CN107208324B - 聚丙烯腈纤维的致密化 - Google Patents
聚丙烯腈纤维的致密化 Download PDFInfo
- Publication number
- CN107208324B CN107208324B CN201580071758.7A CN201580071758A CN107208324B CN 107208324 B CN107208324 B CN 107208324B CN 201580071758 A CN201580071758 A CN 201580071758A CN 107208324 B CN107208324 B CN 107208324B
- Authority
- CN
- China
- Prior art keywords
- bath
- fibers
- fiber
- temperature
- acrylic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
- D01F9/225—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles from stabilised polyacrylonitriles
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/06—Wet spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
- D01D5/14—Stretch-spinning methods with flowing liquid or gaseous stretching media, e.g. solution-blowing
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J1/00—Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
- D02J1/22—Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
- D02J1/223—Stretching in a liquid bath
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J1/00—Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
- D02J1/22—Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
- D02J1/228—Stretching in two or more steps, with or without intermediate steps
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J1/00—Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
- D02J1/22—Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
- D02J1/229—Relaxing
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/10—Inorganic fibres based on non-oxides other than metals
- D10B2101/12—Carbon; Pitch
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Fibers (AREA)
- Artificial Filaments (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201462097391P | 2014-12-29 | 2014-12-29 | |
| US62/097391 | 2014-12-29 | ||
| PCT/US2015/067639 WO2016109414A1 (en) | 2014-12-29 | 2015-12-28 | Densification of polyacrylonitrile fiber |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107208324A CN107208324A (zh) | 2017-09-26 |
| CN107208324B true CN107208324B (zh) | 2020-06-16 |
Family
ID=56163528
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201580071758.7A Active CN107208324B (zh) | 2014-12-29 | 2015-12-28 | 聚丙烯腈纤维的致密化 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10344403B2 (enExample) |
| EP (1) | EP3240920B1 (enExample) |
| JP (1) | JP6664401B2 (enExample) |
| KR (1) | KR102507899B1 (enExample) |
| CN (1) | CN107208324B (enExample) |
| ES (1) | ES2880376T3 (enExample) |
| WO (1) | WO2016109414A1 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112567082A (zh) * | 2018-06-06 | 2021-03-26 | 塞特工业公司 | 用于生产碳纤维的方法以及由其制造的碳纤维 |
| EP3856959A4 (en) * | 2018-09-26 | 2023-04-19 | Cytec Industries Inc. | Controlling the degree of swelling of polymer fibers during coagulation |
| US12258683B2 (en) * | 2019-05-02 | 2025-03-25 | Cytec Industries Inc. | Process for preparing carbon fibers from low polydispersity polyacrylonitrile |
| KR102674488B1 (ko) * | 2019-10-16 | 2024-06-14 | 주식회사 엘지화학 | 아크릴로니트릴계 섬유 전구체의 제조방법 |
| CN111282340A (zh) * | 2020-03-31 | 2020-06-16 | 无锡双象超纤材料股份有限公司 | 一种用于海岛纤维纺丝油剂的超滤装置 |
| KR20230152714A (ko) * | 2021-03-05 | 2023-11-03 | 사이텍 인더스트리스 인코포레이티드 | 중합체 섬유를 생성하기 위한 공정 및 그로부터 제조된 중합체 섬유 |
| US20230001618A1 (en) * | 2021-06-30 | 2023-01-05 | Connie Jackson | Carbon-fiber fuel tank |
| IT202100029576A1 (it) * | 2021-11-23 | 2023-05-23 | Montefibre Mae Tech S R L | Processo di produzione di fibre acriliche ad alta velocità e relativo apparato |
| CN115182077B (zh) * | 2022-07-28 | 2024-05-24 | 中国科学院苏州纳米技术与纳米仿生研究所 | 高稳定性碳纳米管纤维连续强化装置、系统及其应用 |
| CN115559005B (zh) * | 2022-09-27 | 2024-05-07 | 温州佳远生物科技有限公司 | 一种壳聚糖纤维一步法纺丝装置 |
| CN115874295B (zh) * | 2022-12-01 | 2025-07-01 | 山西钢科碳材料有限公司 | 碳纤维原丝喷丝组件及干喷湿纺制备碳纤维原丝的方法 |
| CN116334777B (zh) * | 2023-05-26 | 2023-07-21 | 吉林富博纤维研究院有限公司 | 一种水浴牵伸装置及pan基碳纤维原丝的生产系统 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5439495B2 (enExample) | 1972-10-11 | 1979-11-28 | ||
| JPS6042286B2 (ja) * | 1982-06-09 | 1985-09-21 | 東レ株式会社 | 炭素繊維前駆体の製造方法 |
| CN1007740B (zh) * | 1985-04-30 | 1990-04-25 | 吉林化学工业公司研究院 | 碳纤维用多元组分聚丙烯腈原丝 |
| TW459075B (en) * | 1996-05-24 | 2001-10-11 | Toray Ind Co Ltd | Carbon fiber, acrylic fiber and preparation thereof |
| ES2252953T3 (es) | 1998-07-22 | 2006-05-16 | Mitsubishi Rayon Co., Ltd. | Fibra precursora a base de acrilonitrilo para fibra de carbono y procedimiento para preparar la misma. |
| HU227286B1 (en) | 2000-06-23 | 2011-01-28 | Mitsubishi Rayon Co | Carbon fiber precursor fiber bundle and process for making it |
| JP2002080280A (ja) | 2000-06-23 | 2002-03-19 | Sumitomo Electric Ind Ltd | 高熱伝導性複合材料及びその製造方法 |
| DE602005022281D1 (de) | 2004-02-13 | 2010-08-26 | Mitsubishi Rayon Co | Carbonfaservorgängerfaserbündel, produktionsverfahren und produktions-vorrichtung dafür sowie carbonfaser und produktionsverfahren dafür |
| US7749479B2 (en) | 2006-11-22 | 2010-07-06 | Hexcel Corporation | Carbon fibers having improved strength and modulus and an associated method and apparatus for preparing same |
| JP2008308776A (ja) * | 2007-06-13 | 2008-12-25 | Toray Ind Inc | ポリアクリロニトリル系前駆体繊維の製造方法、炭素繊維の製造方法、および炭素繊維 |
| ES2389832T3 (es) | 2007-12-30 | 2012-11-02 | Toho Tenax Co., Ltd. | Procedimiento de producción de fibras ignífugas y fibra de carbono |
| US8372323B2 (en) | 2009-09-10 | 2013-02-12 | International Fibers, Ltd. | Process of making polyacrylonitrile fibers |
| JP5708965B2 (ja) * | 2009-06-10 | 2015-04-30 | 三菱レイヨン株式会社 | アクリロニトリル系前駆体繊維束および炭素繊維束の製造方法 |
| US20120088104A1 (en) * | 2009-06-10 | 2012-04-12 | Mitsubishi Rayon Co., Ltd. | Acrylonitrile swollen fiber for carbon fiber, precursor fiber bundle, stabilized fiber bundle, carbon fiber bundle and production methods thereof |
| CN102459728B (zh) * | 2009-06-10 | 2013-09-18 | 三菱丽阳株式会社 | 机械性能表现优异的碳纤维束 |
| CN102766989B (zh) * | 2012-07-25 | 2014-12-10 | 北京化工大学 | 一种具有中模量的高强度聚丙烯腈基碳纤维及其制备方法 |
-
2015
- 2015-12-28 CN CN201580071758.7A patent/CN107208324B/zh active Active
- 2015-12-28 EP EP15837124.5A patent/EP3240920B1/en active Active
- 2015-12-28 ES ES15837124T patent/ES2880376T3/es active Active
- 2015-12-28 WO PCT/US2015/067639 patent/WO2016109414A1/en not_active Ceased
- 2015-12-28 US US14/980,547 patent/US10344403B2/en active Active
- 2015-12-28 KR KR1020177021190A patent/KR102507899B1/ko active Active
- 2015-12-28 JP JP2017534649A patent/JP6664401B2/ja active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US10344403B2 (en) | 2019-07-09 |
| ES2880376T3 (es) | 2021-11-24 |
| JP6664401B2 (ja) | 2020-03-13 |
| US20160186365A1 (en) | 2016-06-30 |
| KR20170105026A (ko) | 2017-09-18 |
| EP3240920B1 (en) | 2021-04-21 |
| CN107208324A (zh) | 2017-09-26 |
| KR102507899B1 (ko) | 2023-03-07 |
| WO2016109414A1 (en) | 2016-07-07 |
| JP2018500480A (ja) | 2018-01-11 |
| EP3240920A1 (en) | 2017-11-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107208324B (zh) | 聚丙烯腈纤维的致密化 | |
| US10647844B2 (en) | Polyacrylonitrile (PAN) polymers with low polydispersity index (PDI) and carbon fibers made therefrom | |
| JP7225173B2 (ja) | 中間弾性率炭素繊維の製造 | |
| US12129575B2 (en) | Controlling the degree of swelling of polymer fibers during coagulation |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |