CN109832659A - A kind of Dendrobidium huoshanness cigarette and preparation method thereof - Google Patents
A kind of Dendrobidium huoshanness cigarette and preparation method thereof Download PDFInfo
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Abstract
The present invention provides a kind of Dendrobidium huoshanness cigarette, including tobacco rod and filter tip；Pipe tobacco is surrounded by tobacco rod, pipe tobacco surface is covered with Dendrobidium huoshanness stem Ultramicro-powder；It is surrounded by filter stick in filter tip, quick-fried pearl is embedded in filter stick, the quick-fried pearl solution of package flower essential oil containing Dendrobidium huoshanness in quick-fried pearl；Dendrobidium huoshanness stem superfine preparation method are as follows: take Dendrobidium huoshanness stem section, cleaning after air-drying surface, is placed in 115-125 DEG C of baking oven and heats 8-12s, then change to 65-75 DEG C, be heated to constant weight, then crush；Dendrobidium huoshanness flower essential oil is the preparation method comprises the following steps: win Dendrobidium huoshanness flower extraction.The present invention also provides a kind of preparation methods of Dendrobidium huoshanness cigarette.Advantage of the present invention are as follows: (1) Dendrobidium huoshanness stem Ultramicro-powder is made an addition into pipe tobacco surface, keep flue gas form mellow and full, increased fine and smooth soft degree, reduce dry sensation, increase perfume quantity；(2) Dendrobidium huoshanness flower essential oil is added in quick-fried pearl, weakens the irritation of cigarette, improvement and abundant cigarette flavor.
Description
Technical field
The present invention relates to technical field of tobacco more particularly to a kind of Dendrobidium huoshanness cigarette and preparation method thereof.
Background technique
Basic raw material of the essence spice for cigarette as cigarette blending, exploitation innovation receive much attention.From raw material angle pair
Existing essence spice for cigarette, which carries out classification, can be divided into tealeaves class, fruits and vegetables class, fragrant flower class, kind subclass, Chinese herbal medicine, tobacco etc..
Currently, with the progress of science and technology, people increasingly pay close attention to harm problem brought by smoking, and smoker is to volume
The quality requirement of cigarette is higher and higher, and it is imperative to produce low evil, high-quality cigarette.Therefore the higher Chinese herbal medicine class cigarette of medical value
It is trend with the exploitation of fragrance.
Dendrobidium huoshanness (scientific name: Dendrobium huoshanense C.Z.Tang et S.J.Cheng) is commonly called as a meter dry measure used in former times,
It is the herbaceous plant of orchid family Dendrobium, china national geography famous special product.Main product is in Huoshan County, Anhui Province of Da Bie Mountain area, mostly
It is grown between the overhanging cliff cliffstone gap that cloud and mist curls up and on old trees that reach into the skies, is born in the woods of mountainous region on trunk and mountain valley rock
On.Dendrobidium huoshanness can increase substantially SOD in human body (main matter of anti-aging) level, to often stay up late, with brain, tobacco and wine
Excessively, the crowd of asthenia, often drinks and is particularly suitable for.Dendrobidium huoshanness has function of improving eyesight, also can YIN and YANG balance regulating, establishing-Yang benefit
Kidney, beauty treatment, which are stayed, to be held, thus the effect of reaching health-care.
Accordingly, it is badly in need of at present a kind of using Dendrobidium huoshanness as Dendrobidium huoshanness cigarette of raw material and preparation method thereof.
Summary of the invention
Technical problem to be solved by the present invention lies in provide it is a kind of using Dendrobidium huoshanness as the Dendrobidium huoshanness cigarette of raw material and
Preparation method.
The present invention solves above-mentioned technical problem using following technical scheme:
A kind of Dendrobidium huoshanness cigarette, including tobacco rod and filter tip are surrounded by pipe tobacco in the tobacco rod, and pipe tobacco surface is covered with Huoshan
Stem of Dendrobium Ultramicro-powder, Dendrobidium huoshanness stem Ultramicro-powder and tobacco quality ratio are (0.1-10): 1000；It is surrounded by the filter tip
Filter stick, filter stick middle part are embedded with quick-fried pearl, the quick-fried pearl solution of the package flower essential oil of Dendrobidium huoshanness containing 0.1%-30% in quick-fried pearl；
The Dendrobidium huoshanness stem Ultramicro-powder the preparation method comprises the following steps: enter winter or the beginning of spring, when fallen leaves do not sprout, take life in 2 years with
The Dendrobidium huoshanness stem section of upper field Emulational culture, selects no disease and pests harm stem item, and cleaning after air-drying surface, is placed in 115-125 DEG C
8-12s is heated in baking oven, then changes to 65-75 DEG C rapidly, is heated to constant weight；Then, using fluidized bed jet mill micronizer
Dendrobidium huoshanness stem item after above-mentioned drying and processing is ground into Ultramicro-powder, is collected and fed into bag and vacuumizes, saved under low temperature
For use；
The Dendrobidium huoshanness flower essential oil the preparation method comprises the following steps: month in spring 4-6, win the above field Ecology of life in 2 years and plant
The Dendrobidium huoshanness flower of training, is immediately fed into extraction chamber after fresh flower picking, extracts corresponding Dendrobidium huoshanness flower essential oil.
As one of preferred embodiment of the invention, the ingredient in the quick-fried pearl solution in addition to Dendrobidium huoshanness flower essential oil is specific
Send alkene, linalool, gaultherolin, myrcene, myrrh oil, neodecanoic acid glyceride, propylene glycol, triacetic acid sweet for peppermint oil, β-
One of oil, olive oil, corn oil are a variety of.
As one of preferred embodiment of the invention, the formula of each raw material is as follows in the quick-fried pearl solution: Dendrobidium huoshanness anthosin
Oil 2%, peppermint oil 0.2%, neodecanoic acid glyceride 20%, olive oil 20%, remaining is corn oil.
As one of preferred embodiment of the invention, the formula of each raw material is as follows in the quick-fried pearl solution: Dendrobidium huoshanness anthosin
Oil 5%, 0.1% β-sends alkene, 0.1% linalool, 2% gaultherolin, 0.1% myrcene, 0.1% myrrh oil, the 20% new last of the ten Heavenly stems
Acid glyceride, remaining is triacetic acid glycerol.
As one of preferred embodiment of the invention, in the preparation method of the Dendrobidium huoshanness stem Ultramicro-powder, under low temperature
Preservation refers to be saved at a temperature of (- 22)-(- 18) DEG C.
As one of preferred embodiment of the invention, in the preparation method of the Dendrobidium huoshanness flower essential oil, Dendrobidium huoshanness anthosin
The extracting process of oil is steam distillation or carbon dioxide supercritical extraction method；
When the extracting process of Dendrobidium huoshanness flower essential oil is specially steam distillation, the method is as follows: it is fresh to weigh 100g
Dendrobidium huoshanness flower in flask, if then 2000mL water, 5mL n-hexane and dry granular zeolite are added thereto, lead to after sufficiently shaking up
It crosses the atmospheric steam way of distillation and extracts 6h, cooling and standings 2h；Then, obtained oil water mixture 20mL n-hexane will be collected to extract
It takes 2 times, separates oil-yielding stratum and n-hexane therein is recovered under reduced pressure, obtains grease 0.56mL after anhydrous sodium sulfate is dry；
When the extracting process of Dendrobidium huoshanness flower essential oil is specially carbon dioxide supercritical extraction method, the method is as follows: weigh
100g fresh Dendrobidium huoshanness flower, is put into high pressure extraction still and carries out supercritical carbon dioxide extracting, extraction kettle pressure 27MPa,
40 DEG C of temperature, flow velocity 15kg/kgh, separate a kettle pressure 10MPa, temperature 45 C, separate two kettle pressure 6MPa, 42 DEG C of temperature,
Extraction time 1.5h；Then, dendrobium nobile flower essential oil is collected, recycles anhydrous sodium sulfate or discoloration silica gel to be dehydrated, obtains grease
0.63mL。
A kind of preparation method of Dendrobidium huoshanness cigarette, includes the following steps:
(1) preparation of Dendrobidium huoshanness stem Ultramicro-powder
Enter winter or the beginning of spring, when fallen leaves do not sprout, takes the Dendrobidium huoshanness stem section of 2 years above field Emulational cultures of life, select
No disease and pests harm stem item, cleaning after air-drying surface, are placed in 115-125 DEG C of baking oven and heat 8-12s, then change to 65-75 DEG C rapidly,
It is heated to constant weight；Then, the Dendrobidium huoshanness stem item after above-mentioned drying and processing is crushed using fluidized bed jet mill micronizer
It at Ultramicro-powder, is collected and fed into bag and vacuumizes, saved under low temperature stand-by；
(2) preparation of Dendrobidium huoshanness flower essential oil
Month in spring 4-6 the Dendrobidium huoshanness flower of 2 years above field Emulational cultures of life is won, is sent immediately after fresh flower picking
Enter extraction chamber, extracts corresponding Dendrobidium huoshanness flower essential oil；
(3) Dendrobidium huoshanness cigarette is obtained
A. firstly, 50 ° of -60 ° of bent wines of Dendrobidium huoshanness stem 4-6 times of volume of Ultramicro-powder that step (1) is obtained dilute
It stirs evenly, Ultramicro-powder suspension is made；Then, by Ultramicro-powder turbid liquid spraying in tobacco leaf surface, and will sprinkling treated tobacco leaf
5-10min is heated in 65-75 DEG C of baking oven；Finally, the tobacco leaf for being switched to pipe tobacco is wrapped to form tobacco rod by cigarette paper；Wherein,
The mass ratio of Dendrobidium huoshanness stem Ultramicro-powder and pipe tobacco used in Ultramicro-powder suspension is (0.1-10): 1000；
B. firstly, the Dendrobidium huoshanness flower essential oil and peppermint oil, β-that step (2) obtains are sent alkene, linalool, salicylic acid first
One of ester, myrcene, myrrh oil, neodecanoic acid glyceride, propylene glycol, triacetic acid glycerol, olive oil, corn oil or it is a variety of into
Row mixing, is made quick-fried pearl solution；Then, quick-fried pearl solution people is wrapped in quick-fried pearl in a manner of injecting flavoring, quick-fried pearl is made；Most
Afterwards, quick-fried pearl is put into the middle part of filter stick, and in filter stick surface package forming paper to form filter tip；Wherein, Dendrobidium huoshanness flower
The additive amount of essential oil is 0.1%-30%；
C. tobacco rod is connect to get Dendrobidium huoshanness cigarette needed for target with filter tip by connecting paper.
As one of preferred embodiment of the invention, low temperature is specially (- 22)-(- 18) DEG C in the step (1).
As one of preferred embodiment of the invention, the extracting process of Dendrobidium huoshanness flower essential oil is water steaming in the step (2)
Steam distillation method or carbon dioxide supercritical extraction method.
As one of preferred embodiment of the invention, the specific of Dendrobidium huoshanness flower essential oil is extracted by the steam distillation
Method are as follows: weigh 100g it is fresh Dendrobidium huoshanness flower in flask, then thereto be added 2000mL water, 5mL n-hexane with it is several
Grain zeolite, extracts 6h, cooling and standings 2h by the atmospheric steam way of distillation after sufficiently shaking up；Then, grease collection obtained
Mixture is separated oil-yielding stratum and n-hexane therein is recovered under reduced pressure, is obtained after anhydrous sodium sulfate is dry with 20mL n-hexane extraction 2 times
Grease 0.56mL.
As one of preferred embodiment of the invention, Dendrobidium huoshanness anthosin is extracted by the carbon dioxide supercritical extraction method
Oil method particularly includes: weigh the fresh Dendrobidium huoshanness flower of 100g, be put into progress supercritical carbon dioxide extraction in high pressure extraction still
It takes, extraction kettle pressure 27MPa, 40 DEG C of temperature, flow velocity 15kg/kgh, separates a kettle pressure 10MPa, temperature 45 C, separation two
Kettle pressure 6MPa, 42 DEG C of temperature, extraction time 1.5h；Then, dendrobium nobile flower essential oil is collected, anhydrous sodium sulfate or discoloration silicon are recycled
Glue is dehydrated, and grease 0.63mL is obtained.
As one of preferred embodiment of the invention, the Huoshan stone of 2 years above field Emulational cultures of life in the step (2)
The picking of dry measure used in former times flower requires to should also conform to following standard: it is required that the flowers are in blossom, noon to afternoon on the same day is harvested, and the rainy day does not adopt.
As one of preferred embodiment of the invention, bent wine is specially 52 ° of bent wines in the step (3).
As one of preferred embodiment of the invention, the quick-fried pearl, tobacco leaf are direct purchase in the normal of existing circulation market
Advise object.
The present invention compared with prior art the advantages of be:
(1) Dendrobidium huoshanness stem Ultramicro-powder of the invention contains Dendrobidium huoshanness and imitates substance, including albumen, polysaccharide, biology entirely
The primary such as alkali, flavones and secondary metabolite；Dendrobidium huoshanness stem item passes through high-temperature fixation and low temperature drying；On the one hand, low temperature dries
It is dry to remain more active constituents from destroying；On the other hand, it is processed by baking, dendrobium nobile nature and flavor is made to switch to temperature by cold
Property, meanwhile, Maillard reaction generates distinctive light burnt odor；Dendrobidium huoshanness stem Ultramicro-powder is added to pipe tobacco surface by the present invention
In, keep flue gas form mellow and full, increases fine and smooth soft degree, reduce dry sensation, increase perfume quantity；
(2) Dendrobidium huoshanness flower essential oil extract is added in the quick-fried pearl of filter tip by the present invention, can preferably weaken cigarette
Irritation, improve and abundant cigarette flavor, the fragrance for being obviously improved cigarette is rich, the interest of aesthetic quality and suction,
And the economic benefits and social benefits immunoregulation function with tranquilizing the mind relieve stagnation.
Specific embodiment
It elaborates below to the embodiment of the present invention, the present embodiment carries out under the premise of the technical scheme of the present invention
Implement, the detailed implementation method and specific operation process are given, but protection scope of the present invention is not limited to following implementation
Example.
Embodiment 1
A kind of Dendrobidium huoshanness cigarette of the present embodiment, including tobacco rod and filter tip；Pipe tobacco is surrounded by tobacco rod, pipe tobacco surface is covered
There is Dendrobidium huoshanness stem Ultramicro-powder (Dendrobidium huoshanness stem Ultramicro-powder is 0.1:1000 with tobacco quality ratio)；It was surrounded by filter tip
Filter stick, filter stick middle part are embedded with quick-fried pearl, are enclosed with quick-fried pearl solution in quick-fried pearl.Wherein, the specific formula of quick-fried pearl solution are as follows: Huoshan stone
Dry measure used in former times flower essential oil 0.1%, peppermint oil 0.2%, neodecanoic acid glyceride 20%, olive oil 20%, remaining is corn oil.
Dendrobidium huoshanness stem Ultramicro-powder the preparation method comprises the following steps: enter winter or the beginning of spring, when fallen leaves do not sprout, 2 years raw fields is taken to imitate
The Dendrobidium huoshanness stem section of ecological cultivation, selects no disease and pests harm stem item, and cleaning after air-drying surface, is placed in 115 DEG C of baking ovens and heats
8s, then 65 DEG C are changed to rapidly, it is heated to constant weight；It then, will be after above-mentioned drying and processing using fluidized bed jet mill micronizer
Dendrobidium huoshanness stem item be ground into Ultramicro-powder, be collected and fed into bag and vacuumize, saved at a temperature of -22 DEG C stand-by.
Dendrobidium huoshanness flower essential oil the preparation method comprises the following steps: in month in spring 4-6, win the Huoshan of 2 years raw field Emulational cultures
Stone flower is immediately fed into extraction chamber after fresh flower picking, extracts corresponding Dendrobidium huoshanness flower essential oil using steam distillation.Its
In, specific extracting process are as follows: weigh the fresh Dendrobidium huoshanness flower of 100g and 2000mL water, 5mL is being added just in flask, then thereto
If hexane and dry granular zeolite extract 6h, cooling and standings 2h by the atmospheric steam way of distillation after sufficiently shaking up；Then, it will collect
Obtained oil water mixture is separated oil-yielding stratum and is recovered under reduced pressure wherein after anhydrous sodium sulfate is dry with 20mL n-hexane extraction 2 times
N-hexane, obtain grease 0.56mL.
Embodiment 2
A kind of Dendrobidium huoshanness cigarette of the present embodiment, including tobacco rod and filter tip；Pipe tobacco is surrounded by tobacco rod, pipe tobacco surface is covered
There is Dendrobidium huoshanness stem Ultramicro-powder (Dendrobidium huoshanness stem Ultramicro-powder is 1:100 with tobacco quality ratio)；Filtering is surrounded by filter tip
Stick, filter stick middle part are embedded with quick-fried pearl, are enclosed with quick-fried pearl solution in quick-fried pearl.Wherein, the specific formula of quick-fried pearl solution are as follows: Dendrobidium huoshanness
Flower essential oil 30%, peppermint oil 0.3%, neodecanoic acid glyceride 10%, propylene glycol 10%, remaining is corn oil.
Dendrobidium huoshanness stem Ultramicro-powder the preparation method comprises the following steps: enter winter or the beginning of spring, when fallen leaves do not sprout, 4 years raw fields is taken to imitate
The Dendrobidium huoshanness stem section of ecological cultivation, selects no disease and pests harm stem item, and cleaning after air-drying surface, is placed in 125 DEG C of baking ovens and heats
12s, then 75 DEG C are changed to rapidly, it is heated to constant weight；It then, will be after above-mentioned drying and processing using fluidized bed jet mill micronizer
Dendrobidium huoshanness stem item be ground into Ultramicro-powder, be collected and fed into bag and vacuumize, saved at a temperature of -18 DEG C stand-by.
Dendrobidium huoshanness flower essential oil the preparation method comprises the following steps: in month in spring 4-6, win the Huoshan of 4 years raw field Emulational cultures
Stone flower is immediately fed into extraction chamber after fresh flower picking, extracts corresponding Dendrobidium huoshanness flower using carbon dioxide supercritical extraction method
Essential oil.Wherein, specific extracting process are as follows: weigh 100g it is fresh Dendrobidium huoshanness flower, be put into high pressure extraction still carry out it is overcritical
Carbon dioxide abstraction, extraction kettle pressure 27MPa, separate a kettle pressure 10MPa, temperature 45 by 40 DEG C of temperature, flow velocity 15kg/kgh
DEG C, separate two kettle pressure 6MPa, 42 DEG C of temperature, extraction time 1.5h；Then, dendrobium nobile flower essential oil is collected, anhydrous slufuric acid is recycled
Sodium or discoloration silica gel are dehydrated, and grease 0.63mL is obtained.
Embodiment 3
A kind of Dendrobidium huoshanness cigarette of the present embodiment, including tobacco rod and filter tip；Pipe tobacco is surrounded by tobacco rod, pipe tobacco surface is covered
There is Dendrobidium huoshanness stem Ultramicro-powder (Dendrobidium huoshanness stem Ultramicro-powder is 1:200 with tobacco quality ratio)；Filtering is surrounded by filter tip
Stick, filter stick middle part are embedded with quick-fried pearl, are enclosed with quick-fried pearl solution in quick-fried pearl；Wherein, the specific formula of quick-fried pearl solution are as follows: Dendrobidium huoshanness
Flower essential oil 5%, 0.1% β-send alkene, 0.1% linalool, 2% gaultherolin, 0.1% myrcene, 0.1% myrrh oil, and 20%
Neodecanoic acid glyceride, remaining is triacetic acid glycerol.
Dendrobidium huoshanness stem Ultramicro-powder the preparation method comprises the following steps: enter winter or the beginning of spring, when fallen leaves do not sprout, take triennial field imitative
The Dendrobidium huoshanness stem section of ecological cultivation, selects no disease and pests harm stem item, and cleaning after air-drying surface, is placed in 120 DEG C of baking ovens and heats
10s, then 70 DEG C are changed to rapidly, it is heated to constant weight；It then, will be after above-mentioned drying and processing using fluidized bed jet mill micronizer
Dendrobidium huoshanness stem item be ground into Ultramicro-powder, be collected and fed into bag and vacuumize, saved at a temperature of -20 DEG C stand-by.
Dendrobidium huoshanness flower essential oil the preparation method comprises the following steps: in month in spring 4-6, win the Huoshan of triennial field Emulational culture
Stone flower is immediately fed into extraction chamber after fresh flower picking, extracts corresponding Dendrobidium huoshanness flower using carbon dioxide supercritical extraction method
Essential oil.Wherein, specific extracting process are as follows: weigh 100g it is fresh Dendrobidium huoshanness flower, be put into high pressure extraction still carry out it is overcritical
Carbon dioxide abstraction, extraction kettle pressure 27MPa, separate a kettle pressure 10MPa, temperature 45 by 40 DEG C of temperature, flow velocity 15kg/kgh
DEG C, separate two kettle pressure 6MPa, 42 DEG C of temperature, extraction time 1.5h；Then, dendrobium nobile flower essential oil is collected, anhydrous slufuric acid is recycled
Sodium or discoloration silica gel are dehydrated, and grease 0.63mL is obtained.
Embodiment 4
The preparation method of Dendrobidium huoshanness cigarette, includes the following steps: in a kind of above-described embodiment of the present embodiment
(1) preparation of Dendrobidium huoshanness stem Ultramicro-powder
Enter winter or the beginning of spring, when fallen leaves do not sprout, takes the Dendrobidium huoshanness stem section of 2 years raw field Emulational cultures, select disease-free
Insect pest stem item, cleaning after air-drying surface, are placed in 115 DEG C of baking ovens and heat 8s, then change to 65 DEG C rapidly, be heated to constant weight；It connects
, the Dendrobidium huoshanness stem item after above-mentioned drying and processing is ground into Ultramicro-powder using fluidized bed jet mill micronizer, is collected
And be fitted into bag and vacuumize, it is saved at a temperature of -22 DEG C stand-by.
(2) preparation of Dendrobidium huoshanness flower essential oil
Win the Dendrobidium huoshanness flower of 2 years raw field Emulational cultures, it is desirable that noon is under on the day of the flowers are in blossom in month in spring 4-6
Noon harvesting, and the rainy day does not adopt, and is immediately fed into extraction chamber after fresh flower picking, extracts corresponding Dendrobidium huoshanness using steam distillation
Flower essential oil；Wherein, specific extracting process are as follows: weigh the fresh Dendrobidium huoshanness flower of 100g and be added in flask, then thereto
If 2000mL water, 5mL n-hexane and dry granular zeolite extract 6h, cooling and standings by the atmospheric steam way of distillation after sufficiently shaking up
2h；Then, obtained oil water mixture will be collected with 20mL n-hexane extraction 2 times, separate oil-yielding stratum, anhydrous sodium sulfate is dry
Afterwards, n-hexane therein is recovered under reduced pressure, obtains grease 0.56mL.
(3) Dendrobidium huoshanness cigarette is obtained
A. it firstly, the 50 ° of bent wines dilution for 4 times of volumes of Dendrobidium huoshanness stem Ultramicro-powder that step (1) obtains is stirred evenly, makes
At Ultramicro-powder suspension；Then, by Ultramicro-powder turbid liquid spraying in tobacco leaf surface, and sprinkling treated tobacco leaf is dried in 65 DEG C
5min is heated in case；Finally, the tobacco leaf for being switched to pipe tobacco is wrapped to form tobacco rod by cigarette paper；Wherein, in Ultramicro-powder suspension
The mass ratio of the Dendrobidium huoshanness stem Ultramicro-powder and pipe tobacco that use is 0.1:1000；
B. firstly, according to quick-fried pearl solution: Dendrobidium huoshanness flower essential oil 0.1%, peppermint oil 0.2%, the new last of the ten Heavenly stems is prepared as following formula
Acid glyceride 20%, olive oil 20%, remaining is corn oil；Then, quick-fried pearl solution people is wrapped in a manner of injecting flavoring
In quick-fried pearl, quick-fried pearl is made；Finally, quick-fried pearl is put into the middle part of filter stick, and forming paper is wrapped up to form filtering on filter stick surface
Mouth；
C. tobacco rod is connect to get Dendrobidium huoshanness cigarette needed for target with filter tip by connecting paper.
Embodiment 5
The preparation method of Dendrobidium huoshanness cigarette, includes the following steps: in a kind of above-described embodiment of the present embodiment
(1) preparation of Dendrobidium huoshanness stem Ultramicro-powder
Enter winter or the beginning of spring, when fallen leaves do not sprout, takes the Dendrobidium huoshanness stem section of 4 years raw field Emulational cultures, select disease-free
Insect pest stem item, cleaning after air-drying surface, are placed in 125 DEG C of baking ovens and heat 12s, then change to 75 DEG C rapidly, be heated to constant weight；It connects
, the Dendrobidium huoshanness stem item after above-mentioned drying and processing is ground into Ultramicro-powder using fluidized bed jet mill micronizer, is collected
And be fitted into bag and vacuumize, it is saved at a temperature of -18 DEG C stand-by.
(2) preparation of Dendrobidium huoshanness flower essential oil
Win the Dendrobidium huoshanness flower of 4 years raw field Emulational cultures, it is desirable that noon is under on the day of the flowers are in blossom in month in spring 4-6
Noon harvesting, and the rainy day does not adopt, and is immediately fed into extraction chamber after fresh flower picking, is extracted accordingly using carbon dioxide supercritical extraction method
Dendrobidium huoshanness flower essential oil；Wherein, specific extracting process are as follows: weigh the fresh Dendrobidium huoshanness flower of 100g, be put into high pressure extraction still
Supercritical carbon dioxide extracting is carried out, extraction kettle pressure 27MPa, separates a kettle pressure by 40 DEG C of temperature, flow velocity 15kg/kgh
10MPa, temperature 45 C, separate two kettle pressure 6MPa, 42 DEG C of temperature, extraction time 1.5h；Then, dendrobium nobile flower essential oil is collected, then
It is dehydrated using anhydrous sodium sulfate or discoloration silica gel, obtains grease 0.63mL.
(3) Dendrobidium huoshanness cigarette is obtained
A. it firstly, the 60 ° of bent wines dilution for 6 times of volumes of Dendrobidium huoshanness stem Ultramicro-powder that step (1) obtains is stirred evenly, makes
At Ultramicro-powder suspension；Then, by Ultramicro-powder turbid liquid spraying in tobacco leaf surface, and sprinkling treated tobacco leaf is dried in 75 DEG C
10min is heated in case；Finally, the tobacco leaf for being switched to pipe tobacco is wrapped to form tobacco rod by cigarette paper；Wherein, in Ultramicro-powder suspension
The mass ratio of the Dendrobidium huoshanness stem Ultramicro-powder and pipe tobacco that use is 1:100；
B. firstly, according to quick-fried pearl solution: Dendrobidium huoshanness flower essential oil 30%, peppermint oil 0.3%, neodecanoic acid is prepared as following formula
Glyceride 10%, propylene glycol 10%, remaining is corn oil；Then, quick-fried pearl solution people is wrapped in a manner of injecting flavoring quick-fried
In pearl, quick-fried pearl is made；Finally, quick-fried pearl is put into the middle part of filter stick, and in filter stick surface package forming paper to form filter tip；
C. tobacco rod is connect to get Dendrobidium huoshanness cigarette needed for target with filter tip by connecting paper.
Embodiment 6
The preparation method of Dendrobidium huoshanness cigarette, includes the following steps: in a kind of above-described embodiment of the present embodiment
(1) preparation of Dendrobidium huoshanness stem Ultramicro-powder
Enter winter or the beginning of spring, when fallen leaves do not sprout, takes the Dendrobidium huoshanness stem section of triennial field Emulational culture, select disease-free
Insect pest stem item, cleaning after air-drying surface, are placed in 120 DEG C of baking ovens and heat 10s, then change to 70 DEG C rapidly, be heated to constant weight；It connects
, the Dendrobidium huoshanness stem item after above-mentioned drying and processing is ground into Ultramicro-powder using fluidized bed jet mill micronizer, is collected
And be fitted into bag and vacuumize, it is saved at a temperature of -20 DEG C stand-by.
(2) preparation of Dendrobidium huoshanness flower essential oil
Win the Dendrobidium huoshanness flower of triennial field Emulational culture, it is desirable that noon is under on the day of the flowers are in blossom in month in spring 4-6
Noon harvesting, and the rainy day does not adopt, and is immediately fed into extraction chamber after fresh flower picking, is extracted accordingly using carbon dioxide supercritical extraction method
Dendrobidium huoshanness flower essential oil；Wherein, specific extracting process are as follows: weigh the fresh Dendrobidium huoshanness flower of 100g, be put into high pressure extraction still
Supercritical carbon dioxide extracting is carried out, extraction kettle pressure 27MPa, separates a kettle pressure by 40 DEG C of temperature, flow velocity 15kg/kgh
10MPa, temperature 45 C, separate two kettle pressure 6MPa, 42 DEG C of temperature, extraction time 1.5h；Then, dendrobium nobile flower essential oil is collected, then
It is dehydrated using anhydrous sodium sulfate or discoloration silica gel, obtains grease 0.63mL.
(3) Dendrobidium huoshanness cigarette is obtained
A. it firstly, the 52 ° of bent wines dilution for 5 times of volumes of Dendrobidium huoshanness stem Ultramicro-powder that step (1) obtains is stirred evenly, makes
At Ultramicro-powder suspension；Then, by Ultramicro-powder turbid liquid spraying in tobacco leaf surface, and sprinkling treated tobacco leaf is dried in 70 DEG C
8min is heated in case；Finally, the tobacco leaf for being switched to pipe tobacco is wrapped to form tobacco rod by cigarette paper；Wherein, in Ultramicro-powder suspension
The mass ratio of the Dendrobidium huoshanness stem Ultramicro-powder and pipe tobacco that use is 1:200；
B. firstly, according to quick-fried pearl solution: Dendrobidium huoshanness flower essential oil 5% is prepared as following formula, 0.1% β-sends alkene, 0.1% virtue
Camphor tree alcohol, 2% gaultherolin, 0.1% myrcene, 0.1% myrrh oil, 20% neodecanoic acid glyceride, remaining is triacetic acid glycerol；
Then, quick-fried pearl solution people is wrapped in quick-fried pearl in a manner of injecting flavoring, quick-fried pearl is made；Finally, quick-fried pearl is put into filter stick
Middle part, and in filter stick surface package forming paper to form filter tip；
C. tobacco rod is connect to get Dendrobidium huoshanness cigarette needed for target with filter tip by connecting paper.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (10)
1. a kind of Dendrobidium huoshanness cigarette, including tobacco rod and filter tip, which is characterized in that be surrounded by pipe tobacco, pipe tobacco table in the tobacco rod
Face is covered with Dendrobidium huoshanness stem Ultramicro-powder, and Dendrobidium huoshanness stem Ultramicro-powder and tobacco quality ratio are (0.1-10): 1000；The mistake
It is surrounded by filter stick in filter tip, quick-fried pearl is embedded in the middle part of filter stick, the package flower essential oil of Dendrobidium huoshanness containing 0.1%-30% is quick-fried in quick-fried pearl
Pearl solution；
The Dendrobidium huoshanness stem Ultramicro-powder the preparation method comprises the following steps: enter winter or the beginning of spring, when fallen leaves do not sprout, take life in 2 years with u'eno
The Dendrobidium huoshanness stem section of outer Emulational culture, selects no disease and pests harm stem item, and cleaning after air-drying surface, is placed in 115-125 DEG C of baking oven
Middle heating 8-12s, then 65-75 DEG C is changed to rapidly, it is heated to constant weight；It then, will be upper using fluidized bed jet mill micronizer
Dendrobidium huoshanness stem item after stating drying and processing is ground into Ultramicro-powder, is collected and fed into bag and vacuumizes, and saves under low temperature stand-by；
The Dendrobidium huoshanness flower essential oil the preparation method comprises the following steps: month in spring 4-6, win 2 years above field Emulational cultures of life
Dendrobidium huoshanness flower is immediately fed into extraction chamber after fresh flower picking, extracts corresponding Dendrobidium huoshanness flower essential oil.
2. Dendrobidium huoshanness cigarette according to claim 1, which is characterized in that remove Dendrobidium huoshanness anthosin in the quick-fried pearl solution
Ingredient other than oil be specially peppermint oil, β-send alkene, linalool, gaultherolin, myrcene, myrrh oil, neodecanoic acid glyceride,
One of propylene glycol, triacetic acid glycerol, olive oil, corn oil are a variety of.
3. Dendrobidium huoshanness cigarette according to claim 1, which is characterized in that the preparation of the Dendrobidium huoshanness stem Ultramicro-powder
In method, is saved under low temperature and refer to and saved at a temperature of (- 22)-(- 18) DEG C.
4. Dendrobidium huoshanness cigarette according to claim 1, which is characterized in that the preparation method of the Dendrobidium huoshanness flower essential oil
In, the extracting process of Dendrobidium huoshanness flower essential oil is steam distillation or carbon dioxide supercritical extraction method；
When the extracting process of Dendrobidium huoshanness flower essential oil is specially steam distillation, the method is as follows: it is fresh suddenly to weigh 100g
Mountain stone flower in flask, if then 2000mL water, 5mL n-hexane and dry granular zeolite are added thereto, by normal after sufficiently shaking up
Press extraction by steam distillation 6h, cooling and standings 2h；Then, the oil water mixture 20mL n-hexane extraction 2 collection obtained
It is secondary, it separates oil-yielding stratum and n-hexane therein is recovered under reduced pressure, obtains grease 0.56mL after anhydrous sodium sulfate is dry；
When the extracting process of Dendrobidium huoshanness flower essential oil is specially carbon dioxide supercritical extraction method, the method is as follows: weigh 100g
Fresh Dendrobidium huoshanness flower, is put into high pressure extraction still and carries out supercritical carbon dioxide extracting, extraction kettle pressure 27MPa, temperature
40 DEG C, flow velocity 15kg/kgh, a kettle pressure 10MPa is separated, temperature 45 C separates two kettle pressure 6MPa, 42 DEG C of temperature, extracts
Time 1.5h；Then, dendrobium nobile flower essential oil is collected, recycles anhydrous sodium sulfate or discoloration silica gel to be dehydrated, obtains grease
0.63mL。
5. a kind of method for preparing the Dendrobidium huoshanness cigarette as described in claim 1-4 is any, which is characterized in that including walking as follows
It is rapid:
(1) preparation of Dendrobidium huoshanness stem Ultramicro-powder
Enter winter or the beginning of spring, when fallen leaves do not sprout, takes the Dendrobidium huoshanness stem section of 2 years above field Emulational cultures of life, select disease-free
Insect pest stem item, cleaning after air-drying surface, are placed in 115-125 DEG C of baking oven and heat 8-12s, then change to 65-75 DEG C rapidly, heat
To constant weight；Then, the Dendrobidium huoshanness stem item after above-mentioned drying and processing is ground into using fluidized bed jet mill micronizer super
Micro mist is collected and fed into bag and vacuumizes, and saves under low temperature stand-by；
(2) preparation of Dendrobidium huoshanness flower essential oil
Month in spring 4-6 the Dendrobidium huoshanness flower of 2 years above field Emulational cultures of life is won, is immediately fed into and mentions after fresh flower picking
Room is taken, corresponding Dendrobidium huoshanness flower essential oil is extracted；
(3) Dendrobidium huoshanness cigarette is obtained
A. firstly, 50 ° of -60 ° of bent wines dilution of Dendrobidium huoshanness stem 4-6 times of volume of Ultramicro-powder that step (1) obtains is stirred evenly,
Ultramicro-powder suspension is made；Then, by Ultramicro-powder turbid liquid spraying in tobacco leaf surface, and will sprinkling treated tobacco leaf in 65-
5-10min is heated in 75 DEG C of baking ovens；Finally, the tobacco leaf for being switched to pipe tobacco is wrapped to form tobacco rod by cigarette paper；Wherein, Ultramicro-powder
The mass ratio of Dendrobidium huoshanness stem Ultramicro-powder and pipe tobacco used in suspension is (0.1-10): 1000；
B. firstly, the Dendrobidium huoshanness flower essential oil and peppermint oil, β-that step (2) obtains are sent alkene, linalool, gaultherolin, perfume (or spice)
One of leaf alkene, myrrh oil, neodecanoic acid glyceride, propylene glycol, triacetic acid glycerol, olive oil, corn oil a variety of are mixed
It closes, quick-fried pearl solution is made；Then, quick-fried pearl solution people is wrapped in quick-fried pearl in a manner of injecting flavoring, quick-fried pearl is made；Finally,
Quick-fried pearl is put into the middle part of filter stick, and in filter stick surface package forming paper to form filter tip；Wherein, Dendrobidium huoshanness flower essential oil
Additive amount be 0.1%-30%；
C. tobacco rod is connect to get Dendrobidium huoshanness cigarette needed for target with filter tip by connecting paper.
6. the preparation method of Dendrobidium huoshanness cigarette according to claim 5, which is characterized in that low temperature in the step (1)
Specially (- 22)-(- 18) DEG C.
7. the preparation method of Dendrobidium huoshanness cigarette according to claim 5, which is characterized in that Huoshan in the step (2)
The extracting process of dendrobium nobile flower essential oil is steam distillation or carbon dioxide supercritical extraction method.
8. the preparation method of Dendrobidium huoshanness cigarette according to claim 7, which is characterized in that pass through the steam distillation
Method extracts Dendrobidium huoshanness flower essential oil method particularly includes: weighs the fresh Dendrobidium huoshanness flower of 100g and adds in flask, then thereto
If entering 2000mL water, 5mL n-hexane and dry granular zeolite, 6h is extracted by the atmospheric steam way of distillation after sufficiently shaking up, cooling is quiet
Set 2h；Then, obtained oil water mixture will be collected with 20mL n-hexane extraction 2 times, separate oil-yielding stratum, anhydrous sodium sulfate is dry
Afterwards, n-hexane therein is recovered under reduced pressure, obtains grease 0.56mL.
9. the preparation method of Dendrobidium huoshanness cigarette according to claim 7, which is characterized in that super by the carbon dioxide
Critical extraction extraction Dendrobidium huoshanness flower essential oil method particularly includes: weigh the fresh Dendrobidium huoshanness flower of 100g, be put into high pressure extraction
It takes and carries out supercritical carbon dioxide extracting in kettle, extraction kettle pressure 27MPa, separates a kettle by 40 DEG C of temperature, flow velocity 15kg/kgh
Pressure 10MPa, temperature 45 C, separate two kettle pressure 6MPa, 42 DEG C of temperature, extraction time 1.5h；Then, dendrobium nobile anthosin is collected
Oil recycles anhydrous sodium sulfate or discoloration silica gel to be dehydrated, obtains grease 0.63mL.
10. the preparation method of Dendrobidium huoshanness cigarette according to claim 5, which is characterized in that 2 years in the step (2)
The picking of the Dendrobidium huoshanness flower of the raw above field Emulational culture requires to should also conform to following standard: requiring on the day of the flowers are in blossom noon extremely
Harvesting in afternoon, and the rainy day does not adopt.
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