CN107183592A - The preparation method of Wild jujube piece - Google Patents

The preparation method of Wild jujube piece Download PDF

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Publication number
CN107183592A
CN107183592A CN201710373801.6A CN201710373801A CN107183592A CN 107183592 A CN107183592 A CN 107183592A CN 201710373801 A CN201710373801 A CN 201710373801A CN 107183592 A CN107183592 A CN 107183592A
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CN
China
Prior art keywords
wild jujube
preparation
magma
jujube piece
drying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710373801.6A
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Chinese (zh)
Inventor
林飞武
尹志刚
李红梅
林朝阳
杨晓彤
李晓
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hebei Linyitang Pharmaceutical Co Ltd
Original Assignee
Hebei Linyitang Pharmaceutical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hebei Linyitang Pharmaceutical Co Ltd filed Critical Hebei Linyitang Pharmaceutical Co Ltd
Priority to CN201710373801.6A priority Critical patent/CN107183592A/en
Publication of CN107183592A publication Critical patent/CN107183592A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/01Instant products; Powders; Flakes; Granules
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00Shaping or working of foodstuffs characterised by the products
    • A23P10/20Agglomerating; Granulating; Tabletting
    • A23P10/28Tabletting; Making food bars by compression of a dry powdered mixture
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a kind of preparation method of Wild jujube piece.Belong to natural plants health candy type food technology field.Wild jujube piece component:Soluble solid containing Wild jujube 27%~54%, remaining is sweetener;Raw material concentrates magma from market purchasing Wild jujube, preparation method includes drying and granulating, mixing, three steps of tabletting, Wild jujube concentration magma therein contains 31 kinds of mineral matters and trace element, multivitamin, the Wild jujube piece of preparation is in brownish red, sweet and sour, with the effect, beneficial health such as reducing blood lipid, anti-arrhythmia and decompression, calmness, hypnosis, expansion blood vessel.

Description

The preparation method of Wild jujube piece
Technical field
The present invention relates to a kind of preparation method of Wild jujube piece, belong to natural plants juice solid beverage technical field.
Background technology
Wild jujube contains 31 kinds of mineral matters and potassium, sodium, iron, zinc, selenium and other trace elements, multivitamin, the dimension being rich in Raw element is 2~3 times of jujube, and 20~30 times of citrus, be the outstanding person of all fruit.Recent study shows that Wild jujube has There are the effects such as reducing blood lipid, anti-arrhythmia and decompression, calmness, hypnosis, expansion blood vessel, sleep quality can be improved with antitoxic heart-soothing and sedative, It is calming the nerves, there is its original place in insomnia field, and evident in efficacy, by doctor patient's laudatory title " sleeping fruit in east ".It is simultaneously wild Wild jujube is also CFDA(National beverage pharmaceuticals administration general bureau)Integration of drinking and medicinal herbs, the plant component of medicine-food two-purpose promulgated earliest, Liked by people.
Wild jujube can be made into plurality kinds of health care beverage, health products, market as integration of drinking and medicinal herbs, medical and edible dual purpose plant fruit Prospect is huge, meets the health care consciousness of modern people.
The content of the invention
The technical problem to be solved in the invention is to provide a kind of preparation method of Wild jujube piece, and it is in brownish red, taste It is sour-sweet, suitable long-term consumption.
In order to solve the above technical problems, the technical solution adopted in the present invention is:
A kind of preparation method of Wild jujube piece, comprises the following steps:
Step 1, drying and granulating:Wild jujube concentration magma is added into sweetener and is mixed into slurry, vacuum drying granulator is placed in and does Dry granulation;
Step 2, mixing:Obtained dry particle is placed in into three-dimensional mixer to mix;
Step 3, tabletting:Mixed particle is subjected to tabletting with rotary tablet machine.
Technical solution of the present invention further improvement is that:Wild jujube concentration magma is wild from market purchasing in step 1 Raw wild jujube concentrates magma, and Wild jujube concentration magma relative density is 1.10~1.15g/cm3, soluble solid content 27% ~30%.
Technical solution of the present invention further improvement is that:Wild jujube concentration magma, the mass ratio of sweetener in step 1 1:0.23~1:0.71;Sweetener is sucrose.
Technical solution of the present invention further improvement is that:Liquid cryogen belt vacuum drying and granulating machine is used in step 1 Group drying and granulating, vacuum is -0.08~-0.1Mpa, and 20~80 DEG C of temperature, obtained dry particle is 10~50 mesh, is dried Granule moisture level < 5.0%.
Technical solution of the present invention further improvement is that:Incorporation time is 15~30 minutes in step 2.
Technical solution of the present invention further improvement is that:Substrate piece weight in step 3 after tabletting is 0.1~3g/ pieces, weight It is ± 5%~± 7.5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture < 5.0% to measure difference.
Technical solution of the present invention further improvement is that:The compression mold that rotary tablet machine is used in step 3 is ellipse Circle, triangle, square, pentagon, olive shape xenotype mold.
Technical solution of the present invention further improvement is that:The Wild jujube piece soluble solid containing Wild jujube of preparation 27%~54%.
By adopting the above-described technical solution, the technological progress that the present invention is obtained is:
Wild jujube piece is a kind of candy type food rich in Vc, and present invention preparation is adopted Wild jujube concentration magma and mixed with sweetener Close drying and granulating technology stability by force, raw material uses the Wild jujube that pollution-free Wild jujube is processed through modern extraction process Magma is concentrated, mouthfeel is unique, and good taste more saves the nutritional ingredient and peculiar taste of Wild jujube, and product has Tranquilizing soporific, disappear it is tired go it is dry, reduce blood pressure, the health-care efficacy such as anti-inflammatory diuresis, can anti-aging, physical fitness, body beauty, beneficial people Body health.
The vacuum source of low temperature belt vacuum drying and granulating machine is Roots's water ring pump assembly, and heating source is 60~100 DEG C of hot water Or heating oil, the water of heating or the oily fixation heating plate interlayer entered by pipeline in low temperature belt vacuum drying and granulating machine drum body Circulated, conveyer belt is in close contact with heating plate makes it be heated and run, mixing slurry is by screw pump through distributing device in conveying Take uniform distribution and heating plate and carry out heat exchange, the heated rapid vaporization of mixing slurry moisture, by provided by refrigeration system- The vacuum condenser of 20 DEG C of freezing liquids cooling, volume, which reduces rapidly, is changed into liquid, forms high vacuum, vacuum can up to- 0.1Mpa, temperature can control to carry out low temperature drying at 20~80 DEG C.Dried medicinal extract is broken by the crushing system in cylinder It is broken into 10~50 mesh particles.
Low temperature belt vacuum drying and granulating machine drying temperature is relatively low, thus to mineral matter contained by Wild jujube piece and micro member The heat labile nutritional ingredient such as element and multivitamin does not constitute destruction, and can keep the original fragrance of material, is sufficiently reserved The effective nutritional ingredient of Wild jujube and biological natural activity.Wild jujube particle water content < 5% after drying and granulating, favorably Preserved for a long time in product, and the peculiar flavour of Wild jujube piece can be kept.
Link is mixed, Wild jujube particle nutritional ingredient content distribution during manufacture particle is uneven, passes through mixing Link, makes nutritional ingredient mixed distribution pockety in Wild jujube particle uniform, improves particle nutritional ingredient uniformity With the control of product quality of production process.
Three-dimensional mixer is employed herein, is Mixers with Multi-direction Movement, tempering tank is realized in X-Y-Z three dimensions Make multi-direction motion, in the running of three-dimensional mixer, because tempering tank has multi-direction motion, make material mixed During conjunction, flowing and diffusion are accelerated, while avoiding the machine of generally mixing with because of the material ratio produced by centrifugal action Segregation and accumulation phenomenon, mix high without dead angle, not stratified, well mixed and production efficiency again, simple to operate, will not also pollute Raw material, can effectively ensure the best in quality of mixed material, mixture homogeneity is up to 99%(Auger, V-type, two-dimensional mixing machine do not have There is this effect).
Substrate piece weight after compacting is 0.1~3g/ pieces, and weight differential is ± 5%~± 7.5%, and hardness >=3kg/ ㎝ 2 is crisp Broken degree≤1%, moisture < 5.0%.Wild jujube piece component:Soluble solid containing Wild jujube 27%~54%.Piece wicking surface light It is clean, no color differnece, mobility of particle is good in tableting processes, and substrate product appearance character and hardness meet candy type food quality mark Standard, category green, safety food.Carry convenient to take, in good taste, preparation technology is simple, and cost is low.The Wild jujube piece processed The effective nutritional ingredient of wild jujube and its biological natural activity, the Wild jujube piece flat appearance suppressed, technique can be sufficiently reserved Step is simple, process time is short, be easy to preserve.
The Wild jujube piece that the inventive method is obtained, the nutritional ingredient such as trace element, multivitamin is saved from damage preferably, green Health, instant, and water content is low, stability is good, and shelf lives are long;Easily sufficiently digested and assimilated comprehensively for human body, and And be easy to take, it is easy to carry.With antitoxic heart-soothing and sedative, the effect of sleep quality is improved, is organic, pollution-free food.
Wild jujube concentration magma be with drying Wild jujube or fresh Wild jujube broken skin, dipping, squeezing stoning, filtering, Concentrate the Wild jujube concentration magma processed.Wild jujube concentrates magma, merges modern crafts, extracts the essence of wild jujube fruit China, sour-sweet pleasant, body and mind in sweet flavor is naturally happy.The Wild jujube piece of the preparation taste of when containing change is sour-sweet, fruity is strong.
Embodiment
The present invention is described in further details with reference to embodiment:
Embodiment 1
A kind of preparation method of Wild jujube piece, the preparing raw material of Wild jujube piece is planted using Taihang the foot of a mountain genunie medicinal materials Rhamnaceae Thing Wild jujube (scientific name:Ziziphus jujuba Mill.var.spinosa (Bunge) Hu ex H.F.Chou) it is dry, The Wild jujube that fresh ripening fruits is processed through modern extraction process concentrates magma.Wild jujube concentration magma can be city Sell, can be oneself processing, as long as relative density and the parameter of soluble solid meet the requirements.Process is such as Under:
Step 1, drying and granulating:Wild jujube concentrates magma, and relative density is 1.10~1.15g/cm3, soluble solid 27%~30%;The mass ratio 1 that Wild jujube concentration magma, sucrose are added:0.23~1:0.71, it is mixed into slurry;Mixing slurry is adopted With liquid cryogen belt vacuum drying and granulating unit drying and granulating, vacuum is -0.08~-0.1Mpa, 20~80 DEG C of temperature, Obtained dry particle is 10~50 mesh, dry particle moisture < 5.0%.The Wild jujube concentration that the present embodiment is used is former Slurry, relative density is 1.15g/cm3, containing soluble solid 30%;Wild jujube concentration magma, sucrose mass ratio 1:0.71, It is mixed into slurry;Drying and granulating, vacuum -0.1Mpa, 40 DEG C of temperature, the obtained mesh of dry particle 20, dry particle moisture < 4.0%.
Step 2, mixing:Particle is placed in into three-dimensional mixer to mix, incorporation time is 15~30 minutes.The present embodiment is mixed Time is 30 minutes.
Step 3, tabletting:Mixed particle is subjected to tabletting, the pressure that rotary tablet machine is used with rotary tablet machine Die is ellipse, triangle, square, pentagon, olive shape xenotype mold.
Substrate piece weight after tabletting is 0.1~3g/ pieces, and weight differential is ± 5%~± 7.5%, and hardness >=3kg/ ㎝ 2 is crisp Broken degree≤1%, moisture < 5.0%, Wild jujube piece component:Soluble solid containing Wild jujube 27%~54%.The present embodiment piece Weight is 1g/ pieces, and weight differential is ± 5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture < 4.0%;Wild jujube piece component: Soluble solid containing Wild jujube 30%.
Embodiment 2
The present embodiment is distinguished as with embodiment 1:
Step 1, drying and granulating:The present embodiment is that Wild jujube concentrates magma, and relative density is 1.13 g/cm3, it is solid containing solubility Shape thing 29%;Wild jujube concentration magma, sucrose mass ratio 1:0.71, it is mixed into slurry;Drying and granulating, vacuum -0.09Mpa, temperature 50 DEG C, the mesh of particle 15, granule moisture level < 4.5%.
Step 2, mixing:The present embodiment incorporation time is 20 minutes.
Step 3, tabletting:The present embodiment piece weight is 0.5g/ pieces, and weight differential is ± 5%, hardness >=3kg/ ㎝ 2, friability The Wild jujube piece component of≤1%, moisture < 4.5%:Soluble solid containing Wild jujube 29%.
Embodiment 3
The present embodiment is distinguished as with embodiment 1:
Step 1, drying and granulating:The present embodiment is that Wild jujube concentrates magma, and relative density is 1.10 g/cm3, it is solid containing solubility Shape thing 28%;Wild jujube concentration magma, sucrose mass ratio 1:0.23, it is mixed into slurry;Drying and granulating, vacuum -0.08Mpa, temperature 60 DEG C, the mesh of particle 12, granule moisture level < 5.0%.
Step 2, mixing:The present embodiment incorporation time is 15 minutes.
Step 3, tabletting:The present embodiment piece weight is 0.25g/ pieces, and weight differential is ± 7.5%, hardness >=3kg/ ㎝ 2, friability Degree≤1%, moisture < 5.0%, Wild jujube piece component:Soluble solid containing Wild jujube 54%.
Embodiment 4
The present embodiment is distinguished as with embodiment 1:
Step 1, drying and granulating:The present embodiment is that Wild jujube concentrates magma, and relative density is 1.12 g/cm3, it is solid containing solubility Shape thing 27.8%;Wild jujube concentration magma, sucrose mass ratio 1:0.56, it is mixed into slurry;Drying and granulating, vacuum -0.09Mpa, temperature 56 DEG C of degree, the mesh of particle 23, granule moisture level < 4.9%.
Step 2, mixing:The present embodiment incorporation time is 23 minutes.
Step 3, tabletting:The present embodiment piece weight is 0.2g/ pieces, and weight differential is ± 7.5%, hardness >=3kg/ ㎝ 2, friability Degree≤1%, moisture < 5.0%, Wild jujube piece component:Soluble solid containing Wild jujube 34%.
Embodiment 5
The present embodiment is distinguished as with embodiment 1:
Step 1, drying and granulating:The present embodiment is that Wild jujube concentrates magma, and relative density is 1.14 g/cm3, it is solid containing solubility Shape thing 29.3%;Wild jujube concentration magma, sucrose mass ratio 1:0.66, it is mixed into slurry;Drying and granulating, vacuum -0.095Mpa, 75 DEG C of temperature, the mesh of particle 40, granule moisture level < 4.9%.
Step 2, mixing:The present embodiment incorporation time is 28 minutes.
Step 3, tabletting:The present embodiment piece weight is 0.2g/ pieces, and weight differential is ± 7.5%, hardness >=3kg/ ㎝ 2, friability Degree≤1%, moisture < 5.0%, Wild jujube piece component:Soluble solid containing Wild jujube 42%.

Claims (8)

1. a kind of preparation method of Wild jujube piece, it is characterised in that comprise the following steps:
Step 1, drying and granulating:Wild jujube concentration magma is added into sweetener and is mixed into slurry, vacuum drying granulator is placed in and does Dry granulation;
Step 2, mixing:Obtained dry particle is placed in into three-dimensional mixer to mix;
Step 3, tabletting:Mixed particle is subjected to tabletting with rotary tablet machine.
2. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:Wild jujube is concentrated in step 1 Magma concentrates magma from market purchasing Wild jujube, and Wild jujube concentration magma relative density is 1.10~1.15g/cm3, can Dissolubility solid content 27%~30%.
3. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:Wild jujube is concentrated in step 1 The mass ratio 1 of magma, sweetener:0.23~1:0.71;Sweetener is sucrose.
4. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:Liquid cryogen is used in step 1 Belt vacuum drying and granulating unit drying and granulating, vacuum is -0.08~-0.1Mpa, 20~80 DEG C of temperature, obtained drying Grain is 10~50 mesh, dry particle moisture < 5.0%.
5. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:Incorporation time is 15 in step 2 ~30 minutes.
6. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:Substrate in step 3 after tabletting Piece weight is 0.1~3g/ pieces, and weight differential is ± 5%~± 7.5%, hardness >=3kg/ ㎝ 2, friability≤1%, moisture < 5.0%.
7. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:Rotary tablet machine in step 3 The compression mold used is ellipse, triangle, square, pentagon, olive shape xenotype mold.
8. the preparation method of Wild jujube piece according to claim 1, it is characterised in that:The Wild jujube piece of preparation is containing open country Raw wild jujube soluble solid 27%~54%.
CN201710373801.6A 2017-05-24 2017-05-24 The preparation method of Wild jujube piece Pending CN107183592A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113080356A (en) * 2020-12-21 2021-07-09 罗玉琴 Preparation process of slurry-explosion tablet-type instant solid beverage

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1362034A (en) * 2001-11-30 2002-08-07 北京东方兴企食品工业技术有限公司 Production process of fruit and vegetable extract tablet food
CN104904978A (en) * 2015-05-22 2015-09-16 南京泽朗医药科技有限公司 A kiwi fruit candy tablet and a preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1362034A (en) * 2001-11-30 2002-08-07 北京东方兴企食品工业技术有限公司 Production process of fruit and vegetable extract tablet food
CN104904978A (en) * 2015-05-22 2015-09-16 南京泽朗医药科技有限公司 A kiwi fruit candy tablet and a preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张志红等: "植物原粉压片糖果品质影响因素的研究", 《食品与发酵科技》 *
李超 等: "《老年人饮食起居保健常识》", 28 February 2003, 金盾出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113080356A (en) * 2020-12-21 2021-07-09 罗玉琴 Preparation process of slurry-explosion tablet-type instant solid beverage

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Application publication date: 20170922

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