CN107331523A - 一种活性炭/碳纳米管/石墨烯复合材料及其制备方法和应用 - Google Patents
一种活性炭/碳纳米管/石墨烯复合材料及其制备方法和应用 Download PDFInfo
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- CN107331523A CN107331523A CN201710612851.5A CN201710612851A CN107331523A CN 107331523 A CN107331523 A CN 107331523A CN 201710612851 A CN201710612851 A CN 201710612851A CN 107331523 A CN107331523 A CN 107331523A
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- carbon
- graphene
- composite material
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- activated carbon
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 348
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 128
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 91
- 239000002131 composite material Substances 0.000 title claims abstract description 78
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 239000003990 capacitor Substances 0.000 claims abstract description 23
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910001416 lithium ion Inorganic materials 0.000 claims abstract description 19
- 238000003828 vacuum filtration Methods 0.000 claims abstract description 5
- 230000009467 reduction Effects 0.000 claims description 43
- 238000002604 ultrasonography Methods 0.000 claims description 26
- 239000000725 suspension Substances 0.000 claims description 25
- 239000008367 deionised water Substances 0.000 claims description 20
- 229910021641 deionized water Inorganic materials 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 11
- 239000004094 surface-active agent Substances 0.000 claims description 11
- 238000012545 processing Methods 0.000 claims description 4
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- KAESVJOAVNADME-UHFFFAOYSA-N Pyrrole Chemical compound C=1C=CNC=1 KAESVJOAVNADME-UHFFFAOYSA-N 0.000 claims 2
- 230000006641 stabilisation Effects 0.000 claims 1
- 238000011105 stabilization Methods 0.000 claims 1
- 229920002554 vinyl polymer Polymers 0.000 claims 1
- LLYXJBROWQDVMI-UHFFFAOYSA-N 2-chloro-4-nitrotoluene Chemical compound CC1=CC=C([N+]([O-])=O)C=C1Cl LLYXJBROWQDVMI-UHFFFAOYSA-N 0.000 abstract description 60
- 239000007772 electrode material Substances 0.000 abstract description 20
- 239000000463 material Substances 0.000 abstract description 13
- 230000004888 barrier function Effects 0.000 abstract description 11
- 239000006258 conductive agent Substances 0.000 abstract description 10
- 239000011230 binding agent Substances 0.000 abstract description 7
- 150000001875 compounds Chemical class 0.000 abstract description 6
- 239000011165 3D composite Substances 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 4
- 238000012360 testing method Methods 0.000 description 23
- 239000006185 dispersion Substances 0.000 description 17
- 230000000694 effects Effects 0.000 description 17
- 238000000034 method Methods 0.000 description 15
- -1 graphite Alkene Chemical class 0.000 description 14
- 239000010410 layer Substances 0.000 description 14
- 239000012528 membrane Substances 0.000 description 14
- 239000002002 slurry Substances 0.000 description 14
- 239000003792 electrolyte Substances 0.000 description 13
- 239000002041 carbon nanotube Substances 0.000 description 12
- 239000003610 charcoal Substances 0.000 description 11
- 230000008569 process Effects 0.000 description 11
- 238000000967 suction filtration Methods 0.000 description 11
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical group C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 10
- 229920003081 Povidone K 30 Polymers 0.000 description 10
- 238000001035 drying Methods 0.000 description 10
- 229910002804 graphite Inorganic materials 0.000 description 10
- 239000010439 graphite Substances 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 9
- MHCFAGZWMAWTNR-UHFFFAOYSA-M lithium perchlorate Chemical compound [Li+].[O-]Cl(=O)(=O)=O MHCFAGZWMAWTNR-UHFFFAOYSA-M 0.000 description 9
- 229910001486 lithium perchlorate Inorganic materials 0.000 description 9
- 239000004698 Polyethylene Substances 0.000 description 8
- 238000004146 energy storage Methods 0.000 description 8
- 229920000573 polyethylene Polymers 0.000 description 8
- 239000000203 mixture Substances 0.000 description 7
- 150000004040 pyrrolidinones Chemical class 0.000 description 7
- 239000011149 active material Substances 0.000 description 6
- 229910021393 carbon nanotube Inorganic materials 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 229910021392 nanocarbon Inorganic materials 0.000 description 5
- 150000001336 alkenes Chemical class 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000006479 redox reaction Methods 0.000 description 3
- 230000002441 reversible effect Effects 0.000 description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- 239000002238 carbon nanotube film Substances 0.000 description 2
- 239000003575 carbonaceous material Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000000280 densification Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000002114 nanocomposite Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 241000446313 Lamella Species 0.000 description 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 229910009361 YP-50F Inorganic materials 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000002322 conducting polymer Substances 0.000 description 1
- 239000002482 conductive additive Substances 0.000 description 1
- 229920001940 conductive polymer Polymers 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000005518 electrochemistry Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229920000767 polyaniline Polymers 0.000 description 1
- 229920000128 polypyrrole Polymers 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 238000001338 self-assembly Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000003319 supportive effect Effects 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/04—Hybrid capacitors
- H01G11/06—Hybrid capacitors with one of the electrodes allowing ions to be reversibly doped thereinto, e.g. lithium ion capacitors [LIC]
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/24—Electrodes characterised by structural features of the materials making up or comprised in the electrodes, e.g. form, surface area or porosity; characterised by the structural features of powders or particles used therefor
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/34—Carbon-based characterised by carbonisation or activation of carbon
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/36—Nanostructures, e.g. nanofibres, nanotubes or fullerenes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/50—Electrodes characterised by their material specially adapted for lithium-ion capacitors, e.g. for lithium-doping or for intercalation
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Nanotechnology (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
Description
Claims (10)
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CN201710612851.5A CN107331523B (zh) | 2017-07-25 | 2017-07-25 | 一种活性炭/碳纳米管/石墨烯复合材料及其制备方法和应用 |
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CN201710612851.5A CN107331523B (zh) | 2017-07-25 | 2017-07-25 | 一种活性炭/碳纳米管/石墨烯复合材料及其制备方法和应用 |
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CN107331523A true CN107331523A (zh) | 2017-11-07 |
CN107331523B CN107331523B (zh) | 2019-10-15 |
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CN201710612851.5A Active CN107331523B (zh) | 2017-07-25 | 2017-07-25 | 一种活性炭/碳纳米管/石墨烯复合材料及其制备方法和应用 |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108807008A (zh) * | 2018-06-06 | 2018-11-13 | 广东天劲新能源科技股份有限公司 | 一种锂离子电容器用纳米针状柔性钛酸锂/碳纳米管/石墨烯复合材料及其制备方法 |
CN109950054A (zh) * | 2019-03-13 | 2019-06-28 | 镇江市高等专科学校 | 一种三元碳基复合电极材料及其制备方法和应用 |
CN109985534A (zh) * | 2017-12-30 | 2019-07-09 | 浙江大学 | 一种纯活性炭过滤膜及其制备方法与应用 |
CN110797202A (zh) * | 2019-09-26 | 2020-02-14 | 威海三合永新能源科技有限公司 | 一种碳纳米管/石墨烯/活性炭复合电极材料及其制备方法及其应用 |
CN111223684A (zh) * | 2020-01-07 | 2020-06-02 | 西安理工大学 | 一种咖啡渣基超级电容器电极材料的制备方法 |
CN111243870A (zh) * | 2020-01-14 | 2020-06-05 | 中国科学院苏州纳米技术与纳米仿生研究所南昌研究院 | 柔性自支撑中空活性炭微管基复合薄膜电极、制法与应用 |
CN111628176A (zh) * | 2020-06-17 | 2020-09-04 | 苏州盟维动力科技有限公司 | 多组分三维导电碳网络、自支撑复合电极、其制法及应用 |
CN113053676A (zh) * | 2021-03-18 | 2021-06-29 | 合肥工业大学 | 一种复合薄膜电极材料及其电极与制备方法 |
CN113690428A (zh) * | 2021-08-24 | 2021-11-23 | 北京化工大学 | 一种SiOx/碳纳米管/石墨烯复合膜及其制备方法 |
CN115548246A (zh) * | 2022-08-30 | 2022-12-30 | 哈尔滨工程大学 | 一种锂亚硫酰氯电池正极反应载体材料的制备方法 |
EP4128298A4 (en) * | 2020-03-24 | 2024-05-01 | Yazaki Corp | SUPERCAPACITOR CELL WITH CARBONACEOUS ELECTRODE FREE OF HIGH-PURITY BINDER |
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CN102719693A (zh) * | 2012-06-11 | 2012-10-10 | 上海交通大学 | 石墨烯与碳纳米管混杂增强金属基复合材料及其制备方法 |
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Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109985534A (zh) * | 2017-12-30 | 2019-07-09 | 浙江大学 | 一种纯活性炭过滤膜及其制备方法与应用 |
CN108807008A (zh) * | 2018-06-06 | 2018-11-13 | 广东天劲新能源科技股份有限公司 | 一种锂离子电容器用纳米针状柔性钛酸锂/碳纳米管/石墨烯复合材料及其制备方法 |
CN109950054A (zh) * | 2019-03-13 | 2019-06-28 | 镇江市高等专科学校 | 一种三元碳基复合电极材料及其制备方法和应用 |
CN110797202A (zh) * | 2019-09-26 | 2020-02-14 | 威海三合永新能源科技有限公司 | 一种碳纳米管/石墨烯/活性炭复合电极材料及其制备方法及其应用 |
CN111223684B (zh) * | 2020-01-07 | 2021-12-17 | 西安理工大学 | 一种咖啡渣基超级电容器电极材料的制备方法 |
CN111223684A (zh) * | 2020-01-07 | 2020-06-02 | 西安理工大学 | 一种咖啡渣基超级电容器电极材料的制备方法 |
CN111243870A (zh) * | 2020-01-14 | 2020-06-05 | 中国科学院苏州纳米技术与纳米仿生研究所南昌研究院 | 柔性自支撑中空活性炭微管基复合薄膜电极、制法与应用 |
CN111243870B (zh) * | 2020-01-14 | 2021-10-26 | 中国科学院苏州纳米技术与纳米仿生研究所南昌研究院 | 柔性自支撑中空活性炭微管基复合薄膜电极、制法与应用 |
EP4128298A4 (en) * | 2020-03-24 | 2024-05-01 | Yazaki Corp | SUPERCAPACITOR CELL WITH CARBONACEOUS ELECTRODE FREE OF HIGH-PURITY BINDER |
CN111628176A (zh) * | 2020-06-17 | 2020-09-04 | 苏州盟维动力科技有限公司 | 多组分三维导电碳网络、自支撑复合电极、其制法及应用 |
CN113053676A (zh) * | 2021-03-18 | 2021-06-29 | 合肥工业大学 | 一种复合薄膜电极材料及其电极与制备方法 |
CN113690428A (zh) * | 2021-08-24 | 2021-11-23 | 北京化工大学 | 一种SiOx/碳纳米管/石墨烯复合膜及其制备方法 |
CN113690428B (zh) * | 2021-08-24 | 2024-02-02 | 北京化工大学 | 一种SiOx/碳纳米管/石墨烯复合膜及其制备方法 |
CN115548246A (zh) * | 2022-08-30 | 2022-12-30 | 哈尔滨工程大学 | 一种锂亚硫酰氯电池正极反应载体材料的制备方法 |
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