CN107260620A - A kind of sunlight screening skin-protecting product and preparation method thereof - Google Patents
A kind of sunlight screening skin-protecting product and preparation method thereof Download PDFInfo
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- CN107260620A CN107260620A CN201710700857.8A CN201710700857A CN107260620A CN 107260620 A CN107260620 A CN 107260620A CN 201710700857 A CN201710700857 A CN 201710700857A CN 107260620 A CN107260620 A CN 107260620A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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Abstract
A kind of sunlight screening skin-protecting product and preparation method thereof, is related to skin care field.A kind of sunlight screening skin-protecting product, is mainly made up of raw material, and raw material includes：The parts by weight of oil phase composition 4.7 45, the parts by weight of aqueous phase composition 46.53 106.1, the parts by weight of tetrahydroxypropyl ethylenediamine 0.05 0.2, the parts by weight of oat beta glucan 15, the parts by weight of oligopeptides 1 0.005 0.02, the aqueous phase composition of 46.53 106.1 parts by weight include the Huai Goat and the parts by weight of aloe extract 18 of 1 15 parts by weight.Which overcome sunlight screening skin-protecting product UV absorption wavelength it is single, multiplexing sunlight screening skin-protecting product security there is problem.The sunlight screening skin-protecting product to UVA UVB there is broad absorption effect, and absorption is stronger, and with stronger oxidation resistance, free radical can be removed, mitigate damage of the ultraviolet to skin, and have after-sun, effect of moisturizing concurrently.
Description
Technical field
The present invention relates to skin care field, and more particularly to a kind of sunlight screening skin-protecting product and preparation method thereof.
Background technology
Prolonged exposure can cause skin injury, and this is mainly ultraviolet radiation (UVR) effect and caused.Ultraviolet draws
The disease of skin risen will constantly expand with the growth at people's age.Short-term effect caused by UVR is mainly shown as sunburn.Skin
Optical active substance absorbs UVR in skin can produce erythema after 2~24 hours, and this is most common acute UVR effects.This erythema companion
There are oedema, blister, decortication, serious even has constitutional symptom appearance.280-320nm ultraviolet B radiation (UVB) is to cause skin
The main component of skin erythema.Skin is exposed to the sun for a long time may cause the diseases such as cutaneum carcinoma, according to U.S.'s sun-screening agent TFM (examinations in 1993
The final monograph of the property tested) and national sanitary research institute saying, UVB and 320nm-400nm long wave ultraviolet (UVA) all tables
Reveal the carcinogenesis to skin, but the former effect is stronger；In the presence of UVB, UVA can strengthen its carcinogenesis.With
The in-depth recognized daylight UV radiation, people are seeking the various methods for preventing its harm, wherein using sun care preparations just
It is the most frequently used effective ways.
The sun care preparations of prior art synthesis is remained in unsafe factor, is had been reported that because sun-screening agent usage amount and combining makes
With the increase of kind of number, contact dermatitis and intercrossing allergic reaction increase.Titanium dioxide used, zinc oxide etc. these shelter
Agent does not have absorption to ultraviolet, only has the effect of blocking, is easily come off from skin and ineffective, or even has blocking hair
The carcinogenic equivalent risk in hole.
In addition, sun care preparations effect of prior art synthesis is single, sun-proof single effect is only played, it is not simultaneous
Has after-sun, moisturizing is anti-oxidant to wait skin effect.
The content of the invention
It is an object of the invention to provide a kind of sunlight screening skin-protecting product, sunlight screening skin-protecting product UV absorption wavelength list is which overcomed
First, there is problem in multiplexing sunlight screening skin-protecting product security.The sunlight screening skin-protecting product to UVA UVB there is broad absorption effect, and absorb
Effect is stronger, and has stronger oxidation resistance, can remove free radical, mitigates damage of the ultraviolet to skin, and have concurrently
After-sun, effect of moisturizing.
Another object of the present invention is to provide a kind of preparation method of sunlight screening skin-protecting product, the preparation method is simple, easily grasp
Make, and can preferably preserve the active ingredient of each component.
The present invention is solved its technical problem and realized using following technical scheme.
The present invention proposes a kind of sunlight screening skin-protecting product, is mainly made up of raw material, raw material includes：Oil phase composition 4.7-45 weight
Part, aqueous phase composition 46.53-106.1 parts by weight, tetrahydroxypropyl ethylenediamine 0.05-0.2 parts by weight, avenabeta glucosan 1-5 weight
Amount part, the 0.005-0.02 of oligopeptides -1 parts by weight, the aqueous phase composition of 46.53-106.1 parts by weight include the Chinese scholartree of 1-15 parts by weight
Rice extracts and aloe extract 1-8 parts by weight.
The present invention also proposes a kind of preparation method of sunlight screening skin-protecting product, including：
Oil phase composition is mixed, 83-87 DEG C is warming up to；Aqueous phase composition is mixed to be warming up to after 83-87 DEG C, homogeneous and protected
Temperature sterilizing.
Adjust the temperature of oil phase composition and aqueous phase composition to 80-84 DEG C, by oil phase composition and aqueous phase composition
Mixing, homogeneous obtain the first mixture.
It is to be emulsified it is complete after, keep vacuum state under, cooling the first mixture to temperature be 53-57 DEG C with four hydroxypropyl second two
Amine is mixed, and treats that temperature is down to 45-46 DEG C and mixed with avenabeta glucosan, oligopeptides -1.
A kind of beneficial effect of sunlight screening skin-protecting product of the embodiment of the present invention and preparation method thereof is：Water in sunlight screening skin-protecting product
The collective effect of combined thing and oil phase composition can play the effect of moisturizing water lock.Include sophora bud extraction in aqueous phase composition
Thing and aloe extract, both of which have good sun-proof result.Meanwhile, Huai Goat has very strong inoxidizability, energy
Eliminate oxygen radical；Aloe extract, which has, makes skin contraction, softness, moisturizing and the effect of anti-inflammatory.Huai Goat and aloe
Extract is natural plant sun agent, non-stimulated to skin, is had no toxic side effect.Avenabeta glucosan in sunlight screening skin-protecting product and
Oligopeptides -1 is compounded, and both cooperate with the effect for playing more preferable anti-aging, can be reduced fine wrinkles, be improved skin elasticity, improves
Dermatoglyph degree, the effect with preferably sun-proof and after-sun.
The preparation method of sunlight screening skin-protecting product, the preparation method is simple, easy to operate, and different groups are added in different temperature
Point, and can preferably preserve the active ingredient of each component.
Embodiment
, below will be in the embodiment of the present invention to make the purpose, technical scheme and advantage of the embodiment of the present invention clearer
Technical scheme be clearly and completely described.Unreceipted actual conditions person, builds according to normal condition or manufacturer in embodiment
The condition of view is carried out.Agents useful for same or the unreceipted production firm person of instrument, are the conventional production that can be obtained by commercially available purchase
Product.
A kind of sunlight screening skin-protecting product of the embodiment of the present invention and preparation method thereof is specifically described below.
A kind of sunlight screening skin-protecting product, is mainly made up of raw material, and raw material includes：Oil phase composition 4.7-45 parts by weight, aqueous phase group
Compound 46.53-106.1 parts by weight, tetrahydroxypropyl ethylenediamine 0.05-0.2 parts by weight, avenabeta glucosan 1-5 parts by weight, widow
The 0.005-0.02 of peptide -1 parts by weight, the aqueous phase composition of 46.53-106.1 parts by weight include the Huai Goat of 1-15 parts by weight
With aloe extract 1-8 parts by weight.
Aqueous phase composition in sunlight screening skin-protecting product is mainly used in moisturizing, and oil phase composition is mainly used in water lock, of the invention
The collective effect of aqueous phase composition and oil phase composition can play the effect of moisturizing water lock in embodiment.In addition, aqueous phase composition
In include Huai Goat and aloe extract, both of which has good sun-proof result.Meanwhile, Huai Goat has very
Strong inoxidizability, can eliminate oxygen radical；Aloe extract, which has, makes skin contraction, softness, moisturizing and the effect of anti-inflammatory.Chinese scholartree
Rice extracts and aloe extract are natural plant sun agent, non-stimulated to skin, are had no toxic side effect.
Avenabeta glucosan, is a kind of SNSP for being present in oat endosperm and gluten cell wall.It possesses excellent
Different senile-resistant efficacy, can smooth fine wrinkles, improve skin elasticity, improve dermatoglyph degree；With unique straight chain point
Minor structure, imparts good Transdermal absorption performance；Promote fibroblast synthesis collagen, promote wound healing, repair
Impaired skin.
Oligopeptides -1, also referred to as EGF.It has quick reparation damaged skin, calms down eye wrinkle-removing, firm skin,
Skin care, enhancing skin elasticity, whitening spot-removing, sun-proof and after-sun, anti-acne, remove scar and other effects.
Avenabeta glucosan and oligopeptides -1 in the sunlight screening skin-protecting product of the embodiment of the present invention are compounded, and both cooperate with performance more preferable
Anti-aging effect, can reduce fine wrinkles, improve skin elasticity, improve dermatoglyph degree, with preferably it is sun-proof and
The effect of after-sun.
In a kind of optional embodiment, tetrahydroxypropyl ethylenediamine is 0.1-0.2 parts by weight, and avenabeta glucosan is 2-4
Parts by weight, oligopeptides -1 is 0.01-0.02 parts by weight, and Huai Goat is 3-10 parts by weight, and aloe extract is 2-6 parts by weight.
In an embodiment of the present invention, the aqueous phase composition of 46.53-106.1 parts by weight also includes：Deionized water 42-65
Parts by weight, xanthans 0.01-0.5 parts by weight, the cross-linked polymer of acrylic compounds or esters of acrylic acid and alkylol acrylamide acid esters
0.01-0.5 parts by weight, disodium ethylene diamine tetraacetate 0.01-0.1 parts by weight, glycerine 1-8 parts by weight, two polyglycereol 0.5-4 weight
Part and glycerine polymethacrylates 1-5 parts by weight.
Each group distribution ratio in the aqueous phase composition is suitable, with preferable Water-saving effect.Further, the present invention's
In embodiment, the alkane of alkylol acrylamide acid esters is C10-C30.
In addition, in an embodiment of the present invention, the oil phase composition of 4.7-45 parts by weight includes：The stearate of polyglycereol -6
1-5 parts by weight, polyoxyethylene stearic acid ester 0.1-2 parts by weight, cetostearyl alcohol 0.5-3 parts by weight, dimethyl silicone polymer 1-
10 parts by weight, isononyl isononanoate 1-10 parts by weight, diethyl hexylcarbonate 1-10 parts by weight and vitamin E 0.1-5 weight
Part.
Each group distribution ratio in the oil phase composition is suitable, with preferable water lock effect.
Further, raw material also includes：Citrus extracts 0.1-1 parts by weight, peony extract 0.5-2 parts by weight and rose
Rare flower extract 1-5 parts by weight.
Peony extract has natural antipathogenic composition, and with corrosion-resistant effect.Using natural plants are antibacterial, anti-corrosion,
The chemical preservative for having injury effect to skin is instead of, the risk of harm skin is reduced.
There is citrus extracts the rose polyphenol in preferably sterilization, the effect of anti-inflammatory, Flos Rosae Rugosae extract to have beauty treatment
The effect of moisturizing.
A kind of preparation method of sunlight screening skin-protecting product, including：
Oil phase composition is mixed, 83-87 DEG C is warming up to；Aqueous phase composition is mixed to be warming up to after 83-87 DEG C, homogeneous and protected
Temperature sterilizing.
It should be noted that aqueous phase composition should be first by the crosslinking of acrylic compounds or esters of acrylic acid and alkylol acrylamide acid esters
Polymer is with the scattered addition main cooker of glycerine, then adding the other components of aqueous phase composition.So be conducive to aqueous phase group
The fully dispersed mixing of compound.In an embodiment of the present invention, oil phase composition is added in oil phase pot.
After oil phase composition and aqueous phase composition are stirred with 35Hz frequency, 83-87 DEG C is warming up to, then by aqueous phase group
Sterilized after compound homogeneous 2-5min, insulation 15-25mim.
Adjust the temperature of oil phase composition and aqueous phase composition to 80-84 DEG C, under vacuum by oil phase composition
Mixed with aqueous phase composition, homogeneous obtains the first mixture.
It should be noted that the temperature of aqueous phase composition and the temperature difference of oil phase composition are no more than 2 DEG C.Such water
When combined thing is mixed with oil phase composition, it can be easier well mixed.And the oil phase composition in the temperature range and
Aqueous phase composition is conducive to being well mixed fully to melt, so.
In the embodiment of invention, mixed using oil phase composition is pumped into main cooker by the way of vacuumizing with aqueous phase composition
Close.After mixing, stirred with 30Hz frequency, then homogeneous 5-8min obtains the first mixture.It is to be emulsified it is complete after, keep vacuum
Under state, the first mixture of cooling to temperature is 53-57 DEG C and is mixed to get the second mixture with tetrahydroxypropyl ethylenediamine, treats temperature
45-46 DEG C is down to mix the second mixture with avenabeta glucosan, oligopeptides -1.
In an embodiment of the present invention, mainly the first mixture is cooled down by cooling water.Tetrahydroxypropyl ethylenediamine
It is fusible in 53-57 DEG C of temperature range, and will not break and understand its active ingredient.Avenabeta glucosan, oligopeptides -1 are at 45-46 DEG C
It is fusible in temperature range, and its active ingredient will not be destroyed.For different raw materials, different temperature are set, not only can be with
Each raw material is sufficiently mixed, moreover it is possible to keep the active ingredient of each component.
It should be noted that in some embodiments of the invention, cooling the temperature to 45-46 DEG C by the second mixture and swallow
When wheat beta glucan, oligopeptides -1 are mixed, in addition to the mixing with citrus extracts 0.1-1 parts by weight.Then 42- is cooled the temperature to
44 DEG C are mixed with peony extract 0.5-2 parts by weight and Flos Rosae Rugosae extract 1-5 parts by weight, and 10- is stirred with 38Hz frequency
20mim；Froth breaking is vacuumized, 34-36 DEG C is cooled to.
The feature and performance to the present invention are described in further detail with reference to embodiments.
Embodiment 1
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.1
Part, the parts by weight of avenabeta glucosan 2, the parts by weight of oligopeptides -1 0.001, the parts by weight of citrus extracts 0.5, the weight of peony extract 0.5
Measure part and the parts by weight of Flos Rosae Rugosae extract 3.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 42, the parts by weight of xanthans 0.01, esters of acrylic acid and alkane
The parts by weight of cross-linked polymer 0.01, the parts by weight of disodium ethylene diamine tetraacetate 0.01, the parts by weight of glycerine 1, the dimerization of alcohol acrylate
The parts by weight of glycerine 0.5 and the parts by weight of glycerine polymethacrylates 1.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 1, the parts by weight of polyoxyethylene stearic acid ester 0.1, spermaceti
The parts by weight of stearyl alcohol 0.5, the parts by weight of dimethyl silicone polymer 1, the parts by weight of isononyl isononanoate 1, the weight of diethyl hexylcarbonate 1
Part and the parts by weight of vitamin E 0.1.
The preparation method of the sunlight screening skin-protecting product includes：
Oil phase composition is added in oil phase pot, aqueous phase composition is added in aqueous phase pot.By oil phase composition, water
After combined thing is with 35Hz frequency stirring, 85 DEG C are warming up to.Then by aqueous phase composition homogeneous 3min, gone out after insulation 20mim
Bacterium.
Aqueous phase composition is cooled down to 80 DEG C, cooling oil phase composition to 82 DEG C, vacuumizes, oil phase is pumped into main cooker, so
Stirred afterwards with 30Hz frequency, open main cooker homogeneous 6min.After the completion of emulsification, using water cooling is cooled down, main cooker is then stirred into frequency
Rate is adjusted to 35Hz, keeps vacuum state.Temperature adds disodium ethylene diamine tetraacetate when being down to 55 DEG C, temperature is added when being down to 45 DEG C
Avenabeta glucosan, oligopeptides -1 and citrus extracts, temperature are down to 43 DEG C and add Flos Rosae Rugosae extract and peony extract, with
After 38Hz frequency stirring 15min, froth breaking is vacuumized, 36 DEG C are cooled to.
Embodiment 2
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.08
Measure part, the parts by weight of avenabeta glucosan 3, the parts by weight of oligopeptides -1 0.008, the parts by weight of citrus extracts 0.3, the weight of peony extract 1
Measure part and the parts by weight of Flos Rosae Rugosae extract 5.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 52, the parts by weight of xanthans 0.2, esters of acrylic acid and alkanol
The parts by weight of cross-linked polymer 0.3 of acrylate, the parts by weight of disodium ethylene diamine tetraacetate 0.03, the parts by weight of glycerine 5, two polyglycereol
1 parts by weight and the parts by weight of glycerine polymethacrylates 4.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 3, the parts by weight of polyoxyethylene stearic acid ester 0.5, spermaceti
The parts by weight of stearyl alcohol 2, the parts by weight of dimethyl silicone polymer 2, the parts by weight of isononyl isononanoate 3, the parts by weight of diethyl hexylcarbonate 5
And the parts by weight of vitamin E 2.
The preparation method of the sunlight screening skin-protecting product of the present embodiment is same as Example 1.
Embodiment 3
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.05
Measure part, the parts by weight of avenabeta glucosan 5, the parts by weight of oligopeptides -1 0.015, the parts by weight of citrus extracts 0.1, peony extract 1.5
Parts by weight and the parts by weight of Flos Rosae Rugosae extract 2.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 48, the parts by weight of xanthans 0.3, esters of acrylic acid and alkanol
The parts by weight of cross-linked polymer 0.1 of acrylate, the parts by weight of disodium ethylene diamine tetraacetate 0.05, the parts by weight of glycerine 2, two polyglycereol
3 parts by weight and the parts by weight of glycerine polymethacrylates 2.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 2, the parts by weight of polyoxyethylene stearic acid ester 1, spermaceti are hard
The parts by weight of lipidol 1, the parts by weight of dimethyl silicone polymer 4, the parts by weight of isononyl isononanoate 5, the parts by weight of diethyl hexylcarbonate 4 with
And the parts by weight of vitamin E 1.
The preparation method of the sunlight screening skin-protecting product of the present embodiment is same as Example 1.
Embodiment 4
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.12
Measure part, the parts by weight of avenabeta glucosan 1, the parts by weight of oligopeptides -1 0.01, the parts by weight of citrus extracts 0.8, the weight of peony extract 2
Measure part and the parts by weight of Flos Rosae Rugosae extract 1.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 55, the parts by weight of xanthans 0.05, esters of acrylic acid and alkane
The parts by weight of cross-linked polymer 0.4, the parts by weight of disodium ethylene diamine tetraacetate 0.08, the parts by weight of glycerine 3, the dimerization of alcohol acrylate are sweet
Oily 2 parts by weight and the parts by weight of glycerine polymethacrylates 4.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 2.5, the parts by weight of polyoxyethylene stearic acid ester 1.2, whale
The parts by weight of wax stearyl alcohol 2.3, the parts by weight of dimethyl silicone polymer 3, the parts by weight of isononyl isononanoate 2, the weight of diethyl hexylcarbonate 9
Measure part and the parts by weight of vitamin E 2.5.
The preparation method of the sunlight screening skin-protecting product of the present embodiment is same as Example 1.
Embodiment 5
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.15
Measure part, the parts by weight of avenabeta glucosan 4, the parts by weight of oligopeptides -1 0.012, the parts by weight of citrus extracts 1, the weight of peony extract 0.8
Measure part and the parts by weight of Flos Rosae Rugosae extract 3.5.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 60, the parts by weight of xanthans 0.08, esters of acrylic acid and alkane
The parts by weight of cross-linked polymer 0.2, the parts by weight of disodium ethylene diamine tetraacetate 0.02, the parts by weight of glycerine 4, the dimerization of alcohol acrylate are sweet
Oily 2.5 parts by weight and the parts by weight of glycerine polymethacrylates 3.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 3.5, the parts by weight of polyoxyethylene stearic acid ester 1.5, whale
The parts by weight of wax stearyl alcohol 1.5, the parts by weight of dimethyl silicone polymer 5, the parts by weight of isononyl isononanoate 8, the weight of diethyl hexylcarbonate 3
Measure part and the parts by weight of vitamin E 3.
The preparation method of the sunlight screening skin-protecting product includes：
Oil phase composition is added in oil phase pot, aqueous phase composition is added in aqueous phase pot.By oil phase composition, water
After combined thing is with 35Hz frequency stirring, 83 DEG C are warming up to.Then by aqueous phase composition homogeneous 5min, gone out after insulation 15mim
Bacterium.
Aqueous phase composition is cooled down to 82 DEG C, cooling oil phase composition to 84 DEG C, vacuumizes, oil phase is pumped into main cooker, so
Stirred afterwards with 30Hz frequency, open main cooker homogeneous 5min.After the completion of emulsification, using water cooling is cooled down, main cooker is then stirred into frequency
Rate is adjusted to 35Hz, keeps vacuum state.Temperature adds disodium ethylene diamine tetraacetate when being down to 53 DEG C, temperature is added when being down to 46 DEG C
Avenabeta glucosan, oligopeptides -1 and citrus extracts, temperature are down to 44 DEG C and add Flos Rosae Rugosae extract and peony extract, with
After 38Hz frequency stirring 10min, froth breaking is vacuumized, 35 DEG C are cooled to.
Embodiment 6
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.2
Part, the parts by weight of avenabeta glucosan 2.5, the parts by weight of oligopeptides -1 0.005 and the parts by weight of citrus extracts 0.5.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 62, the parts by weight of xanthans 0.1, esters of acrylic acid and alkanol
The parts by weight of cross-linked polymer 0.15, the parts by weight of disodium ethylene diamine tetraacetate 0.06, the parts by weight of glycerine 6, the dimerization of acrylate are sweet
Oily 3 parts by weight and the parts by weight of glycerine polymethacrylates 2.5.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 3, the parts by weight of polyoxyethylene stearic acid ester 2, spermaceti are hard
The parts by weight of lipidol 2.5, the parts by weight of dimethyl silicone polymer 9, the parts by weight of isononyl isononanoate 9, the parts by weight of diethyl hexylcarbonate 8
And the parts by weight of vitamin E 3.
The preparation method of the sunlight screening skin-protecting product includes：
Oil phase composition is added in oil phase pot, aqueous phase composition is added in aqueous phase pot.By oil phase composition, water
After combined thing is with 35Hz frequency stirring, 87 DEG C are warming up to.Then by aqueous phase composition homogeneous 2min, gone out after insulation 25mim
Bacterium.
Aqueous phase composition is cooled down to 82 DEG C, cooling oil phase composition to 81 DEG C, vacuumizes, oil phase is pumped into main cooker, so
Stirred afterwards with 30Hz frequency, open main cooker homogeneous 8min.After the completion of emulsification, using water cooling is cooled down, main cooker is then stirred into frequency
Rate is adjusted to 35Hz, keeps vacuum state.Temperature adds disodium ethylene diamine tetraacetate when being down to 57 DEG C, temperature is added when being down to 45 DEG C
Avenabeta glucosan, oligopeptides -1 and citrus extracts, after 38Hz frequency stirring 20min, vacuumize froth breaking, are cooled to 34
℃。
Embodiment 7
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.18
Measure part, the parts by weight of avenabeta glucosan 3.5, the parts by weight of oligopeptides -1 0.02 and the parts by weight of peony extract 1.2.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 50, the parts by weight of xanthans 0.4, esters of acrylic acid and alkanol
The parts by weight of cross-linked polymer 0.25, the parts by weight of disodium ethylene diamine tetraacetate 0.05, the parts by weight of glycerine 7, the dimerization of acrylate are sweet
Oily 2 parts by weight and the parts by weight of glycerine polymethacrylates 1.5.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 4, the parts by weight of polyoxyethylene stearic acid ester 0.8, spermaceti
The parts by weight of stearyl alcohol 2, the parts by weight of dimethyl silicone polymer 8, the parts by weight of isononyl isononanoate 8, the parts by weight of diethyl hexylcarbonate 7
And the parts by weight of vitamin E 4.
The preparation method of the sunlight screening skin-protecting product includes：
Oil phase composition is added in oil phase pot, aqueous phase composition is added in aqueous phase pot.By oil phase composition, water
After combined thing is with 35Hz frequency stirring, 84 DEG C are warming up to.Then by aqueous phase composition homogeneous 4min, gone out after insulation 20mim
Bacterium.
Aqueous phase composition is cooled down to 81 DEG C, cooling oil phase composition to 82 DEG C, vacuumizes, oil phase is pumped into main cooker, so
Stirred afterwards with 30Hz frequency, open main cooker homogeneous 5min.After the completion of emulsification, using water cooling is cooled down, main cooker is then stirred into frequency
Rate is adjusted to 35Hz, keeps vacuum state.Temperature adds disodium ethylene diamine tetraacetate when being down to 54 DEG C, temperature is added when being down to 46 DEG C
Avenabeta glucosan and oligopeptides -1, temperature are down to 42 DEG C of addition peony extracts, after 38Hz frequency stirring 20min, take out true
Empty froth breaking, is cooled to 34 DEG C.
Embodiment 8
A kind of sunlight screening skin-protecting product, its raw material includes：Aqueous phase composition, oil phase composition, the weight of tetrahydroxypropyl ethylenediamine 0.15
Measure part, the parts by weight of avenabeta glucosan 1.5 and the parts by weight of oligopeptides -1 0.017.
Wherein, aqueous phase composition includes：The parts by weight of deionized water 65, the parts by weight of xanthans 0.5, esters of acrylic acid and alkanol
The parts by weight of cross-linked polymer 0.5 of acrylate, the parts by weight of disodium ethylene diamine tetraacetate 0.1, the parts by weight of glycerine 8, two polyglycereol 4
Parts by weight and the parts by weight of glycerine polymethacrylates 5.
Oil phase composition includes：The parts by weight of the stearate of polyglycereol -6 5, the parts by weight of polyoxyethylene stearic acid ester 2, spermaceti are hard
The parts by weight of lipidol 3, the parts by weight of dimethyl silicone polymer 10, the parts by weight of isononyl isononanoate 10, the weight of diethyl hexylcarbonate 10
Part and the parts by weight of vitamin E 5.
The preparation method of the sunlight screening skin-protecting product includes：
Oil phase composition is added in oil phase pot, aqueous phase composition is added in aqueous phase pot.By oil phase composition, water
After combined thing is with 35Hz frequency stirring, 84 DEG C are warming up to.Then by aqueous phase composition homogeneous 4min, gone out after insulation 20mim
Bacterium.
Aqueous phase composition is cooled down to 81 DEG C, cooling oil phase composition to 82 DEG C, vacuumizes, oil phase is pumped into main cooker, so
Stirred afterwards with 30Hz frequency, open main cooker homogeneous 5min.After the completion of emulsification, using water cooling is cooled down, main cooker is then stirred into frequency
Rate is adjusted to 35Hz, keeps vacuum state.Temperature adds disodium ethylene diamine tetraacetate when being down to 54 DEG C, temperature is added when being down to 46 DEG C
Avenabeta glucosan and oligopeptides -1, after 38Hz frequency stirring 20min, vacuumize froth breaking, are cooled to 35 DEG C.
Test example
Commission detection unit：Shanghai Intertek Verified Service Co., Ltd.
Detection project：Sunscreen product SPF and PFA protect effect instrumental method to test
Detection method：With reference to ISO 2443:2012
1. test material
1.1 standard reference materials：P2 and S2 standard items, purchased from Cosmetech Laooratories companies.
1.2PMMA plate：Methyl methacrylate plate
1.3 detecting instrument：UV 2000S ultraviolet transmittances analyzer, the Newport of Lab sphere companies production are public
Take charge of the SOL-UV-6 solar simulators of production
2. detection method
(1) according to ISO 24443:2012 requirement, with 1.3mg/cm2Consumption, draw one respectively with special syringe
Determine the sunlight screening skin-protecting product and standard items P2 of the embodiment 2 of volume, uniform point is added in PMMA surface, and sample is smeared with medical latex fingerstall
Product simultaneously make it be uniformly distributed in PMMA surface.Entire plate is placed in the environment of 23-26 DEG C of room temperature and relative humidity 40%~60%
Lower lucifuge 30min.Then the transmitance of ultraviolet light is detected with UV 2000S instruments, each sample repeats 4 pieces of test boards, is respectively
Test board 1, test board 2, test board 3 and test board 4, every piece of plate 5 points of detection, difference record standard product P2 and embodiment 2
The spf value of sunlight screening skin-protecting product.Its result is recorded in table 1.
(2) the PMMA plates of the sunlight screening skin-protecting product and standard items S2 of smearing embodiment 2 are placed into SOL-UV-6 sun optical analogs
Device irradiates, and then detects the transmitance of ultraviolet light with UV 2000S instruments again, and each sample repeats 4 pieces of test boards, respectively surveyed
Test plate (panel) 5, test board 6, test board 7 and test board 8, every block of plate detect 5 points, and record standard product S2 and embodiment 2 is anti-respectively
Shine the PFA values of skin care item.Its result is recorded in table 2.
The sunlight screening skin-protecting product of the embodiment 2 of table 1 and standard items S2 SPF test results
From table 1 it follows that the SPF average values of the sunlight screening skin-protecting product of embodiment 2 are 31.14, standard deviation is ± 2.35,
Illustrating the sunlight screening skin-protecting product of the present invention has preferably resistance UVB effect.
The test test result of the sunlight screening skin-protecting product of the embodiment 2 of table 2 and standard items P2 PFA
| Sequence number | Embodiment 2 (forecast +++) | Standard items P2 (SPF12.7) |
| Test board 5 | 31.09 | 13.27 |
| Test board 6 | 30.59 | 13.31 |
| Test board 7 | 36.79 | 13.08 |
| Test board 8 | 34.36 | 13.98 |
| It is average | 33.21 | 13.41 |
| Standard deviation | ±2.92 | ±0.39 |
From Table 2, it can be seen that the PFA values of the sunlight screening skin-protecting product of embodiment 2 are more than 30, be " ++++", standard deviation for ±
2.92, illustrating the sunlight screening skin-protecting product of the present invention has preferably resistance UVA effect.With reference to the result of table 1, this hair is illustrated
The sunlight screening skin-protecting product of bright embodiment has preferable sun-proof result.
In summary, a kind of sunlight screening skin-protecting product of the embodiment of the present invention and preparation method thereof, the aqueous phase in sunlight screening skin-protecting product
The collective effect of composition and oil phase composition can play the effect of moisturizing water lock.Include Huai Goat in aqueous phase composition
And aloe extract, both of which has good sun-proof result.Meanwhile, Huai Goat has very strong inoxidizability, can disappear
Except oxygen radical；Aloe extract, which has, makes skin contraction, softness, moisturizing and the effect of anti-inflammatory.Huai Goat and aloe carry
It is natural plant sun agent to take thing, non-stimulated to skin, is had no toxic side effect.Avenabeta glucosan and widow in sunlight screening skin-protecting product
Peptide -1 is compounded, and both cooperate with the effect for playing more preferable anti-aging, can be reduced fine wrinkles, be improved skin elasticity, improves skin
Skin texture, the effect with preferably sun-proof and after-sun.
The preparation method of sunlight screening skin-protecting product, the preparation method is simple, easy to operate, and different groups are added in different temperature
Point, and can preferably preserve the active ingredient of each component.
Embodiments described above is a part of embodiment of the invention, rather than whole embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
Claims (10)
1. a kind of sunlight screening skin-protecting product, it is characterised in that be mainly made up of raw material, the raw material includes：Oil phase composition 4.7-45
Parts by weight, aqueous phase composition 46.53-106.1 parts by weight, tetrahydroxypropyl ethylenediamine 0.05-0.2 parts by weight, avenabeta glucosan
1-5 parts by weight, oligopeptides -10.005-0.02 parts by weight, the aqueous phase composition of 46.53-106.1 parts by weight include 1-15 weights
Measure the Huai Goat and aloe extract 1-8 parts by weight of part.
2. sunlight screening skin-protecting product according to claim 1, it is characterised in that the aqueous phase group of 46.53-106.1 parts by weight
Compound also includes：Deionized water 42-65 parts by weight, xanthans 0.01-0.5 parts by weight, acrylic compounds or esters of acrylic acid and alkane
The cross-linked polymer 0.01-0.5 parts by weight of alcohol acrylate, disodium ethylene diamine tetraacetate 0.01-0.1 parts by weight, glycerine 1-8 weights
Measure part, two polyglycereol 0.5-4 parts by weight and glycerine polymethacrylates 1-5 parts by weight.
3. sunlight screening skin-protecting product according to claim 2, it is characterised in that the alkylol acrylamide acid esters is C10-C30 alkanols
Acrylate.
4. the sunlight screening skin-protecting product according to claim any one of 1-3, it is characterised in that the oil phase of 4.7-45 parts by weight
Composition includes：The stearate 1-5 of polyglycereol -6 parts by weight, polyoxyethylene stearic acid ester 0.1-2 parts by weight, cetostearyl alcohol
0.5-3 parts by weight, dimethyl silicone polymer 1-10 parts by weight, isononyl isononanoate 1-10 parts by weight, diethyl hexylcarbonate 1-
10 parts by weight and vitamin E 0.1-5 parts by weight.
5. sunlight screening skin-protecting product according to claim 1, it is characterised in that the tetrahydroxypropyl ethylenediamine is 0.1-0.2 weights
Part is measured, the avenabeta glucosan is 2-4 parts by weight, and the oligopeptides -1 is 0.01-0.02 parts by weight, and the Huai Goat is
3-10 parts by weight, the aloe extract is 2-6 parts by weight.
6. sunlight screening skin-protecting product according to claim 1 or 5, it is characterised in that the raw material also includes：Citrus extracts
0.1-1 parts by weight, peony extract 0.5-2 parts by weight and Flos Rosae Rugosae extract 1-5 parts by weight.
7. a kind of sunlight screening skin-protecting product preparation method as described in claim any one of 1-6, it is characterised in that including：
The oil phase composition is mixed, 83-87 DEG C is warming up to；The aqueous phase composition is mixed and is warming up to 83-87 DEG C, homogeneous
Insulated sterilizing afterwards；
Adjust the temperature of the oil phase composition and the aqueous phase composition to 80-84 DEG C, by the oil phase composition and institute
State aqueous phase composition mixing, homogeneous and obtain the first mixture；
It is to be emulsified it is complete after, keep under vacuum state, it is 53-57 DEG C and four hydroxypropyl second two to cool down first mixture to temperature
Amine is mixed to get the second mixture, treats that temperature is down to 45-46 DEG C and mixes second mixture and avenabeta glucosan, oligopeptides -1
Close.
8. sunlight screening skin-protecting product preparation method according to claim 7, it is characterised in that temperature is down to 45-46 DEG C will be described
Second mixture is mixed to get after the 3rd mixture with the avenabeta glucosan, the oligopeptides -1, in addition to treats that temperature is down to
42-44 DEG C mixes the 3rd mixture with peony extract 0.5-2 parts by weight and Flos Rosae Rugosae extract 1-5 parts by weight.
9. sunlight screening skin-protecting product preparation method according to claim 7, it is characterised in that temperature is down to 45-46 DEG C will be described
When second mixture is mixed with the avenabeta glucosan, the oligopeptides -1, in addition to citrus extracts 0.1-1 parts by weight
Mixing.
10. sunlight screening skin-protecting product preparation method according to claim 8, it is characterised in that treat that temperature is down to 42-44 DEG C by institute
State after the 3rd mixture mixes with the peony extract and the Flos Rosae Rugosae extract, progress vacuumizes froth breaking, is cooled to
34-36℃。
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710700857.8A CN107260620A (en) | 2017-08-15 | 2017-08-15 | A kind of sunlight screening skin-protecting product and preparation method thereof |
| PCT/CN2017/109785 WO2019033584A1 (en) | 2017-08-15 | 2017-11-07 | Sunscreen skincare product and preparation method therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710700857.8A CN107260620A (en) | 2017-08-15 | 2017-08-15 | A kind of sunlight screening skin-protecting product and preparation method thereof |
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| CN107260620A true CN107260620A (en) | 2017-10-20 |
Family
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| CN201710700857.8A Pending CN107260620A (en) | 2017-08-15 | 2017-08-15 | A kind of sunlight screening skin-protecting product and preparation method thereof |
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| WO (1) | WO2019033584A1 (en) |
Cited By (3)
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| CN108420779A (en) * | 2018-06-15 | 2018-08-21 | 广州无添加主义化妆品有限公司 | A kind of sunscreen and preparation method thereof |
| WO2019033584A1 (en) * | 2017-08-15 | 2019-02-21 | 广州无添加主义化妆品有限公司 | Sunscreen skincare product and preparation method therefor |
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| WO2019033584A1 (en) | 2019-02-21 |
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