CN107259427A - The preparation method of Wild jujube original powder piece - Google Patents
The preparation method of Wild jujube original powder piece Download PDFInfo
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- CN107259427A CN107259427A CN201710373340.2A CN201710373340A CN107259427A CN 107259427 A CN107259427 A CN 107259427A CN 201710373340 A CN201710373340 A CN 201710373340A CN 107259427 A CN107259427 A CN 107259427A
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- wild jujube
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- former powder
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- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 18
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- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/34—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using microwaves
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of preparation method of the former powder piece of Wild jujube.Belong to natural plants candy type food technology field.Wild jujube original powder piece component:Containing Wild jujube 100%;Raw material selects market purchasing Wild jujube face, contain 31 kinds of mineral matters and trace element, multivitamin in Wild jujube face, the former powder piece of the Wild jujube of preparation is in brown color, sweet and sour, for natural plants health candy type food, with the effect, beneficial health such as reducing blood lipid, anti-arrhythmia and decompression, calmness, hypnosis, expansion blood vessel.Preparation method includes broken raw material, drying sterilizing, crushing, granulation, mixing, six steps of tabletting, the present invention is without any auxiliary material, with fabulous dispersibility and absorbability, both original flavor is remained, more improve healthcare function, it is possible to dose is reduced at double.
Description
Technical field
The present invention relates to a kind of preparation method of the former powder piece of Wild jujube, belong to natural plants candy type food technology neck
Domain.
Background technology
Wild jujube contains 31 kinds of mineral matters and potassium, sodium, iron, zinc, selenium and other trace elements, multivitamin, the dimension being rich in
Raw element is 2~3 times of jujube, and 20~30 times of citrus, be the outstanding person of all fruit.Recent study shows that Wild jujube has
There are the effects such as reducing blood lipid, anti-arrhythmia and decompression, calmness, hypnosis, expansion blood vessel, sleep quality can be improved with antitoxic heart-soothing and sedative,
It is calming the nerves, there is its original place in insomnia field, and evident in efficacy, by doctor patient's laudatory title " sleeping fruit in east ".It is simultaneously wild
Wild jujube is also CFDA(National beverage pharmaceuticals administration general bureau)Integration of drinking and medicinal herbs, the plant component of medicine-food two-purpose promulgated earliest,
Liked by people.
Wild jujube can be made into plurality kinds of health care beverage, health products, market as integration of drinking and medicinal herbs, medical and edible dual purpose plant fruit
Prospect is huge, meets the health care consciousness of modern people.
The content of the invention
The technical problem to be solved in the invention is to provide a kind of preparation method of the former powder piece of Wild jujube, and it is in reddish brown
Color, sweet and sour, suitable long-term consumption.
In order to solve the above technical problems, the technical solution adopted in the present invention is:
A kind of preparation method of the former powder piece of Wild jujube, comprises the following steps:
Step 1, raw material are crushed:Wild jujube face is broken into a diameter of 1~10mm particle with super power crusher;
Step 2, drying sterilizing:Sterilization is dried in crushed particles:
Step 3, crushing:By the good Wild jujube face particle of drying sterilizing, it is into average grain diameter with micronizer low-temperature grinding
800~0.1 μm of micro mist;
Step 4, granulation:Micro mist after crushing is inserted to the particle that 8~50 mesh are made in dry crowded granulator;
Step 5, mixing:Particle is placed in into three-dimensional mixer to mix;
Step 6, tabletting:Mixed particle is subjected to tabletting with rotary tablet machine.
Technical solution of the present invention further improvement is that:Wild jujube flour/powder in step 1 selects market purchasing raw material
Or oneself processes raw material, Wild jujube face is to be enucleated with dry Wild jujube, leave the size-reduced acid processed that sieves of skin and flesh
Jujube flour/powder, the drying of its quality, particle exquisiteness, free from admixture, without dust.Manufacturer is domestic enterprise, or in Taobao, Arriba
The electric business websites such as bar are bought.
Technical solution of the present invention further improvement is that:Super power crusher is using centering rotor block in step 1.
Technical solution of the present invention further improvement is that:Sterilization is dried using microwave drying sterilization machine in step 2,
Microwave drying sterilization machine is tunnel type, and drying sterilizing temperature is 70 DEG C~105 DEG C, and the drying sterilizing time is 90~180 seconds.
Technical solution of the present invention further improvement is that:The temperature of low-temperature grinding is≤- 36 DEG C, low temperature powder in step 3
The broken time is 1~30 minute.
Technical solution of the present invention further improvement is that:Refrigerant in step 3 used in micronizer is cold for Type B
Freeze liquid, content is respectively the component of Type B freezing liquid by mass percentage:Methylcellulose 2%~8%, fructose syrup 16%~20%,
Propane diols 25%~35%, sodium chloride 3%~7%, gelatin hydrolysate 2%~3%, surplus is water.
Technical solution of the present invention further improvement is that:It is stainless steel that crowded granulator is done in step 4, is pressed into 8
The particle of~12 mesh.
Technical solution of the present invention further improvement is that:Incorporation time is 15~30 minutes in step 5.
Technical solution of the present invention further improvement is that:Substrate piece weight in step 6 after tabletting is 0.1~3g/ pieces, weight
It is ± 5~± 7.5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture < 5.0% to measure difference limit.
Technical solution of the present invention further improvement is that:The compression mold that rotary tablet machine is used in step 6 is ellipse
Circle, triangle, square, pentagon, olive shape xenotype mold.
By adopting the above-described technical solution, the technological progress that the present invention is obtained is:
Wild jujube original powder piece is a kind of candy type food rich in Vc, and raw material is enucleated using pollution-free dry Wild jujube, stayed
The broken Wild jujube face processed of hypodermis digested tankage, mouthfeel is unique, good taste, more save the nutrition of Wild jujube into
Point and peculiar taste, product have tranquilizing soporific, disappear it is tired go it is dry, reduce blood pressure, the health-care efficacy such as anti-inflammatory diuresis, can anti-aging,
Physical fitness, body beauty, beneficial health.
The present invention is improved existing preparation technology, and traditional Wild jujube breaking method is improved into low temperature ultra micro
Crush, be easy to, by Wild jujube breaking-wall cell, make active ingredient more preferably discharge, stability is good, in good taste, suitable mouth containing.
Stable preparation process of the present invention is strong, and product Wild jujube original powder piece is disintegrated rapidly in oral cavity, no sand type, tool
There is fabulous dispersibility and absorbability, it is nonirritant to mucous membrane of mouth, make the active ingredient of the former powder piece of Wild jujube rapid
Into internal, original flavor is both remained, more improve healthcare function, it is possible to dose is reduced at double, effectively improve wild acid
The utilization rate of jujube resource.
Wild jujube face product characteristics are bulk, and moisture content is higher, are difficult to crush, it is necessary to be crushed, at drying sterilizing
Manage into attritive powder.
The broken super power crusher used carries out Wild jujube face coarse crushing, and operation principle is:Material is entered by feed hopper
Crushing chamber, is impacted using rotating knife and fixing cutter, sheared and obtain crushed particles, the effect of rotated centrifugal force, material passes through
Certain pore size sieve plate automatic stream exit, obtains the particle of certain particle size.The super power crusher is designed by " GMP " standard, whole
Machine using stainless steel material manufacture, it is simple in construction, easy to clean, noise is low, be currently coarse crushing in comparatively ideal equipment.
The super power crusher has advantages below:
1st, simple and compact for structure, stable transmission, adjustment is flexible, shock resistance, adapts to more severe production environment;
2nd, what is used electrically activates mode from even decompression, steady with starting, the uniform feature of operating;
3rd, rational in infrastructure, operation maintenance is convenient, durable electricity-saving, Applied economy;
4th, provided with multinomial safety guard, it is ensured that safe operation;
5th, cast hopper double layer design, reduces noise;
6th, grinding particle size is controlled, crushing is big in the unit interval, and performance safety is reliable;
7th, using multichannel discharge, reach that requirement qualified material is excluded in time, extend the consumable accessory life-span, improve unit-hour output;
8th, using centering rotor block, rotary inertia is big, and force de frappe is strong, has a power failure do not result in equipment blocking suddenly.
Microwave drying process, is microwave and material direct interaction, and uhf electromagnetic wave is converted into heat energy dries open country
Without any auxiliary material in raw wild jujube face, drying process, at utmost retain the valid density of nutritional ingredient.Microwave drying
Process can be sufficiently reserved Wild jujube flour nutrition composition and its biological natural activity.
Microwave disinfection process is microwave heating effect and the coefficient result of biological effect.Electricity of the microwave to bacterial membrane section
Bit distribution influences cell membrane ambient electron and ion concentration, so as to change membrane passage energy, bacterium is therefore malnutritive,
Eubolism is unable to, interrupted death of growing.From the point of view of biochemical angle, the nucleic acid of bacterium normal growth and breeding
(RNA) and DNA (DNA) is the curling macromolecular being closely formed by connecting by some hydrogen bonds, microwave causes hydrogen bond pine
Relax, be broken and recombinate, so that gene or chromosome aberration are induced, or even fracture.Microwave disinfection is exactly imitated using electromagnetic field
The killing action to microorganism should be played with biological effect.It facts have proved using microwave device in sterilization temperature, sterilizing time, production
Product quality is kept, shelf life of products and energy-conservation aspect have obvious advantage.
1st, the fuel factor of microwave energy:In the presence of some strength microwave field, insects and thalline in food can be because of molecules
Polarization phenomena, absorb microwave energy heating, so that its protein denaturation, loses bioactivity.The fuel factor of microwave mainly rises soon
Speed heating bactericidal action;
2nd, the non-thermal effect of microwave energy:The electric field of high frequency also makes its film potential, polar molecular structure change;Make microorganism
Vivo protein and physiological activator morph, and devitalization or death.Typical physical sterilization is served in sterilization
Unexistent special role, is also to cause one of bacterial death reason;
3rd, microwave disinfection is microwave heating effect and the coefficient result of non-thermal effect.Therefore, microwave disinfection temperature is less than conventional
Method, generally, conventional method sterilization temperature want 120 DEG C -130 DEG C, about 1 hour time, and microwave disinfection temperature only will
70 DEG C -105 DEG C, about 90-180 seconds time;
Ultramicro grinding uses micronizer, and the temperature that the micronizer can be below -36 DEG C carries out low-temperature grinding, prevents thing
The heat produced during feed powder is broken raises crushing chamber temperature, retains the nutritional ingredient of material, will not destroy material active matter
Matter, energy consumption is low;The micro mist that average grain diameter is 800~0.1 μm is ground into, micron orderization is crushed, it is ensured that detailed-oriented, the raising of material
The quality and efficiency of low-temperature grinding, and control safe and reliable, it is easy to promotion and implementation.
Refrigerant used in micronizer is Type B freezing liquid, outer clip of the Type B freezing liquid in micronizer crushing chamber
Extremely cold space is formed in set, the function of low temperature Quench material in crushing chamber is realized.The component of Type B freezing liquid contains by mass percentage
Measuring is respectively:Methylcellulose 2%~8%, fructose syrup 16%~20%, propane diols 25%~35%, sodium chloride 3%~7% is hydrolyzed bright
Glue 2%~3%, surplus is water.Major part is used as using fructose syrup, propane diols so that the production cost of Type B freezing liquid compared with
Low, simple production process;Wherein fructose syrup can be from F42 fructose syrups, F55 fructose syrups, F90 fructose syrups at least
One kind, sorting is convenient;Propane diols is moderate, and good fluidity is not volatile, and fusing point is low, harmless, to equipment without corruption
Erosion, there is anti-corrosion, sterilizing, while propane diols is soluble in water, preparing process is simple, can arbitrarily be made into various freezing points, its
Minimum reachable -78 DEG C of freezing point, refrigerating effect is good.Without ethanol, the potential safety hazard in process of manufacture is reduced, without second two
Alcohol, safety non-toxic;Contained sodium chloride concentration is relatively low, reduces the corrosion to equipment;The a small amount of gelatin hydrolysate and Methyl cellulose added
Element, plays a part of stabilizer and thickening oil lubrication, is conducive to improving the service life of Type B freezing liquid.Fructose syrup, the third two
Alcohol, sodium chloride, gelatin hydrolysate use food grade materials, using safety non-toxic, with boiling point is high, foam tendency is low, viscous warm nature
Can good, good fluidity, anti-corrosion, the features such as easily configure.
The micro mist that average grain diameter is 800~0.1 μm is ground into, particle diameter is small, increases because powder specific-surface area detection is huge, be significantly greatly increased
Nutritional ingredient and the active area of human enzymes, it is easily that human body is comprehensively sufficient to make to enrich nourishing ingredients contained by Wild jujube face
Digest and assimilate, improve Wild jujube face tonic effect and nutritional ingredient utilization rate.
In field of food preparation, particle is thinner, and the molecular number on surface is more, and the interfacial energy of particle is also got over
Greatly, the trophism of food can be improved from physical angle;On the other hand, particle is thinner, is more easily absorbed by the body.Wild jujube
The nutrition in face is typically distributed about in cell membrane, and nutritional ingredient is difficult to be absorbed by the body, when cell membrane is by ultramicro grinding broken wall
Afterwards, intracellular nutritional composition is able to abundant exposure, greatly improves and adds into the rate of release of internal rear nutritional ingredient and release two
Fast absorption process, these particulates are strong because of adhesive force, excrete time lengthening, absorbed easily by intestinal wall, improve nutrition into
The absorptivity divided.
When being ground into the micro mist that average grain diameter is 800~0.1 μm, unique taste at Wild jujube nutrition position can be substantially smelt
Road.
Micro mist after crushing is directly carried out it is dry extrude grain, using the surface tension of micro mist is big and contained humidity itself, viscous
Property, it is directly dry to extrude grain, do that crowded granulator extruding work is continuous, efficiency high, the material compacting degree of extruding is uniform, finished particle into
Grain rate is high.
Link is mixed, Wild jujube original powder particles nutritional ingredient content distribution during manufacture particle is uneven, passes through
Mix link, make in the former powder particles of Wild jujube that nutritional ingredient mixed distribution pockety is uniform, improve particle nutrition into
Divide the control of product quality of uniformity and production process.
Three-dimensional mixer is employed herein, in the running of three-dimensional mixer, because mix cylinder is with more
Direction motion, makes material in mixed process, accelerate flowing and diffusion, while avoid the machine of generally mixing with because from
Material gravity segregation and accumulation phenomenon produced by mental power function, are mixed without dead angle, not stratified, well mixed and production efficiency
Height, it is simple to operate, raw material will not be also polluted, the best in quality of mixed material can be effectively ensured, mixture homogeneity can reach
More than 90%(Auger, V-type, two-dimensional mixing machine are without this effect).
Substrate piece weight after compacting is 0.1~3g/ pieces, and limit test of weight variation is ± 5~± 7.5%, hardness >=3kg/ ㎝ 2,
Friability≤1%, moisture < 5.0%.Mobility of particle is good in label any surface finish, no color differnece, tableting processes, substrate product outward appearance
Character and hardness meet candy type food quality standard, category green, safety food.Carry convenient to take, it is in good taste, prepare work
Skill is simple, and cost is low.The candy matrix processed can be sufficiently reserved Wild jujube nutritional ingredient and its biological natural activity, pressure
The former powder piece flat appearance of the Wild jujube made, processing step is simple, process time is short, be easy to preserve.
The former powder piece of Wild jujube that the inventive method is obtained, the nutritional ingredient such as trace element, multivitamin is saved from damage preferably,
Green and healthy, instant, and water content is low, stability is good, and shelf lives are long;Easily for human body, sufficiently digestion is inhaled comprehensively
Receive, and be easy to take, it is easy to carry.With antitoxic heart-soothing and sedative, the effect of sleep quality is improved, is organic, pollution-free food.
Embodiment
The present invention is described in further details with reference to embodiment:
Embodiment 1
A kind of preparation method of the former powder piece of Wild jujube, the preparing raw material of Wild jujube original powder piece uses Taihang the foot of a mountain genunie medicinal materials
Rhamnaceae plant Wild jujube(Scientific name:Ziziphus jujuba Mill. var.spinosa (Bunge) Hu ex
H.F.Chou)Dry mature fruit stoning, stay the size-reduced Wild jujube face that processes of sieving of skin and flesh.Process is such as
Under:
Step 1, raw material are crushed:By the Wild jujube face of purchase(Easily make moist caking), a diameter of 1 is broken into super power crusher
~10mm particle, super power crusher is using centering rotor block.
Step 2, drying sterilizing:The particle crushed is carried out into microwave drying using tunnel type micro wave drying-sterilizing machine to kill
Bacterium, drying sterilizing temperature 70 C~105 DEG C, 90~180 seconds time, the present embodiment is 80 DEG C, 180 seconds time.
Step 3, crushing:The good Wild jujube face particle of drying sterilizing, micronizer crushing chamber is inserted by refrigerant
External jacket in, make micronizer external jacket temperature control at -36 DEG C, it is final to crush to carry out low-temperature grinding 1~30 minute
Into the micro mist that average grain diameter is 800~0.1 μm, the present embodiment is 500 μm;Refrigerant is Type B freezing liquid, Type B freezing liquid
Content is respectively component by mass percentage:F42 fructose syrups 28%, propane diols 35%, sodium chloride 7%, gelatin hydrolysate 3%, methyl
Cellulose 2%, surplus is water, can be by the external jacket temperature control of micronizer crushing chamber in -36 DEG C, grinding time 20 minutes.
Step 4, granulation:8~12 purposes are made in the dry crowded granulator that micro mist after crushing is inserted to stainless steel
Grain, the present embodiment is the particle of 8 mesh, moisture < 5.0%.
Step 5, mixing:Particle is placed in into three-dimensional mixer to mix, incorporation time is 15~30 minutes, the present embodiment mixing
Time is 30 minutes.
Step 6, tabletting:Mixed particle is subjected to tabletting with rotary tablet machine, the substrate piece weight after tabletting is 0.1
~3g/ pieces, limit test of weight variation is ± 5~± 7.5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture < 5.0%, this implementation
Example piece weight is 1g/ pieces, and limit test of weight variation is ± 5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture < 4.0%, rotary pressure
The compression mold that piece machine is used is ellipse, triangle, square, pentagon, olive shape xenotype mold.
Embodiment 2
The present embodiment is distinguished as with embodiment 1:
It is step 1, broken:By Wild jujube face, a diameter of 1~8mm particle is broken into super power crusher.
Step 2, drying sterilizing:The present embodiment microwave drying sterilization temperature is 90 DEG C, and the time is 120 seconds.
Step 3, crushing:The present embodiment micronizer low-temperature grinding into average grain diameter be 200 μm of micro mist;Ultramicro-powder
The refrigerant that broken machine is used is Type B freezing liquid, and content is respectively the component of Type B freezing liquid by mass percentage:F42 high fructose corns
Slurry 20%, propane diols 25%, sodium chloride 3%, gelatin hydrolysate 2%, methylcellulose 3%, surplus is water, can crush micronizer
The external jacket temperature control of chamber is in -46 DEG C, grinding time 30 minutes.
Step 4, granulation:The present embodiment is the mesh of particle 15, granule moisture level < 4.5%.
Step 5, mixing:The present embodiment incorporation time is 20 minutes.
Step 6, tabletting:The present embodiment piece weight is 0.5g/ pieces, and limit test of weight variation is ± 5%, and hardness >=3kg/ ㎝ 2 is crisp
Broken degree≤1%, moisture < 4.5%.
Embodiment 3
The present embodiment is distinguished as with embodiment 1:
It is step 1, broken:By Wild jujube face, a diameter of 2~6mm particle is broken into super power crusher.
Step 2, drying sterilizing:The present embodiment microwave drying sterilization temperature is 70 DEG C, and the time is 150 seconds.
Step 3, crushing:The present embodiment powder particle diameter is 300 μm;Refrigerant is Type B freezing liquid, the component of refrigerant
Content is respectively by mass percentage:F42 fructose syrups 16%, F55 fructose syrups 10%, propane diols 26%, sodium chloride 3.5%, water
Gelatin 3% is solved, surplus is water, can be by the external jacket temperature control of micronizer crushing chamber in -38 DEG C, grinding time 15 minutes.
Step 4, granulation:The mesh of the present embodiment particle 12, granule moisture level < 5.0%.
Step 5, mixing:The present embodiment incorporation time is 15 minutes.
Step 6, tabletting:The present embodiment piece weight is 0.25g/ pieces, and limit test of weight variation is ± 7.5%, hardness >=3kg/ ㎝ 2,
Friability≤1%, moisture < 5.0%.
Embodiment 4
The present embodiment is distinguished as with embodiment 1:
It is step 1, broken:By Wild jujube face, a diameter of 4mm particle is broken into super power crusher.
Step 2, drying sterilizing:The present embodiment microwave drying sterilization temperature is 100 DEG C, and the time is 170 seconds.
Step 3, crushing:The present embodiment micronizer low-temperature grinding into average grain diameter be 600 μm of micro mist;Ultramicro-powder
The refrigerant that broken machine is used is Type B freezing liquid, and content is respectively the component of Type B freezing liquid by mass percentage:F42 high fructose corns
Slurry 20%, propane diols 26%, sodium chloride 3.1%, gelatin hydrolysate 2.7%, methylcellulose 2.9%, surplus is water, can be by ultramicro grinding
The external jacket temperature control of machine crushing chamber is in -38 DEG C, grinding time 30 minutes.
Step 4, granulation:The present embodiment is the mesh of particle 25, granule moisture level < 4.5%.
Step 5, mixing:The present embodiment incorporation time is 26 minutes.
Step 6, tabletting:The present embodiment piece weight is 3g/ pieces, and limit test of weight variation is ± 5%, hardness >=3kg/ ㎝ 2, friability
Degree≤1%, moisture < 4.5%.
Claims (10)
1. the preparation method of the former powder piece of a kind of Wild jujube, it is characterised in that comprise the following steps:
Step 1, raw material are crushed:Wild jujube face is broken into a diameter of 1~10mm particle with super power crusher;
Step 2, drying sterilizing:Sterilization is dried in crushed particles:
Step 3, crushing:By the good Wild jujube face particle of drying sterilizing, it is into average grain diameter with micronizer low-temperature grinding
800~0.1 μm of micro mist;
Step 4, granulation:Micro mist after crushing is inserted to the particle that 8~50 mesh are made in dry crowded granulator;
Step 5, mixing:Particle is placed in into three-dimensional mixer to mix;
Step 6, tabletting:Mixed particle is subjected to tabletting with rotary tablet machine.
2. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Wild acid in step 1
Market purchasing raw material is selected in jujube face.
3. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Strongly crushed in step 1
Machine is using centering rotor block.
4. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Microwave is used in step 2
Sterilization is dried in drying-sterilizing machine, and microwave drying sterilization machine is tunnel type, and drying sterilizing temperature is 70 DEG C~105 DEG C, is dried
Sterilizing time is 90~180 seconds.
5. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Low-temperature grinding in step 3
Temperature be≤- 36 DEG C, time of low-temperature grinding is 1~30 minute.
6. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Ultramicro grinding in step 3
Refrigerant used in machine is Type B freezing liquid, and content is respectively the component of Type B freezing liquid by mass percentage:Methylcellulose
2%~8%, fructose syrup 16%~20%, propane diols 25%~35%, sodium chloride 3%~7%, gelatin hydrolysate 2%~3%, surplus is water.
7. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:It is dry in step 4 to extrude grain
Machine is stainless steel, is pressed into the particle of 8~12 mesh.
8. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Incorporation time in step 5
For 15~30 minutes.
9. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:In step 6 after tabletting
Substrate piece weight is 0.1~3g/ pieces, and limit test of weight variation is ± 5~± 7.5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture
< 5.0%.
10. the preparation method of the former powder piece of Wild jujube according to claim 1, it is characterised in that:Rotatably pressed in step 6
The compression mold that piece machine is used is ellipse, triangle, square, pentagon, olive shape xenotype mold.
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Citations (2)
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CN105796621A (en) * | 2016-04-29 | 2016-07-27 | 河北林益堂药业有限公司 | Preparation method of Linxiashanshen raw powder tablet |
CN105902587A (en) * | 2016-04-29 | 2016-08-31 | 河北林益堂药业有限公司 | Preparation method of panax quinquefolius raw powder tablets |
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2017
- 2017-05-24 CN CN201710373340.2A patent/CN107259427A/en active Pending
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Publication number | Priority date | Publication date | Assignee | Title |
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CN105796621A (en) * | 2016-04-29 | 2016-07-27 | 河北林益堂药业有限公司 | Preparation method of Linxiashanshen raw powder tablet |
CN105902587A (en) * | 2016-04-29 | 2016-08-31 | 河北林益堂药业有限公司 | Preparation method of panax quinquefolius raw powder tablets |
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