CN107029115A - A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat - Google Patents
A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat Download PDFInfo
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- CN107029115A CN107029115A CN201710204198.9A CN201710204198A CN107029115A CN 107029115 A CN107029115 A CN 107029115A CN 201710204198 A CN201710204198 A CN 201710204198A CN 107029115 A CN107029115 A CN 107029115A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0014—Skin, i.e. galenical aspects of topical compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
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Abstract
A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat, includes the mass ratio of following components：Dendrobium candidum caul-fat 70% 90%, HERBA DENDROBII caul-fat 10 30%.Beneficial effects of the present invention are：（1）Nonirritant, smell delicate fragrance of the invention；（2）This is educated hair stem of noble dendrobium caul-fat and more than 90% is reached to the effective treatment rate of long-term alopecia, especially reaches 100% to effective treatment rate of alopecia seborrheica.
Description
Technical field
The present invention relates to Chinese medicine deep process technology field, and in particular to a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat.
Background technology
Due to the social pressures constantly increased, the rhythm of life gradually accelerated, the natural environment constantly deteriorated, cause people
Non-health, inferior health health it is growing day by day, Chinese hair loss patient is more and more.
The hair normally come off is at catagen and the hair of stand-down, due to entering catagen with new into growth
The hair of phase is constantly in dynamic equilibrium, therefore can maintain the hair of normal quantity.Generally alopecia refer to hair it is abnormal or
Excessive comes off, and its reason is a lot.Alopecia is clinical common disease, though do not belong to serious disease, spirit, the heart to people
Reason produces large effect, with the improvement of living standards, requirement of the people to cosmetology is increasingly urgent, modern medicine and biography
System medical science also increasingly payes attention to the research to alopecia.
A kind of multipotential cell is found in the raw coal bunker knuckle portion of people, is named as people's hair follicle stem cells.Belong into
Somatic stem cell, adult stem cell is the cell with propagation and differentiation potential, and the ability replicated with self-renewing can be produced
Well differentiated functioning cell and pluripotent cell.It is the initial cell that a class is present in tissue, with versatility and self
Updating ability, can produce more than at least one other height noble cells.As long as thus activation hair follicle stem cells, promote its point
Change, update, then can solve the problems, such as alopecia caused by hair follicle necrosis.
The medicine and method for being applied to clinic at present do not realize the purpose of effective hair growth also, and there are different journeys
The side effects such as sensitization, excitant, carcinogenicity are spent, and have the shortcomings that easily recurrence after being discontinued.Therefore a kind of safety, low thorn are developed
Swash property, efficient hair-loss preventing and hair-restoring liquid to have very important significance for the exploitation of associated downstream product for improving hair-growing.
The content of the invention
The invention aims to overcome deficiency of the prior art there is provided a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat,
The problems such as solving that security in existing product is poor, sensitization strong, easily recur.
In order to solve the above technical problems, the technical scheme is that：
A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat, including the raw material of following mass parts is dendrobium candidum caul-fat 70%-90%, Jin Chai
Stem of noble dendrobium caul-fat 10-30%.
Preferably, the dendrobium candidum caul-fat is made by SCF-CO 2 method, and step is as follows：
（1）The petal for drying dendrobium candidum flower is added in disintegrating machine, 10-40 mesh powder is ground into；
（2）By step（1）In the drying dendrobium candidum pollen end that crushes be added to the extraction kettle of SCF-CO 2 equipment
In, then to extraction kettle, separating still, separating stillHeated, extraction kettle heating-up temperature is 30-55 DEG C, separating stillHeating
Temperature is 35-60 DEG C, separating stillHeating-up temperature is 30-50 DEG C；Then cold refrigeration is started, CO2 is cold by cold storage tank
After solidifying, extraction kettle, separating still are delivered into by high-pressure pumpAnd separating still, control valve, make extraction kettle pressure for 25-
45MPa, separating stillPressure is 5-10 MPa, separating stillPressure is 6-11 MPa, starts the cycle over extraction, extracts 2-4h,
After to be extracted, from separating stillAnd separating stillMiddle blowing.
Preferably, the step of making dendrobium candidum caul-fat（1）In, the particle diameter at dendrobium candidum pollen end is 20-30 mesh.
Preferably, the step of making dendrobium candidum caul-fat（2）In, extraction kettle pressure is 35 MPa, temperature 45 C；Separating stillPressure is 8 MPa, and temperature is 50 DEG C；Separating stillPressure is 9 MPa, and temperature is 40 DEG C；The time of extraction is 3h.
Preferably, the HERBA DENDROBII caul-fat is made by SCF-CO 2 method, and step is as follows：
（1）The petal for drying HERBA DENDROBII flower is added in disintegrating machine, 10-40 mesh powder is ground into；
（2）By step（1）In the drying HERBA DENDROBII pollen end that crushes be added to the extraction kettle of SCF-CO 2 equipment
In, then to extraction kettle, separating still, separating stillHeated, extraction kettle heating-up temperature is 30-55 DEG C, separating stillHeating
Temperature is 35-60 DEG C, separating stillHeating-up temperature is 30-50 DEG C；Then cold refrigeration is started, CO2 is cold by cold storage tank
After solidifying, extraction kettle, separating still are delivered into by high-pressure pumpAnd separating still, control valve, make extraction kettle pressure for 25-
45MPa, separating stillPressure is 5-10 MPa, separating stillPressure is 6-11 MPa, starts the cycle over extraction, extracts 2-4h,
After to be extracted, from separating stillAnd separating stillMiddle blowing.
Preferably, the step of making HERBA DENDROBII caul-fat（1）In, the particle diameter at HERBA DENDROBII pollen end is 20-30 mesh.
Preferably, the step of making HERBA DENDROBII caul-fat（2）In, extraction kettle pressure is 35 MPa, temperature 45 C；Separating stillPressure is 8 MPa, and temperature is 50 DEG C；Separating stillPressure is 9 MPa, and temperature is 40 DEG C；The time of extraction is 3h.
Beneficial effects of the present invention are：（1）Nonirritant, smell delicate fragrance of the invention；（2）This educates hair stem of noble dendrobium caul-fat to long-term
The effective treatment rate of alopecia reaches more than 90%, especially reaches 100% to effective treatment rate of alopecia seborrheica.
Brief description of the drawings
Accompanying drawing 1 is dendrobium candidum caul-fat and the mixed gas chromatograph-matter of HERBA DENDROBII caul-fat in the embodiment of the present invention 1
Spectrum（GC-MS）Detect collection of illustrative plates；
Accompanying drawing 2 is the zoopery effect contrast figure of the natural hair-loss preventing and hair-restoring of the embodiment of the present invention two oil.
Embodiment
To make to have a better understanding and awareness to architectural feature of the invention and the effect reached, to preferably
Embodiment and accompanying drawing coordinate detailed description, are described as follows：
Embodiment one：
A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat, including the raw material of following mass parts is dendrobium candidum caul-fat 70%-90%, Jin Chai
Stem of noble dendrobium caul-fat 10-30%.
The dendrobium candidum caul-fat is made by SCF-CO 2 method, and step is as follows：
（1）The petal for drying dendrobium candidum flower is added in disintegrating machine, 10-40 mesh powder is ground into；
（2）By step（1）In the drying dendrobium candidum pollen end that crushes be added to the extraction kettle of SCF-CO 2 equipment
In, then to extraction kettle, separating still, separating stillHeated, extraction kettle heating-up temperature is 30-55 DEG C, separating stillHeating
Temperature is 35-60 DEG C, separating stillHeating-up temperature is 30-50 DEG C；Then cold refrigeration is started, CO2 is cold by cold storage tank
After solidifying, extraction kettle, separating still are delivered into by high-pressure pumpAnd separating still, control valve, make extraction kettle pressure for 25-
45MPa, separating stillPressure is 5-10 MPa, separating stillPressure is 6-11 MPa, starts the cycle over extraction, extracts 2-4h,
After to be extracted, from separating stillAnd separating stillMiddle blowing.
Wherein, the step of making dendrobium candidum caul-fat（1）In, the particle diameter at dendrobium candidum pollen end is 20-30 mesh.Make
The step of dendrobium candidum caul-fat（2）In, extraction kettle pressure is 35 MPa, temperature 45 C；Separating stillPressure is 8 MPa, and temperature is
50℃；Separating stillPressure is 9 MPa, and temperature is 40 DEG C；The time of extraction is 3h.
The HERBA DENDROBII caul-fat is made by SCF-CO 2 method, and step is as follows：
（1）The petal for drying HERBA DENDROBII flower is added in disintegrating machine, 10-40 mesh powder is ground into；
（2）By step（1）In the drying HERBA DENDROBII pollen end that crushes be added to the extraction kettle of SCF-CO 2 equipment
In, then to extraction kettle, separating still, separating stillHeated, extraction kettle heating-up temperature is 30-55 DEG C, separating stillHeating
Temperature is 35-60 DEG C, separating stillHeating-up temperature is 30-50 DEG C；Then cold refrigeration is started, CO2 is cold by cold storage tank
After solidifying, extraction kettle, separating still are delivered into by high-pressure pumpAnd separating still, control valve, make extraction kettle pressure for 25-
45MPa, separating stillPressure is 5-10 MPa, separating stillPressure is 6-11 MPa, starts the cycle over extraction, extracts 2-4h,
After to be extracted, from separating stillAnd separating stillMiddle blowing.
Specifically, the step of making HERBA DENDROBII caul-fat（1）In, the particle diameter at HERBA DENDROBII pollen end is 20-30 mesh.System
The step of making HERBA DENDROBII caul-fat（2）In, extraction kettle pressure is 35 MPa, temperature 45 C；Separating stillPressure is 8 MPa, temperature
For 50 DEG C；Separating stillPressure is 9 MPa, and temperature is 40 DEG C；The time of extraction is 3h.
Accompanying drawing 1 is that mass ratio is that dendrobium candidum caul-fat 70%, HERBA DENDROBII caul-fat 30% compare in embodiment described below 1
Mixed gas chromatograph-the mass spectrum of example（GC-MS）Detect collection of illustrative plates.It can be seen that the natural hair-loss preventing and hair-restoring stone of the present invention
Dry measure used in former times caul-fat mainly has six kinds of aliphatic acid, based on linoleic acid polyunsaturated fatty acid.
The animal efficacy test of the products obtained therefrom of embodiment two：
1st, material animal：The female C57BL/6 mouse of 6 weeks；Positive control is minoxidil；
2nd, method：The female C57BL/6 mouse of 6 weeks first feed one week to shake down（12h illumination, the C of temperature 23 ± 2,
Humidity 35-60%）, the 7th week（The mouse hair of 7 weeks grows into stand-down）The hair of all mouse backs is shaved off（Depilation
Cream）, to ensure that all hair follicles are synchronous, the gained hair-loss preventing and hair-restoring of embodiment 1 oil or 0.1% minoxidil are smeared at back daily, even
It is continuous 3 weeks, every three days observation back growing states, including skin color and hair change, as a result see accompanying drawing 2.
Shown in test result accompanying drawing 2, it can be seen that the gained hair-loss preventing and hair-restoring of embodiment two oil started at first week
To hair-growing effects, effect is suitable with minoxidil effect after the 3rd week.
Human efficiency's test of products obtained therefrom：
The hair follicle that 500 ages are chosen at 20-40 Sui is damaged de- originator, and men and women half and half, and smearing experiment is carried out using the present invention,
Respectively according to the embodiment 1-5 in table 1 below, the composition quality ratio of the invention is respectively：The dendrobium candidum caul-fat of embodiment 1
70%th, HERBA DENDROBII caul-fat 30%；The dendrobium candidum caul-fat 90% of embodiment 2, HERBA DENDROBII caul-fat 10%；The iron sheet stone of embodiment 3
Dry measure used in former times caul-fat 80%, HERBA DENDROBII caul-fat 20%；The dendrobium candidum caul-fat 75% of embodiment 4, HERBA DENDROBII caul-fat 25%；Embodiment
5 dendrobium candidum caul-fats 85%, HERBA DENDROBII caul-fat 15%.100 people of each embodiment correspondence（Men and women half and half）, daily using 1
Secondary, Continuous Observation 5-10 weeks carries out number of hairs to the alopecia affected part of 1 square centimeter of experimenter weekly and measured, takes 100 people
Average.
Test result is as shown in table 1, it can be seen that fed back after the clinical test use of various embodiments of the present invention
Effective percentage, which was reached in 100%, and three weeks, just can play pharmacological action, can return within ten weeks or so normal hair density.
Table 1
Beneficial effects of the present invention are：（1）Nonirritant, smell delicate fragrance of the invention；（2）This educates hair stem of noble dendrobium caul-fat to long-term alopecia
Effective treatment rate reaches more than 90%, especially reaches 100% to effective treatment rate of alopecia seborrheica.
It should be understood by those skilled in the art that, the present invention is not limited to the above embodiments, above-described embodiment and explanation
The principle of the simply present invention described in book, it is of the invention without departing from the spirit and scope of the present invention also to have various changes
Change and improve, these changes and improvements are both fallen within the range of claimed invention.The protection domain of application claims by
Appended claims and its equivalent are defined.
Claims (7)
1. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat, it is characterised in that：Raw material including following mass parts is dendrobium candidum caul-fat
70%-90%, HERBA DENDROBII caul-fat 10-30%.
2. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat according to claim 1, it is characterised in that：The dendrobium candidum caul-fat
It is made by SCF-CO 2 method, step is as follows：
（1）The petal for drying dendrobium candidum flower is added in disintegrating machine, 10-40 mesh powder is ground into；
（2）By step（1）In the drying dendrobium candidum pollen end that crushes be added to the extraction kettle of SCF-CO 2 equipment
In, then to extraction kettle, separating still, separating stillHeated, extraction kettle heating-up temperature is 30-55 DEG C, separating stillHeating
Temperature is 35-60 DEG C, separating stillHeating-up temperature is 30-50 DEG C；Then cold refrigeration is started, CO2 is cold by cold storage tank
After solidifying, extraction kettle, separating still are delivered into by high-pressure pumpAnd separating still, control valve, make extraction kettle pressure for 25-
45MPa, separating stillPressure is 5-10 MPa, separating stillPressure is 6-11 MPa, starts the cycle over extraction, extracts 2-4h,
After to be extracted, from separating stillAnd separating stillMiddle blowing.
3. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat according to claim 2, it is characterised in that：Step（1）In, iron sheet stone
The particle diameter at dry measure used in former times pollen end is 20-30 mesh.
4. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat according to claim 2, it is characterised in that：Step（2）In, extraction kettle
Pressure is 35 MPa, temperature 45 C；Separating stillPressure is 8 MPa, and temperature is 50 DEG C；Separating stillPressure is 9 MPa, temperature
For 40 DEG C；The time of extraction is 3h.
5. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat according to claim 1, it is characterised in that：The HERBA DENDROBII caul-fat
It is made by SCF-CO 2 method, step is as follows：
（1）The petal for drying HERBA DENDROBII flower is added in disintegrating machine, 10-40 mesh powder is ground into；
（2）By step（1）In the drying HERBA DENDROBII pollen end that crushes be added to the extraction kettle of SCF-CO 2 equipment
In, then to extraction kettle, separating still, separating stillHeated, extraction kettle heating-up temperature is 30-55 DEG C, separating stillHeating
Temperature is 35-60 DEG C, separating stillHeating-up temperature is 30-50 DEG C；Then cold refrigeration is started, CO2 is cold by cold storage tank
After solidifying, extraction kettle, separating still are delivered into by high-pressure pumpAnd separating still, control valve, make extraction kettle pressure for 25-
45MPa, separating stillPressure is 5-10 MPa, separating stillPressure is 6-11 MPa, starts the cycle over extraction, extracts 2-4h,
After to be extracted, from separating stillAnd separating stillMiddle blowing.
6. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat according to claim 5, it is characterised in that：Step（1）In, golden hairpin stone
The particle diameter at dry measure used in former times pollen end is 20-30 mesh.
7. a kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat according to claim 5, it is characterised in that：Step（2）In, extraction kettle
Pressure is 35 MPa, temperature 45 C；Separating stillPressure is 8 MPa, and temperature is 50 DEG C；Separating stillPressure is 9 MPa, temperature
For 40 DEG C；The time of extraction is 3h.
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| CN201710204198.9A CN107029115A (en) | 2017-03-30 | 2017-03-30 | A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat |
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| CN201710204198.9A CN107029115A (en) | 2017-03-30 | 2017-03-30 | A kind of natural hair-loss preventing and hair-restoring stem of noble dendrobium caul-fat |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109832659A (en) * | 2018-07-09 | 2019-06-04 | 皖西学院 | A kind of Dendrobidium huoshanness cigarette and preparation method thereof |
| CN111093621A (en) * | 2017-09-04 | 2020-05-01 | 株式会社Lg生活健康 | Cosmetic composition containing dendrobium officinale flower extract |
| CN115487267A (en) * | 2022-09-27 | 2022-12-20 | 贵州汇腾萃取技术应用研究院有限责任公司 | A Chinese medicinal extract with sleep improving effect, and its preparation method |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111093621A (en) * | 2017-09-04 | 2020-05-01 | 株式会社Lg生活健康 | Cosmetic composition containing dendrobium officinale flower extract |
| CN109832659A (en) * | 2018-07-09 | 2019-06-04 | 皖西学院 | A kind of Dendrobidium huoshanness cigarette and preparation method thereof |
| CN109832659B (en) * | 2018-07-09 | 2021-10-15 | 皖西学院 | Dendrobium huoshanense cigarette and preparation method thereof |
| CN115487267A (en) * | 2022-09-27 | 2022-12-20 | 贵州汇腾萃取技术应用研究院有限责任公司 | A Chinese medicinal extract with sleep improving effect, and its preparation method |
| CN115487267B (en) * | 2022-09-27 | 2024-04-09 | 贵州汇腾萃取技术应用研究院有限责任公司 | A Chinese medicinal extract with sleep improving effect, and its preparation method |
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Application publication date: 20170811 |