invention of killing 99.9% test organisms thalline of take is minimum bactericidal concentration (MBC).Use the same method and adopt the camellia seed meal solution of same concentrations to carry out the comparison and detection test.
Result: see the following form shown in 6.
The comparison and detection result (mg/mL) of the antibiotic degree of table 6.
Conclusion: can find out from table 5,6, the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention obviously is better than camellia seed meal to the antibacterial and germicidal action of staphylococcus epidermidis, streptococcus aureus, Candida albicans bacterium, beta hemolytic streptococcus, the safety and environmental protection tea seed detergent liquid that is to say various embodiments of the present invention has improved germicidal action with respect to its main raw material camellia seed meal, and the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention is better as the washes disinfectant properties than using separately camellia seed meal.
Three. detergent action detects
Purpose: the safety and environmental protection tea seed detergent powder liquid of test various embodiments of the present invention and the camellia seed meal solution detergent power of same concentrations.
Method: by the safety and environmental protection tea seed detergent liquid of distilled water, various embodiments of the present invention and the camellia seed meal solution of same concentrations, by GB GB9985-2000 method, measure detergent power.
Result: see the following form shown in 7.
The comparison and detection result (N=6, %) of table 7. detergent action
Conclusion: as can be seen from Table 7: the detersive power of the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention is distilled water 2.6 times, for 1.8 times of camellia seed meal, the detergency of testing the safety and environmental protection tea seed detergent liquid that also shows various embodiments of the present invention is more much better than than simple camellia seed meal.
Four. animal toxicity test
Purpose: observe rabbit intact skin and damaged skin and contact in a short time the toxic reaction produced after tested material (the safety and environmental protection tea seed detergent liquids of embodiments of the invention), for the safety and environmental protection tea seed detergent liquid of embodiments of the invention provides the security foundation.
Method: select 12 of white new zealand rabbits, be divided at random 3 groups, 4 every group.A group: intact skin group, B group: damaged skin group, C group: blank group.The test position is skin of back, control group is to distilled water, the tested material group is to the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention, directly be coated on intact skin and damaged skin, Tu Houfu is with polyethylene film, then gauze is fixed, guarantee itself and skin contact 24 hours, be coated with examination after 24 hours, as be not poisoned to death, available warm water or other nonirritant solvents go tested material (the safety and environmental protection tea seed detergent liquids of various embodiments of the present invention).Continuous Observation 7 days, observe and record whole body poisoning manifestations and death condition to animal after tested material every day, comprises the variation of the weight of animals, skin, hair, eyes and mucous membrane, the variation of breathing, circulation, central nervous system, four limbs activity etc.
Result: white new zealand rabbit gives to have no whole body poisoning manifestations and death condition after the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention, and the weight of animals increases, on breathing, circulation, central nervous system, four limbs activity etc. without impact.Damaged skin is had no to erythema, oedema.
Conclusion: the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention is to white new zealand rabbit intact skin and damaged skin non-toxic reaction.
Five. irritation test
Purpose: detect the skin irritation reaction of the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention, for clinical application provides the security foundation.
Method: carry out according to the relevant requirements in " irritation test and skin allergy test governing principle ".Rabbit skin gives the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention, chemical liquid detergent, distilled water, observes the skin irritation reaction.
Result: after rabbit skin gives the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention, intact skin and damaged skin are showed no to the skin irritation reactions such as erythema, oedema.After rabbit skin gives chemical liquid detergent, intact skin is showed no to the skin irritation reactions such as erythema, oedema, damaged skin is shown in to the skin irritation reactions such as obvious erythema, oedema.
Conclusion: the safety and environmental protection tea seed detergent liquid percutaneous drug delivery of various embodiments of the present invention, to complete normal skin and the equal nonirritant of damaged skin.And chemical liquid detergent produces pungency to damaged skin.
Six. skin allergy test
Purpose: the anaphylaxis of the intact skin of the safety and environmental protection tea seed detergent liquid of detection various embodiments of the present invention, for clinical application provides the security foundation.
Method: carry out according to the relevant requirements in " irritation test and skin allergy test governing principle ", the cavy sensitization contact and excite the contact detection various embodiments of the present invention safety and environmental protection tea seed detergent liquid, distilled water and positive control medicine 2, the 4-dinitrochlorobenzene, observe the skin hypersensitivity reaction.
Result: cavy detect various embodiments of the present invention safety and environmental protection tea seed detergent liquid after, do not find that the anaphylaxis such as erythema, oedema appear in the local skin of tested cavy.
Conclusion: the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention without supersensitivity.
Seven, Detection of Stability
1, under normal temperature, test 1 year, the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention is without demixing phenomenon.
2, place 24 h in the refrigerator of subzero 3 ℃ to subzero 10 ℃, take out while returning to room temperature and observe, the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention is without crystallization, without precipitation; Place 24 h in the insulation can of (40 scholar I) ℃, take out immediately and observe, the safety and environmental protection tea seed detergent liquid of various embodiments of the present invention is not stratified, haze-free, and does not change original tea dregs of rice smell.
Eight, biological degradability
According to GB/T15818 surfactant biodegradation test method, the biological degradability of the safety and environmental protection tea seed detergent liquid gross activity thing of various embodiments of the present invention reaches more than 99%.
Claims (10)
1. the preparation method of a safety and environmental protection tea seed detergent liquid, it is characterized in that: it comprises following processing step:
One, produce safety and environmental protection tea seed detergent powder
Take raw material by following proportion by weight: 12～14 parts of camellia seed meals, 3～6 parts, Chinese honey locust, 1～2 part of Leafy twigs of Oriental Arborvitae, 0.1～0.6 part of Silktree Albizzia Bark, 0.1～0.6 part of pomegranate rind, 0.1～0.5 part of natural Broneolum Syntheticum; The raw material of obtaining is pulverized respectively, crossed 55～65 mesh sieves, obtained each raw material powder; By each raw material powder mixing and stirring, obtain mixing meal; By the sterilization of gained mixing meal, obtain safety and environmental protection tea seed detergent powder;
Two, produce concentrated solution
Take raw material by following proportion by weight: 10～20 parts of the safety and environmental protection tea seed detergent powders of step 1 gained, 180～190 parts of deionized waters; The deionized water of 25～35 quality % is added in safety and environmental protection tea seed detergent powder, water temperature is controlled to 36～38 ℃ of stirrings, get supernatant liquor, obtain extracting solution for the first time; Add again 45～55 quality % of remaining deionized water, water temperature is controlled to 36～38 ℃ of stirrings, get supernatant liquor, obtain extracting solution for the second time; Add remaining deionized water, water temperature is controlled to 36～38 ℃ of stirrings, get the liquid after stirring, obtain extracting solution for the third time; Above No. three extracting solutions are mixed, and in the water temperature of 93～97 ℃, water-bath is concentrated into the concentrated solution that concentration is 0.105～0.161 gram effective ingredient/milliliter, to be concentrated in every milliliter of concentrated solution, contains 0.105～0.161 gram safety and environmental protection tea seed detergent powder;
Three, produce safety and environmental protection tea seed detergent liquid
Take raw material by following proportion by weight: 85～95 parts of the concentrated solutions that step 2 obtains, 2～8 parts of AMONYL 380LC, 2～4 parts of cocoanut fatty acid diethanolamides, 0.3～3 part of Xylo-Mucine; After concentrated solution is heated to 75～80 ℃, then other raw material that will obtain adds in concentrated solution, stirs and dissolves fully, is down to normal temperature, and sterilization, obtain safety and environmental protection tea seed detergent liquid.
2. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 1, it is characterized in that: the raw material of step 1 is pulverized by pulverizer respectively; Each raw material powder mix and blend in stirred pot of step 1, churning time is 20～40min; The mixing meal of step 1 is by ultraviolet or microwave disinfection.
3. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 1 and 2, it is characterized in that: while in step 2, producing extracting solution, safety and environmental protection tea seed detergent powder and deionized water are all stirred in stirred pot; Obtaining the churning time of extracting solution for the first time is 2.5～3.5 hours, and obtaining the churning time of extracting solution for the second time is 2.5～3.5 hours, and obtaining the churning time of extracting solution for the third time is 1.5～2.5 hours; Extracting solution in step 2 is concentrated in every milliliter of concentrated solution and contains 0.138 gram safety and environmental protection tea seed detergent powder.
4. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 1 and 2, it is characterized in that: the stirring of step 3 is all carried out in stirred pot; Safety and environmental protection tea seed detergent liquid also will pack after ultraviolet-sterilization.
5. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 3, it is characterized in that: the stirring of step 3 is all carried out in stirred pot; Safety and environmental protection tea seed detergent liquid also will pack after ultraviolet-sterilization.
6. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 1 and 2, it is characterized in that: step 1 takes raw material by following proportion by weight: 12.5～13.5 parts of camellia seed meals, 3.76～5.26 parts, Chinese honey locust, 1.26～1.76 parts of Leafy twigs of Oriental Arborvitae, 0.24～0.48 part of Silktree Albizzia Bark, 0.22～0.48 part of pomegranate rind, 0.2～0.4 part of natural Broneolum Syntheticum;
Step 2 takes raw material by following proportion by weight: 13～17 parts of safety and environmental protection tea seed detergent powders, 183～187 parts of deionized waters;
Step 3 takes raw material by following proportion by weight: 87.7～92.7 parts of the concentrated solutions that step 2 obtains, 3.5～6.5 parts of AMONYL 380LC, 2.5～3.5 parts of cocoanut fatty acid diethanolamides, 1～2.4 part of Xylo-Mucine.
7. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 3, it is characterized in that: step 1 takes raw material by following proportion by weight: 12.5～13.5 parts of camellia seed meals, 3.76～5.26 parts, Chinese honey locust, 1.26～1.76 parts of Leafy twigs of Oriental Arborvitae, 0.24～0.48 part of Silktree Albizzia Bark, 0.22～0.48 part of pomegranate rind, 0.2～0.4 part of natural Broneolum Syntheticum;
Step 2 takes raw material by following proportion by weight: 13～17 parts of safety and environmental protection tea seed detergent powders, 183～187 parts of deionized waters;
Step 3 takes raw material by following proportion by weight: 87.7～92.7 parts of the concentrated solutions that step 2 obtains, 3.5～6.5 parts of AMONYL 380LC, 2.5～3.5 parts of cocoanut fatty acid diethanolamides, 1～2.4 part of Xylo-Mucine.
8. the preparation method of safety and environmental protection tea seed detergent liquid according to claim 1 and 2, it is characterized in that: step 1 takes raw material by following proportion by weight: 13 parts of camellia seed meals, 4.5 parts, Chinese honey locust, 1.5 parts of Leafy twigs of Oriental Arborvitae, 0.36 part of Silktree Albizzia Bark, 0.34 part of pomegranate rind, 0.3 part of natural Broneolum Syntheticum;
Step 2 takes raw material by following proportion by weight: 15 parts of safety and environmental protection tea seed detergent powders, 185 parts of deionized waters;
Step 3 takes raw material by following proportion by weight: 90.3 parts of the concentrated solutions that step 2 obtains, 5 parts of AMONYL 380LC, 3 parts of cocoanut fatty acid diethanolamides, 1.7 parts of Xylo-Mucines.
9. a safety and environmental protection tea seed detergent liquid is characterized in that: it is that preparation method by the described safety and environmental protection tea of claim 1 or 2 seed detergent liquid makes.
10. a safety and environmental protection tea seed detergent liquid is characterized in that: it is that preparation method by safety and environmental protection tea seed detergent liquid claimed in claim 7 makes.
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| CN106590983A (en) * | 2016-11-23 | 2017-04-26 | 郑州源冉生物技术有限公司 | Safe and environment-friendly bactericidal detergent for kitchen and preparation method of bactericidal detergent |
| CN108865518A (en) * | 2018-08-28 | 2018-11-23 | 河南省联兴油茶产业开发有限公司 | Cleaning solution and preparation method thereof |
| CN109957466A (en) * | 2017-12-23 | 2019-07-02 | 青岛麦迪尔生物工程有限公司 | A kind of melon and fruit dish washing detergent |
| CN115141851A (en) * | 2022-08-12 | 2022-10-04 | 江苏雪豹日化有限公司 | Degreasing detergent for kitchens and preparation method and application thereof |
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| CN108913403A (en) * | 2018-08-28 | 2018-11-30 | 湖南大三湘茶油股份有限公司 | Detergent and preparation method thereof |
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| CN102973469A (en) * | 2012-12-25 | 2013-03-20 | 江南大学 | Mild hand sanitizer containing camellia oil cake extract |
| CN103232904A (en) * | 2013-04-02 | 2013-08-07 | 安徽省旌德县祥云绿色食品有限公司 | Tea seed meal cleaning ball, its preparation method and application |
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| CN109957466A (en) * | 2017-12-23 | 2019-07-02 | 青岛麦迪尔生物工程有限公司 | A kind of melon and fruit dish washing detergent |
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Inventor after: Lai Qiongwei Inventor after: Yu Dejun Inventor after: Tian Si Inventor after: Liu Fang Inventor after: Yang Jie Inventor after: Duan Wenxiu Inventor after: Yang Yaoxue Inventor after: Liao Guang Inventor after: Pei Jianru Inventor after: Lu Fangguo Inventor after: Tian Hua Inventor after: Kong Yingge Inventor after: Huang Bo Inventor after: Chen Jinsong Inventor after: Liu Haicheng Inventor after: Gu Wenao Inventor before: Lai Qiongwei Inventor before: Pei Jianru Inventor before: Lu Fangguo Inventor before: Tian Hua Inventor before: Kong Yingge Inventor before: Huang Bo Inventor before: Chen Jinsong |
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Free format text: CORRECT: INVENTOR; FROM: LAI QIONGWEI PEI JIANRU LU FANGGUO TIAN HUA KONG YINGGE HUANG BO CHEN JINSONG TO: LAI QIONGWEI PEI JIANRU LU FANGGUO TIAN HUA KONG YINGGE HUANG BO CHEN JINSONG LIU HAICHENG GU WENAO YU DEJUN TIAN SI LIU FANG YANG JIE DUAN WENXIU YANG YAOXUE LIAO GUANG |
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Address after: 421311 Hengnan City, Hunan province gathered in the industrial park, Hengyang Patentee after: Hunan Dasanxiang Camellia Oil Technology Co., Ltd. Address before: 421311 Hengnan City, Hunan province gathered in the industrial park, Hengyang Patentee before: Hunan Great Sanxiang Camellia Technology Co., Ltd. |
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Effective date of registration: 20200323 Address after: 410205 16 / F, building 8, Xincheng science and Technology Park, 588 yueluxi Avenue, Changsha hi tech Development Zone, Changsha City, Hunan Province Patentee after: HUNAN GREEN TEA EXTRACT COSMETICS Co.,Ltd. Address before: 421311 Hengnan County, Hunan City, Hengyang Province, gathered in the Industrial Park Patentee before: HUNAN GREAT SANXIANG CAMELLIA OIL RESOURCES Co.,Ltd. |
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