CN107094811A - A kind of saliferous sterilization effervescent tablet used for aquiculture and preparation method thereof - Google Patents
A kind of saliferous sterilization effervescent tablet used for aquiculture and preparation method thereof Download PDFInfo
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- CN107094811A CN107094811A CN201710401087.7A CN201710401087A CN107094811A CN 107094811 A CN107094811 A CN 107094811A CN 201710401087 A CN201710401087 A CN 201710401087A CN 107094811 A CN107094811 A CN 107094811A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/34—Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/50—1,3-Diazoles; Hydrogenated 1,3-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/08—Alkali metal chlorides; Alkaline earth metal chlorides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
Abstract
The present invention relates to aquaculture field, a kind of saliferous sterilization effervescent tablet used for aquiculture and preparation method thereof is disclosed, is characterized in that：Using sodium chloride, sodium sulphate, quaternary ammonium salt, garlic powder, adhesive, effervescent agent, disintegrant, lubricant as main component, cultivation sterilization effervescent tablet is prepared by techniques such as inclusion, mixing, whole grain and tablettings.Effervescent tablet prepared by the technology is because the excellent efficiency of compound quaternary ammonium salt therein is high, sterilizing ability is strong, the pH value scope of application is wide and small toxicity, garlic can improve the premunition of animal body, strengthen its immunity, the features such as also there is bactericidal effect simultaneously, with the synergy of salt, it can also increase dissolved oxygen in water as sterilization, sterilization and insecticide in aquaculture, there is diseases prevention, aspect of curing the disease to have remarkable result to aquatic products.Product of the present invention is easy to use, stably, safety, environmental protection.
Description
Technical field
Concretely it is a kind of saliferous sterilization effervescent tablet used for aquiculture and its system the present invention relates to aquaculture field
Preparation Method.
Background technology
In aquaculture process, aquatic economic animal usually can be quick-fried by the infringement of bacterium, fungi, virus and protozoon
Disease is sent out, and propagates that general cultivation density is larger artificially, the bait of dispensing and the excreta of aquatic economic animal etc. is added, often
Cause water body environment to deteriorate, influence growth of animal.Water sterilization sterilization is the guarantee of aquaculture health and safety, is also cultivation
One of key technology of water process.Current water body disinfection method both domestic and external mainly has ozonization, disinfection by ultraviolet light, chemical drugs
Product are sterilized, and the order of above-mentioned several sterilization methods is used and is used in combination.The principle of these water body disinfection methods is different, makes
With effect, there is also very big difference.Quaternary ammonium salt bactericide has good kill to microorganisms such as bacterium, fungi, algae and viruses
Bacterium effect, simultaneously because sterilization speed is fast, excitant is small, will not cause allergic reaction, and lower-price characteristic, and in crowd
It is multi-field to be used widely, including culture fishery.But there is also resistance problem, dissipation is influenceed to a certain extent
The development of class quaternary ammonium salt, also limits its application field.
Existing aquatic products sterilization is more to carry out sterilizing using Organic Ingredients such as the Chinese bulbul, perilla leaf, giant knotweeds, but these have
Machine raw material does not carry out extracts active ingredients, in order to ensure that bactericidal effect generally requires to add more Organic Ingredients, although kill
Bacterium in water, but will also result in water eutrophication words.
Existing patent of invention (application number 200510089903.2) discloses a kind of solid quaternary ammonium salts compounding sterilizing deodoriferant
And preparation method, include the composition of the quaternary ammonium salt such as benzethonium chloride, benzene rope bromine ammonium；Publication No. CN102302039A (application numbers
2011101619617) Chinese patent literature discloses a kind of dication quaternary ammonium salt complexing iodine disinfectant；Publication No.
CN101161070 (application number 2006101226956) Chinese patent literature discloses a kind of compound adjacent benzene two of double-chain quaternary ammonium salt
Formaldehyde disinfectant.These methods have used the disinfectant with quaternary ammonium salt and its compound composition, and disinfection is with composition quaternary ammonium salt
Based on, it is relatively single.In aquaculture process, salt for sterilization, bactericidal action gained public acceptance, by salt, new season
The bag that effervescent tablet prepared by ammonium salt and garlic powder combination has safety, disinfection obvious, easy to use rises piece.
New quaternary ammonium salt is used in inventive formulation, such quaternary ammonium salt has strong antibacterial, safety feature；Salt and season
Ammonium salt combination has obvious antibacterial concertedness；The premunition of animal body can be improved using garlic powder simultaneously, strengthens it
The characteristics of immunity；Develop excellent, the safe sterilization effervescent tablet of anti-microbial property.
The content of the invention
The present invention by Organic Ingredients carries out aquatic products sterilization to there is bactericidal effect undesirable for existing, easily causes water body
It is excellent that the problem of eutrophication, prepares a kind of anti-microbial property there is provided a kind of Synergistic antimicrobial ability for making full use of salt and new quaternary ammonium salt
Different, safe sterilization effervescent tablet.
The present invention solves above-mentioned technical problem, and the technical scheme of use is, a kind of saliferous sterilization effervescent tablet used for aquiculture
Include following raw material, 25~35 parts of sodium chloride, 5~10 parts of quaternary ammonium salt, 2~5 parts of garlic powder, 5~10 parts of adhesive, bubble
Rise 35~50 parts of agent, 10~15 parts of sodium sulphate, 1~3 part of lubricant.
Further, comprising following raw material, 28~32 parts of sodium chloride, 6~9 parts of quaternary ammonium salt, 3~4 parts of garlic powder,
6~8 parts of adhesive, 38~44 parts of effervescent agent, 11~14 parts of sodium sulphate, 1~3 part of lubricant.
Further, comprising following raw material, 30 parts of sodium chloride, 8 parts of quaternary ammonium salt, 3 parts of garlic powder, 7 parts of adhesive,
42 parts of effervescent agent, 13 parts of sodium sulphate, 2 parts of lubricant.
Optionally, quaternary ammonium salt is dodecyl dimethyl benzyl ammonium bromide, bialkyl methyl ethoxyl ammonium bromide, 2- (2-
Ethoxy)-methyl-(1- methyl-imidazoles -2- methylene) ammonium chloride, one kind in the double ammonium chlorides of alkyl benzyl ether.
Optionally, adhesive is one in polyvinyl alcohol, copolyvidone, polyvinylpyrrolidone, sodium carboxymethylcellulose
Kind.
Optionally, effervescent agent is made up of acid source and carbon dioxide source, acid source be oxalic acid, adipic acid, butanedioic acid, glutaric acid,
One kind in aminotriacetic acid, carbon dioxide source is one kind in sodium carbonate, sodium acid carbonate, SODIUM PERCARBONATE；Acid source and titanium dioxide
Carbon source weight ratio is 1:1.3~3:4.1.
Optionally, lubricant is magnesium stearate and one kind in talcum powder.
In order to solve the above-mentioned technical problem the present invention, additionally provides a kind of saliferous sterilization effervescent tablet preparation side used for aquiculture
Method, is comprised the steps of：
The first step, weighs sodium chloride, quaternary ammonium salt, garlic powder, effervescent agent acid source, the sodium sulphate of parts by weight, is well mixed, system
Obtain mixture；
Second step, mixture is ground, and by screen cloth, powder is made；
3rd step, adds effervescent agent carbon dioxide source, binder and the lubricant of parts by weight in powder, and mixing is equal
It is even, dry, tabletting, sterilization effervescent tablet is made.
Further, in second step, screen cloth is 20~40 mesh.
The beneficial effect of the inventive method at least includes one below,
1st, saliferous sterilization effervescent tablet used for aquiculture prepared by the present invention, make use of new quaternary ammonium salt, garlic and salt
Synergistic antimicrobial ability, at the same have its sterilizing ability of Synergistic biocidal effect be substantially better than single salt, quaternary ammonium salt and salt with
Quat compositions.
2nd, the new quaternary ammonium salt safety that is used in product, consumption are low.
3rd, product prepares simple, easy to use.
4th, product is used for thin in Cytophaga Columnaris, Aeromonas hydrophila, Vibrio anguillarum in aquaculture etc. and cultivation water
The sterilizing ability test of bacterium, shows bactericidal effect more preferable than positive control.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments to the present invention
It is described in further detail.It should be appreciated that specific embodiment described herein is used only for explaining the present invention, limit is not used to
The fixed present invention.
Embodiment 1
(1) 5g dodecyl dimethyl benzyl ammonium bromides, 2g garlic powders, 15g oxalic acid, 35g sodium chloride, 10g sulfuric acid are weighed
Sodium is well mixed；
(2) particle crosses 20 mesh sieves, and powder is made；
(3) 20g sodium carbonate, 1g talcum powder and 5g polyvinyl alcohol are added in the powder of step (2), mixed, tabletting,
Sterilization effervescent tablet is made.
(4) the sterilization effervescent tablet for preparing step (3) includes Cytophaga Columnaris, thermophilic aqueous vapor list to Common Fish
Antibacterial ability in born of the same parents bacterium, Vibrio anguillarum and cultivation water is tested, and is carried out according to the following steps：
1. the measure of minimum bactericidal concentration：The sterilization effervescent tablet of preparation is prepared into 1000-0.25mg/ with sterilizing double distilled water
L 13 concentration, dilute 10 times by each strength solution with FWA culture mediums, fill in the test tube of 2.9mL culture mediums and add to every pipe
0.1mL concentration is 107Cfu/mL living bacterial liquids, under the conditions of 25 DEG C, after cultivating 5 days, observation is confirmed in asepsis growth test tube respectively
0.1mL culture mediums are sucked, is inoculated in bouillon agar plate, under the conditions of 25 DEG C, is further cultured for 5 days, it is sterile in agar plate to occur
Corresponding test tube in minimum effervescent tablet concentration, i.e. minimum bactericidal concentration of the effervescent tablet to bacterium.
2. sterilization effect of the effervescent tablet in cultivation water：The triangular glass flask of 300mL sterilizing pond reclaimed waters will be filled, respectively
It is about 10 to adding 3.0mL bacteria concentrations in each flask in the water bath with thermostatic control whirlpool for being placed in 10 DEG C, 20 DEG C, 30 DEG C8Cfu/mL confession
Bacterium living bacterial liquid is tried, effervescent tablet is finally quantitatively added, effervescent tablet ultimate density in water body is reached 1.0mg/L, 2.0mg/
L, 3.0mg/L, 4.0mg/L and 5.0mg/L.Jog flask, makes thalline and effervescent tablet liquid be evenly distributed in water.In addition, point
Control group without bacterium solution or effervescent tablet liquid is not set, sterilization effect is detected.
3. cultivation water sterilization determination：Aseptically, 0.1mL water is taken out from each beaker, is applied to and uses HBTA
On the agar plate of preparation, under the conditions of 25 DEG C, after culture 48h, the colony counts in each plate are counted, according to the growth shape of bacterium colony
Condition, judges sterilization effect of the effervescent tablet in cultivation water.
4. 1 is shown in Table to the thermophilic fiber bacterium bactericidal effect of shape, 2 are shown in Table to Aeromonas hydrophila bactericidal effect, Vibrio anguillarum is sterilized
The bactericidal effect that effect is shown in Table in 3, cultivation water is shown in Table 4.
Embodiment 2
(1) 6g bialkyl methyl ethoxyls ammonium bromide, 3g garlic powders, 20g butanedioic acids, 25g sodium chloride, 12g sulfuric acid are weighed
Sodium is well mixed；
(2) particle crosses 20 mesh sieves, and powder is made；
(3) 20g SODIUM PERCARBONATEs, 1g magnesium stearates and 6g copolyvidones are added in the powder of step (2), mixed,
Tabletting, is made sterilization effervescent tablet.
(4) the sterilization effervescent tablet for preparing step (3) includes Cytophaga Columnaris, thermophilic aqueous vapor list to Common Fish
Antibacterial ability in born of the same parents bacterium, Vibrio anguillarum and cultivation water is tested, and is carried out according to the following steps：
1. the measure of minimum bactericidal concentration：The sterilization effervescent tablet of preparation is prepared into 1000-0.25mg/ with sterilizing double distilled water
L 13 concentration, dilute 10 times by each strength solution with FWA culture mediums, fill in the test tube of 2.9mL culture mediums and add to every pipe
0.1mL concentration is 107Cfu/mL living bacterial liquids, under the conditions of 25 DEG C, after cultivating 5 days, observation is confirmed in asepsis growth test tube respectively
0.1mL culture mediums are sucked, is inoculated in bouillon agar plate, under the conditions of 25 DEG C, is further cultured for 5 days, it is sterile in agar plate to occur
Corresponding test tube in minimum effervescent tablet concentration, i.e. minimum bactericidal concentration of the effervescent tablet to bacterium.
2. sterilization effect of the effervescent tablet in cultivation water：The triangular glass flask of 300mL sterilizing pond reclaimed waters will be filled, respectively
It is about 10 to adding 3.0mL bacteria concentrations in each flask in the water bath with thermostatic control whirlpool for being placed in 10 DEG C, 20 DEG C, 30 DEG C8Cfu/mL confession
Bacterium living bacterial liquid is tried, effervescent tablet is finally quantitatively added, effervescent tablet ultimate density in water body is reached 1.0mg/L, 2.0mg/
L, 3.0mg/L, 4.0mg/L and 5.0mg/L.Jog flask, makes thalline and effervescent tablet liquid be evenly distributed in water.In addition, point
Control group without bacterium solution or effervescent tablet liquid is not set, sterilization effect is detected.
3. cultivation water sterilization determination：Aseptically, 0.1mL water is taken out from each beaker, is applied to and uses HBTA
On the agar plate of preparation, under the conditions of 25 DEG C, after culture 48h, the colony counts in each plate are counted, according to the growth shape of bacterium colony
Condition, judges sterilization effect of the effervescent tablet in cultivation water.
4. 1 is shown in Table to the thermophilic fiber bacterium bactericidal effect of shape, 2 are shown in Table to Aeromonas hydrophila bactericidal effect, Vibrio anguillarum is sterilized
The bactericidal effect that effect is shown in Table in 3, cultivation water is shown in Table 4.
Embodiment 3
(1) 8g2- (2- ethoxys)-methyl-(1- methyl-imidazoles -2- methylene) ammonium chloride, 4g garlic powders, 20g are weighed
Adipic acid, 30g sodium chloride, 14g sodium sulphate are well mixed；
(2) particle crosses 20 mesh sieves, and powder is made；
(3) 12g sodium carbonate, 10g sodium acid carbonates, 6g SODIUM PERCARBONATE 2g magnesium stearates and 10g polyvinylpyrrolidones are added
In the powder for being added to step (2), mix, tabletting, sterilization effervescent tablet is made.
(4) the sterilization effervescent tablet for preparing step (3) includes Cytophaga Columnaris, thermophilic aqueous vapor list to Common Fish
Antibacterial ability in born of the same parents bacterium, Vibrio anguillarum and cultivation water is tested, and is carried out according to the following steps：
1. the measure of minimum bactericidal concentration：The sterilization effervescent tablet of preparation is prepared into 1000-0.25mg/ with sterilizing double distilled water
L 13 concentration, dilute 10 times by each strength solution with FWA culture mediums, fill in the test tube of 2.9mL culture mediums and add to every pipe
0.1mL concentration is 107Cfu/mL living bacterial liquids, under the conditions of 25 DEG C, after cultivating 5 days, observation is confirmed in asepsis growth test tube respectively
0.1mL culture mediums are sucked, is inoculated in bouillon agar plate, under the conditions of 25 DEG C, is further cultured for 5 days, it is sterile in agar plate to occur
Corresponding test tube in minimum effervescent tablet concentration, i.e. minimum bactericidal concentration of the effervescent tablet to bacterium.
2. sterilization effect of the effervescent tablet in cultivation water：The triangular glass flask of 300mL sterilizing pond reclaimed waters will be filled, respectively
It is about 10 to adding 3.0mL bacteria concentrations in each flask in the water bath with thermostatic control whirlpool for being placed in 10 DEG C, 20 DEG C, 30 DEG C8Cfu/mL confession
Bacterium living bacterial liquid is tried, effervescent tablet is finally quantitatively added, effervescent tablet ultimate density in water body is reached 1.0mg/L, 2.0mg/
L, 3.0mg/L, 4.0mg/L and 5.0mg/L.Jog flask, makes thalline and effervescent tablet liquid be evenly distributed in water.In addition, point
Control group without bacterium solution or effervescent tablet liquid is not set, sterilization effect is detected.
3. cultivation water sterilization determination：Aseptically, 0.1mL water is taken out from each beaker, is applied to and uses HBTA
On the agar plate of preparation, under the conditions of 25 DEG C, after culture 48h, the colony counts in each plate are counted, according to the growth shape of bacterium colony
Condition, judges sterilization effect of the effervescent tablet in cultivation water.
4. 1 is shown in Table to the thermophilic fiber bacterium bactericidal effect of shape, 2 are shown in Table to Aeromonas hydrophila bactericidal effect, Vibrio anguillarum is sterilized
The bactericidal effect that effect is shown in Table in 3, cultivation water is shown in Table 4.
Embodiment 4
(1) 8g alkyl benzyl ether double ammonium chloride, 3g garlic powders, 20g aminotriacetic acids, 30g sodium chloride, 13g sulfuric acid are weighed
Sodium is well mixed；
(2) particle crosses 20 mesh sieves, and powder is made；
(3) 22g sodium carbonate, 2g talcum powder and 7g sodium carboxymethylcelluloses are added in the powder of step (2), mixed
Even, sterilization effervescent tablet is made in tabletting.
(4) the sterilization effervescent tablet for preparing step (3) includes Cytophaga Columnaris, thermophilic aqueous vapor list to Common Fish
Antibacterial ability in born of the same parents bacterium, Vibrio anguillarum and cultivation water is tested, and is carried out according to the following steps：
1. the measure of minimum bactericidal concentration：The sterilization effervescent tablet of preparation is prepared into 1000-0.25mg/ with sterilizing double distilled water
L 13 concentration, dilute 10 times by each strength solution with FWA culture mediums, fill in the test tube of 2.9mL culture mediums and add to every pipe
0.1mL concentration is 107Cfu/mL living bacterial liquids, under the conditions of 25 DEG C, after cultivating 5 days, observation is confirmed in asepsis growth test tube respectively
0.1mL culture mediums are sucked, is inoculated in bouillon agar plate, under the conditions of 25 DEG C, is further cultured for 5 days, it is sterile in agar plate to occur
Corresponding test tube in minimum effervescent tablet concentration, i.e. minimum bactericidal concentration of the effervescent tablet to bacterium.
2. sterilization effect of the effervescent tablet in cultivation water：The triangular glass flask of 300mL sterilizing pond reclaimed waters will be filled, respectively
It is about 10 to adding 3.0mL bacteria concentrations in each flask in the water bath with thermostatic control whirlpool for being placed in 10 DEG C, 20 DEG C, 30 DEG C8Cfu/mL confession
Bacterium living bacterial liquid is tried, effervescent tablet is finally quantitatively added, effervescent tablet ultimate density in water body is reached 1.0mg/L, 2.0mg/
L, 3.0mg/L, 4.0mg/L and 5.0mg/L.Jog flask, makes thalline and effervescent tablet liquid be evenly distributed in water.In addition, point
Control group without bacterium solution or effervescent tablet liquid is not set, sterilization effect is detected.
3. cultivation water sterilization determination：Aseptically, 0.1mL water is taken out from each beaker, is applied to and uses HBTA
On the agar plate of preparation, under the conditions of 25 DEG C, after culture 48h, the colony counts in each plate are counted, according to the growth shape of bacterium colony
Condition, judges sterilization effect of the effervescent tablet in cultivation water.
4. 1 is shown in Table to the thermophilic fiber bacterium bactericidal effect of shape, 2 are shown in Table to Aeromonas hydrophila bactericidal effect, Vibrio anguillarum is sterilized
The bactericidal effect that effect is shown in Table in 3, cultivation water is shown in Table 4.
Embodiment 5
Following table is made according to embodiment 1-4
Table 1 sterilizes effervescent tablet to the thermophilic fiber bacterium bactericidal effect of shape
Table 2 sterilizes effervescent tablet to Aeromonas hydrophila bactericidal effect
Table 3 sterilizes effervescent tablet to Vibrio anguillarum bactericidal effect
Table 4 sterilizes bactericidal effect of the effervescent tablet in cultivation water
* the numeral in bracket is degerming rate
Table 5 sterilizes the bactericidal effect of effervescent tablet, quaternary ammonium salt effervescent tablet and sodium chloride quaternary ammonium salt effervescent tablet in cultivation water
As can be seen from the above embodiments, what prepared by the present invention uses sterilization effervescent tablet to the pathogenic bacteria in aquaculture of aquatic animal
There is preferable bactericidal effect, compared with the bleaching powder that in the market is commonly used, effect is suitable, but small toxicity.To the bactericidal effect of cultivation water
Preferably, when concentration reaches 5.0mg/L, degerming rate is more than more than 90%.The result of table 5 shows, sterilization effervesce prepared by the present invention
Its bactericidal effect of piece is better than quaternary ammonium salt effervescent tablet and sodium chloride quaternary ammonium salt effervescent tablet.
Claims (9)
1. a kind of saliferous sterilization effervescent tablet used for aquiculture, it is characterised in that：Include following raw material, sodium chloride 25~35
Part, 5~10 parts of quaternary ammonium salt, 2~5 parts of garlic powder, 5~10 parts of adhesive, 35~50 parts of effervescent agent, 10~15 parts of sodium sulphate, profit
1~3 part of lubrication prescription.
2. a kind of saliferous sterilization effervescent tablet used for aquiculture according to claim 1, it is characterised in that：Include following weight
Part raw material, 28~32 parts of sodium chloride, 6~9 parts of quaternary ammonium salt, 3~4 parts of garlic powder, 6~8 parts of adhesive, 38~44 parts of effervescent agent,
11~14 parts of sodium sulphate, 1~3 part of lubricant.
3. a kind of saliferous sterilization effervescent tablet used for aquiculture according to claim 1, it is characterised in that：Include following weight
Part raw material, 30 parts of sodium chloride, 8 parts of quaternary ammonium salt, 3 parts of garlic powder, 7 parts of adhesive, 42 parts of effervescent agent, 13 parts of sodium sulphate, lubricant 2
Part.
4. a kind of saliferous sterilization effervescent tablet used for aquiculture according to claim 1, it is characterised in that：The quaternary ammonium salt is
Dodecyl dimethyl benzyl ammonium bromide, bialkyl methyl ethoxyl ammonium bromide, 2- (2- ethoxys)-methyl-(1- methyl-miaow
Azoles -2- methylene) ammonium chloride, one kind in the double ammonium chlorides of alkyl benzyl ether.
5. a kind of saliferous sterilization effervescent tablet used for aquiculture according to claim 1, it is characterised in that：The adhesive is
One kind in polyvinyl alcohol, copolyvidone, polyvinylpyrrolidone, sodium carboxymethylcellulose.
6. a kind of saliferous sterilization effervescent tablet used for aquiculture according to claim 1, it is characterised in that：The effervescent agent by
Acid source and carbon dioxide source composition, acid source is one kind in oxalic acid, adipic acid, butanedioic acid, glutaric acid, aminotriacetic acid, dioxy
Change carbon source is one kind in sodium carbonate, sodium acid carbonate, SODIUM PERCARBONATE；Acid source is 1 with carbon dioxide source weight ratio:1.3~
3:4.1。
7. a kind of saliferous sterilization effervescent tablet used for aquiculture according to claim 1, it is characterised in that：The lubricant is
Magnesium stearate and one kind in talcum powder.
8. a kind of saliferous sterilization effervesce piece preparation method used for aquiculture, it is characterised in that：Comprise the steps of：
The first step, weighs sodium chloride, quaternary ammonium salt, garlic powder, effervescent agent acid source, the sodium sulphate of parts by weight, is well mixed, and is made mixed
Compound；
Second step, mixture is ground, and by screen cloth, powder is made；
3rd step, adds effervescent agent carbon dioxide source, binder and the lubricant of parts by weight in powder, is well mixed, and does
Dry, sterilization effervescent tablet is made in tabletting.
9. a kind of saliferous sterilization effervesce piece preparation method used for aquiculture according to claim 8, it is characterised in that：It is described
In second step, screen cloth is 20~40 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710401087.7A CN107094811A (en) | 2017-05-31 | 2017-05-31 | A kind of saliferous sterilization effervescent tablet used for aquiculture and preparation method thereof |
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| CN112956595A (en) * | 2021-04-01 | 2021-06-15 | 南通大学 | Livestock and poultry breeding sterilization nutrition tablet and preparation method thereof |
| CN115028243A (en) * | 2022-05-24 | 2022-09-09 | 吴金轩 | Water purification chitin composite effervescent tablet |
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| CN108434115A (en) * | 2018-03-09 | 2018-08-24 | 新疆埃乐欣药业有限公司 | Anti-fungal infection allicin effervescent tablet and its preparation method and application |
| CN112956595A (en) * | 2021-04-01 | 2021-06-15 | 南通大学 | Livestock and poultry breeding sterilization nutrition tablet and preparation method thereof |
| CN115028243A (en) * | 2022-05-24 | 2022-09-09 | 吴金轩 | Water purification chitin composite effervescent tablet |
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