CN107125533A - A kind of preparation method of Xuancheng's pawpaw effervescent tablet - Google Patents
A kind of preparation method of Xuancheng's pawpaw effervescent tablet Download PDFInfo
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- CN107125533A CN107125533A CN201710434264.1A CN201710434264A CN107125533A CN 107125533 A CN107125533 A CN 107125533A CN 201710434264 A CN201710434264 A CN 201710434264A CN 107125533 A CN107125533 A CN 107125533A
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- xuancheng
- pawpaw
- effervescent tablet
- extract
- preparation
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- 235000009467 Carica papaya Nutrition 0.000 title claims abstract description 43
- 235000006264 Asimina triloba Nutrition 0.000 title claims abstract description 40
- 239000007938 effervescent tablet Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 244000189799 Asimina triloba Species 0.000 title abstract 4
- 229940000492 pawpaw extract Drugs 0.000 claims abstract description 33
- 239000000843 powder Substances 0.000 claims abstract description 19
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 13
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 11
- 239000003765 sweetening agent Substances 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 8
- 150000007524 organic acids Chemical class 0.000 claims abstract description 6
- 238000011017 operating method Methods 0.000 claims abstract description 3
- 240000006432 Carica papaya Species 0.000 claims description 36
- 239000003795 chemical substances by application Substances 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 11
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 claims description 8
- ZTOJFFHGPLIVKC-YAFCTCPESA-N (2e)-3-ethyl-2-[(z)-(3-ethyl-6-sulfo-1,3-benzothiazol-2-ylidene)hydrazinylidene]-1,3-benzothiazole-6-sulfonic acid Chemical compound S\1C2=CC(S(O)(=O)=O)=CC=C2N(CC)C/1=N/N=C1/SC2=CC(S(O)(=O)=O)=CC=C2N1CC ZTOJFFHGPLIVKC-YAFCTCPESA-N 0.000 claims description 8
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 claims description 8
- 235000005487 catechin Nutrition 0.000 claims description 8
- 229950001002 cianidanol Drugs 0.000 claims description 8
- 230000007760 free radical scavenging Effects 0.000 claims description 8
- 229930006000 Sucrose Natural products 0.000 claims description 6
- 239000005720 sucrose Substances 0.000 claims description 6
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 5
- 235000013824 polyphenols Nutrition 0.000 claims description 5
- 229920001282 polysaccharide Polymers 0.000 claims description 5
- 239000005017 polysaccharide Substances 0.000 claims description 5
- 150000004804 polysaccharides Chemical class 0.000 claims description 5
- 230000000694 effects Effects 0.000 claims description 4
- 235000021552 granulated sugar Nutrition 0.000 claims description 4
- 235000010447 xylitol Nutrition 0.000 claims description 4
- 241000219173 Carica Species 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 3
- 230000003064 anti-oxidating effect Effects 0.000 claims description 3
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000000811 xylitol Substances 0.000 claims description 3
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 3
- 229960002675 xylitol Drugs 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 238000005057 refrigeration Methods 0.000 claims description 2
- 125000000185 sucrose group Chemical group 0.000 claims description 2
- 229920001221 xylan Polymers 0.000 claims description 2
- 150000004823 xylans Chemical class 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 235000015424 sodium Nutrition 0.000 claims 1
- 239000012153 distilled water Substances 0.000 abstract description 6
- 239000000654 additive Substances 0.000 abstract description 4
- 230000000996 additive effect Effects 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 235000013399 edible fruits Nutrition 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract description 2
- 229920000858 Cyclodextrin Polymers 0.000 abstract 1
- 239000001116 FEMA 4028 Substances 0.000 abstract 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 abstract 1
- 229960004853 betadex Drugs 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 238000009777 vacuum freeze-drying Methods 0.000 abstract 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 10
- 239000002253 acid Substances 0.000 description 9
- 239000000853 adhesive Substances 0.000 description 5
- 230000001070 adhesive effect Effects 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 229920001353 Dextrin Polymers 0.000 description 4
- 239000004375 Dextrin Substances 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 235000019425 dextrin Nutrition 0.000 description 4
- 239000000314 lubricant Substances 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 229920001503 Glucan Polymers 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- 241001507936 Chaenomeles Species 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 240000005250 Chrysanthemum indicum Species 0.000 description 1
- 244000086443 Craterellus fallax Species 0.000 description 1
- 235000007926 Craterellus fallax Nutrition 0.000 description 1
- 241000736199 Paeonia Species 0.000 description 1
- 235000006484 Paeonia officinalis Nutrition 0.000 description 1
- 240000005001 Paeonia suffruticosa Species 0.000 description 1
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/40—Effervescence-generating compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Molecular Biology (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of preparation method of Xuancheng's pawpaw effervescent tablet.Operating procedure is as follows:In mass ratio by Xuancheng's pawpaw extract medicinal extract and beta cyclodextrin, add distilled water and be well mixed, Xuancheng's pawpaw extract powder is obtained after vacuum freeze drying;Xuancheng's pawpaw extract powder is mixed with sodium acid carbonate, sweetener etc. by a certain percentage, tabletting produces Xuancheng's pawpaw effervescent tablet.The characteristics of present invention is using Xuancheng's pawpaw fruit chemical composition organic acid and abundant polyoses content, reduces the use of additive in effervescent tablet, and the security and acceptable degree of effervescent tablet are improved while reducing production cost.
Description
Technical field
The present invention relates to field of food, the few effervescent tablet of more particularly to a kind of additive level.
Background technology
Xuancheng's pawpaw, is the peculiar Chaenomeles Cultivars of Xuancheng City of Anhui Province, is the food and medicament dual-purpose Chinese medicine for having higher-value, with tribute
Chrysanthemum, Bo Chinese herbaceous peony, root bark of tree peony nominal are the big authentic medicinal herbs in Anhui four, the title for having " hundred benefits fruit ".Xuancheng's pawpaw is because containing having compared with horn of plenty
Machine acid, tannin, make its sour-puckery flavor and are used for medicinal purpose more.However, Xuancheng's pawpaw extract is by appropriate regulation, can be by sour and astringent mouth
Sensing control system is in the acceptable scope of consumer.The polysaccharide and organic acid isoreactivity composition enriched in Xuancheng's pawpaw extract, is adapted to
The exploitation of effervescent tablet.At present, the effervescent tablet of in the market circulation is containing lubricant, adhesive, effervescent agent acid source and alkali source, sweet taste
The substantial amounts of food additives such as agent.Therefore, easily there are security concerns in consumer before purchase.
The content of the invention
The present invention combines the characteristics of Xuancheng's pawpaw organic acid, polysaccharide isoreactivity component content are abundant, and food is carried out to Xuancheng's pawpaw
Exploitation, the use of food additive in manufacturing process is reduced using Xuancheng's pawpaw active component feature.The present invention provide it is a kind of with
Xuancheng's pawpaw is the preparation method of the effervescent tablet of main body.
The operating procedure of effervescent tablet of the preparation based on Xuancheng's pawpaw is as follows:
(1)Take Xuancheng's pawpaw extract medicinal extract and beta-schardinger dextrin in mass ratio 1:0.5-1:11, it is mixed with water;Vacuum refrigeration is done
It is dry, pulverize, obtain Xuancheng's pawpaw extract powder;Xuancheng's pawpaw extract medicinal extract is what Xuancheng's pawpaw was obtained through 70% alcohol steep
Xuancheng's pawpaw extract medicinal extract, pH value is 2.0~2.7, includes organic acid, polysaccharide, polyphenol active component;
(2)By Xuancheng's pawpaw extract powder and sodium acid carbonate in mass ratio 1:0.2-1:1.2 ground and mixeds are uniform, obtain effervesce
Agent;
(3)Sweetener was pulverized 80 mesh sieves, by effervescent agent and sweetener in mass ratio by 1:0.5-1:1.5 mixing are equal
Even, Xuancheng's pawpaw effervescent tablet is made in tabletting;The Xuancheng's pawpaw effervescent tablet content is only containing Xuancheng's pawpaw extract medicinal extract, β-ring paste
Essence, sweetener and sodium acid carbonate.
The monolithic quality of the Xuancheng's pawpaw effervescent tablet is 0.2 g, and polyphenol content is equivalent to catechin 3.81-22.9 mg, profit
The antioxidation activity of effervescent tablet is surveyed with ABTS methods, when free radical scavenging activity is 50%, the polyphenoils phase that inside is contained
Added when in Vc 0.13-0.75 mg, not containing the food such as adhesive, effervescent agent acid source and lubricant compared with other effervescent tablets
Agent.
The technical scheme further limited is as follows:
Step(1)In, take Xuancheng's pawpaw extract medicinal extract and beta-schardinger dextrin in mass ratio 1:0.5-1:11, it is mixed with water, obtains
To Xuancheng's pawpaw extract powder.
Step(1)In, Xuancheng's pawpaw extract powder crosses 80 mesh sieves.
Step(2)In, by Xuancheng's pawpaw extract powder and sodium acid carbonate in mass ratio 1:0.2-1:1.2 ground and mixeds are equal
It is even, obtain effervescent agent.
Step(2)In, by ground 80 mesh sieve of sodium acid carbonate.
Step(3)In, the sweetener is sucrose or white granulated sugar or xylan or xylitol.
Step(3)In, it is 1 in mass ratio by effervescent agent and sweetener:0.5-1:1.5.
The advantageous effects of the present invention embody in the following areas:
1. make papaya extractives that there is good moisture-absorption characteristics and larger viscosity rich in there is abundant polysaccharide in Xuancheng's pawpaw.Cause
This, step of the present invention(1)Middle use beta-schardinger dextrin is prepared after being mixed with Xuancheng's pawpaw extract, can effectively be reduced pawpaw and be carried
The moisture-absorption characteristics of thing is taken, Xuancheng's pawpaw is kept pulverulence, it is prevented from caking and dry rapid, while also retains appropriate suction
Wet, adhesive power, makes effervescent tablet to complete nothing in tableting processes, and tableting processes without addition adhesive and lubricant in addition
Sticking phenomenon, tabletting shows that smooth and hardness is good, and the disintegration time of tabletting meets national standard.
2. step of the present invention(2)Rich in abundant organic acid, including citric acid, malic acid, winestone in middle utilization Xuancheng's pawpaw
The active ingredient such as acid and ascorbic acid, acidity reaches as high as pH 2.5 or so.Using this characteristic, effervescent agent acid source can be removed from
Addition, only add effervescent agent alkali source can complete the making of effervescent agent, reduce the addition of additive acid source.
3. the obtained effervescent tablet monolithic quality of the present invention is 0.2 g, polyphenol content is equivalent to catechin 3.81-22.90
Mg, the antioxidation activity of effervescent tablet is surveyed using ABTS methods, when free radical scavenging activity is 50%, the polyphenoils that inside is contained
Matter is equivalent to Vc 0.13-0.75 mg.Effervescent tablet made from the inventive method compared with other effervescent tablets, do not contain lubricant,
Adhesive, it is not necessary to use effervescent agent acid source.The reduction of additive, improves foodsafety, while reducing food production
The production cost of enterprise.
Embodiment
With reference to embodiment, the present invention is further described.
Embodiment 1
(1)Take 10 g Xuancheng's pawpaw extract medicinal extract and 20 g beta-schardinger dextrins(The mass ratio of the two is 1:2), add 300 mL and steam
Distilled water is well mixed;- 20 DEG C of h of pre-freeze 12, are less than 100 Pa in vacuum, and condenser temperature is less than under the conditions of -50 DEG C, and vacuum is cold
Freeze dry 36 h;Pulverized 80 mesh sieves, and obtained Xuancheng's pawpaw extract powder;
(2)By ground 80 mesh sieve of sodium acid carbonate, take 12 g sodium acid carbonates and 10 g Xuancheng's pawpaws extract powders well mixed(Two
The mass ratio 1 of person:0.8), effervescent agent is made;
(3)80 mesh sieves are crossed after sucrose is ground, 12.5 g sucrose are added in 10 g effervescent agents and are well mixed(The mass ratio of the two
For 1:1.25), tabletting produces Xuancheng's pawpaw effervescent tablet.The quality of monolithic be 0.2g, through Forint phenol method determine total phenol content equivalent to
The mg of catechin 22.9, when to ABTS free radical scavenging activities are 50% when, the polyphenoils that contains of inside is equivalent to Vc 0.75
mg。
Embodiment 2
(1)Take 10 g Xuancheng's pawpaw extract medicinal extract and 20 g beta-schardinger dextrins(The mass ratio of the two is 1:2), add 300 mL and steam
Distilled water is well mixed;- 20 DEG C of h of pre-freeze 12, are less than 100 Pa in vacuum, and condenser temperature is less than under the conditions of -50 DEG C, and vacuum is cold
Freeze dry 36 h;Pulverized 80 mesh sieves, and obtained Xuancheng's pawpaw extract powder;
(2)By ground 80 mesh sieve of sodium acid carbonate, take 25 g sodium acid carbonates and 10 g Xuancheng's pawpaws extract powders well mixed(Two
The mass ratio 1 of person:0.4), effervescent agent is made;
(3)80 mesh sieves are crossed after glucan is ground, 5 g glucans are added in 10 g effervescent agents and are well mixed(The quality of the two
Than for 1:0.5), tabletting produces Xuancheng's pawpaw effervescent tablet.
The quality of monolithic is 0.2 g, total phenol content is determined equivalent to the mg of catechin 15.26 through Forint phenol method, when to ABTS
When free radical scavenging activity is 50%, the polyphenoils that inside is contained is equivalent to the mg of Vc 0.5.
Embodiment 3
(1)Taking 10 g Xuancheng's pawpaw extract medicinal extract and 20 g beta-schardinger dextrins, (mass ratio of the two is 1:2), 300 mL are added to steam
Distilled water is well mixed;- 20 DEG C of h of pre-freeze 12, are less than 100 Pa in vacuum, and condenser temperature is less than under the conditions of -50 DEG C, and vacuum is cold
Freeze dry 36 h;Pulverized 80 mesh sieves, and obtained Xuancheng's pawpaw extract powder;
(2)By ground 80 mesh sieve of sodium acid carbonate, take 16.6 g and 10 g Xuancheng's pawpaws extract powders well mixed(The two
Mass ratio is 1:0.6), effervescent agent is made;
(3)80 mesh sieves are crossed after white granulated sugar is ground, 7.5g white granulated sugars are added in 10 g effervescent agents and are well mixed(The quality of the two
Than for 1:0.75), tabletting produces Xuancheng's pawpaw effervescent tablet.
The quality of monolithic is 0.2 g, total phenol content is determined equivalent to the mg of catechin 10.94 through Forint phenol method, when right
When ABTS free radical scavenging activities are 50%, the polyphenoils that inside is contained is equivalent to the mg of Vc 0.35.
Embodiment 4
(1)Take 10 g Xuancheng's pawpaw extract medicinal extract and 20 g beta-schardinger dextrin(The mass ratio of the two is 1:2), add 300 mL and steam
Distilled water is well mixed;- 20 DEG C of h of pre-freeze 12, are less than 100 Pa in vacuum, and condenser temperature is less than under the conditions of -50 DEG C, and vacuum is cold
Freeze dry 36 h;Pulverized 80 mesh sieves, and obtained Xuancheng's pawpaw extract powder;
(2)By ground 80 mesh sieve of sodium acid carbonate, take 10 g and 10 g Xuancheng's pawpaws extract powders well mixed(The quality of the two
Than for 1:1), effervescent agent is made;
(3)80 mesh sieves are crossed after xylitol is ground, 12.5 g xylitols are added in 10 g effervescent agents and are well mixed(The matter of the two
Amount is than being 1:1.25)Tabletting, produces Xuancheng's pawpaw effervescent tablet.
The quality of monolithic is 0.2 g, total phenol content is determined equivalent to the mg of catechin 22.6 through Forint phenol method, when to ABTS
When free radical scavenging activity is 50%, the polyphenoils that inside is contained is equivalent to the mg of Vc 0.70.
Embodiment 5
(1)Take 10 g Xuancheng's pawpaw extract medicinal extract and 110 g beta-schardinger dextrins(The mass ratio of the two is 1:11), add 1000 mL
Distilled water is well mixed;- 20 DEG C of h of pre-freeze 12, are less than 100 Pa in vacuum, and condenser temperature is less than under the conditions of -50 DEG C, vacuum
It is freeze-dried 36 h;Pulverized 80 mesh sieves, and obtained Xuancheng's pawpaw extract powder;
(2)By ground 80 mesh sieve of sodium acid carbonate, take 12 g with and 10 g Xuancheng's pawpaw extract powders be well mixed(The matter of the two
Amount is than being 1:0.8), effervescent agent is made;
(3)80 mesh sieves are crossed after sucrose is ground, 15 g sucrose are added in 10 g effervescent agents and are well mixed(The mass ratio of the two is
1:1.5), tabletting produces Xuancheng's pawpaw effervescent tablet.
The quality of monolithic is 0.2 g, total phenol content is determined equivalent to the mg of catechin 3.81 through Forint phenol method, when to ABTS
When free radical scavenging activity is 50%, the polyphenoils that inside is contained is equivalent to the mg of Vc 0.13.
Claims (7)
1. a kind of preparation method of Xuancheng's pawpaw effervescent tablet, it is characterised in that operating procedure is as follows:
(1)Take Xuancheng's pawpaw extract medicinal extract and beta-schardinger dextrin in mass ratio 1:0.5-1:20, it is mixed with water;Vacuum refrigeration is done
It is dry, pulverize, obtain Xuancheng's pawpaw extract powder;Xuancheng's pawpaw extract medicinal extract is what Xuancheng's pawpaw was obtained through 70% alcohol steep
Xuancheng's pawpaw extract medicinal extract, pH value is 2.0~2.7, includes organic acid, polysaccharide, polyphenol active component;
(2)By Xuancheng's pawpaw extract powder and sodium acid carbonate in mass ratio 1:0.1-1:1.5 ground and mixeds are uniform, obtain effervesce
Agent;
(3)Sweetener is pulverized, by effervescent agent and sweetener in mass ratio by 1:0.2-1:2.0 are well mixed, tabletting, system
Obtain Xuancheng's pawpaw effervescent tablet;The Xuancheng's pawpaw effervescent tablet content only containing Xuancheng's pawpaw extract medicinal extract, beta-schardinger dextrin, sweetener and
Sodium acid carbonate;
The monolithic quality of the Xuancheng's pawpaw effervescent tablet is 0.2 g, and polyphenol content is utilized equivalent to catechin 3.81-22.9 mg
ABTS methods survey the antioxidation activity of effervescent tablet, and when free radical scavenging activity is 50%, the polyphenoils that inside is contained is suitable
In Vc 0.13-0.75 mg.
2. a kind of preparation method of Xuancheng's pawpaw effervescent tablet according to claim 1, it is characterised in that:Step(1)In, take a surname
Papaya extractives medicinal extract and beta-schardinger dextrin in mass ratio 1:0.5-1:11, it is mixed with water.
3. a kind of preparation method of Xuancheng's pawpaw effervescent tablet according to claim 1, it is characterised in that:Step(2)In, it will declare
Papaya extractives pulvis and sodium acid carbonate in mass ratio 1:0.2-1:1.2 ground and mixeds are uniform, obtain effervescent agent.
4. a kind of preparation method of Xuancheng's pawpaw effervescent tablet according to claim 1, it is characterised in that:Step(2)In, effervesce
80 mesh sieves are crossed in agent.
5. a kind of preparation method of Xuancheng's pawpaw effervescent tablet according to claim 1, it is characterised in that:Step(2)In, by carbon
Sour ground 80 mesh sieve of hydrogen sodium.
6. a kind of preparation method of Xuancheng's pawpaw effervescent tablet according to claim 1, it is characterised in that:Step(3)In, it is described
Sweetener is sucrose or white granulated sugar or xylan or xylitol.
7. a kind of preparation method of Xuancheng's pawpaw effervescent tablet according to claim 1, it is characterised in that:Step(3)In, it will steep
It is 1 in mass ratio with sweetener to rise agent:0.5-1:1.5.
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