CN107260608A - Slimming camellia massage oil of high penetration and preparation method thereof - Google Patents
Slimming camellia massage oil of high penetration and preparation method thereof Download PDFInfo
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- CN107260608A CN107260608A CN201710517802.3A CN201710517802A CN107260608A CN 107260608 A CN107260608 A CN 107260608A CN 201710517802 A CN201710517802 A CN 201710517802A CN 107260608 A CN107260608 A CN 107260608A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/06—Preparations for care of the skin for countering cellulitis
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/006—Refining fats or fatty oils by extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
Abstract
A kind of slimming camellia massage oil of high penetration, is uniformly mixed according to mass fraction by following component:0.1~0.3 part of 70~80 parts of small molecule camellia oil, 5~10 parts of candlenut tree macadamia nut oil, 3~5 parts of evening primrose oil, 3~5 parts of black pepper essential oil, 2~5 parts of hops oil, 25 parts of shaddock oil, 0.5~1 part of ethyl nicotinate, 0.1~0.3 part of capsicum oleoresin, 0.1~0.3 part of Rosmarinus officinalis extract, Tea Polyphenols or its fatty acid ester are uniformly mixed.The camellia massage oil can promote blood and cell interior circulation, dredging blood vessel discharges toxin, and fat metabolism product is excreted without obvious greasy feeling effectively by Cutaneous permeation to subcutaneous fat.
Description
Technical field
The present invention relates to a kind of essential oil, the slimming camellia massage oil of particularly a kind of high penetration.
Background technology
Study and find according to American scientist：The people of more than the 45 years old body weight 10% that are above standard, often beyond 45KG, the life-span will
Shorten 29 days, the people more than 9KG, death rate increase by 18%, the people more than 13KG, death rate increase by 28%, it is seen that obesity is health
Long-lived formidable enemy！
Since the 9's 0 of 20th century, China's diet products industry is developed rapidly, diet products and manufacturing enterprise
Quantity is continuously increased, and diet products production field, which turns into, makes the bright spot of investment that investor widely pays close attention to.In recent years, it is many famous
International corporation the diet products market of China is also extremely paid close attention to, one after another by it is newest on international market, it is state-of-the-art fat-reducing produce
Product are introduced into China, cause China's diet products market competition fiercer.
However, most of diet products are all using medicine for oral administration, side effect or obvious badly influences people
Body function.
Camellia oil, also known as Wild camellia seed oil, tea-seed oil, camellia seed oil, squeeze the seed from tea oil tree.Its monounsaturated fatty acid
Acid content is up to more than 90%, can effectively fat melting, lipid-loweringing, and rich in the day such as natural VE, Tea Polyphenols, squalene, Tea Saponin
So nourish skin care ingredient and a variety of anti-oxidant, anti-inflammations, promote blood microcirculation composition.
Camellia oil, although with above-mentioned advantage, but because main component is fatty glyceride, viscosity is larger, molecule compared with
When greatly, for skin care item, often show that percutaneous absorption is slow, assimilation effect is poor, skin greasy feeling substantially, the shortcomings of be easily sticky with.
The content of the invention
The purpose of the present invention, is to overcome the deficiencies in the prior art to be massaged there is provided a kind of slimming camellia of high penetration
Oil, the camellia massage oil can promote blood and intracellular follow without obvious greasy feeling effectively by Cutaneous permeation to subcutaneous fat
Ring, dredging blood vessel discharges toxin, and fat metabolism product is excreted.
The technical scheme is that：
A kind of slimming camellia massage oil of high penetration, is uniformly mixed according to mass fraction by following component:It is hypertonic
Saturating 70~80 parts of power small molecule camellia oil, 5~10 parts of candlenut tree macadamia nut oil, 3~5 parts of evening primrose oil, 3~5 parts of black pepper essential oil, beer
2~5 parts of hop oil, 2-5 parts of shaddock oil, 0.5~1 part of ethyl nicotinate, 0.1~0.3 part of capsicum oleoresin, Rosmarinus officinalis extract 0.1
0.1~0.3 part of~0.3 part, Tea Polyphenols or its fatty acid ester.
Described small molecule camellia oil, is go glycerine reaction of the camellia oil with ethanol under highly basic existence condition, then through dividing
From, purification, obtained small molecule camellia oil remains the oleic acid for being beneficial to human body in camellia oil, linoleic acid, leukotrienes, also protects
The vitamin E for being beneficial to human body in camellia oil, Tea Polyphenols, sterol, squalene, tsubakisaponin etc. has been stayed naturally to nourish skin care ingredient
And a variety of anti-oxidant, anti-inflammation compositions,
Preferably, small molecule camellia oil by 75~85 parts of camellia oil, 15~25 parts of food-grade ethanol, highly basic 0.2~1.0 reaction and
Into.
Preferably, it can be made up of following processing step：
Step 1: producing small molecule camellia oil crude product
Raw material is weighed by following proportion by weight：75~85 parts of camellia oil, 15~25 parts of food-grade ethanol, highly basic 0.2~1.0
Part；By the camellia oil weighed, 40~60 DEG C are heated to；Load weighted highly basic is added in food-grade ethanol, makes it fully molten
Solution, is made into alcohol aqueous slkali；Alcohol aqueous slkali is slowly added in camellia oil, 40~70 DEG C, constant temperature stirring at low speed 30~60 are heated to
Minute；It is heated to 80~100 DEG C, constant temperature high-speed stirred 1~2 hour；Cooling, stands 3~4 hours, takes edible vegetable oil liquid thereon；Will be upper
Edible vegetable oil liquid is cooled to -5~5 DEG C, stands 3~4 hours, rapid vacuum suction filtration obtains filtrate；In filtrate add proper amount of active carbon and
Atlapulgite, is heated to 80~100 DEG C, constant temperature is stirred 1-3 hours, filters to obtain high penetration small molecule camellia oil crude product；
Step 2: producing cosmetics-stage high penetration small molecule camellia oil
Step one is made into small molecule camellia oil crude product to be separated in short-range molecular distillation device, plate temperature 130~150 is scraped
DEG C, scraper velocity 200-250r/min, 0.04~0.06MPa of vacuum, condensate liquid are collected as small molecule camellia oil, and heavy phase is given up
Liquid is separately collected.
Contained fatty-acid ethyl ester molecule in the small molecule camellia oil is smaller very than contained fatty glyceride in camellia oil
Many, this is the reason for its penetration original is higher than camellia oil place, and in addition, its monounsaturated fatty acids content of small molecule camellia oil is high
Up to more than 80%, can effectively fat melting, lipid-loweringing, and nourish shield rich in natural VE, Tea Polyphenols, squalene, Tea Saponin etc. are natural
Skin composition and a variety of anti-oxidant, anti-inflammations, promotion blood microcirculation composition.
Preferably, in the step one, camellia oil does not add using obtained by camellia seed physical squeezing by further
Work, it is to avoid the unreasonable refining losses of the contained mentioned component beneficial to human body.
Preferably, in the step one, this kind of camellia oil sorting is good, and processing technology is rationally, contained above-mentioned to be beneficial to human body
Composition content it is high.
In the step one, highly basic can be the one or more in sodium hydroxide, potassium hydroxide, caustic alcohol, potassium ethoxide,
It is preferred that sodium hydroxide cheap and easy to get.
Preferably, in the step one, camellia oil conversion ratio is more than 90%.
Preferably, in the step 2, the distillation yield 60~65% of high penetration small molecule camellia oil is controlled, now, is steamed
Distillation unit operating is more steady, and the quality of gained small molecule camellia oil is preferable.
Preferably, the distillation heavy phase waste liquid in the step 2 is reclaimed, and replaces camellia oil raw material, by being similar to step
One method prepares small molecule camellia oil crude product again, then is separated by the method for step 2, and condensate liquid is used as small molecule mountain
Tea oil is collected, and what distillation heavy phase waste liquid was abandoned no longer uses.
The use of the slimming camellia massage oil of high penetration of the present invention, generally with semar technique, such as is applied in right amount
Skin, then the uniform pressing of appropriateness, are moderately rubbed until fully absorbing.
The toxin-expelling and face nourishing camellia soothing oil of high penetration of the present invention, its preparation technology is simple and reliable, small molecule camellia
Oil is up to more than 80% rich in monounsaturated fatty acids content, is compounded with other raw materials, can effectively cooperate with each active factors to penetrate into flesh
Skin, promotes skin metabolism, reaches effective fat melting, lipid-loweringing, and rich in days such as natural VE, Tea Polyphenols, squalene, Tea Saponins
So nourish skin care ingredient and a variety of anti-oxidant, anti-inflammations, promote blood microcirculation composition, it is non-toxic, nonirritant, without allergy
Property, the preferable natural skin care product of the daily skin care of people can be used as.
Primary raw material used in the present invention is described as follows：
Camellia oil：Camellia seed kernel is through cleaning, air-drying（Temperature is less than 100 DEG C）, shelling, seed selection sterilization after, at 20-50 DEG C carry out
Squeezing gained, active material enriches, generally about containing vitamin E 90mg/Kg, sterol 30mg/Kg, squalene 20mg/Kg.
Candlenut tree macadamia nut oil：Also known as bankoul nut oil（Kukui Nut Oil）, INCI：Kukui（aleurites moluccana)
Nut oil, CAS:8015-80-3.It is derived from candlenut tree tree（The state tree of Hawaii）, the seed that bankoul nut oil squeezing is set certainly, locals
There is the history of centuries using it, spread recently all over the world.Directly smearing can update and skin of releiving, and
There is no greasy feeling residual.Bankoul nut oil can be that dry, ripe age and impaired skin provide moisture and nourishing, so that suitable for all types of
Skin.Traditionally, local people are applied to bankoul nut oil with baby, come protect baby skin not by sunlight, salinity and other
The injury of material.In addition, bankoul nut oil is also used for handling allergic, wound and burn.Royalty member, come the oil that gives the massage, has with it
When, massage for up to 7-8 hours as long as！Bankoul nut oil energy rapid osmotic skin, leaves smooth sense of touch such as silk, and milli
Non-greasy.It is often used in rescue and dries impaired skin, rapid due to absorbing, almost at once with regard to that can mitigate symptom, even if
It is skin that is most coarse and drying, can also experience becomes smooth, soft and moist.Bankoul nut oil contains vitamin A, C, E, is rich in
Alpha-linolenic acid and basic aliphatic acid, these compositions can be anti-oxidant and protect skin, when being applied on skin, can penetrate into skin
The bottom, especially to sensitive skin very be applicable,
Evening primrose oil：English name：Evening Primrose Oil, INCI：Evening Primrose（oenothera
biennis) Oil.It is the grease being extract from the seed of oenothera biennis, in faint yellow, about containing 90% unrighted acid,
Wherein content at most be content about 70% linolenic acid (Linoleic Acid, abbreviation LA) and about 7~10% GLA（γ-
Leukotrienes）.Gamma-Linolenic acid, it is otherwise known as vitaminF, is described as flowers of life；Be referred to as in Europe " imperial family imperial medicine " or
" king's medicine ".Evening primrose oil is significant to suppress inflammation, evening primrose oil 2-4ml/kg gavage paraxylene caused by a variety of proinflammatory agents
Induced mice ear swelling, to normal rat and Adrenoprival rats Irish moss colloidality and histamine, prostaglandin E2（PGE2）, blanching
Foot swelling caused by property, formaldehyde, nystatin etc., there is obvious inhibitory action.Oenothera biennis can suppress the increase of fat cell,
Intestinal villus thickening, adjust gastrointestinal tract, reduce body fat accumulation, with slimming, fat-reducing the effect of.
Black pepper essential oil：English name：Black pepper, black pepper is a kind of perennial woody climbing plant, black
The southwest for originating in India of pepper, grows the countries, current city such as China, Malaysia and Madagascar extensively at present
Black pepper essential oil on field mostlys come from the countries in Southeast Asia such as India, Singapore.Extraction mode and position：Distillation extraction is dried
Fruit, main component：Thujene（thujene）, firpene（pinene）, limonene（limonene）, phellandrene
（phellandrene）, amphene（camphene）, sabinene（sabinene）, β-carypohyllene（beta-caryophyllene）、
Laurene（myrcene）.Black pepper essential oil outward appearance is in pistac liquid, can improve blood of human body using black pepper essential oil and follow
Loop system, stimulates circulation；Myalgia can be reduced, is improved a poor appetite, the diseases such as cold, influenza can also be effectively treated
Disease；Black pepper essential oil also has the function that anti-spasm, wind-dispelling are vented；Black pepper essential oil can stimulate circulation, and eliminate many in vivo
Remaining fat；Also there is anti-inflammation and sterilization, so as to reach promoting blood circulation and removing blood stasis and fat-reducing effect.
Hops oil：Also known as hop essential oil, English name：HOP OIL, INCI：HOPS(HUMULUS LUPULUS)
OIL, CAS:8007-04-3.Hop is also known as hops, and hops oil is derived from the petal of hop, colourless, pure and fresh beer
Taste and the wooden taste with a delicate fragrance.Oil can be controlled with clearing heat and detoxicating, cleaning skin, freckle removing and whitening, dispels eye at the tender skin of anti-wrinkle
Bag livid ring around eye, may additionally facilitate the skin-protecting functions such as damaged tissues regeneration recovery；Adrenaline is stimulated, fat-reducing, diuresis promotes blood to follow
Ring, promotes breast development.
Shaddock oil：Also known as grapefruit essential oil, English name：Grapefruit oil, INCI：Grapefruit（citrus
Grandis) oil, CAS:8016-20-4.Grapefruit essential oil be using fresh peel as raw material, produced using method for cold pressing and
Into main chemical composition is sobrerone or firpene, sabinene, laurene, limonene, geraniol, linalool, citronellal, acetic acid
Certain herbaceous plants with big flowers ester and terpinenes or terpinene.Grapefruit essential oil has a taste that kind can be refreshed oneself strongly, and color is yellowish or balas ruby color, water
Matter viscosity.Grapefruit essential oil contains the vitamin C of high concentration, thus highly beneficial with value to immune system.Can be effectively
Preventing cold and influenza, are best suitable for being used for the group of reducing fat（Fat woman's stern, leg）, also have for losing weight with diuresis actively
Effect, moreover it is possible to help body to exclude excessive moisture.By stimulating the circulation of lymph glandular system, internal poison can also be excluded
Element.
Ethyl nicotinate：Also known as：Acetyl methylamine, Niacin Nicitinic Acid ethyl ester, Nicotinicum Acidum ethyl ester, English name：Ethyl
Nicotinate, INCI：Hexyl Nicotinate, CAS：23597-82-2, chemical formula：C12H17NO2, molecular weight：
207.3.Ethyl nicotinate, which has, to reduce fat, and makes the effect of local fat reduction, transdermal flux can be broken down into glycerine and
Aliphatic acid, so as to reduce the moisture content in celluar tissue, and is conducive to aliphatic acid to be removed from these tissues, reaches slimming
Effect.
Capsicum oleoresin：Nickname chilli extract, English name：Capsicum oleoresin, capsicum oleoresin is to use section
Method is extracted from natural material capsicum, and its active ingredient is capsaicine, protein, amino acid and carbohydrate.Capsicum oleoresin
The decomposition rate of fat can be accelerated, and rich in dietary fiber, can be with lowering blood-fat and reducing weight.
Rosmarinus officinalis extract:INCI ROSEMARY (ROSMARINUS OFFICINALIS) EXTRACT, CAS:
84604-14-8.Rosemary, Labiatae Rosmarinus, shrub is high up to 2 meters.Active ingredient includes carnosic acid, Salvia japonica
Phenol, rosmanol, ursolic acid, Rosmarinic acid, major function is anti-oxidant, can improve activities of antioxidant enzymes in human body, suppresses
Lipid peroxidation, the effect with anti-aging, contained Rosmarinic acid and carnosic acid and skin epidermis compatibility are good, are difficult
Be flush with water loss, so good absorbing effect, antioxidation is strong, can also effective stimulus scalp blood circulation, sterilizing and itch-relieving, extensively
It is general to be used for hair products.
Tea Polyphenols：Also known as tea tannin, tannin, English name Tea Polyphenols, CAS:84650-60-2.With extremely strong
Harmful free radicals Scavenging activity, block lipid peroxidation process, improve the activity of human enzymes, thus play anti-mutation, it is anti-
Effect of cancer；Important role is metabolized to body fat, it is possible to decrease the content of cholesterol, triglycerides etc., removes blood vessel
Inwall fat deposition and atheromatous plaque；LOX and lipid peroxidation in skin mitochondria can be suppressed, so that
With anti-aging effect.Antioxidant is substantially better than vitamin E, and has synergy with injection Vitamin B_6；It is water-soluble substances, energy
The greasy of face is removed, pore is restrained, with sterilization, sterilizing, resisting age of skin, the ultraviolet radiation in daylight is reduced to skin
Damage the effects such as, can stop ultraviolet and remove ultraviolet induction free radical, so as to protect the normal of melanocyte
Function, suppresses the formation of melanin, suppresses lipid oxidation, mitigates pigmentation.
Embodiment
Embodiment 1
The high penetration small molecule camellia oil of embodiment 1, is made up of following processing step：
Step 1: producing high penetration small molecule camellia oil crude product
Camellia oil 7500g, food-grade ethanol 2000g, sodium hydroxide 20g are weighed by mass fraction；Camellia oil is heated to 60 DEG C；
Sodium hydroxide is added in food-grade ethanol, it is fully dissolved, is made into alcohol aqueous slkali；Alcohol aqueous slkali is slowly added to camellia oil
In, it is heated to 70 DEG C, constant temperature stirring at low speed 0.5 hour；It is heated to 80 DEG C, constant temperature high-speed stirred 2 hours；It is quickly cooled to often
Temperature, stands 4 hours, takes edible vegetable oil liquid thereon；Supernatant fluid is cooled fast to -5 DEG C（The temperature stood after the cooling of supernatant fluid）,
Stand 3 hours（The time stood after the cooling of supernatant fluid）, fast vacuum suction filtration obtains filtrate 7434ml（Amount of filtrate）；In filtrate
Middle addition 100g activated carbons（Activated carbon addition in filtrate）With 300g atlapulgites（Atlapulgite addition in filtrate）, heating
To 100 DEG C（Filtrate extraction temperature）, constant temperature stirring 1 hour（Filtrate Refining times）, filter to obtain high penetration small molecule camellia oil
Crude product 6528ml；
Step 2: producing cosmetics-stage high penetration small molecule camellia oil
Step one is made into high penetration small molecule camellia oil crude product to be separated in short-range molecular distillation device, plate temperature is scraped
130 DEG C, scraper velocity 200r/min, vacuum 0.06MPa, condensate liquid are collected as small molecule camellia oil, obtain 4047ml, heavy phase
Waste collection, obtains 2481ml.
Embodiment 2-6
Embodiment 2-6 high penetration small molecule camellia oil, the basic be the same as Example 1 of its preparation process condition, simply reaction raw materials
And the condition such as proportion scale, temperature, time is slightly different, specifically as listed in table 1.
Embodiment 7
Gained heavy phase waste liquid will be separated and collected in embodiment 1-6 medium or short range molecular distillation apparatus, it is every kind of respectively to take 1300g, altogether
7800g, substitution camellia oil adds food-grade ethanol 1000g, other basic be the same as Examples of step of preparation process as reaction raw materials
1, simply the condition such as proportion scale, temperature, time be slightly different, specifically as listed in table 1.
The embodiment 1-7 of table 1 high penetration small molecule camellia oil preparation process condition
Embodiment 8-14
Respectively with embodiment 1-7 high penetration small molecule camellia oil, other raw materials are equipped with, through uniform mixing, reality is obtained successively
The slimming camellia massage oil of the high penetration of a 8-14 is applied, specific dispensing situation is as listed in table 2.
Comparative example 1
High penetration small molecule camellia oil in the raw materials used camellia oil of embodiment 1, substitution embodiment 8, other dispensings and ratio
Be the same as Example 8, is well mixed, and the slimming camellia massage oil of high penetration is made, as a comparison case, table 2 is specifically listed in.
Comparative example 2
Comparative example 2 eliminates hops oil on the basis of embodiment 8, and other are same as Example 8.
Comparative example 3
Comparative example 3 eliminates Rosmarinus officinalis extract on the basis of embodiment 8, and other are same as Example 8.
The embodiment 8-14 of table 2 and comparative example dispensing situation, gram
The slimming camellia massage oil of embodiment 8-14 high penetrations and the behavior pattern of comparative example 1-3 compound camellia oils, bag
Viscosity, osmotic absorption speed, performance of keeping humidity, slimming effect, antioxidative stabilizer are included, table 3 is specifically listed in.
The embodiment 8-14 of table 3 and comparative example behavior pattern
Used method of testing is as follows in table 3:
(1) viscosity of the slimming camellia massage oil of high penetration and compound camellia oil, is determined using capillary tube method.
(2) osmotic absorption speed is the impression after human hand back use；
(3) slimming measure of merit
Example 8-14 slimming camellia compound essential oil carries out premise slimming effect test, and subjects are three-dimensional, body
High, the 20-30 Sui young woman of body weight relatively 80, is randomly divided into 8 groups, every group of 10 people.Wherein, 7 groups use embodiment
8-14 slimming camellia compound essential oil, 1 group of camellia oil using comparative example carries out whole body massage 1h, and coordinate thin every night
Body is moved.An every 15 days body weight of measurement and measurements of the chest, waist and hips, record its change such as table 4.
Table 4
(4) antioxidative stabilizer method of testing：
Test objective：When oxidation of the camellia compound essential oil of Observe and measure embodiments of the invention under different high-temperature conditions is induced
Between calculate that oxidation stability is fixed and shelf life, the slimming camellia massage oil for the high penetration of embodiments of the invention is provided
Product stability foundation.
Test apparatus：Oil oxidative stability analyzer（743 types are led in Switzerland ten thousand）
Experimental procedure：Randomly select the 8-11 embodiments of the present invention camellia compound essential oil weigh respectively it is appropriate in 100,110,
120th, oxidation induction time is determined at 130 DEG C, pass through system plug-in and export shelf life.Result of the test is shown in Table 5.
Table 5
Conclusion (of pressure testing)：The slimming camellia massage oil of the high penetration of various embodiments of the present invention has significant oxidation-stabilized
Property.
Result explanation listed by table 3,4,5, the slimming camellia massage oil of high penetration of the present invention, including viscosity, infiltration
Infiltration rate, performance of keeping humidity, slimming effect, antioxidative stabilizer, corresponding control group is better than etc. performance.
In addition, by the slimming camellia massage oil of the high penetration obtained by embodiment 8-14, by examining microorganism to refer to
Mark, sanitary index《Cosmetics health specification》（Version in 2007）, obtain the testing result shown in table 6 below：
Table 6
The slimming camellia massage oil toxicology test of high penetration of the present invention：Skin irritation test（Multiple skin irritatin
Property experiment）.
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The camellia of embodiments of the invention is answered
Square essential oil）Produced skin irritation reaction afterwards, is the slimming camellia massage of the high penetration of embodiments of the invention
Oil provides security foundation.
Test basis：《Cosmetics health specification》Version in 2007.
Test method：From white New Zealand rabbits 8,2 groups, every group 4 are randomly divided into.A groups:Intact skin group, B groups:
Olive sunflower oil control group.24h cuts family's rabbit back backbone both sides hair before experiment, not injured skin surface in cropping, goes
Hair scope is 3cm × 3cm, and application area is 2.5cm × 2.5cm., high penetration of the tested material group to various embodiments of the present invention
The camellia compound essential oil of anti-skin aging, takes tested material 0.5ml to be coated directly on the side of back backbone, and opposite side applies 0.5ml pairs
According to a group olive sunflower oil, smear 1 time daily, continuously smear 14d.Since second day, olive sunflower was used in cropping when smearing every time
Oil removes residual tested material.Result is observed after one hour, according to《Cosmetics health specification》The skin irritation of version in 2007
Table scoring is tested, check plot and trial zone are equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
Result of the test：Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
High penetration slimming camellia massage oil after, rabbit has no erythema, oedema.Have no systemic toxicity profiles performance and dead feelings
Condition, the weight of animals increase, on breathing, circulation, central nervous system, four limbs activity etc. without influence.
Conclusion (of pressure testing)：The slimming camellia massage oil of the high penetration of various embodiments of the present invention is to white New Zealand rabbits
Intact skin is nonirritant.
Claims (7)
1. a kind of slimming camellia massage oil of high penetration, is made up according to mass fraction of following component:High penetration is small
70~80 parts of molecule camellia oil, 5~10 parts of candlenut tree macadamia nut oil, 3~5 parts of evening primrose oil, 3~5 parts of black pepper essential oil, hops oil
2~5 parts, 2-5 parts of shaddock oil, 0.5~1 part of ethyl nicotinate, 0.1~0.3 part of capsicum oleoresin, Rosmarinus officinalis extract 0.1~0.3
0.1~0.3 part of part, Tea Polyphenols or its fatty acid ester.
2. the slimming camellia massage oil of high penetration according to claim 1, it is characterised in that：Described Thief zone
Power small molecule camellia oil, is made via following processing step：
Raw material is weighed by following proportion by weight：75~85 parts of camellia oil, 15~25 parts of food-grade ethanol, highly basic 0.2~1.0
Part；By the camellia oil weighed, 50~60 DEG C are heated to；Load weighted highly basic is added in food-grade ethanol, makes it fully molten
Solution, is made into alcohol aqueous slkali；Alcohol aqueous slkali is slowly added in camellia oil, 60~70 DEG C, constant temperature stirring at low speed 30~60 are heated to
Minute；It is then heated to 80~100 DEG C, constant temperature high-speed stirred 1~2 hour；Cooling, stands 3~4 hours, takes edible vegetable oil liquid thereon；
Supernatant fluid is cooled to -5~5 DEG C, 3~4 hours are stood, rapid vacuum suction filtration obtains filtrate；Appropriate activity is added in filtrate
Charcoal and atlapulgite, are heated to 80~100 DEG C, constant temperature is stirred 1-3 hours, filters to obtain high penetration small molecule camellia oil crude product；
Step 2: producing cosmetics-stage high penetration small molecule camellia oil
Step one is made into high penetration small molecule camellia oil crude product to be separated in short-range molecular distillation device, plate temperature is scraped
130~150 DEG C, scraper velocity 200-250r/min, 0.04~0.06MPa of vacuum, condensate liquid is used as high penetration small molecule
Camellia oil is collected, and heavy phase waste liquid is separately collected.
3. the slimming camellia massage oil of high penetration according to claim 2, it is characterised in that：The step one
In, camellia oil is using obtained by physical squeezing.
4. the slimming camellia massage oil of high penetration according to claim 2, it is characterised in that：The step one
In, highly basic is the one or more in sodium hydroxide, potassium hydroxide, caustic alcohol, potassium ethoxide.
5. the slimming camellia massage oil of high penetration according to claim 2, it is characterised in that：The step 2
In, the distillation yield of high penetration small molecule camellia oil is 60~65%.
6. the slimming camellia massage oil of high penetration according to claim 2, it is characterised in that：In the step 2
Heavy phase waste liquid reclaimed, replace camellia oil raw material, prepare high penetration small molecule again by the method for being similar to step one
Camellia oil crude product, then separated by the method for step 2, condensate liquid is high penetration small molecule camellia oil, distills heavy phase waste liquid
Abandon it.
7. the preparation method of high penetration slimming camellia massage oil according to claim 1, it is characterised in that：Will be each
Component is uniformly mixed.
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| CN109464354A (en) * | 2018-12-23 | 2019-03-15 | 广州航美化妆品有限公司 | With the skin care compositions for reducing subcutaneous fat content and the compact effect of lifting |
| CN110449052A (en) * | 2018-05-07 | 2019-11-15 | 袁宏磊 | Prepare the atomization mixing arrangement and method of Chinese medicinal herb weight-losing lipid-loweringing essential oil |
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| CN101717691A (en) * | 2009-10-30 | 2010-06-02 | 华南理工大学 | Method for refining cosmetic camellia oil by adopting short-path distillation |
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| CN110449052A (en) * | 2018-05-07 | 2019-11-15 | 袁宏磊 | Prepare the atomization mixing arrangement and method of Chinese medicinal herb weight-losing lipid-loweringing essential oil |
| CN109464354A (en) * | 2018-12-23 | 2019-03-15 | 广州航美化妆品有限公司 | With the skin care compositions for reducing subcutaneous fat content and the compact effect of lifting |
| CN109464354B (en) * | 2018-12-23 | 2021-07-06 | 广州航美化妆品有限公司 | Skin care composition with effects of reducing subcutaneous fat content and improving skin firmness |
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Application publication date: 20171020 |