CN107306946A - A kind of egg oil agricultural chemicals and its preparation method and application - Google Patents

A kind of egg oil agricultural chemicals and its preparation method and application Download PDF

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Publication number
CN107306946A
CN107306946A CN201710325878.6A CN201710325878A CN107306946A CN 107306946 A CN107306946 A CN 107306946A CN 201710325878 A CN201710325878 A CN 201710325878A CN 107306946 A CN107306946 A CN 107306946A
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oil
egg
plant
yolk
agricultural chemicals
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CN107306946B (en
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杨合法
李季
张泽宇
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China Agricultural University
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China Agricultural University
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G13/00Protecting plants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Toxicology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention provides a kind of egg oil agricultural chemicals, the egg oil agriculture the effective elements of the medicine includes vegetable oil and yolk;The vegetable oil is the one or more in rapeseed oil, peanut oil, olive oil, siritch, sesame oil, corn oil, castor oil, soybean oil, cottonseed oil, rice bran oil, sunflower oil, and the yolk is the one or more in egg yolk, goose egg yolk, Ovum Anas domestica yolk, pigeon eggs Huang.The present invention also provides the preparation and application of the egg oil agricultural chemicals.Vegetable oil contains abundant aliphatic acid, can form emulsifying film on plant surface, plant can not be pierced by making the mouthpart of trialeurodes vaporariorum, and the ascospore of powdery mildew can not penetrate plant and be infected.Emulsifying film can equally increase other biogenic pesticides such as matrine, Dalmatian chrysanthemum medicament blade face attachment degree, so as to increase drug effect.Egg yolk provides abundant nutriment for plant, promotes the growth of plant.

Description

A kind of egg oil agricultural chemicals and its preparation method and application
Technical field
The present invention relates to the methods for making and using same of a kind of agricultural chemicals for preventing and treating plant pest, and the agricultural chemicals.
Background technology
Recently as the development of industrialized agriculture, the cultivated area of Curcurbitaceae industrial crops gradually expands, Curcurbitaceae economy In crop, such as cucumber, sponge gourd, watermelon commercially occupy highly important status, therefore are also agriculturally Greenhouse Major economic crops.
Trialeurodes vaporariorum and powdery mildew are two kinds of pest and disease damages that vegetable at protected field is caused harm heavier, trialeurodes vaporariorum also known as little Bai moths, are The important pests of long-term cropping in greenhouse.Trialeurodes vaporariorum adult excreta influences the breathing of plant, and trialeurodes vaporariorum is secreted in plant blade back Honeydew, causes fungus breeding, so as to reduce vegetables fruit quality.Existing prophylactico-therapeutic measures mainly includes eradicating when nursery or field planting Worm sources, the Encarsia formosa for discharging artificial propagation, are sprayed in trialeurodes vaporariorum early period of origination with pyrrole worm prestige or buprofezin missible oil.Protecting field It can be fumigated with ddvp smoke agent and combine spraying.
Powdery mildew is a kind of fungal disease, is one of the Major Diseases of cucumber growth middle and later periods.At present for powdery mildew Main prevention and controls be to apply the chemical control such as thiophanate methyl, but Practice for Pesticide Residue in Agricultural Products, the Genes For Plant Tolerance medicine thus brought The problems such as property, causes the concern of scholar;The measure such as grafting diseases prevention and crop rotation is tight by land resource in cultural control method Scarce limitation, cost accounting is higher, therefore application biogenic pesticide is the optimal selection for preventing and treating powdery mildew and trialeurodes vaporariorum.This patent A kind of preparation method of egg oil agricultural chemicals is disclosed, the prevention effect to trialeurodes vaporariorum and powdery mildew is notable.
The content of the invention
The weak point existed for this area, it is an object of the present invention to provide a kind of egg oil agricultural chemicals, and the egg oil agriculture The preparation and application of medicine.
The technical scheme for realizing above-mentioned purpose of the present invention is:
A kind of egg oil agricultural chemicals, the egg oil agriculture the effective elements of the medicine includes vegetable oil and yolk;
The vegetable oil be rapeseed oil, peanut oil, olive oil, siritch, sesame oil, corn oil, castor oil, soybean oil, One or more in cottonseed oil, rice bran oil, sunflower oil, the yolk be egg yolk, goose egg yolk, Ovum Anas domestica yolk, pigeon eggs it is yellow in One or more.
Wherein, the mass ratio of vegetable oil and yolk is 1 in the egg oil agricultural chemicals:0.1~10.
Preferably, the mass ratio of vegetable oil and yolk is 1 in the egg oil agricultural chemicals:0.1~2.
Alternatively, described egg oil agricultural chemicals also contains auxiliary material, and the auxiliary material is water, surfactant, filler, stabilizer In one or more;The surfactant is selected from emulsifier op-10, and dodecyl sodium sulfate is polyoxyethylene nonylphenol ether -21, agricultural One or more in emulsifier 600 number and agricultural emulsifier BY130, the filler be malic acid, calcium carbonate, maltodextrin, One or more in concavo-convex rod soil, the stabilizer is one kind in xanthans, potassium sorbate or sodium benzoate;Auxiliary material plus It is 100~500 times of active ingredient quality to enter amount.
The preparation method of the egg oil agricultural chemicals, active ingredient is mixed in proportion, stirred evenly, using preceding addition auxiliary material.
Further, active ingredient is mixed in proportion, stirred evenly, using being before diluted with water 200~500 times.
Application of the egg oil agricultural chemicals of the present invention in preventing and treating plant trialeurodes vaporariorum, powdery mildew.
Wherein, the plant is Curcurbitaceae industrial crops, Solanaceae industrial crops and Cruciferae industrial crops.
Further, when trialeurodes vaporariorum and/or powdery mildew disease occur for plant, by the egg oil applications of pesticide to leaves of plants Face, each plant sprays 5~30mL, sprays weekly once, continuously sprays 1~6 week;
Or the prevention for plant trialeurodes vaporariorum and powdery mildew, according to 5~30mL of each plant consumption, by egg oil agricultural chemicals It is administered to plant leaf surface.
It is preferred that the industrial crops that the egg oil applications of pesticide are transplanted in greenhouse.
A preferred technical solution of the present invention is to apply egg oil agricultural chemicals and matrine or Dalmatian chrysanthemum composite reagent.
The beneficial effects of the present invention are:
Vegetable oil is the compound being bound up by unrighted acid and glycerine, is distributed widely in nature, be from Fruit, the grease that seed is extracted, such as peanut oil, soya-bean oil, rapeseed oil.Vegetable oil contains abundant aliphatic acid, fat It is the abundant source of nutrition of plant, nutriment is provided for plant.Aliphatic acid can form emulsifying film on plant surface simultaneously, make white The mouthpart of aleyrodid can not pierce plant, and the ascospore of powdery mildew can not penetrate plant and be infected.Emulsifying film can equally increase Plus other biogenic pesticides such as matrine, Dalmatian chrysanthemum medicament blade face attachment degree, so as to increase drug effect.Egg yolk is plant There is provided abundant nutriment, egg oil refers to protect using the organic agronomic crop that egg yolk carries out edible oil emulsification treatment Material, is widely used using yolk oil guard crops in terms of organic crops protection, for powdery mildew, trialeurodes vaporariorum, aphid etc. The prevention effect of pest and disease damage is notable.Egg oil can make medicament be uniformly dispersed as a kind of good emulsifying agent simultaneously, be a kind of Preferable insecticides adjuvant.
To sum up, egg oil agricultural chemicals proposed by the present invention has wide development prospect.
Embodiment
Following examples further illustrate present disclosure, but should not be construed as limiting the invention.Without departing substantially from In the case of spirit and essence of the invention, the modifications or substitutions made to the inventive method, step or condition belong to the present invention Scope.
Embodiment 1:
Vegetable oil is soybean oil, and yolk is egg yolk.
By vegetable oil, yolk according to 1:0.5 mass ratio mixing, is stirred evenly.Using being before diluted with water 300 times, according to every Strain 15g consumptions are uniformly sprayed, and are sprayed weekly once.
The cucumber of plant in greenhouse, applies in trialeurodes vaporariorum early period of origination (every plant has adult 2~3), complete after four weeks It totally disappeared the trialeurodes vaporariorum gone out, prevention effect is up to 100%.Also the generation of powdery mildew is not observed after dispenser in greenhouse.
Compared with the cucumber of pesticide control (comparative example 1), yield increase by 10% or so, the cucumber of output does not have agricultural chemicals residual Stay.
Comparative example 1
The cucumber of plant in greenhouse, 10% buprofezin missible oil is applied in trialeurodes vaporariorum early period of origination (every plant has adult 2~3) 1000 times of liquid, have eliminated trialeurodes vaporariorum completely after four weeks, and prevention effect is up to 100%.
But buprofezin can detect residual on cucumber.
Embodiment 2:Prevent and treat powdery mildew of cucumber experiment
Vegetable oil, yolk are according to 1:0.5、1:1 mass ratio mixing, and blank control (clear water).For examination cucumber product It is Chang Chun Mi Ci to plant, and is seeded in the plastic seeding culturing alms bowl equipped with sowing media, per 1, alms bowl, 20~25 DEG C of warm indoor raising of seedling.
For the fresh sick leaf that examination strain is scientia Agricultura Sinica research institute vegetables and the plastic greenhouse harvesting of flowers research institute.
In the Powdery Mildew Epidemic phase, the sick leaf of cucumber of the collection with typical powdery mildew scab brushes off the old spore on blade face, used The Fresh spores grown on clean writing brush swipe blade are made spore suspension, use spray-on process in filling in the beaker of sterilized water It is inoculated with powdery mildew.
Vegetable oil, yolk confection are diluted to 300 respectively with water, compared with clear water, it is equal according to every plant of 15g consumption It is even to spray, spray weekly once.Each processing set three it is parallel.
The sick grade scale such as table 1 for surveying level in greenhouse.
Table 1:Sick level grade scale
Drug effect computational methods:
Disease index=[Σ (plant number × rating value of each disease level)/(plant sums × highest level number)] × 100 (1)
Prevention effect (%)=1-[(CK0 × PT1)/(CK1 × PT0)] × 100 (2)
In formula (2):CK0 is disease index before blank district dispenser;
CK1 is disease index after blank district dispenser;
PT0 is disease index before chemicals treatment district dispenser;
PT1 is disease index after chemicals treatment district dispenser.
Result of the test is shown in Table 2.
Table 2:Prevent and treat powdery mildew of cucumber result of the test
Test result indicates that, 1:0.5 and 1:1 proportioning has obvious prevention effect, vegetable oil and yolk 1 to powdery mildew:1 is Optimal proportioning.
Embodiment 3:
Vegetable oil is rapeseed oil, and yolk is egg yolk.
By vegetable oil, yolk according to 1:1 mass ratio mixing, is stirred evenly.Using being before diluted with water 300 times, according to every plant 15g consumptions are uniformly sprayed, and are sprayed weekly once.
The cucumber of plant in greenhouse, occurs serious period administration in trialeurodes vaporariorum, is counted after four weeks, trialeurodes vaporariorum is prevented Effect is controlled up to 70%.Also the generation of powdery mildew is not observed after dispenser in greenhouse.
Embodiment 4:
Vegetable oil is rapeseed oil, and yolk is egg yolk.
By vegetable oil, yolk according to 1:1.5 mass ratio mixing, is stirred evenly.Using being before diluted with water 300 times, according to every Strain 15g consumptions are uniformly sprayed, and are sprayed weekly once.
The cucumber of plant in greenhouse, occurs serious period administration in trialeurodes vaporariorum, and the preventing and treating to trialeurodes vaporariorum after four weeks is imitated Really up to 80%.Also the generation of powdery mildew is not observed after dispenser in greenhouse.
Embodiment 5:
Vegetable oil is rapeseed oil, and yolk is egg yolk.
By vegetable oil, yolk according to 1:1 mass ratio mixing, is stirred evenly.Using being before diluted with water 300 times, according to every plant 15g consumptions are uniformly sprayed.Spray weekly once.
The eggplant of plant in greenhouse, is applied in trialeurodes vaporariorum early period of origination, is counted after four weeks, and the preventing and treating to trialeurodes vaporariorum is imitated Really up to 80%.Also the generation of powdery mildew is not observed after dispenser in greenhouse.
Embodiment 6:
Vegetable oil is rapeseed oil, and yolk is egg yolk.
By vegetable oil, yolk according to 1:1 mass ratio mixing, is stirred evenly.Using being before diluted with water 300 times, according to every plant 15g consumptions are uniformly sprayed.Spray weekly once.
The broccoli of plant in greenhouse, is applied in trialeurodes vaporariorum early period of origination, to the prevention effect of trialeurodes vaporariorum after four weeks Up to 70%.Also the generation of powdery mildew is not observed after dispenser in greenhouse.
Embodiment 7:
Vegetable oil is rapeseed oil, and yolk is egg yolk.
By vegetable oil, yolk according to 1:1 mass ratio mixing, is stirred evenly.Using being before diluted with water 300 times, according to every plant 15g consumptions are uniformly sprayed.Spray weekly once.
The cucumber of plant in greenhouse, occurs serious period administration in powdery mildew, is counted after four weeks, trialeurodes vaporariorum is prevented Effect is controlled up to 100%, to the prevention effect of powdery mildew up to 94.1%.
Embodiment above is only that the preferred embodiment of the present invention is described, and not the scope of the present invention is entered Row is limited, on the premise of design spirit of the present invention is not departed from, technical side of this area ordinary skill technical staff to the present invention In all variations and modifications that case is made, the protection domain that claims of the present invention determination all should be fallen into.

Claims (10)

1. a kind of egg oil agricultural chemicals, it is characterised in that the egg oil agriculture the effective elements of the medicine includes vegetable oil and yolk;
The vegetable oil is rapeseed oil, peanut oil, olive oil, siritch, sesame oil, corn oil, castor oil, soybean oil, cottonseed One or more in oil, rice bran oil, sunflower oil, the yolk is one in egg yolk, goose egg yolk, Ovum Anas domestica yolk, pigeon eggs Huang Plant or a variety of.
2. egg oil agricultural chemicals as claimed in claim 1, it is characterised in that the matter of vegetable oil and yolk in the egg oil agricultural chemicals Amount ratio is 1:0.1~10.
3. egg oil agricultural chemicals as claimed in claim 2, it is characterised in that the matter of vegetable oil and yolk in the egg oil agricultural chemicals Amount ratio is 1:0.1~2.
4. the egg oil agricultural chemicals described in any one of claims 1 to 3, it is characterised in that also contain auxiliary material, the auxiliary material be water, One or more in surfactant, filler, stabilizer;The surfactant is selected from emulsifier op-10, dodecyl sulphur One or more in sour sodium, polyoxyethylene nonylphenol ether -21, agricultural emulsifier 600 and agricultural emulsifier BY130, the filler is apple One or more in tartaric acid, calcium carbonate, maltodextrin, concavo-convex rod soil, the stabilizer is xanthans, potassium sorbate or benzene first One kind in sour sodium;The addition of auxiliary material is 100~500 times of active ingredient quality.
5. the preparation method of any one of Claims 1 to 4 egg oil agricultural chemicals, it is characterised in that by active ingredient in proportion Mixing, is stirred evenly, using being before diluted with water 200~500 times.
6. application of any one of Claims 1 to 4 egg oil agricultural chemicals in preventing and treating plant trialeurodes vaporariorum, powdery mildew.
7. application according to claim 6, it is characterised in that the plant is Curcurbitaceae industrial crops, Solanaceae economy work Thing and Cruciferae industrial crops.
8. the method for any one of the application Claims 1 to 4 egg oil agricultural chemicals, it is characterised in that occur trialeurodes vaporariorum in plant And/or during powdery mildew disease, by the egg oil applications of pesticide to plant leaf surface, each plant is sprayed 5~30g, sprayed weekly once, Continuous sprinkling 1~6 week;
Or the prevention for plant trialeurodes vaporariorum and powdery mildew, according to 5~30g of each plant consumption, by the egg oil applications of pesticide To plant leaf surface.
9. method according to claim 8, it is characterised in that the economic work for transplanting the egg oil applications of pesticide in greenhouse Thing.
10. method according to claim 8, it is characterised in that answer egg oil agricultural chemicals with matrine or Dalmatian chrysanthemum medicament With administration.
CN201710325878.6A 2017-05-10 2017-05-10 Egg yolk oil pesticide and preparation method and application thereof Active CN107306946B (en)

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CN110024782A (en) * 2019-05-05 2019-07-19 中国农业科学院烟草研究所 A kind of pesticide control of powdery mildew

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109169645A (en) * 2018-09-26 2019-01-11 中国农业大学 A kind of composite assistant for the micro- spore biological agent of locust
CN110024782A (en) * 2019-05-05 2019-07-19 中国农业科学院烟草研究所 A kind of pesticide control of powdery mildew

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