CN107056443A - A kind of early rice plantation high sustained release compoiste fertilizer and preparation method thereof - Google Patents

A kind of early rice plantation high sustained release compoiste fertilizer and preparation method thereof Download PDF

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CN107056443A
CN107056443A CN201710244373.7A CN201710244373A CN107056443A CN 107056443 A CN107056443 A CN 107056443A CN 201710244373 A CN201710244373 A CN 201710244373A CN 107056443 A CN107056443 A CN 107056443A
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parts
early rice
sustained release
potassium
sulfate
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高青山
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

Compoiste fertilizer is sustained with high the invention discloses a kind of plantation of early rice, its raw material includes urea, MAP, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, ferrous sulfate, manganese sulfate, zinc sulfate, ammonium molybdate, multiple ammonium nitrate, peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste, borax, biological function bacterium, modified sustained release agent and filler.The invention also discloses a kind of preparation method of the above-mentioned high sustained release compoiste fertilizer of early rice plantation.The compoiste fertilizer of the present invention applies to the plantation of early rice, and abundant nutriment can be provided for early rice, nutrition in a balanced way is provided for the whole growth course of early rice, and the supply of nutriment is efficiently high-quality, effectively increases the yield and quality of early rice.

Description

A kind of early rice plantation high sustained release compoiste fertilizer and preparation method thereof
Technical field
The present invention relates to the technical field of fertilizer, more particularly to a kind of plantation of early rice high sustained release compoiste fertilizer and its system Preparation Method.
Background technology
China is Rice Cropping big country, and current Rice Cropping is mostly straight fertilizer with fertilizer, due to straight fertilizer cost It is low, current China's Rice Production with fertilizer still using the straight fertilizer such as carbon ammonium, urea, calcium superphosphate or calcium magnesium phosphate, potassium chloride as Main, for peasant, although China widelys popularize Formula fertilization by soil testing, how scientific and reasonable fertilising is still difficult.When Before, compound compound fertilizer development trend is very fast, but compound fertilizer formula is using chaotic, irrational to be formulated applied to crops more Crop production reduction or fertilizer loss aggravation are easily caused, and with economic development, peasant's fertilising pursuit recruitment is few and operation is simple Single single fertilization, and fertilizer release rule and crop growth demand in soil is complete on the contrary, so causing seedling stage to need Soil nutrient content reaches highest when fertilizer is few, and soil nutrient is but preferably minimized when needing fertile more into growth period, therefore current Fertilizer and corresponding fertilizer practice so that China's utilization rate of fertilizer is chronically at reduced levels, have had a strong impact on the kind grain of peasant Enthusiasm, and significant negative effect is produced to environment, it is unfavorable for building the Modern Agriculture of the high-yield and high-efficiency of China's sustainable development Industry technical system.So design a kind of early rice plantation solves the problems of the prior art with height sustained release compoiste fertilizer.
The content of the invention
To solve technical problem present in background technology, the present invention proposes a kind of early rice plantation with high sustained release organic composite Fertilizer and preparation method thereof, the compoiste fertilizer prepared applies to the plantation of early rice, and abundant nutrition can be provided for early rice Material, nutrition in a balanced way is provided for the whole growth course of early rice, and the supply of nutriment is efficiently high-quality, effectively increases early rice Yield and quality.
A kind of early rice plantation proposed by the present invention is included by weight with high sustained release compoiste fertilizer, its raw material:Urea 15- 25 parts, 3-9 parts of MAP, 2-4 parts of potassium fulvate, 1-4 parts of ammonium chloride, 3-5 parts of diammonium hydrogen phosphate, 2-4 parts of potassium dihydrogen phosphate, 3-6 parts of dipotassium hydrogen phosphate, 3.5-4.5 parts of potassium chloride, 1-3 parts of potassium sulfate, 2-4 parts of ferrous sulfate, 3-5 parts of manganese sulfate, zinc sulfate 3-6 parts, again 1-4 parts of ammonium molybdate, 2-5 parts of ammonium nitrate, 5-15 parts of peanut press pulp, 6-12 parts of dregs of beans, 8-16 parts of excrement of animals, cotton dregs powder 4- 8 parts, 6-12 parts of manioc waste, 4-8 parts of borax, 2-5 parts of biological function bacterium, modified 3-9 parts of sustained release agent, 4-9 parts of filler.
Preferably, biological function bacterium is by bifidocaterium, photosynthetic bacteria and acetic acid bacteria 1-3 by weight:2-5:0.5-1.5 is mixed Uniformly.
Preferably, the raw material of filler includes by weight:2-5 parts of maize straw, 2-4 parts of rapeseed cake, 2-4 parts of soya-bean cake, cow dung 3-5 parts, 2-4 parts of powdered rice hulls, 2-5 parts of furfural dregs, 3-5 parts of bacteria residue, 2-5 parts of vermiculite, 3-6 parts of pulverized limestone, 4-8 parts of borax, silkworm excrement 2-5 parts.
Preferably, filler is prepared by following technique:By maize straw, rapeseed cake, soya-bean cake, cow dung, powdered rice hulls, furfural Accumulated after slag, bacteria residue, vermiculite, pulverized limestone, borax and silkworm excrement mixing, room temperature 3-5d is crushed to 15-25 mesh and produces filler.
Preferably, modified sustained release agent is prepared by following technique:By dimethyl diallyl ammonium chloride, dodecyl three Ammonio methacrylate, kaolin, attapulgite and bentonite are well mixed, in 650-850r/min rotating speed magnetic agitations 10- 20min, then heats to 70-90 DEG C, is incubated 1-3h, is cooled to 50-70 DEG C, adds potassium dihydrogen phosphate, acrylic acid, N, N- methylenes Base bisacrylamide and ammonium persulfate are well mixed, are warming up to 60-70 DEG C, are incubated 3-4h, are then stayed overnight with soaked in absolute ethyl alcohol, After washing, it is placed in 70-80 DEG C of baking oven and dries to constant weight, size-reduced sieving obtains being modified sustained release agent.
Preferably, in the preparation technology of modified sustained release agent, dimethyl diallyl ammonium chloride, trimethyl chlorination Ammonium, kaolin, attapulgite, bentonite, potassium dihydrogen phosphate, acrylic acid, N,N methylene bis acrylamide and ammonium persulfate Weight ratio is 2-5:1-3:2-4:3-5:4-6:2-6:1-4:3-6:2-5.
A kind of early rice plantation of present invention preparation method of high sustained release compoiste fertilizer, comprises the following steps:
S1, by peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste and borax it is well mixed after, be ground into 30-50 mesh Room temperature is cooled to after material, primary drying, biological function bacterium is then added and ferments at room temperature 2-4d, be subsequently added into urea, phosphorus A sour ammonium, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, sulfuric acid are sub- Iron, manganese sulfate, zinc sulfate, ammonium molybdate and multiple ammonium nitrate are well mixed, and are ground into after 20-40 mesh, redrying and are cooled to room temperature thing Expect a;
S2, material a and filler be well mixed, be warming up to 50-70 DEG C, slurry is stirred into 3500-5500r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 25-30rpm, forms fertilizer Expect particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 50-60 DEG C, deliver to sustained release agent bag Coating is carried out in film machine and using the modification sustained release agent of proportioning, the sustained release agent coating machine rotating speed is 10-15rpm;
S5, it will be dried by the fertiliser granulates of coating by dispelling, being cooled to room temperature, to obtain high yield slow-release bio matter organic Fertilizer.
A kind of early rice plantation proposed by the present invention includes urea, MAP, Huang with high sustained release compoiste fertilizer, its raw material Rotten acid potassium, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, ferrous sulfate, manganese sulfate, Zinc sulfate, ammonium molybdate, multiple ammonium nitrate, peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste, borax, biological function bacterium, modification Sustained release agent and filler.It is with urea, MAP, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, phosphoric acid hydrogen two Potassium, potassium chloride, potassium sulfate, ferrous sulfate, manganese sulfate, zinc sulfate, ammonium molybdate and multiple ammonium nitrate are supplemented as inorganic nutritive element and expected, Using peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder and manioc waste as organic material, using borax and filler as hole material is increased, with biology Function bacterium is supplemented as microorganism species expects, the early rice plantation height sustained release obtained after the coating of modified sustained release agent is organic multiple Hefei disclosure satisfy that the nutritional need in early rice growth course, and with excellent sustained release performance, can avoid soil hardening, have Effect improves the yield and quality of early rice.Wherein, biological function bacterium is mixed by a certain percentage by bifidocaterium, photosynthetic bacteria and acetic acid bacteria Close uniform, in the plantation for applying to early rice, the organic matter for the soil that can effectively degrade for early rice absorption, and can purification soil, For the microorganism species needed for plant root provides the more growth in Jiankang, the growth of early rice is promoted, the production of early rice is improved Amount and quality.Wherein, the filler of addition is by by maize straw, rapeseed cake, soya-bean cake, cow dung, powdered rice hulls, furfural dregs, bacteria residue, leech Accumulated after stone, pulverized limestone, borax and silkworm excrement mixing, room temperature, crushing produces filler, can not only supplement organic material, moreover it is possible to The increasing hole to organic fertilizer is realized, gas permeability is improved, enhances sustained release performance, more attachment positions are provided for organic and inorganic material Point.The modification sustained release agent wherein added is by by dimethyl diallyl ammonium chloride, DTAC, kaolinite Soil, attapulgite and bentonite are well mixed, in magnetic agitation, then heat up, and are incubated, and cooling adds potassium dihydrogen phosphate, propylene Acid, N, N- methylene-bisacrylamides and ammonium persulfate are well mixed, are incubated, are then stayed overnight with soaked in absolute ethyl alcohol after heating, After washing, it is placed in baking oven and dries to constant weight, size-reduced sieving obtains being modified sustained release agent, applies to the preparation of high Slow release organic fertilizer In, the slow release of height sustained release compoiste fertilizer of the invention can be effectively improved, and coordinate with filler, the imparting present invention is excellent to be delayed Release performance.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair In bright protection domain.
In embodiment, the parts by weight of urea can for 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts;The parts by weight of MAP can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts;The parts by weight of potassium fulvate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts; The parts by weight of ammonium chloride can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts;The parts by weight of diammonium hydrogen phosphate can be with For 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of potassium dihydrogen phosphate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts;Phosphorus The parts by weight of sour hydrogen dipotassium can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts;The parts by weight of potassium chloride can be 3.5 parts, 3.6 parts, 3.7 parts, 3.8 parts, 3.9 parts, 4.0 parts, 4.1 parts, 4.2 parts, 4.3 parts, 4.4 parts, 4.5 parts;The weight of potassium sulfate It can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts to measure part;The parts by weight of ferrous sulfate can for 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 Part;The parts by weight of manganese sulfate can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of zinc sulfate can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts;The parts by weight of ammonium molybdate can for 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 Part;The parts by weight of multiple ammonium nitrate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of peanut press pulp can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts;The parts by weight of dregs of beans can for 6 parts, 7 parts, 8 Part, 9 parts, 10 parts, 11 parts, 12 parts;The parts by weight of excrement of animals can for 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts;The parts by weight of cotton dregs powder can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;Wood The parts by weight of potato slag can be 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts;The parts by weight of borax can for 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;The parts by weight of biological function bacterium can for 2 parts, 2.5 parts, 3 parts, 3.5 Part, 4 parts, 4.5 parts, 5 parts;The parts by weight of modified sustained release agent can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts;The weight of filler It can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts to measure part.
Embodiment 1
A kind of early rice plantation proposed by the present invention is included by weight with high sustained release compoiste fertilizer, its raw material:Urea 20 Part, 6 parts of MAP, 3 parts of potassium fulvate, 2.5 parts of ammonium chloride, 4 parts of diammonium hydrogen phosphate, 3 parts of potassium dihydrogen phosphate, dipotassium hydrogen phosphate 4.5 parts, 4 parts of potassium chloride, 2 parts of potassium sulfate, 3 parts of ferrous sulfate, 4 parts of manganese sulfate, 4.5 parts of zinc sulfate, 2.5 parts of ammonium molybdate, multiple nitre 3.5 parts of ammonium, 10 parts of peanut press pulp, 9 parts of dregs of beans, 12 parts of excrement of animals, 6 parts of cotton dregs powder, 9 parts of manioc waste, 6 parts of borax, biological function 3.5 parts of bacterium, modified 6 parts of sustained release agent, 6.5 parts of filler.
Embodiment 2
A kind of early rice plantation proposed by the present invention is included by weight with high sustained release compoiste fertilizer, its raw material:Urea 15 Part, 9 parts of MAP, 2 parts of potassium fulvate, 4 parts of ammonium chloride, 3 parts of diammonium hydrogen phosphate, 4 parts of potassium dihydrogen phosphate, dipotassium hydrogen phosphate 3 Part, 4.5 parts of potassium chloride, 1 part of potassium sulfate, 4 parts of ferrous sulfate, 3 parts of manganese sulfate, 6 parts of zinc sulfate, 1 part of ammonium molybdate, multiple 5 parts of ammonium nitrate, 5 parts of peanut press pulp, 12 parts of dregs of beans, 8 parts of excrement of animals, 8 parts of cotton dregs powder, 6 parts of manioc waste, 8 parts of borax, 2 parts of biological function bacterium, modification 9 parts of sustained release agent, 4 parts of filler.
Biological function bacterium is by bifidocaterium, photosynthetic bacteria and acetic acid bacteria by weight 1:5:0.5 is well mixed.
Wherein, filler is prepared by following technique:By weight by 2 parts of maize straws, 4 parts of rapeseed cakes, 2 portions of soya-bean cakes, 5 parts Heap after cow dung, 2 parts of powdered rice hulls, 5 parts of furfural dregs, 3 parts of bacteria residues, 5 parts of vermiculites, 3 parts of pulverized limestones, 8 parts of boraxs and 2 parts of silkworm excrement mixing Product, room temperature 5d is crushed to 15 mesh and produces filler.
Wherein, modified sustained release agent is prepared by following technique:By weight by 2 parts of dimethyl diallyl ammonium chlorides, 3 Part DTAC, 2 parts of kaolin, 5 parts of attapulgites and 4 parts of bentonites are well mixed, and are turned in 850r/min Fast magnetic agitation 10min, then heats to 90 DEG C, is incubated 1h, is cooled to 70 DEG C, add 2 parts of potassium dihydrogen phosphates, 4 parts of acrylic acid, 3 parts of N, N- methylene-bisacrylamides and 5 parts of ammonium persulfates are well mixed, and are warming up to 60 DEG C, are incubated 4h, then use absolute ethyl alcohol Soaked overnight, after washing, is placed in 70 DEG C of baking ovens and dries to constant weight, size-reduced sieving obtains being modified sustained release agent.
Embodiment 3
A kind of early rice plantation proposed by the present invention is included by weight with high sustained release compoiste fertilizer, its raw material:Urea 25 Part, 3 parts of MAP, 4 parts of potassium fulvate, 1 part of ammonium chloride, 5 parts of diammonium hydrogen phosphate, 2 parts of potassium dihydrogen phosphate, dipotassium hydrogen phosphate 6 Part, 3.5 parts of potassium chloride, 3 parts of potassium sulfate, 2 parts of ferrous sulfate, 5 parts of manganese sulfate, 3 parts of zinc sulfate, 4 parts of ammonium molybdate, multiple 2 parts of ammonium nitrate, 15 parts of peanut press pulp, 6 parts of dregs of beans, 16 parts of excrement of animals, 4 parts of cotton dregs powder, 12 parts of manioc waste, 4 parts of borax, 5 parts of biological function bacterium, change 3 parts of sustained release agent of property, 9 parts of filler.
A kind of early rice plantation of present invention preparation method of high sustained release compoiste fertilizer, comprises the following steps:
S1, by peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste and borax it is well mixed after, be ground into 50 mesh things Material, is cooled to room temperature after primary drying, then adds biological function bacterium and ferments at room temperature 2d, is subsequently added into urea, phosphoric acid one Ammonium, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, ferrous sulfate, sulphur Sour manganese, zinc sulfate, ammonium molybdate and multiple ammonium nitrate are well mixed, and are ground into after 40 mesh, redrying and are cooled to room temperature material a;
S2, material a and filler be well mixed, be warming up to 50 DEG C, slurry is stirred into 5500r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 25rpm, forms fertilizer Particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 60 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 10rpm;
S5, it will be dried by the fertiliser granulates of coating by dispelling, being cooled to room temperature, to obtain high yield slow-release bio matter organic Fertilizer.
Embodiment 4
A kind of early rice plantation proposed by the present invention is included by weight with high sustained release compoiste fertilizer, its raw material:Urea 18 Part, 8 parts of MAP, 2.5 parts of potassium fulvate, 3 parts of ammonium chloride, 3.5 parts of diammonium hydrogen phosphate, 3.5 parts of potassium dihydrogen phosphate, phosphoric acid hydrogen 4 parts of dipotassium, 4.2 parts of potassium chloride, 1.5 parts of potassium sulfate, 3.5 parts of ferrous sulfate, 3.5 parts of manganese sulfate, 5 parts of zinc sulfate, ammonium molybdate 2 Part, multiple 4 parts of ammonium nitrate, 8 parts of peanut press pulp, 11 parts of dregs of beans, 9 parts of excrement of animals, 7 parts of cotton dregs powder, 8 parts of manioc waste, 7 parts of borax, biology 3 parts of function bacterium, modified 8 parts of sustained release agent, 5 parts of filler.
Biological function bacterium is by bifidocaterium, photosynthetic bacteria and acetic acid bacteria by weight 1.5:4:0.8 is well mixed.
Wherein, filler is prepared by following technique:By weight by 3 parts of maize straws, 3.5 parts of rapeseed cakes, 2.5 parts of beans Cake, 4.5 parts of cow dungs, 2.5 parts of powdered rice hulls, 4 parts of furfural dregs, 3.5 parts of bacteria residues, 4 parts of vermiculites, 4 parts of pulverized limestones, 7 parts of boraxs and 3 portions of silkworms Accumulated after sand mixing, room temperature 4.5d is crushed to 18 mesh and produces filler.
Wherein, modified sustained release agent is prepared by following technique:By weight by 3 parts of dimethyl diallyl ammonium chlorides, 2.5 parts of DTACs, 2.5 parts of kaolin, 4.5 parts of attapulgites and 4.5 parts of bentonites are well mixed, in 820r/min rotating speed magnetic agitation 12min, then heat to 85 DEG C, are incubated 1.5h, are cooled to 65 DEG C, add 3 parts of biphosphates Potassium, 3 parts of acrylic acid, 4 parts of N, N- methylene-bisacrylamides and 4 parts of ammonium persulfates are well mixed, and are warming up to 62 DEG C, insulation 3.8h, is then stayed overnight with soaked in absolute ethyl alcohol, after washing, is placed in 72 DEG C of baking ovens and is dried to constant weight, size-reduced sieving is changed Property sustained release agent.
A kind of early rice plantation of present invention preparation method of high sustained release compoiste fertilizer, comprises the following steps:
S1, by peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste and borax it is well mixed after, be ground into 35 mesh things Material, is cooled to room temperature after primary drying, then adds biological function bacterium and ferments at room temperature 3.5d, is subsequently added into urea, phosphoric acid One ammonium, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, ferrous sulfate, Manganese sulfate, zinc sulfate, ammonium molybdate and multiple ammonium nitrate are well mixed, and are ground into after 25 mesh, redrying and are cooled to room temperature material a;
S2, material a and filler be well mixed, be warming up to 65 DEG C, slurry is stirred into 3800r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 29rpm, forms fertilizer Particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 52 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 14rpm;
S5, it will be dried by the fertiliser granulates of coating by dispelling, being cooled to room temperature, to obtain high yield slow-release bio matter organic Fertilizer.
Embodiment 5
A kind of early rice plantation proposed by the present invention is included by weight with high sustained release compoiste fertilizer, its raw material:Urea 22 Part, 4 parts of MAP, 3.5 parts of potassium fulvate, 2 parts of ammonium chloride, 4.5 parts of diammonium hydrogen phosphate, 2.5 parts of potassium dihydrogen phosphate, phosphoric acid hydrogen 5 parts of dipotassium, 3.8 parts of potassium chloride, 2.5 parts of potassium sulfate, 2.5 parts of ferrous sulfate, 4.5 parts of manganese sulfate, 4 parts of zinc sulfate, ammonium molybdate 3 Part, multiple 3 parts of ammonium nitrate, 12 parts of peanut press pulp, 7 parts of dregs of beans, 15 parts of excrement of animals, 5 parts of cotton dregs powder, 10 parts of manioc waste, 5 parts of borax, life 3 parts of thing function bacterium, modified 8 parts of sustained release agent, 5 parts of filler.
Biological function bacterium is by bifidocaterium, photosynthetic bacteria and acetic acid bacteria by weight 2.5:3:1.2 it is well mixed.
Wherein, filler is prepared by following technique:By weight by 4 parts of maize straws, 2.5 parts of rapeseed cakes, 3.5 parts of beans Cake, 3.5 parts of cow dungs, 3.5 parts of powdered rice hulls, 3 parts of furfural dregs, 4.5 parts of bacteria residues, 3 parts of vermiculites, 5 parts of pulverized limestones, 5 parts of boraxs and 4 portions of silkworms Accumulated after sand mixing, room temperature 3.5d is crushed to 22 mesh and produces filler.
Wherein, modified sustained release agent is prepared by following technique:By weight by 4 parts of dimethyl diallyl ammonium chlorides, 1.5 parts of DTACs, 3.5 parts of kaolin, 3.5 parts of attapulgites and 5.5 parts of bentonites are well mixed, in 680r/min rotating speed magnetic agitation 18min, then heat to 75 DEG C, are incubated 2.5h, are cooled to 55 DEG C, add 5 parts of biphosphates Potassium, 2 parts of acrylic acid, 5 parts of N, N- methylene-bisacrylamides and 3 parts of ammonium persulfates are well mixed, and are warming up to 68 DEG C, insulation 3.2h, is then stayed overnight with soaked in absolute ethyl alcohol, after washing, is placed in 78 DEG C of baking ovens and is dried to constant weight, size-reduced sieving is changed Property sustained release agent.
A kind of early rice plantation of present invention preparation method of high sustained release compoiste fertilizer, comprises the following steps:
S1, by peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste and borax it is well mixed after, be ground into 45 mesh things Material, is cooled to room temperature after primary drying, then adds biological function bacterium and ferments at room temperature 2.5d, is subsequently added into urea, phosphoric acid One ammonium, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, ferrous sulfate, Manganese sulfate, zinc sulfate, ammonium molybdate and multiple ammonium nitrate are well mixed, and are ground into after 35 mesh, redrying and are cooled to room temperature material a;
S2, material a and filler be well mixed, be warming up to 55 DEG C, slurry is stirred into 5200r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 26rpm, forms fertilizer Particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 58 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 11rpm;
S5, it will be dried by the fertiliser granulates of coating by dispelling, being cooled to room temperature, to obtain high yield slow-release bio matter organic Fertilizer.
By sample fertilizer before rice transplanting, by every 53kg/667m2Amount disposably apply, contrast groups are according to a conventional method Basal dressing and topdress, total fertilization amount is 70kg/667m2, fertilizer is nitrogen-phosphorus-potassium compound fertilizer, wherein, nitrogenous fertilizer and potash fertilizer are spread in two times Apply;
Yield-increasing efficiency=(experimental group yield/contrast groups yield -1) * 100%
Table 1:
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (7)

1. a kind of early rice plantation is sustained compoiste fertilizer with high, it is characterised in that its raw material includes by weight:Urea 15-25 Part, 3-9 parts of MAP, 2-4 parts of potassium fulvate, 1-4 parts of ammonium chloride, 3-5 parts of diammonium hydrogen phosphate, 2-4 parts of potassium dihydrogen phosphate, phosphorus Sour 3-6 parts of hydrogen dipotassium, 3.5-4.5 parts of potassium chloride, 1-3 parts of potassium sulfate, 2-4 parts of ferrous sulfate, 3-5 parts of manganese sulfate, zinc sulfate 3-6 Part, 1-4 parts of ammonium molybdate, multiple 2-5 parts of ammonium nitrate, 5-15 parts of peanut press pulp, 6-12 parts of dregs of beans, 8-16 parts of excrement of animals, cotton dregs powder 4-8 Part, 6-12 parts of manioc waste, 4-8 parts of borax, 2-5 parts of biological function bacterium, modified 3-9 parts of sustained release agent, 4-9 parts of filler.
2. early rice plantation according to claim 1 is sustained compoiste fertilizer with high, it is characterised in that biological function bacterium is by double Qi bacterium, photosynthetic bacteria and acetic acid bacteria are by weight 1-3:2-5:0.5-1.5 is well mixed.
3. early rice plantation according to claim 1 or 2 is sustained compoiste fertilizer with high, it is characterised in that the raw material of filler Include by weight:2-5 parts of maize straw, 2-4 parts of rapeseed cake, 2-4 parts of soya-bean cake, 3-5 parts of cow dung, 2-4 parts of powdered rice hulls, furfural dregs 2- 5 parts, 3-5 parts of bacteria residue, 2-5 parts of vermiculite, 3-6 parts of pulverized limestone, 4-8 parts of borax, 2-5 parts of silkworm excrement.
4. the early rice plantation according to claim any one of 1-3 is sustained compoiste fertilizer with high, it is characterised in that filler is pressed It is prepared by following technique:By maize straw, rapeseed cake, soya-bean cake, cow dung, powdered rice hulls, furfural dregs, bacteria residue, vermiculite, pulverized limestone, boron Accumulated after sand and silkworm excrement mixing, room temperature 3-5d is crushed to 15-25 mesh and produces filler.
5. the early rice plantation according to claim any one of 1-4 is sustained compoiste fertilizer with high, it is characterised in that modified slow Agent is released to be prepared by following technique:By dimethyl diallyl ammonium chloride, DTAC, kaolin, recessed Convex rod soil and bentonite are well mixed, and in 650-850r/min rotating speed magnetic agitation 10-20min, then heat to 70-90 DEG C, 1-3h is incubated, 50-70 DEG C is cooled to, potassium dihydrogen phosphate, acrylic acid, N is added, N- methylene-bisacrylamides and ammonium persulfate are mixed Close uniform, be warming up to 60-70 DEG C, be incubated 3-4h, then stayed overnight, after washing, be placed in 70-80 DEG C of baking oven with soaked in absolute ethyl alcohol Dry to constant weight, size-reduced sieving obtains being modified sustained release agent.
6. the early rice plantation according to claim any one of 1-5 is sustained compoiste fertilizer with high, it is characterised in that modified slow It is dimethyl diallyl ammonium chloride, DTAC, kaolin, attapulgite, swollen in the preparation technology for releasing agent The weight ratio for moistening soil, potassium dihydrogen phosphate, acrylic acid, N,N methylene bis acrylamide and ammonium persulfate is 2-5:1-3:2-4:3- 5:4-6:2-6:1-4:3-6:2-5.
7. a kind of early rice plantation according to claim any one of 1-6 preparation method of high sustained release compoiste fertilizer, its It is characterised by, comprises the following steps:
S1, by peanut press pulp, dregs of beans, excrement of animals, cotton dregs powder, manioc waste and borax it is well mixed after, be ground into 30-50 mesh things Material, is cooled to room temperature after primary drying, then adds biological function bacterium and ferments at room temperature 2-4d, is subsequently added into urea, phosphoric acid One ammonium, potassium fulvate, ammonium chloride, diammonium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, potassium chloride, potassium sulfate, ferrous sulfate, Manganese sulfate, zinc sulfate, ammonium molybdate and multiple ammonium nitrate are well mixed, and are ground into after 20-40 mesh, redrying and are cooled to room temperature material a;
S2, material a and filler be well mixed, be warming up to 50-70 DEG C, slurry is stirred into 3500-5500r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 25-30rpm, forms fertilizer Grain;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 50-60 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 10-15rpm;
S5, the fertiliser granulates that will pass through coating are dried by dispelling, are cooled to room temperature and obtain high yield slow-release bio matter organic fertilizer.
CN201710244373.7A 2017-04-14 2017-04-14 A kind of early rice plantation high sustained release compoiste fertilizer and preparation method thereof Withdrawn CN107056443A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107778088A (en) * 2017-11-25 2018-03-09 安徽正丰农业科技有限公司 A kind of rice breeding dedicated fertilizer
CN108440154A (en) * 2018-06-04 2018-08-24 芜湖通农生态农业有限公司 A kind of special the fertilizer of retaining water and releasing nutrients slowly of Nursery Stock
CN112279731A (en) * 2020-10-22 2021-01-29 广西晋有有机肥有限公司 Water-soluble fertilizer
CN117063655A (en) * 2023-08-15 2023-11-17 湖南省土壤肥料研究所 Method for preventing and controlling rice field submerged cultivation and cooperatively reducing cadmium in water flooding environment

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106396982A (en) * 2016-11-29 2017-02-15 袁家和 Compound fertilizer having growth promotion and high slow-release properties and used for rice planting as well as preparation method of compound fertilizer

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106396982A (en) * 2016-11-29 2017-02-15 袁家和 Compound fertilizer having growth promotion and high slow-release properties and used for rice planting as well as preparation method of compound fertilizer

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107778088A (en) * 2017-11-25 2018-03-09 安徽正丰农业科技有限公司 A kind of rice breeding dedicated fertilizer
CN108440154A (en) * 2018-06-04 2018-08-24 芜湖通农生态农业有限公司 A kind of special the fertilizer of retaining water and releasing nutrients slowly of Nursery Stock
CN112279731A (en) * 2020-10-22 2021-01-29 广西晋有有机肥有限公司 Water-soluble fertilizer
CN117063655A (en) * 2023-08-15 2023-11-17 湖南省土壤肥料研究所 Method for preventing and controlling rice field submerged cultivation and cooperatively reducing cadmium in water flooding environment
CN117063655B (en) * 2023-08-15 2024-04-23 湖南省土壤肥料研究所 Method for preventing and controlling rice field submerged cultivation and cooperatively reducing cadmium in water flooding environment

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Application publication date: 20170818