CN107056462A - A kind of organic fertilizer of antibiotic property and preparation method thereof - Google Patents
A kind of organic fertilizer of antibiotic property and preparation method thereof Download PDFInfo
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- CN107056462A CN107056462A CN201710295351.3A CN201710295351A CN107056462A CN 107056462 A CN107056462 A CN 107056462A CN 201710295351 A CN201710295351 A CN 201710295351A CN 107056462 A CN107056462 A CN 107056462A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/647—Triazoles; Hydrogenated triazoles
- A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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Abstract
The present invention relates to a kind of organic fertilizer of antibiotic property, the organic fertilizer includes following components:11 13 parts of 33 36 parts of rape stalk, 20 25 parts of wheat stalk, 21 28 parts of soybean stalk, 11 18 parts of manioc waste, 6 11 parts of antiseptic, 18 23 parts of diatomite, 48 53 parts of urea, 24 27 parts of potassium dihydrogen phosphate, 21 25 parts of ammonium hydrogen carbonate, 14 17 parts of calcium superphosphate, 10 17 parts of potassium chloride and calcium ammonium nitrate；A kind of organic fertilizer of antibiotic property in the present invention, effectively reduce the production cost of raw material, cost reduction by 50% 60% can be made, extracted in the present invention from rape stalk, wheat stalk, soybean stalk, and be organic fertilizer by stover, it can effectively reduce pollution of the fertilizer to environment；Using a kind of experimental plot of the preparation method of the organic fertilizer of antibiotic property, yield effectively improves 23.33 24.54%；Completely filled fruit, lovely luster can be made, resistance against diseases is strong, and antibacterial ability effectively improves 18 22%.
Description
Technical field
The invention belongs to the production field of organic fertilizer, and in particular to a kind of organic fertilizer of antibiotic property and its preparation side
Method.
Background technology
Fertilizer can provide nutrient for crops, produce more agricultural product.Although the usage amount of fertilizer is increasingly
Greatly, but the various chemical fertilizer of using in farmland can not possibly be all absorbed and used by plants.The utilization rate of chemical fertilizer is low, does not have after
Have and be absorbed by crops the fertilizer utilized and largely enter environment, environment is polluted, land resource has been not only broken up, and to people
Class health also constitutes threat.At present, the chemical fertilizer that China applies is based on nitrogenous fertilizer, and phosphate fertilizer, potash fertilizer, composite fertilizer are less, for a long time
Using causing soil nutrient to lack of proper care, aggravate not containing antibiotic property in soil phophorus, the exhaustion of potassium, existing fertilizer, not only make fertilizer
It without antibiotic property, and can be lost in the element of promotion plant growth, it is impossible to play effective fixed nitrogen, phosphorus decomposing, solution
Effect of potassium, can cause the loss of fertilizer.
The content of the invention
There is provided a kind of organic fertilizer of antibiotic property and its preparation side for the deficiencies in the prior art by the present invention
Method, to solve problems of the prior art.
To achieve the above object, the technical solution adopted by the present invention is as follows：
A kind of organic fertilizer of antibiotic property, the organic fertilizer includes following components:33-36 parts of rape stalk, wheat stalk
20-25 parts, 21-28 parts of soybean stalk, 11-18 parts of manioc waste, 6-11 parts of antiseptic, 18-23 parts of diatomite, 48-53 parts of urea,
24-27 parts of potassium dihydrogen phosphate, 21-25 parts of ammonium hydrogen carbonate, 14-17 parts of calcium superphosphate, 10-17 parts of potassium chloride and calcium ammonium nitrate
11-13 parts.
As a modification of the present invention, the antiseptic includes following components：13-16 parts of tea free, folium artemisiae argyi 14-18
Part, golden 14-18 parts of clock rattan, 16-19 parts of elscholtiza, 17-22 parts of kaolin, 8-11 parts of amino acid, starch grafted acrylate copolymerization
2-4 parts of 4-7 parts of cross-linking agent, 1-2 parts of paclobutrazol, 3-5 parts of vinegar and thiophanate methyl.
As a modification of the present invention, the preparation method of the antiseptic is as follows：（1）By 3-6 parts of nitrogen-fixing bacteria, thermophilic bud
4-7 parts of spore bacterium, 3-5 parts of bacillus subtilis are put in a kettle., and will be mixed
After compound is sealed 2-3 days after stirring at normal temperatures, 1-2 parts of glutathione peroxidase, color are added into material
2-3 parts of propylhomoserin protein kinase, 1-3 parts of aspergillus niger and after being mixed, material are put into PDA liquid medium, and make thing
Material reaction 3-3.5 days；
（2）After 13-16 parts of tea free, 14-18 parts of folium artemisiae argyi are pulverized and mixed, and material is put at 70-75 DEG C progress
Boiling 20-30 minutes；
（3）Ethanol will be added in golden 14-18 parts of clock rattan, 16-19 parts of elscholtiza, and material is filtered after carrying out immersion 30-40 minutes,
Added into filtrate and pass through step（2）Reacted material is simultaneously stirred, and the material after stirring is carried out to extract 4 times, each 1-
1.5 hours, merge extract solution；
（4）Step will be passed through（3）After addition carbohydrase, protease are mixed in filtrate after extraction, 22-27 parts of water is added
Water, and material is put into distilling apparatus, and material is subjected to distillation 2-4 hours；
（5）Step will be passed through（4）Material after distillation is put into filter, and material is filtered；
（6）Step will be passed through（3）Reacted extract solution is with passing through step（5）After reacted filtered fluid is mixed, add
By step（1）After reacted material is mixed, 4-7 parts of starch grafted acrylate crosslinking copolymerization thing, multiple-effect are added
1-2 parts of azoles, 3-5 parts of vinegar, and material is stirred after 1-2 days, and seal 2-3 days after material is stirred at normal temperatures
After filter, take filtered fluid；
（7）After 17-22 parts of kaolin, 8-11 parts of amino acid, 2-4 parts of thiophanate methyl are mixed, material is put into powder
After being crushed in crushing device, 33-34 parts of water is added into material, and material is put into agitating device, and material is entered
Row stirring 50-60 minutes；
（8）Step will be passed through（7）Reacted material is put into 500-530 DEG C of high temperature furnace, and carries out 19-22 points of roasting
Clock, material is put into and crushed into reducing mechanism, is added into the material after crushing and is passed through step（6）Reacted thing
Material, and material is stirred, the material after stirring is put into processor for ultrasonic wave, at 100-130W ultrasonic wave
Material is passed through extruder grain, you can obtain bactericide by reason after 1-1.5 hours.
As a modification of the present invention, the step（3）The addition of middle ethanol is 12-14 times of the amount of material, plus
The concentration of alcohol entered is 50-58%.
As a modification of the present invention, the step（4）Middle carbohydrase, the mass ratio of protease are 4:5.
As a modification of the present invention, the step（7）The rotating speed of middle agitating device is 250-300r/min.
A kind of preparation method of the organic fertilizer of antibiotic property, is comprised the following steps that：（1）By 33-36 parts of rape stalk, wheat
20-25 parts of stalk, 21-28 parts of soybean stalk are broken into after 2-4cm powder, and with 1：1.5-2 ratio adds corresponding deal
Water, stirs when adding water and stands 10-13 hours after 8-12 hours；
（2）Material is put into fermentation vat, 11-18 parts of manioc waste, 6-11 parts of antiseptic is added, and material is subjected to reaction 1-
Material is taken out after 3 days；
（3）Water is added into the material after fermentation, and makes the water content of material for 61-63%, material is carried out at 51-56 DEG C
After stirring 43-47 minutes, and material is dehydrated with 270-285 DEG C of heat smoke, and make the water content of material for 60-
64%；
（4）Reacted material is put into solar energy fermentation greenhouse, and it is rotten to carry out whole storehouse heap；
（5）After material is placed 7-9 days in solar energy fermentation greenhouse when temperature reaches 60-64 DEG C, appropriate water is added, and
Make the water content of material under conditions of 39-42%, and material is proceeded fermentation 13-17 days；
（7）The material of gained after fermentation is piled into bank, bank is carried out to carry out turning and throwing once after standing 4 days, later every 7
Its turning once, and records daily temperature；When the temperature after material turning is 63-68 DEG C, material is spread out and dried in the air
Shine 18-20 days, and control its water content to be 25-29%；
（8）By 18-23 parts of diatomite, 48-53 parts of urea, 24-27 parts of potassium dihydrogen phosphate, 21-25 parts of ammonium hydrogen carbonate, calcium superphosphate
11-13 parts of 14-17 parts, 10-17 parts of potassium chloride and calcium ammonium nitrate are mixed and crushed；
（9）By step（7）Product and step（8）Product mixed, and the material of generation is put into mixer
In be stirred after granulation, dry, crush, sieving, obtained product is packed.
As a result of above technology, the present invention compared with the prior art, has the advantage that as follows：
A kind of organic fertilizer of antibiotic property in the present invention, effectively reduces the production cost of raw material, can reduce cost
Extracted in 50%-60%, the present invention from rape stalk, wheat stalk, soybean stalk, and be organic fertilizer by stover
Material, can effectively reduce pollution of the fertilizer to environment；Using a kind of experimental plot of the organic fertilizer of antibiotic property, yield is effectively improved
23.33-24.54%；Completely filled fruit, lovely luster can be made, resistance against diseases is strong, antibacterial ability effectively improves 18-22%, nitrogen, phosphorus,
The micronutrient levels such as potassium are improved, and nitrogen can be made to effectively improve 11-17%, P elements effectively improve 11-14%, and potassium element has
Effect improves 15-19%；Use for a long time, plant equilibrium can be accelerated to absorb trace element comprehensively, promote growth and the root of plant
System's development, builds up resistance, prevents pest and disease damage；After a kind of organic fertilizer of antibiotic property, the fertilizer efficiency of soil is effectively improved, fertilizer
The plant recovery of nutrient of material is up to 54-57%, can make continuously to use 2-3.
Embodiment
With reference to embodiment, the present invention is furture elucidated.
Embodiment 1：
A kind of organic fertilizer of antibiotic property, the organic fertilizer includes following components:33 parts of rape stalk, 25 parts of wheat stalk,
21 parts of soybean stalk, 18 parts of manioc waste, 6 parts of antiseptic, 23 parts of diatomite, 48 parts of urea, 27 parts of potassium dihydrogen phosphate, ammonium hydrogen carbonate
13 parts of 21 parts, 17 parts of calcium superphosphate, 10 parts of potassium chloride and calcium ammonium nitrate.
The antiseptic includes following components：13 parts of tea free, 18 parts of folium artemisiae argyi, golden 18 parts of clock rattan, 16 parts of elscholtiza, kaolin
22 parts, 8 parts of amino acid, 7 parts of starch grafted acrylate crosslinking copolymerization thing, 1 part of paclobutrazol, 5 parts of vinegar and thiophanate methyl 2
Part.
The preparation method of the antiseptic is as follows：（1）By 3 parts of nitrogen-fixing bacteria, 7 parts of thermophilic Bacillus, 3 parts of bacillus subtilis
Put in a kettle., and glutathione peroxidating is added into material after sealing 3 days after mixture is stirred at normal temperatures
1 part of thing enzyme, 3 parts of tryptophan protein kinase, 1 part of aspergillus niger and after being mixed, material is put into PDA liquid medium,
And make material reaction 3-3.5 days；
（2）By 13 parts of tea free, 18 parts of folium artemisiae argyi, be pulverized and mixed after, and by material be put at 70 DEG C carry out 20 points of boiling
Clock；
（3）Ethanol will be added in golden 18 parts of clock rattan, 16 parts of elscholtiza, and material is filtered after carrying out immersion 40 minutes, to filtrate
Step is passed through in middle addition（2）Reacted material is simultaneously stirred, and the material after stirring is carried out to extract 4 times, 1 hour every time, merged
Extract solution；The step（3）The addition of middle ethanol is 14 times of the amount of material, and the concentration of alcohol of addition is 58%；
（4）Step will be passed through（3）After addition carbohydrase, protease are mixed in filtrate after extraction, 27 parts of water of water are added,
And material is put into distilling apparatus, and material is subjected to distillation 2 hours；The step（4）The matter of middle carbohydrase, protease
Amount is than being 4:5；
（5）Step will be passed through（4）Material after distillation is put into filter, and material is filtered；
（6）Step will be passed through（3）Reacted extract solution is with passing through step（5）After reacted filtered fluid is mixed, add
By step（1）After reacted material is mixed, 7 parts of starch grafted acrylate crosslinking copolymerization thing, paclobutrazol 1 are added
Part, 5 parts of vinegar, and material is stirred after 1 day, and sealing is filtered after 3 days after material is stirred at normal temperatures, is taken
Filtrate；
（7）After 22 parts of kaolin, 8 parts of amino acid, 2 parts of thiophanate methyl are mixed, material is put into reducing mechanism
After being crushed, 33 parts of water is added into material, and material is put into agitating device, and material is stirred 60 points
Clock；The step（7）The rotating speed of middle agitating device is 250r/min；
（8）Step will be passed through（7）Reacted material is put into 530 DEG C of high temperature furnace, and carries out roasting 19 minutes, by material
It is put into and is crushed into reducing mechanism, is added into the material after crushing and pass through step（6）Reacted material, and by material
It is stirred, the material after stirring is put into processor for ultrasonic wave, after 130W ultrasonication 1 hour, by thing
Material passes through extruder grain, you can obtain bactericide.
A kind of preparation method of the organic fertilizer of antibiotic property, is comprised the following steps that：（1）By 33 parts of rape stalk, Wheat Straw
25 parts of stalk, 21 parts of soybean stalk are broken into after 4cm powder, and with 1：2 ratio adds the water of corresponding deal, is stirred when adding water
10 hours are stood after 12 hours；
（2）Material is put into fermentation vat, 18 parts of manioc waste, 6 parts of antiseptic is added, and material is subjected to general after reacting 3 days
Material takes out；
（3）Water is added into the material after fermentation, and makes the water content of material be 62%, material is stirred 43 at 54 DEG C
After minute, and material is dehydrated with 285 DEG C of heat smoke, and make the water content of material be 60%；
（4）Reacted material is put into solar energy fermentation greenhouse, and it is rotten to carry out whole storehouse heap；
（5）After material is placed 9 days in solar energy fermentation greenhouse when temperature reaches 60 DEG C, appropriate water is added, and make thing
The water content of material makes material proceed fermentation 13 days under conditions of 42%；
（7）The material of gained after fermentation is piled into bank, bank is carried out to carry out turning and throwing once after standing 4 days, later every 7
Its turning once, and records daily temperature；When the temperature after material turning is 68 DEG C, spreads material out progress and dry 18
My god, and control its water content to be 29%；
（8）By 23 parts of diatomite, 48 parts of urea, 27 parts of potassium dihydrogen phosphate, 21 parts of ammonium hydrogen carbonate, 17 parts of calcium superphosphate, potassium chloride
10 parts and 13 parts of calcium ammonium nitrate are mixed and crushed；
（9）By step（7）Product and step（8）Product mixed, and the material of generation is put into mixer
In be stirred after granulation, dry, crush, sieving, obtained product is packed.
Using a kind of experimental plot of the organic fertilizer of antibiotic property, yield effectively improves 23.33-24.54%；Fruit can be made
Full, lovely luster, resistance against diseases is strong, and antibacterial ability effectively improves 18-22%, and the micronutrient levels such as nitrogen, phosphorus, potassium is improved, can
So that nitrogen effectively improves 11-17%, P elements effectively improve 11-14%, and potassium element effectively improves 15-19%；Make for a long time
With, plant equilibrium can be accelerated to absorb trace element comprehensively, promote growth and the root system development of plant, build up resistance, it is anti-
Only pest and disease damage；After a kind of organic fertilizer of antibiotic property, the fertilizer efficiency of soil is effectively improved, the plant recovery of nutrient of fertilizer is up to
54-57%, can make continuously to use 2-3.
Embodiment 2：
A kind of organic fertilizer of antibiotic property, the organic fertilizer includes following components:36 parts of rape stalk, 20 parts of wheat stalk,
28 parts of soybean stalk, 11 parts of manioc waste, 11 parts of antiseptic, 18 parts of diatomite, 53 parts of urea, 24 parts of potassium dihydrogen phosphate, bicarbonate
11 parts of 25 parts of ammonium, 14 parts of calcium superphosphate, 17 parts of potassium chloride and calcium ammonium nitrate.
The antiseptic includes following components：16 parts of tea free, 14 parts of folium artemisiae argyi, golden 18 parts of clock rattan, 16 parts of elscholtiza, kaolin
22 parts, 8 parts of amino acid, 7 parts of starch grafted acrylate crosslinking copolymerization thing, 1 part of paclobutrazol, 5 parts of vinegar and thiophanate methyl 2
Part.
The preparation method of the antiseptic is as follows：（1）By 6 parts of nitrogen-fixing bacteria, 4 parts of thermophilic Bacillus, 5 parts of bacillus subtilis
Put in a kettle., and glutathione peroxidating is added into material after sealing 3 days after mixture is stirred at normal temperatures
1 part of thing enzyme, 3 parts of tryptophan protein kinase, 3 parts of aspergillus niger and after being mixed, material is put into PDA liquid medium,
And make material reaction 3 days；
（2）After 16 parts of tea free, 14 parts of folium artemisiae argyi are pulverized and mixed, and material is put at 75 DEG C 28 points of boiling of progress
Clock；
（3）Ethanol will be added in golden 18 parts of clock rattan, 16 parts of elscholtiza, and material is filtered after carrying out immersion 28 minutes, to filtrate
Step is passed through in middle addition（2）Reacted material is simultaneously stirred, and the material after stirring is carried out to extract 4 times, 1 hour every time, merged
Extract solution；The step（3）The addition of middle ethanol is 14 times of the amount of material, and the concentration of alcohol of addition is 58%；
（4）Step will be passed through（3）After addition carbohydrase, protease are mixed in filtrate after extraction, 27 parts of water of water are added,
And material is put into distilling apparatus, and material is subjected to distillation 4 hours；The step（4）The matter of middle carbohydrase, protease
Amount is than being 4:5；
（5）Step will be passed through（4）Material after distillation is put into filter, and material is filtered；
（6）Step will be passed through（3）Reacted extract solution is with passing through step（5）After reacted filtered fluid is mixed, add
By step（1）After reacted material is mixed, 7 parts of starch grafted acrylate crosslinking copolymerization thing, paclobutrazol 1 are added
Part, 5 parts of vinegar, and material is stirred after 1 day, and sealing is filtered after 3 days after material is stirred at normal temperatures, is taken
Filtrate；
（7）After 22 parts of kaolin, 8 parts of amino acid, 2 parts of thiophanate methyl are mixed, material is put into reducing mechanism
After being crushed, 33 parts of water is added into material, and material is put into agitating device, and material is stirred 50 points
Clock；The step（7）The rotating speed of middle agitating device is 300r/min；
（8）Step will be passed through（7）Reacted material is put into 530 DEG C of high temperature furnace, and carries out roasting 19 minutes, by material
It is put into and is crushed into reducing mechanism, is added into the material after crushing and pass through step（6）Reacted material, and by material
It is stirred, the material after stirring is put into processor for ultrasonic wave, after 130W ultrasonication 1 hour, by thing
Material passes through extruder grain, you can obtain bactericide.
A kind of preparation method of the organic fertilizer of antibiotic property, is comprised the following steps that：（1）By 36 parts of rape stalk, Wheat Straw
20 parts of stalk, 28 parts of parts of soybean stalk are broken into after 3cm powder, and with 1：2 ratio adds the water of corresponding deal, when adding water
Stirring stands 13 hours after 8 hours；
（2）Material is put into fermentation vat, 11 parts of manioc waste, 11 parts of antiseptic is added, and material is subjected to general after reacting 2 days
Material takes out；
（3）Water is added into the material after fermentation, and makes the water content of material be 63%, material is stirred 47 at 51 DEG C
After minute, and material is dehydrated with 270 DEG C of heat smoke, and make the water content of material be 64%；
（4）Reacted material is put into solar energy fermentation greenhouse, and it is rotten to carry out whole storehouse heap；
（5）After material is placed 7 days in solar energy fermentation greenhouse when temperature reaches 64 DEG C, appropriate water is added, and make thing
The water content of material makes material proceed fermentation 13 days under conditions of 42%；
（7）The material of gained after fermentation is piled into bank, bank is carried out to carry out turning and throwing once after standing 4 days, later every 7
Its turning once, and records daily temperature；When the temperature after material turning is 68 DEG C, spreads material out progress and dry 18
My god, and control its water content to be 29%；
（8）By 18 parts of diatomite, 53 parts of urea, 24 parts of potassium dihydrogen phosphate, 25 parts of ammonium hydrogen carbonate, 14 parts of calcium superphosphate, potassium chloride
17 parts and 11 parts of calcium ammonium nitrate are mixed and crushed；
（9）By step（7）Product and step（8）Product mixed, and the material of generation is put into mixer
In be stirred after granulation, dry, crush, sieving, obtained product is packed.
Using a kind of experimental plot of the organic fertilizer of antibiotic property, yield effectively improves 23.31-24.51%；Fruit can be made
Full, lovely luster, resistance against diseases is strong, and antibacterial ability effectively improves 18-22%, and the micronutrient levels such as nitrogen, phosphorus, potassium is improved, can
So that nitrogen effectively improves 11-16%, P elements effectively improve 11-13%, and potassium element effectively improves 15-18%；Make for a long time
With, plant equilibrium can be accelerated to absorb trace element comprehensively, promote growth and the root system development of plant, build up resistance, it is anti-
Only pest and disease damage；After a kind of organic fertilizer of antibiotic property, the fertilizer efficiency of soil is effectively improved, the plant recovery of nutrient of fertilizer is up to
53-57%, can make continuously to use 2-3.
Embodiment 3：
A kind of organic fertilizer of antibiotic property, the organic fertilizer includes following components:34 parts of rape stalk, 23 parts of wheat stalk,
21 parts of soybean stalk, 17 parts of manioc waste, 6 parts of antiseptic, 18 parts of diatomite, 48 parts of urea, 27 parts of potassium dihydrogen phosphate, ammonium hydrogen carbonate
13 parts of 24 parts, 16 parts of calcium superphosphate, 10 parts of potassium chloride and calcium ammonium nitrate.
The antiseptic includes following components：16 parts of tea free, 17 parts of folium artemisiae argyi, golden 16 parts of clock rattan, 16 parts of elscholtiza, kaolin
17 parts, 1 part of amino acid/11,7 parts of starch grafted acrylate crosslinking copolymerization thing, 1 part of paclobutrazol, 5 parts of vinegar and thiophanate methyl
3 parts.
The preparation method of the antiseptic is as follows：（1）By 5 parts of nitrogen-fixing bacteria, 4 parts of thermophilic Bacillus, 5 parts of bacillus subtilis
Put in a kettle., and glutathione peroxidating is added into material after sealing 2 days after mixture is stirred at normal temperatures
2 parts of thing enzyme, 2 parts of tryptophan protein kinase, 3 parts of aspergillus niger and after being mixed, material is put into PDA liquid medium,
And make material reaction 3.5 days；
（2）After 16 parts of tea free, 17 parts of folium artemisiae argyi are pulverized and mixed, and material is put at 74 DEG C progress boiling 20-30
Minute；
（3）Ethanol will be added in golden 16 parts of clock rattan, 16 parts of elscholtiza, and material is filtered after carrying out immersion 39 minutes, to filtrate
Step is passed through in middle addition（2）Reacted material is simultaneously stirred, and the material after stirring is carried out to extract 4 times, 1.5 hours every time, closed
And extract solution；The step（3）The addition of middle ethanol is 13 times of the amount of material, and the concentration of alcohol of addition is 54%；
（4）Step will be passed through（3）After addition carbohydrase, protease are mixed in filtrate after extraction, 27 parts of water of water are added,
And material is put into distilling apparatus, and material is subjected to distillation 4 hours；The step（4）The matter of middle carbohydrase, protease
Amount is than being 4:5；
（5）Step will be passed through（4）Material after distillation is put into filter, and material is filtered；
（6）Step will be passed through（3）Reacted extract solution is with passing through step（5）After reacted filtered fluid is mixed, add
By step（1）After reacted material is mixed, 7 parts of starch grafted acrylate crosslinking copolymerization thing, paclobutrazol 1 are added
Part, 5 parts of vinegar, and material is stirred after 2 days, and sealing is filtered after 3 days after material is stirred at normal temperatures, is taken
Filtrate；
（7）After 17 parts of kaolin, 1 part of amino acid/11,3 parts of thiophanate methyl are mixed, material is put into reducing mechanism
After being crushed, 34 parts of water is added into material, and material is put into agitating device, and material is stirred 60 points
Clock；The step（7）The rotating speed of middle agitating device is 275r/min；
（8）Step will be passed through（7）Reacted material is put into 530 DEG C of high temperature furnace, and carries out roasting 22 minutes, by material
It is put into and is crushed into reducing mechanism, is added into the material after crushing and pass through step（6）Reacted material, and by material
It is stirred, the material after stirring is put into processor for ultrasonic wave, after 125W ultrasonication 1 hour, by thing
Material passes through extruder grain, you can obtain bactericide.
A kind of preparation method of the organic fertilizer of antibiotic property, is comprised the following steps that：（1）By 34 parts of rape stalk, Wheat Straw
23 parts of stalk, 21 parts of soybean stalk are broken into after 3cm powder, and with 1：2 ratio adds the water of corresponding deal, is stirred when adding water
10 hours are stood after 11 hours；
（2）Material is put into fermentation vat, 17 parts of manioc waste, 6 parts of antiseptic is added, and material is subjected to general after reacting 3 days
Material takes out；
（3）Water is added into the material after fermentation, and makes the water content of material be 63%, material is stirred 46 at 51 DEG C
After minute, and material is dehydrated with 285 DEG C of heat smoke, and make the water content of material be 64%；
（4）Reacted material is put into solar energy fermentation greenhouse, and it is rotten to carry out whole storehouse heap；
（5）After material is placed 9 days in solar energy fermentation greenhouse when temperature reaches 64 DEG C, appropriate water is added, and make thing
The water content of material makes material proceed fermentation 15 days under conditions of 42%；
（7）The material of gained after fermentation is piled into bank, bank is carried out to carry out turning and throwing once after standing 4 days, later every 7
Its turning once, and records daily temperature；When the temperature after material turning is 68 DEG C, spreads material out progress and dry 20
My god, and control its water content to be 29%；
（8）By 18 parts of diatomite, 48 parts of urea, 27 parts of potassium dihydrogen phosphate, 24 parts of ammonium hydrogen carbonate, 16 parts of calcium superphosphate, potassium chloride
10 parts and 13 parts of calcium ammonium nitrate are mixed and crushed；
（9）By step（7）Product and step（8）Product mixed, and the material of generation is put into mixer
In be stirred after granulation, dry, crush, sieving, obtained product is packed.
Using a kind of experimental plot of the organic fertilizer of antibiotic property, yield effectively improves 23.23-24.54%；Fruit can be made
Full, lovely luster, resistance against diseases is strong, and antibacterial ability effectively improves 18-22%, and the micronutrient levels such as nitrogen, phosphorus, potassium is improved, can
So that nitrogen effectively improves 11-15%, P elements effectively improve 11-13%, and potassium element effectively improves 14-17%；Make for a long time
With, plant equilibrium can be accelerated to absorb trace element comprehensively, promote growth and the root system development of plant, build up resistance, it is anti-
Only pest and disease damage；After a kind of organic fertilizer of antibiotic property, the fertilizer efficiency of soil is effectively improved, the plant recovery of nutrient of fertilizer is up to
54-56%, can make continuously to use 2-3.
Above-described embodiment is only the preferred technical solution of the present invention, and is not construed as the limitation for the present invention, the present invention
The technical scheme that should be recorded with claim of protection domain, including in the technical scheme recorded of claim technical characteristic etc.
It is protection domain with alternative, i.e., equivalent substitution within this range is improved, also within protection scope of the present invention.
Claims (7)
1. a kind of organic fertilizer of antibiotic property, it is characterised in that the organic fertilizer includes following components:Rape stalk 33-36
Part, 20-25 parts of wheat stalk, 21-28 parts of soybean stalk, 11-18 parts of manioc waste, 6-11 parts of antiseptic, 18-23 parts of diatomite,
48-53 parts of urea, 24-27 parts of potassium dihydrogen phosphate, 21-25 parts of ammonium hydrogen carbonate, 14-17 parts of calcium superphosphate, 10-17 parts of potassium chloride with
And 11-13 parts of calcium ammonium nitrate.
2. a kind of organic fertilizer of antibiotic property according to claim 1, it is characterised in that：The antiseptic is included with the following group
Point：13-16 parts of tea free, 14-18 parts of folium artemisiae argyi, golden 14-18 parts of clock rattan, 16-19 parts of elscholtiza, 17-22 parts of kaolin, amino acid 8-
11 parts, 4-7 parts of starch grafted acrylate crosslinking copolymerization thing, 1-2 parts of paclobutrazol, 3-5 parts of vinegar and thiophanate methyl 2-4
Part.
3. a kind of organic fertilizer of antibiotic property according to claim 2, it is characterised in that the preparation method of the antiseptic
It is as follows：（1）3-6 parts of nitrogen-fixing bacteria, thermophilic Bacillus 4-7 parts, 3-5 parts of bacillus subtilis are put in a kettle., and will be mixed
After compound is sealed 2-3 days after stirring at normal temperatures, 1-2 parts of glutathione peroxidase, color are added into material
2-3 parts of propylhomoserin protein kinase, 1-3 parts of aspergillus niger and after being mixed, material are put into PDA liquid medium, and make thing
Material reaction 3-3.5 days；
（2）After 13-16 parts of tea free, 14-18 parts of folium artemisiae argyi are pulverized and mixed, and material is put at 70-75 DEG C progress
Boiling 20-30 minutes；
（3）Ethanol will be added in golden 14-18 parts of clock rattan, 16-19 parts of elscholtiza, and material is filtered after carrying out immersion 30-40 minutes,
Added into filtrate and pass through step（2）Reacted material is simultaneously stirred, and the material after stirring is carried out to extract 4 times, each 1-
1.5 hours, merge extract solution；
（4）Step will be passed through（3）After addition carbohydrase, protease are mixed in filtrate after extraction, 22-27 parts of water is added
Water, and material is put into distilling apparatus, and material is subjected to distillation 2-4 hours；
（5）Step will be passed through（4）Material after distillation is put into filter, and material is filtered；
（6）Step will be passed through（3）Reacted extract solution is with passing through step（5）After reacted filtered fluid is mixed, add
By step（1）After reacted material is mixed, 4-7 parts of starch grafted acrylate crosslinking copolymerization thing, multiple-effect are added
1-2 parts of azoles, 3-5 parts of vinegar, and material is stirred after 1-2 days, and seal 2-3 days after material is stirred at normal temperatures
After filter, take filtered fluid；
（7）After 17-22 parts of kaolin, 8-11 parts of amino acid, 2-4 parts of thiophanate methyl are mixed, material is put into powder
After being crushed in crushing device, 33-34 parts of water is added into material, and material is put into agitating device, and material is entered
Row stirring 50-60 minutes；
（8）Step will be passed through（7）Reacted material is put into 500-530 DEG C of high temperature furnace, and carries out 19-22 points of roasting
Clock, material is put into and crushed into reducing mechanism, is added into the material after crushing and is passed through step（6）Reacted thing
Material, and material is stirred, the material after stirring is put into processor for ultrasonic wave, at 100-130W ultrasonic wave
Material is passed through extruder grain, you can obtain bactericide by reason after 1-1.5 hours.
4. a kind of organic fertilizer of antibiotic property according to claim 2, it is characterised in that：The step（3）Middle ethanol
Addition is 12-14 times of the amount of material, and the concentration of alcohol of addition is 50-58%.
5. a kind of organic fertilizer of antibiotic property according to claim 2, it is characterised in that：The step（4）Middle carbohydrase,
The mass ratio of protease is 4:5.
6. a kind of organic fertilizer of antibiotic property according to claim 2, it is characterised in that：The step（7）Middle stirring dress
The rotating speed put is 250-300r/min.
7. a kind of preparation method of the organic fertilizer of antibiotic property, it is characterised in that comprise the following steps that：（1）By rape stalk 33-
36 parts, 20-25 parts of wheat stalk, 21-28 parts of soybean stalk be broken into after 2-4cm powder, and with 1：1.5-2 ratio adds phase
The water of deal is answered, is stirred when adding water and stands 10-13 hours after 8-12 hours；
（2）Material is put into fermentation vat, 11-18 parts of manioc waste, 6-11 parts of antiseptic is added, and material is subjected to reaction 1-
Material is taken out after 3 days；
（3）Water is added into the material after fermentation, and makes the water content of material for 61-63%, material is carried out at 51-56 DEG C
After stirring 43-47 minutes, and material is dehydrated with 270-285 DEG C of heat smoke, and make the water content of material for 60-
64%；
（4）Reacted material is put into solar energy fermentation greenhouse, and it is rotten to carry out whole storehouse heap；
（5）After material is placed 7-9 days in solar energy fermentation greenhouse when temperature reaches 60-64 DEG C, appropriate water is added, and
Make the water content of material under conditions of 39-42%, and material is proceeded fermentation 13-17 days；
（7）The material of gained after fermentation is piled into bank, bank is carried out to carry out turning and throwing once after standing 4 days, later every 7
Its turning once, and records daily temperature；When the temperature after material turning is 63-68 DEG C, material is spread out and dried in the air
Shine 18-20 days, and control its water content to be 25-29%；
（8）By 18-23 parts of diatomite, 48-53 parts of urea, 24-27 parts of potassium dihydrogen phosphate, 21-25 parts of ammonium hydrogen carbonate, calcium superphosphate
11-13 parts of 14-17 parts, 10-17 parts of potassium chloride and calcium ammonium nitrate are mixed and crushed；
（9）By step（7）Product and step（8）Product mixed, and the material of generation is put into mixer
In be stirred after granulation, dry, crush, sieving, obtained product is packed.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107759319A (en) * | 2017-10-25 | 2018-03-06 | 盘泽昌 | Promote the preparation method of the pear tree fertilizer of result |
| CN108046914A (en) * | 2017-12-22 | 2018-05-18 | 胡守军 | A kind of compound disease-resistant base manure of grape |
| CN108083902A (en) * | 2017-12-22 | 2018-05-29 | 胡守军 | A kind of compound disease-resistant biological base manure of grape |
| CN108308206A (en) * | 2018-01-24 | 2018-07-24 | 合肥华盖生物科技有限公司 | A kind of fish pelargonium is aestivated special resistance reinforcing agent |
| CN109796243A (en) * | 2017-11-16 | 2019-05-24 | 江苏小潘园生态农业科技发展有限公司 | A kind of aquatic vegetable floating fern contains potassic fertilizer |
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| CN103992163A (en) * | 2014-04-18 | 2014-08-20 | 南京明珠肥料有限责任公司 | Production process of organic inorganic compound fertilizer |
| CN105198596A (en) * | 2015-09-29 | 2015-12-30 | 宁国市汉唐盛世农林开发有限公司 | Preparation method of insecticidal and growth-promoting organic fertilizer special for blueberry |
| CN105294320A (en) * | 2015-12-03 | 2016-02-03 | 青岛华仁技术孵化器有限公司 | Special drought-resistant high-efficiency composite fertilizer for planting corns |
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| CN103992163A (en) * | 2014-04-18 | 2014-08-20 | 南京明珠肥料有限责任公司 | Production process of organic inorganic compound fertilizer |
| CN105198596A (en) * | 2015-09-29 | 2015-12-30 | 宁国市汉唐盛世农林开发有限公司 | Preparation method of insecticidal and growth-promoting organic fertilizer special for blueberry |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107759319A (en) * | 2017-10-25 | 2018-03-06 | 盘泽昌 | Promote the preparation method of the pear tree fertilizer of result |
| CN109796243A (en) * | 2017-11-16 | 2019-05-24 | 江苏小潘园生态农业科技发展有限公司 | A kind of aquatic vegetable floating fern contains potassic fertilizer |
| CN108046914A (en) * | 2017-12-22 | 2018-05-18 | 胡守军 | A kind of compound disease-resistant base manure of grape |
| CN108083902A (en) * | 2017-12-22 | 2018-05-29 | 胡守军 | A kind of compound disease-resistant biological base manure of grape |
| CN108308206A (en) * | 2018-01-24 | 2018-07-24 | 合肥华盖生物科技有限公司 | A kind of fish pelargonium is aestivated special resistance reinforcing agent |
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Application publication date: 20170818 |