CN107022416A - A kind of compound method of pomegranate taste flavouring essence for tobacco - Google Patents
A kind of compound method of pomegranate taste flavouring essence for tobacco Download PDFInfo
- Publication number
- CN107022416A CN107022416A CN201710409629.5A CN201710409629A CN107022416A CN 107022416 A CN107022416 A CN 107022416A CN 201710409629 A CN201710409629 A CN 201710409629A CN 107022416 A CN107022416 A CN 107022416A
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- Prior art keywords
- ethyl
- leaf
- methyl
- acetate
- mixed
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Abstract
The invention discloses a kind of compound method of pomegranate taste flavouring essence for tobacco, comprise the following steps:(1) preparation raw material;(2) 2 methylbutanoic acids, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, linalool oxide, peppermint oil, eucalyptus oil, orange oil, the clove bud oil of above-mentioned preparation are uniformly mixed;(3) acetic acid, caproic acid, ethyl hexanoate, linalool, hexanal, menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and ethyl acetate are added, is well mixed;(4) ethyl butyrate, 2 methylbutanoic acid ethyl esters, methyl heptenone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β damascones are added, is well mixed;(5) it is aged.The pomegranate taste flavouring essence for tobacco preparation process is simple, with special strong fresh fragrance, is conducive to the breath freshening of user.
Description
Technical field
The present invention relates to a kind of flavouring essence for tobacco, specifically a kind of compound method of pomegranate taste flavouring essence for tobacco.
Background technology
Electronic cigarette also known as virtual cigarette, electronic atomizer, are mainly used in smoking cessation and cigarette substitute.It has as cigarette
Outward appearance, the taste approximate with cigarette, or even than general cigarette taste to have more a lot, also like cigarette it is the same can suction out cigarette,
Taste is suctioned out with feeling to come.Electronic cigarette does not have other harmful components such as tar, the suspended particulates in cigarette, is mainly used for smoking cessation
And cigarette substitute.
Electronic cigarette is made up of lithium battery, atomizer and cigarette bullet, and electronic cigarette passes through high-tech silicon and airflow sensor device control
Tobacco curing mist output quantity and working condition, nicotine are atomized, and by the solution atomization containing nicotine and essence into particulate, are inhaled by lung
Receive, while discharge simulation smoke.So electronics flavouring essence for tobacco is the indispensable important component of electronic cigarette.
Electronics flavouring essence for tobacco kind in the market is varied, but is specific to the cigarette perfume that women likes taste
Essence is less, it is impossible to meet the demand of people.Therefore, the present invention provides a kind of compound method of pomegranate taste flavouring essence for tobacco.
The content of the invention
It is an object of the invention to provide a kind of compound method of pomegranate taste flavouring essence for tobacco, to solve in above-mentioned background technology
The problem of proposition.
To achieve the above object, the present invention provides following technical scheme:
A kind of compound method of pomegranate taste flavouring essence for tobacco, comprises the following steps:
(1) raw material of following mass percent is prepared:
(2) by the 2-Methyl Butyric Acid of above-mentioned preparation, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, oxidation virtue
Camphor tree alcohol, peppermint oil, eucalyptus oil, orange oil, clove bud oil stir mixing 30-50min in closed space, obtain stirring mixed
Close uniform mixed liquor A;
(3) in mixed liquor A obtained by upper step, sequentially add the acetic acid of above-mentioned preparation, caproic acid, ethyl hexanoate, linalool, oneself
Aldehyde, menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and second
Acetoacetic ester, stirring mixing 20-40min, the mixed liquid B being uniformly mixed in closed space;
(4) in mixed liquid B obtained by upper step, the ethyl butyrate, ethyl 2-methylbutyrate, methyl of above-mentioned preparation are sequentially added
Heptenone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β-damascone, in closed space
Stirring mixing 15-35min, the mixed liquor C being uniformly mixed;
(5) mixed liquor C is placed at 30-45 DEG C and is aged 12-24h.
It is used as further scheme of the invention:The step (2) by the 2-Methyl Butyric Acid of above-mentioned preparation, ethyl isovalerate,
Leaf-alcohol, benzaldehyde, propane diols, acetophenone, linalool oxide, peppermint oil, eucalyptus oil, orange oil, clove bud oil are closed
Stirring mixing 45min, the mixed liquor A being uniformly mixed in space.
It is used as further scheme of the invention:The step (3) sequentially adds above-mentioned match somebody with somebody in mixed liquor A obtained by upper step
The acetic acid of system, caproic acid, ethyl hexanoate, linalool, hexanal, menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla
Beans tincture, triacetyl glycerine, methyl benzoate and ethyl acetate, stirring mixing 30min, obtains stirring mixed in closed space
Close uniform mixed liquid B.
It is used as further scheme of the invention:The step (4) sequentially adds above-mentioned match somebody with somebody in mixed liquid B obtained by upper step
Ethyl butyrate, ethyl 2-methylbutyrate, methyl heptenone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, the capric acid of system
Ethyl ester and β-damascone, the stirring mixing 25min, the mixed liquor C being uniformly mixed in closed space.
It is used as further scheme of the invention:Mixed liquor C is placed at 38 DEG C by the step (5) is aged 20h.
Compared with prior art, the beneficial effects of the invention are as follows:
The compound method of the flavouring essence for tobacco plays synergy by raw material compounding, with special strong fresh fragrance,
It is a kind of electronic cigarette composition of pomegranate taste;The flavouring essence for tobacco preparation process is simple, and the pomegranate taste cigarette of preparation is used
Essence pomegranate is with rich flavor and lasting, is conducive to the breath freshening of user.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Embodiment 1
A kind of compound method of pomegranate taste flavouring essence for tobacco, comprises the following steps:
(1) raw material of following mass percent is prepared:
(2) by the 2-Methyl Butyric Acid of above-mentioned preparation, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, oxidation virtue
Camphor tree alcohol, peppermint oil, eucalyptus oil, orange oil, clove bud oil stir mixing 30min in closed space, obtain stirring mixing
Uniform mixed liquor A;
(3) in mixed liquor A obtained by upper step, sequentially add the acetic acid of above-mentioned preparation, caproic acid, ethyl hexanoate, linalool, oneself
Aldehyde, menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and second
Acetoacetic ester, stirring mixing 20min, the mixed liquid B being uniformly mixed in closed space;
(4) in mixed liquid B obtained by upper step, the ethyl butyrate, ethyl 2-methylbutyrate, methyl of above-mentioned preparation are sequentially added
Heptenone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β-damascone, in closed space
Stirring mixing 15min, the mixed liquor C being uniformly mixed;
(5) mixed liquor C is placed at 30 DEG C and is aged 12h.
Embodiment 2
A kind of compound method of pomegranate taste flavouring essence for tobacco, comprises the following steps:
(1) raw material of following mass percent is prepared:
(2) by the 2-Methyl Butyric Acid of above-mentioned preparation, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, oxidation virtue
Camphor tree alcohol, peppermint oil, eucalyptus oil, orange oil, clove bud oil stir mixing 50min in closed space, obtain stirring mixing
Uniform mixed liquor A;
(3) in mixed liquor A obtained by upper step, sequentially add the acetic acid of above-mentioned preparation, caproic acid, ethyl hexanoate, linalool, oneself
Aldehyde, menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and second
Acetoacetic ester, stirring mixing 40min, the mixed liquid B being uniformly mixed in closed space;
(4) in mixed liquid B obtained by upper step, the ethyl butyrate, ethyl 2-methylbutyrate, methyl of above-mentioned preparation are sequentially added
Heptenone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β-damascone, in closed space
Stirring mixing 35min, the mixed liquor C being uniformly mixed;
(5) mixed liquor C is placed at 45 DEG C and is aged 24h.
Embodiment 3
A kind of compound method of pomegranate taste flavouring essence for tobacco, comprises the following steps:
(1) raw material of following mass percent is prepared:
(2) by the 2-Methyl Butyric Acid of above-mentioned preparation, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, oxidation virtue
Camphor tree alcohol, peppermint oil, eucalyptus oil, orange oil, clove bud oil stir mixing 45min in closed space, obtain stirring mixing
Uniform mixed liquor A.
(3) in mixed liquor A obtained by upper step, sequentially add the acetic acid of above-mentioned preparation, caproic acid, ethyl hexanoate, linalool, oneself
Aldehyde, menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and second
Acetoacetic ester, stirring mixing 30min, the mixed liquid B being uniformly mixed in closed space.
(4) in mixed liquid B obtained by upper step, the ethyl butyrate, ethyl 2-methylbutyrate, methyl of above-mentioned preparation are sequentially added
Heptenone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β-damascone, in closed space
Stirring mixing 25min, the mixed liquor C being uniformly mixed.
(5) mixed liquor C is placed at 38 DEG C and is aged 20h.
The compound method of the flavouring essence for tobacco plays synergy by raw material compounding, with special strong fresh fragrance,
It is a kind of electronic cigarette composition of pomegranate taste;The flavouring essence for tobacco preparation process is simple, and the pomegranate taste cigarette of preparation is used
Essence pomegranate is with rich flavor and lasting, is conducive to the breath freshening of user.
The better embodiment to this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
, can also be on the premise of this patent objective not be departed from formula, the knowledge that one skilled in the relevant art possesses
Make a variety of changes.
Claims (5)
1. a kind of compound method of pomegranate taste flavouring essence for tobacco, it is characterised in that comprise the following steps:
(1) raw material of following mass percent is prepared:
(2) by the 2-Methyl Butyric Acid of above-mentioned preparation, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, the fragrant camphor tree of oxidation
Alcohol, peppermint oil, eucalyptus oil, orange oil, clove bud oil stir mixing 30-50min in closed space, obtain stirring mixing
Uniform mixed liquor A;
(3) in mixed liquor A obtained by upper step, sequentially add the acetic acid of above-mentioned preparation, caproic acid, ethyl hexanoate, linalool, hexanal,
Menthyl acetate, terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and acetic acid second
Ester, stirring mixing 20-40min, the mixed liquid B being uniformly mixed in closed space;
(4) in mixed liquid B obtained by upper step, the ethyl butyrate, ethyl 2-methylbutyrate, methyl heptenyl of above-mentioned preparation are sequentially added
Ketone, Leaf Acetate, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β-damascone, are stirred in closed space
Mix 15-35min, the mixed liquor C being uniformly mixed;
(5) mixed liquor C is placed at 30-45 DEG C and is aged 12-24h.
2. the compound method of pomegranate taste flavouring essence for tobacco according to claim 1, it is characterised in that the step (2) will be upper
State the 2-Methyl Butyric Acid of preparation, ethyl isovalerate, leaf-alcohol, benzaldehyde, propane diols, acetophenone, linalool oxide, peppermint oil, eucalyptus
Leaf oil, orange oil, clove bud oil stir mixing 45min, the mixed liquor A being uniformly mixed in closed space.
3. the compound method of pomegranate taste flavouring essence for tobacco according to claim 1, it is characterised in that the step (3) is upper
In step gained mixed liquor A, sequentially add the acetic acid of above-mentioned preparation, caproic acid, ethyl hexanoate, linalool, hexanal, menthyl acetate,
Terpinyl acetate, methyl cinnamate, vanilla bean tincture, triacetyl glycerine, methyl benzoate and ethyl acetate, closed
Stirring mixing 30min, the mixed liquid B being uniformly mixed in space.
4. the compound method of pomegranate taste flavouring essence for tobacco according to claim 1, it is characterised in that the step (4) is upper
In step gained mixed liquid B, ethyl butyrate, ethyl 2-methylbutyrate, methyl heptenone, the acetic acid leaf-alcohol of above-mentioned preparation are sequentially added
Ester, butyric acid leaf-alcohol ester, ethylmaltol, ethyl caprate and β-damascone, the stirring mixing 25min in closed space,
The mixed liquor C being uniformly mixed.
5. the compound method of pomegranate taste flavouring essence for tobacco according to claim 1, it is characterised in that the step (5) will be mixed
Conjunction liquid C, which is placed at 38 DEG C, is aged 20h.
Priority Applications (1)
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CN201710409629.5A CN107022416A (en) | 2017-06-02 | 2017-06-02 | A kind of compound method of pomegranate taste flavouring essence for tobacco |
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CN201710409629.5A CN107022416A (en) | 2017-06-02 | 2017-06-02 | A kind of compound method of pomegranate taste flavouring essence for tobacco |
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CN201710409629.5A Pending CN107022416A (en) | 2017-06-02 | 2017-06-02 | A kind of compound method of pomegranate taste flavouring essence for tobacco |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101565652A (en) * | 2009-06-02 | 2009-10-28 | 上海英华香精香料有限公司 | Fruity type flue-cured tobacco essence and applications thereof |
CN103849465A (en) * | 2014-02-27 | 2014-06-11 | 恩施市锦华生物工程有限责任公司 | Preparation method of essence for electronic cigarette with strawberry flavor |
CN104116131A (en) * | 2014-07-16 | 2014-10-29 | 湖南中烟工业有限责任公司 | Pomegranate concentrate preparing method and application |
-
2017
- 2017-06-02 CN CN201710409629.5A patent/CN107022416A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101565652A (en) * | 2009-06-02 | 2009-10-28 | 上海英华香精香料有限公司 | Fruity type flue-cured tobacco essence and applications thereof |
CN103849465A (en) * | 2014-02-27 | 2014-06-11 | 恩施市锦华生物工程有限责任公司 | Preparation method of essence for electronic cigarette with strawberry flavor |
CN104116131A (en) * | 2014-07-16 | 2014-10-29 | 湖南中烟工业有限责任公司 | Pomegranate concentrate preparing method and application |
Non-Patent Citations (2)
Title |
---|
JOHN C. BEAULIEU等: "HS-GC–MS volatile compounds recovered in freshly pressed ‘Wonderful’ cultivar and commercial pomegranate juices", 《FOOD CHEMISTRY》 * |
黄嘉礽: "《烟草工业手册》", 30 April 1999, 中国轻工业出版社等 * |
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