CN106977295A - A kind of oxygen supply type growth promotion flowers compoiste fertilizer - Google Patents
A kind of oxygen supply type growth promotion flowers compoiste fertilizer Download PDFInfo
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- CN106977295A CN106977295A CN201710266404.9A CN201710266404A CN106977295A CN 106977295 A CN106977295 A CN 106977295A CN 201710266404 A CN201710266404 A CN 201710266404A CN 106977295 A CN106977295 A CN 106977295A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B3/00—Fertilisers based essentially on di-calcium phosphate
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of oxygen supply type growth promotion flowers compoiste fertilizer, its raw material includes dry pond sludge, modified oxygenation agent, modified sustained release agent, modified filler, urea, MAP, potassium chloride, ammonium chloride, diammonium hydrogen phosphate, calcium dihydrogen phosphate, zinc sulfate, ammonium molybdate, magnesium sulfate, oyster shell powder, kaolin powder, talcum powder, dolomite rock powder, takes stone flour, thiocarbamide, dicyandiamide, chicken manure, cicada excrement, wormcast, maize straw, rapeseed cake, bagasse, flyash, purple perilla seed, humic acid and EM strains.The compoiste fertilizer of the present invention can provide abundant nutriment for the growth of flowers, and the oxygen of abundance can be provided for the basic growth of flowers, effectively facilitated the growth of flowers, improved the survival rate of flowers.
Description
Technical field
The present invention relates to technical field of fertilizers, more particularly to a kind of oxygen supply type growth promotion flowers compoiste fertilizer.
Background technology
Organic fertilizer on the market is only that soil supplies nutrients and trace element mostly at present, and what is had has the slow of sustained release performance
The sustained release performance of organic fertilizer can be improved by releasing fertilizer, but for flowers, the content requirement to oxygen in soil is very high, current city
Organic fertilizer on face can not be fed for the oxygen in soil, therefore it is organic to continue a kind of oxygen supply type growth promotion flowers of design
Composite fertilizer solves the problems of the prior art.
The content of the invention
To solve technical problem present in background technology, the present invention proposes a kind of oxygen supply type growth promotion flowers organic composite
Fertilizer, can provide abundant nutriment for the growth of flowers, and the oxygen of abundance can be provided for the basic growth of flowers, have
Effect promotes the growth of flowers, improves the survival rate of flowers.
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes by weight：Dry pond sludge
20-50 parts, modified 6-9 part of oxygenation agent, 5-15 parts of sustained release agent of modification, 4-9 parts of modified filler, 15-25 parts of urea, MAP 3-
9 parts, 2-4 parts of potassium chloride, 1-4 parts of ammonium chloride, 3-5 parts of diammonium hydrogen phosphate, 2-4 parts of calcium dihydrogen phosphate, 3-6 parts of zinc sulfate, molybdic acid
1-4 parts of ammonium, 2-5 parts of magnesium sulfate, 1-4 parts of oyster shell powder, 2-4 parts of kaolin powder, 3-6 parts of talcum powder, 1-4 parts of dolomite rock powder, take
3-6 parts of stone flour, 4-8 parts of thiocarbamide, 2-5 parts of dicyandiamide, 5-15 parts of chicken manure, 2-8 parts of cicada excrement, 3-9 parts of wormcast, maize straw 1-4
Part, 2-5 parts of rapeseed cake, 4-8 parts of bagasse, 2-6 parts of flyash, 4-8 parts of purple perilla seed, 2-5 parts of humic acid, 4-8 parts of EM strains.
Preferably, modified oxygenation agent is prepared by following technique：By hydrogen peroxide, the urea that mass fraction is 25-35%
Well mixed with calgon, constant temperature is stirred after heating water bath, is then added calcium sulfate land plaster and is well mixed, then in ice
Cooled down in water-bath, by filter cake in drying at room temperature after suction filtration, then add clay, lignin and water and be well mixed, be incubated after heating,
It is cooled to after room temperature and is dried to obtain modified oxygenation agent.
Preferably, modified oxygenation agent is prepared by following technique：By hydrogen peroxide, the urea that mass fraction is 25-35%
Well mixed with calgon, heating water bath is warming up to 25-35 DEG C, and then constant temperature stirring 5-15min adds calcium sulfate gypsum
Powder is well mixed, and stirs 5-15min, is then cooled to filter cake in ice-water bath after 0-5 DEG C, suction filtration in drying at room temperature, then
Add clay, lignin and water well mixed, stir 20-40min in 3500-5500r/min rotating speeds, be then warming up to 70-90
DEG C, 20-40min is incubated, is cooled to after room temperature and is dried to obtain modified oxygenation agent.
Preferably, in the preparation technology of modified oxygenation agent, mass fraction is 25-35% hydrogen peroxide, urea, hexa metaphosphoric acid
Sodium, calcium sulfate land plaster, the weight ratio of clay and lignin are 2-5：1-3：3-6：3-5：1-4：3-6.
Preferably, the raw material of modified sustained release agent includes by weight：2-5 parts of itaconic acid, 4-8 parts of deionized water, hydroxide
1-3 parts of sodium solution, 2-6 parts of acrylamide, 3-5 parts of NVP, N, 2-6 parts of N- methylene bisacrylamide acid amides, change
3-9 parts of starch of property, N, 2-5 parts of N- dimethylene formamides, 1-4 parts of phytic acid, 3-6 parts of urea, 2-4 parts of ammonium persulfate, sulfurous acid
2-8 parts of hydrogen sodium.
Preferably, modified sustained release agent in following technique by being prepared：Itaconic acid and deionized water are well mixed, then
The well mixed material a for obtaining degree of neutralization for 55-75% of sodium hydroxide solution is added, acrylamide, N- vinyl is then added
Pyrrolidones and N, N- methylene bisacrylamide acid amide are well mixed, obtain material b；By modified starch and N, N- dimethylene formyls
Amine is well mixed, and ultrasonically treated rear addition phytic acid and urea are well mixed, and 2 are incubated after heating, is filtered, dries, is cooled to room temperature
Obtain material c；Then material c is heated up, be gelatinized, be subsequently added into material b, ammonium persulfate and sodium hydrogensulfite and be well mixed, wash
Wash, with extracting after dry, pulverize, dry, pulverize, be cooled to room temperature and obtain being modified sustained release agent.
Preferably, modified sustained release agent in following technique by being prepared：Itaconic acid and deionized water are well mixed, then
The well mixed material a for obtaining degree of neutralization for 55-75% of sodium hydroxide solution is added, acrylamide, N- vinyl is then added
Pyrrolidones and N, N- methylene bisacrylamide acid amide are well mixed, obtain material b；By modified starch and N, N- dimethylene formyls
Amine is well mixed, and ultrasonically treated 20-30min is carried out in 35-45kHz, 250-350W, then adds phytic acid and urea mixing is equal
It is even, 50-90 DEG C is warming up to, 2-6h is incubated, filtering, in 45-55 DEG C of dry 20-40min, is cooled to room temperature and obtains material c；Then
Material c is warming up to 70-90 DEG C, 20-40min is gelatinized, material b, ammonium persulfate and sodium hydrogensulfite is subsequently added into and is well mixed,
Washing dries 2-3h after 50-70 DEG C, and with extracting 8-16h after crushing, 50-70 DEG C dry, pulverize, and is cooled to room temperature and is changed
Property sustained release agent.
Preferably, the raw material of modified filler includes by weight：2-5 parts of humic acid, 4-6 parts of sepiolite, attapulgite 1-4
Part, 2-5 parts of mefenacet, 3-5 parts of Klinit dregs, 1-3 parts of ochre, 1-4 parts of wooden slag, 2-4 parts of vermiculite, 3-5 parts of bentonite, silicon
3-5 parts of diatomaceous earth.
Preferably, modified filler is prepared by following technique：By humic acid, sepiolite, attapulgite, Klinit dregs,
Ochre, wooden slag, vermiculite, bentonite and diatomite in powder, which are broken to after 20-40 mesh, to be accumulated, and then room temperature 3-5d adds benzene thiophene acyl
Careless amine is well mixed, and is incubated, is then mixed with water after heating, is dried, modified filler must be beaten by being cooled to room temperature.
Preferably, modified filler is prepared by following technique：By humic acid, sepiolite, attapulgite, Klinit dregs,
Ochre, wooden slag, vermiculite, bentonite and diatomite in powder, which are broken to after 20-40 mesh, to be accumulated, and then room temperature 3-5d adds benzene thiophene acyl
Careless amine is well mixed, and is warming up to 50-60 DEG C, is incubated 1-3h, is then mixed with water, in the stirring of 1500-2500r/min rotating speeds
20-40min, then in 40-50 DEG C of dry 2-4h, modified filler must be beaten by being cooled to room temperature.
The preparation method of the present invention, comprises the following steps：
S1, by dry pond sludge, peanut press pulp, dregs of beans, stalk, schlempe, perlite, mushroom slag and pig manure it is well mixed after, be ground into
30-50 mesh materials, room temperature is cooled to after drying, and is then added biological function bacterium and is fermented at room temperature 2-4d, is subsequently added into cassava
Slag, ispol, urea, potassium chloride, ammonium nitrate, ammonium molybdate, potassium sulfate, borax, manganese sulfate, zinc sulfate, biphosphate
Potassium and phosphoric acid powder are well mixed, are ground into 20-40 mesh, and room temperature material a is cooled to after drying；
S2, material a, modified oxygenation agent and modified filler be well mixed, 50-70 DEG C be warming up to, in 3500-5500r/
Min stirs into slurry；
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 25-30rpm, forms fertilizer
Expect particle；
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 50-60 DEG C, deliver to sustained release agent bag
Coating is carried out in film machine and using the modification sustained release agent of proportioning, the sustained release agent coating machine rotating speed is 10-15rpm；
S5, it will be dried by the fertiliser granulates of coating by dispelling, being cooled to room temperature and obtaining oxygen supply type growth promotion flowers has
Machine composite fertilizer.
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes dry pond sludge, modified oxygenation
Agent, modified sustained release agent, modified filler, urea, MAP, potassium chloride, ammonium chloride, diammonium hydrogen phosphate, calcium dihydrogen phosphate, sulfuric acid
Zinc, ammonium molybdate, magnesium sulfate, oyster shell powder, kaolin powder, talcum powder, dolomite rock powder, take stone flour, thiocarbamide, dicyandiamide, chicken manure, cicada
Excrement, wormcast, maize straw, rapeseed cake, bagasse, flyash, purple perilla seed, humic acid and EM strains.Wherein, modified oxygenation agent leads to
Cross and be well mixed hydrogen peroxide, urea and calgon, constant temperature is stirred after heating water bath, then add calcium sulfate land plaster and mix
Close uniform, then cooled down in ice-water bath, by filter cake in drying at room temperature after suction filtration, then add clay, lignin and water mixing
Uniformly, it is incubated after heating, is cooled to after room temperature and is dried to obtain modified oxygenation agent, peroxide urea energy in humidity or more than 40 DEG C
Decompose and produce oxygen, gradually soften thawing at 65-75 DEG C, and active o content declines rapidly, is melted at 75-85 DEG C and releases work
Property oxygen, contact releasing oxygen with water, acids, soluble in water, lower alcohol and ethylene glycol, ether or acetone can all make hydrogen peroxide from
Extracted in water, but this solution has an explosivity, ionic condition, copper, the lead manganese of metallic state and oxidation state, can accelerate
Peroxide urea is decomposed, and is added in organic fertilizer so that organic fertilizer can be after soil be entered so that the oxygen in soil is obtained
It is effectively increased, effectively increases the survival rate of flowers.Wherein, the modification sustained release agent of addition in following technique by being prepared：Will
Itaconic acid and deionized water are well mixed, and then addition sodium hydroxide solution is well mixed obtains material a, then adds acryloyl
Amine, NVP and N, N- methylene bisacrylamide acid amide are well mixed, obtain material b；By modified starch and N, N-
Dimethylene formamide is well mixed, and ultrasonically treated rear addition phytic acid and urea are well mixed, and 2 are incubated after heating, is filtered, is done
It is dry, it is cooled to room temperature and obtains material c；Then material c is heated up, is gelatinized, is subsequently added into material b, ammonium persulfate and bisulfite
Sodium is well mixed, washing, with extracting after dry, pulverize, be dry, pulverize, is cooled to room temperature and obtains being modified sustained release agent, with this hair
In the preparation of bright organic fertilizer, coordinated with modified oxygenation agent, not only effectively increase the sustained release performance of organic fertilizer, and effectively keep away
The hardened of soil is exempted from so that soil is more loose so that the oxygen in soil is more sufficient, has promoted the growth of flowers and deposit
Motility rate.Wherein, modified filler is by by humic acid, sepiolite, attapulgite, Klinit dregs, ochre, wooden slag, vermiculite, bentonite
Accumulated after being crushed with diatomite, room temperature, then add mefenacet and be well mixed, be incubated, then add water mixed after heating
Close uniform, dry, modified filler must be beaten by being cooled to room temperature, in the preparation for applying to organic fertilizer of the present invention, further increased
The sustained release performance of machine fertilizer, it is to avoid soil it is hardened so that soil is more loose, improve the oxygen-containing tolerance of soil, promote
The growth of flowers.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair
It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair
In bright protection domain.
In embodiment, the parts by weight of dry pond sludge can for 20 parts, 25 parts, 30 parts, 35 parts, 40 parts, 45 parts, 50
Part；The parts by weight of modified oxygenation agent can be 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts；The weight of modified sustained release agent
Part can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts；The parts by weight of modified filler can
Think 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts；The parts by weight of urea can be
15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts；The parts by weight of MAP can be
3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts；The parts by weight of potassium chloride can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；Chlorination
The parts by weight of ammonium can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of diammonium hydrogen phosphate can be 3
Part, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of calcium dihydrogen phosphate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；Zinc sulfate
Parts by weight can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts；The parts by weight of ammonium molybdate can for 1 part, 1.5
Part, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of magnesium sulfate can for 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts,
5 parts；The parts by weight of oyster shell powder can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of kaolin powder
It can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of talcum powder can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5
Part, 6 parts；The parts by weight of dolomite rock powder can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；Take the parts by weight of stone flour
It can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts；The parts by weight of thiocarbamide can for 4 parts, 4.5 parts, 5 parts, 5.5
Part, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts；The parts by weight of dicyandiamide can for 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts,
5 parts；The parts by weight of chicken manure can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts；Cicada excrement
Parts by weight can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts；The parts by weight of wormcast can for 3 parts, 3.5 parts, 4 parts,
4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts；The parts by weight of maize straw can for 1 part,
1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of rapeseed cake can for 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5
Part, 5 parts；The parts by weight of bagasse can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts；Flyash
Parts by weight can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts；The parts by weight of purple perilla seed can for 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6
Part, 6.5 parts, 7 parts, 7.5 parts, 8 parts；The parts by weight of humic acid can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；
The parts by weight of EM strains can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts.
Embodiment 1
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes by weight：Dry pond sludge
35 parts, modified 7.5 parts of oxygenation agent, modified 10 parts of sustained release agent, 6.5 parts of modified filler, 20 parts of urea, 6 parts of MAP, potassium chloride
3 parts, 2.5 parts of ammonium chloride, 4 parts of diammonium hydrogen phosphate, 3 parts of calcium dihydrogen phosphate, 4.5 parts of zinc sulfate, 2.5 parts of ammonium molybdate, magnesium sulfate 3.5
Part, 2.5 parts of oyster shell powder, 3 parts of kaolin powder, 4.5 parts of talcum powder, 2.5 parts of dolomite rock powder, take 4.5 parts of stone flour, it is 6 parts of thiocarbamide, double
3.5 parts of cyanamide, 10 parts of chicken manure, 5 parts of cicada excrement, 6 parts of wormcast, 2.5 parts of maize straw, 3.5 parts of rapeseed cake, 6 parts of bagasse, flyash
4 parts, 6 parts of purple perilla seed, 3.5 parts of humic acid, 6 parts of EM strains.
Embodiment 2
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes by weight：Dry pond sludge
20 parts, modified 9 parts of oxygenation agent, modified 5 parts of sustained release agent, 9 parts of modified filler, 15 parts of urea, 9 parts of MAP, 2 parts of potassium chloride,
4 parts of ammonium chloride, 3 parts of diammonium hydrogen phosphate, 4 parts of calcium dihydrogen phosphate, 3 parts of zinc sulfate, 4 parts of ammonium molybdate, 2 parts of magnesium sulfate, oyster shell powder 4
Part, 2 parts of kaolin powder, 6 parts of talcum powder, 1 part of dolomite rock powder, take 6 parts of stone flour, 4 parts of thiocarbamide, 5 parts of dicyandiamide, 5 parts of chicken manure, cicada excrement
8 parts, 3 parts of wormcast, 4 parts of maize straw, 2 parts of rapeseed cake, 8 parts of bagasse, 2 parts of flyash, 8 parts of purple perilla seed, 2 parts of humic acid, EM
8 parts of strain.
Modified oxygenation agent is prepared by following technique：By weight by 2 parts of mass fractions for 35% hydrogen peroxide, 1 part
Urea and 6 parts of calgons are well mixed, and heating water bath is warming up to 25 DEG C, and then constant temperature stirring 15min adds 3 parts of sulfuric acid
Calcium land plaster is well mixed, and stirs 15min, 0 DEG C is then cooled in ice-water bath, by filter cake in drying at room temperature after suction filtration, so
4 parts of clays, 3 parts of lignin and water are added afterwards well mixed, stir 20min in 5500r/min rotating speeds, be then warming up to 90 DEG C,
20min is incubated, is cooled to after room temperature and is dried to obtain modified oxygenation agent.
Modified sustained release agent in following technique by being prepared：2 parts of itaconic acids and 8 parts of deionized waters are mixed equal by weight
Even, it is 75% material a then to add the well mixed degree of neutralization that obtains of 1 part of sodium hydroxide solution, then adds 2 parts of acryloyls
Amine, 5 parts of NVPs and 2 parts of N, N- methylene bisacrylamides acid amide are well mixed, and obtain material b；By 9 parts of modified shallow lakes
Powder and 2 parts of N, N- dimethylenes formamide are well mixed, and ultrasonically treated 30min is carried out in 45kHz, 250W, then add 1 part of plant
Acid and 6 parts of urea are well mixed, and are warming up to 50 DEG C, are incubated 6h, and filtering, in 45 DEG C of dry 40min, is cooled to room temperature and obtains material
c；Then material c is warming up to 70 DEG C, is gelatinized 40min, be subsequently added into material b, 2 parts of ammonium persulfates and 8 parts of sodium hydrogensulfites and mix
Close uniform, wash after 50 DEG C, dry 3h, with extracting 8h after crushing, 70 DEG C dry, pulverize, be cooled to room temperature and obtain modified slow
Release agent.
Modified filler is prepared by following technique：By weight by 2 parts of humic acid, 6 parts of sepiolites, 1 part of attapulgite,
5 parts of Klinit dregs, 1 part of ochre, 4 parts of wooden slags, 2 parts of vermiculites, 5 parts of bentonites and 3 parts of diatomites in powder, which are broken to after 40 mesh, to be accumulated, normal temperature
3d is placed, 5 parts of mefenacets is then added and is well mixed, be warming up to 50 DEG C, be incubated 3h, be then mixed with water, in
1500r/min rotating speeds stir 40min, and then in 40 DEG C of dry 4h, modified filler must be beaten by being cooled to room temperature.
Embodiment 3
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes by weight：Dry pond sludge
50 parts, modified 6 parts of oxygenation agent, modified 15 parts of sustained release agent, 4 parts of modified filler, 25 parts of urea, 3 parts of MAP, 4 parts of potassium chloride,
1 part of ammonium chloride, 5 parts of diammonium hydrogen phosphate, 2 parts of calcium dihydrogen phosphate, 6 parts of zinc sulfate, 1 part of ammonium molybdate, 5 parts of magnesium sulfate, oyster shell powder 1
Part, 4 parts of kaolin powder, 3 parts of talcum powder, 4 parts of dolomite rock powder, take 3 parts of stone flour, 8 parts of thiocarbamide, 2 parts of dicyandiamide, 15 parts of chicken manure, cicada
2 parts of excrement, 9 parts of wormcast, 1 part of maize straw, 5 parts of rapeseed cake, 4 parts of bagasse, 6 parts of flyash, 4 parts of purple perilla seed, 5 parts of humic acid,
4 parts of EM strains.
Modified oxygenation agent is prepared by following technique：By weight by 5 parts of mass fractions for 25% hydrogen peroxide, 3 parts
Urea and 3 parts of calgons are well mixed, and heating water bath is warming up to 35 DEG C, and then constant temperature stirring 5min adds 5 parts of calcium sulfate
Land plaster is well mixed, and is stirred 5min, 5 DEG C is then cooled in ice-water bath, by filter cake in drying at room temperature, Ran Houjia after suction filtration
Enter 1 part of clay, 6 parts of lignin and water well mixed, 40min is stirred in 3500r/min rotating speeds, be then warming up to 70 DEG C, insulation
40min, is cooled to after room temperature and is dried to obtain modified oxygenation agent.
Modified sustained release agent in following technique by being prepared：5 parts of itaconic acids and 4 parts of deionized waters are mixed equal by weight
Even, it is 55% material a then to add the well mixed degree of neutralization that obtains of 3 parts of sodium hydroxide solutions, then adds 6 parts of acryloyls
Amine, 3 parts of NVPs and 6 parts of N, N- methylene bisacrylamides acid amide are well mixed, and obtain material b；By 3 parts of modified shallow lakes
Powder and 5 parts of N, N- dimethylenes formamide are well mixed, and ultrasonically treated 20min is carried out in 35kHz, 350W, then add 4 parts of plants
Acid and 3 parts of urea are well mixed, and are warming up to 90 DEG C, are incubated 2h, and filtering, in 55 DEG C of dry 20min, is cooled to room temperature and obtains material
c；Then material c is warming up to 90 DEG C, is gelatinized 20min, be subsequently added into material b, 4 parts of ammonium persulfates and 2 parts of sodium hydrogensulfites and mix
Close uniform, wash after 70 DEG C, dry 2h, with extracting 16h after crushing, 50 DEG C dry, pulverize, be cooled to room temperature and obtain modified slow
Release agent.
Modified filler is prepared by following technique：By weight by 5 parts of humic acid, 4 parts of sepiolites, 4 parts of attapulgites,
3 parts of Klinit dregs, 3 parts of ochres, 1 part of wooden slag, 4 parts of vermiculites, 3 parts of bentonites and 5 parts of diatomites in powder, which are broken to after 20 mesh, to be accumulated, normal temperature
5d is placed, 2 parts of mefenacets is then added and is well mixed, be warming up to 60 DEG C, be incubated 1h, be then mixed with water, in
2500r/min rotating speeds stir 20min, and then in 50 DEG C of dry 2h, modified filler must be beaten by being cooled to room temperature.
Embodiment 4
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes by weight：Dry pond sludge
25 parts, modified 8 parts of oxygenation agent, modified 8 parts of sustained release agent, 8 parts of modified filler, 18 parts of urea, 8 parts of MAP, potassium chloride 2.5
It is part, 3 parts of ammonium chloride, 3.5 parts of diammonium hydrogen phosphate, 3.5 parts of calcium dihydrogen phosphate, 4 parts of zinc sulfate, 3 parts of ammonium molybdate, 3 parts of magnesium sulfate, male
3 parts of oyster shells, 2.5 parts of kaolin powder, 5 parts of talcum powder, 2 parts of dolomite rock powder, take 5 parts of stone flour, 5 parts of thiocarbamide, 4 parts of dicyandiamide, chicken
8 parts of excrement, 7 parts of cicada excrement, 4 parts of wormcast, 3 parts of maize straw, 3 parts of rapeseed cake, 7 parts of bagasse, 3 parts of flyash, 7 parts of purple perilla seed, corruption
Grow sour 3 parts, 7 parts of EM strains.
Modified oxygenation agent is prepared by following technique：By weight by 3 parts of mass fractions for 32% hydrogen peroxide, 1.5
Part urea and 5 parts of calgons are well mixed, and heating water bath is warming up to 28 DEG C, and then constant temperature stirring 12min adds 3.5 parts
Calcium sulfate land plaster is well mixed, and stirs 12min, 1 DEG C is then cooled in ice-water bath, does filter cake in room temperature after suction filtration
It is dry, then add 3 parts of clays, 4 parts of lignin and water and be well mixed, stir 25min in 5200r/min rotating speeds, be then warming up to
85 DEG C, 25min is incubated, is cooled to after room temperature and is dried to obtain modified oxygenation agent.
Modified sustained release agent in following technique by being prepared：3 parts of itaconic acids and 7 parts of deionized waters are mixed equal by weight
Even, it is 72% material a then to add the well mixed degree of neutralization that obtains of 1.5 parts of sodium hydroxide solutions, then adds 3 parts of acryloyls
Amine, 4.5 parts of NVPs and 3 parts of N, N- methylene bisacrylamides acid amide are well mixed, and obtain material b；By 8 parts of modifications
Starch and 3 parts of N, N- dimethylenes formamide are well mixed, and are carried out ultrasonically treated 28min in 42kHz, 280W, are then added 2 parts
Phytic acid and 5 parts of urea are well mixed, and are warming up to 55 DEG C, are incubated 5h, and filtering, in 48 DEG C of dry 35min, is cooled to room temperature and obtains thing
Expect c；Then material c is warming up to 75 DEG C, is gelatinized 35min, is subsequently added into material b, 2.5 parts of ammonium persulfates and 7 parts of bisulfites
Sodium is well mixed, and is washed after 55 DEG C, dries 2.8h, and with extracting 9h after crushing, 65 DEG C dry, pulverize, and are cooled to room temperature and obtain
Modified sustained release agent.
Modified filler is prepared by following technique：By weight by 3 parts of humic acid, 5.5 parts of sepiolites, 2 parts of concave convex rods
Soil, 4.5 parts of Klinit dregs, 1.5 parts of ochres, 3 parts of wooden slags, 2.5 parts of vermiculites, 4.5 parts of bentonites and 3.5 parts of diatomites in powder are broken to 35
Accumulated after mesh, room temperature 3.5d, then add 4 parts of mefenacets and be well mixed, be warming up to 52 DEG C, be incubated 2.5h, then
It is mixed with water, 35min is stirred in 1800r/min rotating speeds, then in 42 DEG C of dry 3.5h, modified fill out must be beaten by being cooled to room temperature
Material.
Embodiment 5
A kind of oxygen supply type growth promotion flowers compoiste fertilizer proposed by the present invention, its raw material includes by weight：Dry pond sludge
45 parts, modified 7 parts of oxygenation agent, modified 12 parts of sustained release agent, 5 parts of modified filler, 22 parts of urea, 4 parts of MAP, potassium chloride 3.5
Part, 2 parts of ammonium chloride, 4.5 parts of diammonium hydrogen phosphate, 2.5 parts of calcium dihydrogen phosphate, 5 parts of zinc sulfate, 2 parts of ammonium molybdate, 34 parts of magnesium sulfate,
2 parts of oyster shell powder, 3.5 parts of kaolin powder, 4 parts of talcum powder, 3 parts of dolomite rock powder, take 4 parts of stone flour, 7 parts of thiocarbamide, 3 parts of dicyandiamide,
12 parts of chicken manure, 3 parts of cicada excrement, 8 parts of wormcast, 2 parts of maize straw, 4 parts of rapeseed cake, 5 parts of bagasse, 5 parts of flyash, 5 parts of purple perilla seed,
4 parts of humic acid, 5 parts of EM strains.
Modified oxygenation agent is prepared by following technique：By weight by 4 parts of mass fractions for 28% hydrogen peroxide, 2.5
Part urea and 4 parts of calgons are well mixed, and heating water bath is warming up to 32 DEG C, and then constant temperature stirring 8min adds 4.5 parts of sulphur
Sour calcium land plaster is well mixed, and stirs 8min, 4 DEG C are then cooled in ice-water bath, by filter cake in drying at room temperature after suction filtration, so
2 parts of clays, 5 parts of lignin and water are added afterwards well mixed, stir 35min in 3800r/min rotating speeds, be then warming up to 75 DEG C,
35min is incubated, is cooled to after room temperature and is dried to obtain modified oxygenation agent.
Modified sustained release agent in following technique by being prepared：4 parts of itaconic acids and 5 parts of deionized waters are mixed equal by weight
Even, it is 58% material a then to add the well mixed degree of neutralization that obtains of 2.5 parts of sodium hydroxide solutions, then adds 5 parts of acryloyls
Amine, 3.5 parts of NVPs and 5 parts of N, N- methylene bisacrylamides acid amide are well mixed, and obtain material b；By 4 parts of modifications
Starch and 4 parts of N, N- dimethylenes formamide are well mixed, and are carried out ultrasonically treated 22min in 38kHz, 320W, are then added 3 parts
Phytic acid and 4 parts of urea are well mixed, and are warming up to 85 DEG C, are incubated 3h, and filtering, in 52 DEG C of dry 25min, is cooled to room temperature and obtains thing
Expect c；Then material c is warming up to 85 DEG C, is gelatinized 25min, is subsequently added into material b, 3.5 parts of ammonium persulfates and 3 parts of bisulfites
Sodium is well mixed, and is washed after 65 DEG C, dries 2.2h, and with extracting 15h after crushing, 55 DEG C dry, pulverize, and are cooled to room temperature and obtain
Modified sustained release agent.
Modified filler is prepared by following technique：By weight by 4 parts of humic acid, 4.5 parts of sepiolites, 3 parts of concave convex rods
Soil, 3.5 parts of Klinit dregs, 2.5 parts of ochres, 2 parts of wooden slags, 3.5 parts of vermiculites, 3.5 parts of bentonites and 4.5 parts of diatomites in powder are broken to 25
Accumulated after mesh, room temperature 4.5d, then add 3 parts of mefenacets and be well mixed, be warming up to 58 DEG C, be incubated 1.5h, then
It is mixed with water, 25min is stirred in 2200r/min rotating speeds, then in 48 DEG C of dry 2.5h, modified fill out must be beaten by being cooled to room temperature
Material.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (10)
1. a kind of oxygen supply type growth promotion flowers compoiste fertilizer, it is characterised in that its raw material includes by weight：Dry pond sludge 20-
50 parts, modified 6-9 part of oxygenation agent, 5-15 parts of sustained release agent of modification, 4-9 parts of modified filler, 15-25 parts of urea, MAP 3-9
Part, 2-4 parts of potassium chloride, 1-4 parts of ammonium chloride, 3-5 parts of diammonium hydrogen phosphate, 2-4 parts of calcium dihydrogen phosphate, 3-6 parts of zinc sulfate, ammonium molybdate
1-4 parts, 2-5 parts of magnesium sulfate, 1-4 parts of oyster shell powder, 2-4 parts of kaolin powder, 3-6 parts of talcum powder, 1-4 parts of dolomite rock powder, Fei Shi
3-6 parts of powder, 4-8 parts of thiocarbamide, 2-5 parts of dicyandiamide, 5-15 parts of chicken manure, 2-8 parts of cicada excrement, 3-9 parts of wormcast, 1-4 parts of maize straw,
2-5 parts of rapeseed cake, 4-8 parts of bagasse, 2-6 parts of flyash, 4-8 parts of purple perilla seed, 2-5 parts of humic acid, 4-8 parts of EM strains.
2. oxygen supply type growth promotion flowers compoiste fertilizer according to claim 1, it is characterised in that modified oxygenation agent is by such as
It is prepared by lower technique：Mass fraction is well mixed for 25-35% hydrogen peroxide, urea and calgon, heating water bath
Constant temperature is stirred afterwards, is then added calcium sulfate land plaster and is well mixed, then cooled down in ice-water bath, by filter cake in room temperature after suction filtration
Dry, then add clay, lignin and water and be well mixed, be incubated after heating, be cooled to after room temperature and be dried to obtain modified oxygenation
Agent.
3. oxygen supply type growth promotion flowers compoiste fertilizer according to claim 1 or 2, it is characterised in that modified oxygenation agent
Prepared by following technique：Mass fraction is well mixed for 25-35% hydrogen peroxide, urea and calgon, water-bath
25-35 DEG C is heated to, then constant temperature stirring 5-15min adds calcium sulfate land plaster and be well mixed, stir 5-15min, connect
And be cooled to filter cake in ice-water bath after 0-5 DEG C, suction filtration in drying at room temperature, then add clay, lignin and water mixing equal
It is even, 20-40min is stirred in 3500-5500r/min rotating speeds, 70-90 DEG C is then warming up to, 20-40min is incubated, is cooled to room temperature
After be dried to obtain modified oxygenation agent.
4. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-3, it is characterised in that modified to increase
In the preparation technology of oxygen agent, mass fraction is 25-35% hydrogen peroxide, urea, calgon, calcium sulfate land plaster, clay
Weight ratio with lignin is 2-5：1-3：3-6：3-5：1-4：3-6.
5. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-4, it is characterised in that modified slow
Release the raw material of agent includes by weight：2-5 parts of itaconic acid, 4-8 parts of deionized water, 1-3 parts of sodium hydroxide solution, acrylamide 2-
6 parts, 3-5 parts of NVP, N, 2-6 parts of N- methylene bisacrylamide acid amides, 3-9 parts of modified starch, N, the methylenes of N- bis-
2-5 parts of base formamide, 1-4 parts of phytic acid, 3-6 parts of urea, 2-4 parts of ammonium persulfate, 2-8 parts of sodium hydrogensulfite.
6. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-5, it is characterised in that modified slow
Agent is released by being prepared in following technique：Itaconic acid and deionized water are well mixed, sodium hydroxide solution mixing is then added
It is uniform to obtain the material a that degree of neutralization is 55-75%, then add acrylamide, NVP and N, N- methylene
Double acrylic amines are well mixed, and obtain material b；By modified starch and N, N- dimethylenes formamide is well mixed, ultrasonically treated
Phytic acid is added afterwards and urea is well mixed, and 2 are incubated after heating, is filtered, is dried, is cooled to room temperature and obtains material c；Then by material
C heats up, gelatinization, is subsequently added into material b, ammonium persulfate and sodium hydrogensulfite and is well mixed, washing, with extracting after dry, pulverize,
It dry, pulverize, be cooled to room temperature and obtain being modified sustained release agent.
7. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-6, it is characterised in that modified slow
Agent is released by being prepared in following technique：Itaconic acid and deionized water are well mixed, sodium hydroxide solution mixing is then added
It is uniform to obtain the material a that degree of neutralization is 55-75%, then add acrylamide, NVP and N, N- methylene
Double acrylic amines are well mixed, and obtain material b；By modified starch and N, N- dimethylenes formamide is well mixed, in 35-
45kHz, 250-350W carry out ultrasonically treated 20-30min, then add phytic acid and urea is well mixed, be warming up to 50-90 DEG C,
2-6h is incubated, filtering, in 45-55 DEG C of dry 20-40min, is cooled to room temperature and obtains material c；Then material c is warming up to 70-
90 DEG C, 20-40min is gelatinized, material b, ammonium persulfate and sodium hydrogensulfite is subsequently added into and is well mixed, wash after 50-70 DEG C,
2-3h is dried, with extracting 8-16h after crushing, 50-70 DEG C dry, pulverize, and is cooled to room temperature and obtains being modified sustained release agent.
8. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-7, it is characterised in that modification is filled out
The raw material of material includes by weight：2-5 parts of humic acid, 4-6 parts of sepiolite, 1-4 parts of attapulgite, 2-5 parts of mefenacet, wood
3-5 parts of sugar alcohol slag, 1-3 parts of ochre, 1-4 parts of wooden slag, 2-4 parts of vermiculite, 3-5 parts of bentonite, 3-5 parts of diatomite.
9. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-8, it is characterised in that modification is filled out
Material is prepared by following technique：By humic acid, sepiolite, attapulgite, Klinit dregs, ochre, wooden slag, vermiculite, bentonite
It is broken to after 20-40 mesh and accumulates with diatomite in powder, then room temperature 3-5d adds mefenacet and be well mixed, protected after heating
Temperature, is then mixed with water, and dries, modified filler must be beaten by being cooled to room temperature.
10. the oxygen supply type growth promotion flowers compoiste fertilizer according to claim any one of 1-9, it is characterised in that modified
Filler is prepared by following technique：By humic acid, sepiolite, attapulgite, Klinit dregs, ochre, wooden slag, vermiculite, swelling
Soil and diatomite in powder, which are broken to after 20-40 mesh, to be accumulated, and then room temperature 3-5d adds mefenacet and be well mixed, be warming up to
50-60 DEG C, 1-3h is incubated, is then mixed with water, 20-40min is stirred in 1500-2500r/min rotating speeds, then in 40-
50 DEG C of dry 2-4h, modified filler must be beaten by being cooled to room temperature.
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| CN107573658A (en) * | 2017-09-07 | 2018-01-12 | 芜湖林电子科技有限公司 | A kind of high slow-released pesticide coating 3D printing material of agricultural |
| CN107879797A (en) * | 2017-10-31 | 2018-04-06 | 肥西凤林家庭农场 | A kind of slow-release fertilizer for promoting Chinese rose healthy growth |
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